#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/07/2220797.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220797_Fobs loop_ _publ_author_name 'Dang, Yan-Qiu' 'Yang, Hong-Jun' 'Tian, Lai-Jin' _publ_section_title ; Bis{2-formyl-4-methyl-6-[(tri-2-pyridylmethyl)iminomethyl]phenolato}nickel(II) ; _journal_coeditor_code HB2899 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m231 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.202 _cell_angle_gamma 90.000 _cell_length_a 11.9592 _cell_length_b 17.6301 _cell_length_c 19.6633 _exptl_crystal_F_000 1816.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file hb2899Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070629a in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 400.29 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 325.26 400.64 19.15 o 4 0 0 39.41 102.18 27.61 o 6 0 0 1416.90 1261.08 26.50 o 8 0 0 5.28 11.39 11.14 o 10 0 0 5344.31 5450.72 107.05 o 12 0 0 294.30 332.73 45.24 o 14 0 0 563.58 736.55 64.61 o 1 1 0 299.80 282.36 9.78 o 2 1 0 611.49 664.45 14.40 o 3 1 0 220.63 206.61 11.07 o 4 1 0 114.89 136.21 7.96 o 5 1 0 1212.78 1231.12 19.66 o 6 1 0 562.96 530.14 11.95 o 7 1 0 267.67 219.56 9.23 o 8 1 0 1265.48 1164.96 21.87 o 9 1 0 526.32 513.12 23.43 o 10 1 0 74.78 111.30 19.58 o 11 1 0 14.81 -6.68 19.93 o 12 1 0 104.52 118.84 26.61 o 13 1 0 126.80 139.27 28.83 o 14 1 0 66.91 94.16 29.57 o 1 2 0 2273.82 2297.01 30.14 o 2 2 0 34.25 5.95 4.82 o 3 2 0 214.50 224.96 10.23 o 4 2 0 283.63 254.48 11.20 o 5 2 0 556.86 579.78 13.92 o 6 2 0 820.37 1015.24 17.75 o 7 2 0 43.71 51.07 6.63 o 8 2 0 292.53 328.43 14.40 o 9 2 0 4962.06 5003.05 74.56 o 10 2 0 3142.58 3057.02 71.86 o 11 2 0 105.34 88.85 26.90 o 12 2 0 205.36 156.66 27.02 o 13 2 0 10.45 31.31 27.76 o 14 2 0 360.70 406.53 39.65 o 1 3 0 4040.60 4022.54 44.73 o 2 3 0 160228.39 158109.11 1275.49 o 3 3 0 14718.33 15478.07 120.75 o 4 3 0 220.85 264.47 10.49 o 5 3 0 29.52 22.16 6.34 o 6 3 0 141.70 158.27 7.66 o 7 3 0 67.85 56.05 6.81 o 8 3 0 2615.13 2469.88 36.60 o 9 3 0 2.46 -12.41 12.41 o 10 3 0 140.78 153.71 22.18 o 11 3 0 20.58 32.99 19.66 o 12 3 0 350.47 423.86 39.58 o 13 3 0 591.74 667.10 41.72 o 14 3 0 73.64 72.49 29.48 o 0 4 0 846.95 1013.06 28.57 o 1 4 0 4217.73 4090.97 34.66 o 2 4 0 16597.17 17479.20 128.15 o 3 4 0 2254.31 2331.01 27.66 o 4 4 0 7350.31 7479.61 64.17 o 5 4 0 10921.97 11031.98 91.66 o 6 4 0 214.35 179.40 8.20 o 7 4 0 443.98 504.29 12.88 o 8 4 0 407.95 460.59 18.92 o 9 4 0 2372.98 2263.78 40.99 o 10 4 0 248.45 280.34 25.36 o 11 4 0 40.52 72.05 22.05 o 12 4 0 0.65 -7.75 24.45 o 13 4 0 8.40 -25.07 25.07 o 14 4 0 83.14 64.26 28.86 o 1 5 0 6509.12 7284.29 52.34 o 2 5 0 3207.38 3446.83 29.42 o 3 5 0 10973.36 10897.25 75.18 o 4 5 0 459.19 552.02 11.96 o 5 5 0 5802.04 6471.17 55.34 o 6 5 0 1019.27 1081.42 18.11 o 7 5 0 940.69 896.98 18.95 o 8 5 0 4.98 -7.37 10.11 o 9 5 0 161.81 170.53 16.28 o 10 5 0 6.23 -1.32 16.82 o 11 5 0 551.43 617.34 35.00 o 12 5 0 24.90 25.78 27.38 o 13 5 0 765.82 877.14 54.59 o 14 5 0 42.14 55.93 33.03 o 0 6 0 7639.76 7824.23 77.94 o 1 6 0 2313.69 2206.60 21.15 o 2 6 0 2853.87 2843.88 23.21 o 3 6 0 3813.32 3784.47 32.05 o 4 6 0 4223.59 4513.27 41.75 o 5 6 0 17427.48 16900.93 129.79 o 6 6 0 452.38 501.74 13.22 o 7 6 0 892.86 866.66 21.96 o 8 6 0 29.89 46.95 11.90 o 9 6 0 515.23 542.42 22.71 o 10 6 0 47.92 62.09 20.00 o 11 6 0 31.45 60.27 22.61 o 12 6 0 171.62 197.95 32.58 o 13 6 0 217.61 151.60 42.60 o 14 6 0 36.61 12.00 39.81 o 1 7 0 239.29 168.15 6.23 o 2 7 0 406.09 373.68 8.29 o 3 7 0 2727.43 2562.08 25.15 o 4 7 0 6147.47 6805.47 52.75 o 5 7 0 19.82 22.93 6.04 o 6 7 0 5.53 14.76 7.22 o 7 7 0 2316.53 2357.18 36.50 o 8 7 0 8.26 12.75 11.23 o 9 7 0 336.00 285.01 18.98 o 10 7 0 14.01 13.08 15.20 o 11 7 0 330.33 338.17 39.54 o 12 7 0 141.62 109.97 54.00 o 13 7 0 487.74 528.59 56.06 o 0 8 0 9636.65 9293.16 112.01 o 1 8 0 3190.77 3171.15 34.53 o 2 8 0 1.33 4.95 4.07 o 3 8 0 1140.15 1213.33 15.75 o 4 8 0 24.30 11.12 5.22 o 5 8 0 6018.74 5888.86 58.45 o 6 8 0 440.79 442.27 17.17 o 7 8 0 97.57 110.26 13.41 o 8 8 0 4.15 9.57 11.66 o 9 8 0 134.05 157.14 16.48 o 10 8 0 934.70 927.28 44.28 o 11 8 0 223.07 220.53 41.57 o 12 8 0 79.16 49.94 35.02 o 13 8 0 43.92 108.54 41.10 o 1 9 0 1420.88 1388.76 19.10 o 2 9 0 2483.61 2338.86 24.65 o 3 9 0 3600.15 3416.85 31.95 o 4 9 0 2406.37 2481.62 26.87 o 5 9 0 755.26 773.05 18.68 o 6 9 0 27.42 4.16 7.97 o 7 9 0 1625.24 1616.75 39.28 o 8 9 0 96.23 112.81 16.94 o 9 9 0 997.95 932.04 37.27 o 10 9 0 10.00 12.03 16.45 o 11 9 0 579.39 661.35 77.34 o 12 9 0 164.89 127.28 39.71 o 13 9 0 145.36 154.86 42.43 o 0 10 0 7457.61 7427.15 96.97 o 1 10 0 829.54 802.45 15.97 o 2 10 0 3038.08 3063.08 31.77 o 3 10 0 262.14 321.12 9.94 o 4 10 0 89.02 130.92 8.79 o 5 10 0 1704.29 1665.24 30.46 o 6 10 0 572.60 584.71 18.45 o 7 10 0 18.18 -3.82 12.98 o 8 10 0 91.46 133.67 18.91 o 9 10 0 15.04 30.51 17.17 o 10 10 0 1431.57 1488.55 42.07 o 11 10 0 84.07 136.53 49.74 o 12 10 0 6.87 -5.29 33.02 o 1 11 0 811.53 768.16 16.83 o 2 11 0 2358.90 2255.69 25.95 o 3 11 0 6.17 2.96 6.81 o 4 11 0 552.51 461.41 16.04 o 5 11 0 258.88 270.13 14.94 o 6 11 0 1507.60 1461.32 28.68 o 7 11 0 84.78 60.77 15.40 o 8 11 0 2071.03 2098.65 49.13 o 9 11 0 280.34 259.67 24.75 o 10 11 0 6.88 20.29 19.91 o 11 11 0 8.49 -24.46 26.12 o 12 11 0 250.69 380.05 64.95 o 0 12 0 12343.94 11934.77 132.21 o 1 12 0 16.99 10.60 7.87 o 2 12 0 679.90 669.14 18.59 o 3 12 0 12.42 6.79 7.58 o 4 12 0 1931.27 1836.67 31.29 o 5 12 0 415.56 427.46 18.21 o 6 12 0 917.68 955.44 27.02 o 7 12 0 8.90 -12.01 12.01 o 8 12 0 32.95 12.02 15.42 o 9 12 0 233.38 250.06 30.41 o 10 12 0 1081.15 1213.34 80.06 o 11 12 0 5.74 -26.61 26.61 o 12 12 0 299.71 328.66 78.95 o 1 13 0 18.36 2.47 7.80 o 2 13 0 2412.04 2416.82 36.24 o 3 13 0 22.51 20.81 8.92 o 4 13 0 156.98 148.04 12.48 o 5 13 0 263.49 270.02 16.43 o 6 13 0 329.15 352.44 18.79 o 7 13 0 540.82 561.93 27.41 o 8 13 0 2033.36 2018.93 55.48 o 9 13 0 17.25 21.87 18.63 o 10 13 0 18.95 -9.34 17.34 o 11 13 0 331.29 358.79 37.15 o 0 14 0 727.06 656.07 28.75 o 1 14 0 39.95 30.88 10.01 o 2 14 0 170.40 168.48 14.16 o 3 14 0 25.80 29.35 9.77 o 4 14 0 1575.57 1503.22 32.76 o 5 14 0 214.45 230.11 15.90 o 6 14 0 1166.36 1178.59 32.76 o 7 14 0 1.20 -6.25 13.41 o 8 14 0 31.75 26.54 17.72 o 9 14 0 5.43 65.47 20.66 o 10 14 0 623.14 668.08 37.92 o 11 14 0 11.80 25.93 20.90 o 1 15 0 335.05 328.39 16.76 o 2 15 0 1627.56 1641.47 34.50 o 3 15 0 52.41 42.80 11.66 o 4 15 0 250.18 261.80 20.16 o 5 15 0 2.27 -10.38 10.38 o 6 15 0 171.19 184.99 20.77 o 7 15 0 699.77 789.37 33.59 o 8 15 0 1066.80 1086.54 43.79 o 9 15 0 50.99 90.40 22.25 o 10 15 0 1.78 30.11 20.52 o 0 16 0 867.03 915.50 35.98 o 1 16 0 728.83 696.39 24.12 o 2 16 0 253.37 286.96 18.03 o 3 16 0 121.22 102.84 14.19 o 4 16 0 465.98 472.62 31.99 o 5 16 0 947.45 939.29 33.79 o 6 16 0 26.54 27.79 17.99 o 7 16 0 351.25 367.35 26.24 o 8 16 0 4.60 -8.16 17.57 o 9 16 0 260.69 310.25 30.35 o 1 17 0 459.51 494.74 22.31 o 2 17 0 218.80 196.94 17.24 o 3 17 0 626.88 646.92 33.37 o 4 17 0 34.18 12.53 12.90 o 5 17 0 138.05 145.26 18.97 o 6 17 0 71.25 60.05 19.45 o 7 17 0 713.48 798.25 72.14 o 8 17 0 124.47 168.45 33.94 o 9 17 0 58.16 82.05 23.75 o 0 18 0 1261.82 1281.28 51.33 o 1 18 0 13.57 3.28 13.30 o 2 18 0 6.50 -12.62 12.62 o 3 18 0 164.65 158.95 17.69 o 4 18 0 66.57 72.95 17.03 o 5 18 0 1022.29 1059.82 47.98 o 6 18 0 89.49 51.21 19.85 o 7 18 0 8.47 10.10 19.25 o 8 18 0 37.33 75.49 23.03 o 1 19 0 235.70 276.95 21.52 o 2 19 0 10.87 5.49 13.69 o 3 19 0 1177.17 1132.36 38.99 o 4 19 0 800.34 791.97 34.31 o 5 19 0 22.93 28.52 17.79 o 6 19 0 1.37 -16.58 16.58 o 7 19 0 452.42 504.52 36.90 o 0 20 0 1.02 -7.32 22.75 o 1 20 0 139.11 138.96 19.63 o 2 20 0 58.99 67.47 16.31 o 3 20 0 155.17 166.90 20.11 o 4 20 0 298.53 319.19 25.87 o 5 20 0 643.74 714.49 47.72 o 1 21 0 69.72 50.79 17.12 o 2 21 0 27.01 40.19 16.57 o 3 21 0 699.35 686.79 34.80 o -13 0 1 91.19 47.72 34.77 o -11 0 1 2085.91 2274.18 88.24 o -9 0 1 125.58 95.93 20.08 o -7 0 1 8.52 2.25 8.53 o -5 0 1 1160.67 1152.27 23.92 o -3 0 1 714.52 821.38 20.21 o -1 0 1 106886.08 102505.75 1621.77 o 3 0 1 15438.69 15843.40 341.41 o 5 0 1 267.38 274.97 19.73 o 7 0 1 6.00 8.40 7.84 o 9 0 1 6388.58 6323.56 114.32 o 11 0 1 1082.92 962.00 58.11 o 13 0 1 15.34 12.18 36.14 o -14 1 1 30.79 -23.45 25.97 o -13 1 1 176.36 207.41 30.84 o -12 1 1 19.17 10.12 22.02 o -11 1 1 1767.16 1820.43 70.63 o -10 1 1 7.85 -5.45 17.40 o -9 1 1 2849.64 2984.04 47.23 o -8 1 1 8.72 -0.07 6.83 o -7 1 1 220.25 169.34 8.62 o -6 1 1 156.52 164.08 8.74 o -5 1 1 435.11 323.46 8.60 o -4 1 1 357.44 413.47 10.14 o -3 1 1 951.51 853.22 15.40 o -2 1 1 359.91 278.07 9.66 o -1 1 1 1194.46 1178.47 37.51 o 0 1 1 938.20 953.88 28.17 o 2 1 1 14677.05 14850.01 160.78 o 3 1 1 2741.12 2816.45 42.96 o 4 1 1 117.58 121.63 10.71 o 5 1 1 73.54 57.59 7.30 o 6 1 1 204.47 204.28 9.73 o 7 1 1 1094.93 1061.99 18.96 o 8 1 1 515.44 483.28 18.24 o 9 1 1 39.51 43.67 14.03 o 10 1 1 960.63 1004.37 42.40 o 11 1 1 373.62 403.27 30.43 o 12 1 1 446.74 468.89 34.97 o 13 1 1 152.10 114.99 28.04 o 14 1 1 62.74 33.92 31.92 o -14 2 1 127.37 98.71 46.47 o -13 2 1 122.29 104.67 27.37 o -12 2 1 169.75 179.41 27.32 o -11 2 1 2198.03 2210.30 92.52 o -10 2 1 827.28 862.95 36.02 o -9 2 1 217.56 224.92 18.17 o -8 2 1 796.52 840.68 19.20 o -7 2 1 211.16 258.22 10.02 o -6 2 1 8035.13 7712.84 64.07 o -5 2 1 1399.19 1233.56 17.03 o -4 2 1 35.43 26.12 4.82 o -3 2 1 14464.11 15442.77 128.54 o -2 2 1 629.23 560.68 13.19 o -1 2 1 14581.69 16169.60 222.04 o 0 2 1 9243.56 9537.34 124.75 o 1 2 1 181.76 175.74 7.19 o 2 2 1 3721.06 3945.68 41.25 o 3 2 1 13940.08 14270.05 181.00 o 4 2 1 3010.40 2678.54 37.08 o 5 2 1 490.62 614.99 22.47 o 6 2 1 363.66 427.31 13.25 o 7 2 1 390.76 337.65 11.72 o 8 2 1 2151.09 2222.79 49.92 o 9 2 1 2249.98 2160.23 54.01 o 10 2 1 44.96 62.41 20.91 o 11 2 1 616.84 624.73 31.07 o 12 2 1 1.39 -17.22 21.61 o 13 2 1 285.95 305.69 33.49 o 14 2 1 1.24 5.95 34.06 o -14 3 1 142.27 207.06 32.68 o -13 3 1 130.37 151.35 29.11 o -12 3 1 71.67 71.79 26.81 o -11 3 1 618.36 662.35 38.37 o -10 3 1 42.36 33.97 18.71 o -9 3 1 444.28 436.07 30.60 o -8 3 1 147.19 143.81 10.44 o -7 3 1 32.61 44.46 6.77 o -6 3 1 1729.04 1708.97 22.16 o -5 3 1 1084.65 1367.89 18.33 o -4 3 1 13.63 11.29 4.46 o -3 3 1 276.80 393.79 17.16 o -2 3 1 65056.03 68000.97 480.99 o -1 3 1 4288.17 4538.62 41.85 o 0 3 1 56.93 57.44 6.04 o 1 3 1 7793.39 7997.20 76.03 o 2 3 1 969.15 1198.50 15.17 o 3 3 1 1628.16 1624.13 20.23 o 4 3 1 2158.64 2279.08 36.35 o 5 3 1 347.31 386.66 13.25 o 6 3 1 107.11 60.43 10.08 o 7 3 1 2098.68 2214.23 29.23 o 8 3 1 14.20 29.98 9.25 o 9 3 1 1.34 15.60 17.02 o 10 3 1 229.04 315.04 27.27 o 11 3 1 905.94 911.06 43.33 o 12 3 1 106.18 169.84 30.72 o 13 3 1 175.05 126.08 28.14 o 14 3 1 108.56 84.80 30.64 o -14 4 1 6.98 30.20 27.08 o -13 4 1 140.10 168.77 41.72 o -12 4 1 1182.08 1251.33 57.67 o -11 4 1 1956.33 1988.24 61.01 o -10 4 1 1283.23 1244.04 43.44 o -9 4 1 2261.87 2285.54 41.77 o -8 4 1 1341.07 1334.11 27.00 o -7 4 1 2244.09 2300.17 28.12 o -6 4 1 4871.41 4657.04 43.67 o -5 4 1 14.05 5.18 4.59 o -4 4 1 1157.43 1194.97 16.18 o -3 4 1 219.90 226.52 15.51 o -2 4 1 16555.12 17688.64 137.15 o -1 4 1 5235.51 5731.82 43.82 o 0 4 1 163.59 110.37 6.27 o 1 4 1 1533.32 1661.83 20.34 o 2 4 1 6.75 6.40 3.78 o 3 4 1 28412.61 29399.78 221.71 o 4 4 1 12050.77 11558.51 110.14 o 5 4 1 1878.38 2207.91 29.84 o 6 4 1 14.72 0.17 6.72 o 7 4 1 688.96 698.58 18.58 o 8 4 1 4325.92 4141.47 51.37 o 9 4 1 190.43 191.54 22.44 o 10 4 1 726.97 685.05 34.40 o 11 4 1 190.87 164.32 24.47 o 12 4 1 140.47 126.15 57.92 o 13 4 1 59.25 35.55 30.62 o 14 4 1 939.52 1118.62 52.78 o -14 5 1 450.46 525.50 60.57 o -13 5 1 71.58 116.05 33.28 o -12 5 1 584.47 620.25 43.00 o -11 5 1 58.89 77.10 27.32 o -10 5 1 19.38 19.22 14.63 o -9 5 1 409.60 393.54 21.16 o -8 5 1 262.87 268.14 16.26 o -7 5 1 440.60 482.23 12.85 o -6 5 1 6.40 18.06 5.12 o -5 5 1 37.44 66.85 8.76 o -4 5 1 27459.95 27608.38 196.10 o -3 5 1 15401.31 16747.80 116.69 o -2 5 1 21468.72 21568.00 147.38 o -1 5 1 84.00 96.52 4.90 o 0 5 1 220.73 154.66 5.88 o 1 5 1 1833.76 1760.26 17.37 o 2 5 1 14.50 24.35 3.78 o 3 5 1 1902.57 2067.28 22.52 o 4 5 1 1297.58 1476.77 20.82 o 5 5 1 117.74 95.77 9.16 o 6 5 1 3861.64 3715.32 40.78 o 7 5 1 1.08 2.84 8.82 o 8 5 1 1965.56 1957.22 49.06 o 9 5 1 1327.18 1342.42 36.95 o 10 5 1 1260.28 1292.34 45.20 o 11 5 1 414.18 436.40 31.27 o 12 5 1 435.97 458.07 57.17 o 13 5 1 117.82 59.17 31.68 o 14 5 1 13.25 17.83 31.15 o -14 6 1 41.80 49.67 40.80 o -13 6 1 74.97 48.94 42.66 o -12 6 1 472.93 592.98 43.95 o -11 6 1 87.25 56.41 23.28 o -10 6 1 1361.40 1457.34 39.96 o -9 6 1 5.12 4.99 11.99 o -8 6 1 1024.95 993.55 27.32 o -7 6 1 46.19 48.10 10.02 o -6 6 1 444.20 403.79 10.58 o -5 6 1 3760.98 4046.86 50.22 o -4 6 1 1681.00 1717.43 25.42 o -3 6 1 17434.28 18575.28 142.11 o -2 6 1 10.88 28.78 4.41 o -1 6 1 718.13 716.42 11.78 o 0 6 1 346.12 263.09 7.83 o 1 6 1 159.25 171.93 5.76 o 2 6 1 2629.88 2715.55 23.67 o 3 6 1 6799.01 7106.44 50.63 o 4 6 1 8173.62 7456.72 58.90 o 5 6 1 2118.41 2141.09 28.23 o 6 6 1 355.59 374.29 15.10 o 7 6 1 370.43 399.63 17.56 o 8 6 1 450.33 439.15 19.49 o 9 6 1 498.12 512.95 22.01 o 10 6 1 372.05 302.76 27.31 o 11 6 1 274.23 248.24 32.29 o 12 6 1 323.71 338.76 37.45 o 13 6 1 19.71 26.49 28.98 o -13 7 1 1.55 64.92 38.47 o -12 7 1 544.12 609.43 54.91 o -11 7 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