#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220873.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220873_Fobs loop_ _publ_author_name 'Hua, Yu-Peng' 'Xu, Ying' 'Wei, Xue-Hong' 'Tong, Hong-Bo' _publ_section_title ; 2-Chloropyridine-3-carboxamide ; _journal_coeditor_code NC2131 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o373 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.822 _cell_angle_gamma 90.000 _cell_length_a 6.9804 _cell_length_b 13.6270 _cell_length_c 7.1081 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file nc2131Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s585p in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 122.75 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8.84 10.76 0.45 o 4 0 0 660.94 665.54 12.32 o 6 0 0 336.52 325.86 8.16 o 8 0 0 0.04 0.52 1.20 o 1 1 0 1030.77 1039.21 19.88 o 2 1 0 383.88 438.77 6.28 o 3 1 0 226.77 215.77 2.79 o 4 1 0 21.43 28.82 0.70 o 5 1 0 12.68 13.47 0.88 o 6 1 0 50.51 52.62 1.70 o 7 1 0 118.94 120.46 4.62 o 8 1 0 23.46 23.29 2.83 o 0 2 0 254.76 253.11 7.15 o 1 2 0 672.67 590.23 16.09 o 2 2 0 445.20 495.35 6.28 o 3 2 0 1574.34 1702.86 20.85 o 4 2 0 516.90 590.40 7.09 o 5 2 0 284.42 286.02 5.01 o 6 2 0 27.57 28.04 1.81 o 7 2 0 0.59 2.57 0.72 o 8 2 0 16.66 19.66 2.07 o 2 3 0 1486.88 1545.82 18.91 o 3 3 0 781.25 861.39 10.83 o 4 3 0 807.58 885.04 10.39 o 5 3 0 77.60 77.29 4.02 o 6 3 0 0.25 1.04 0.58 o 7 3 0 26.68 25.36 1.65 o 8 3 0 112.16 109.90 6.80 o 0 4 0 216.99 208.93 6.38 o 1 4 0 1084.45 1047.45 16.56 o 2 4 0 256.86 240.18 3.69 o 3 4 0 3.22 3.88 0.33 o 4 4 0 352.38 347.36 5.49 o 5 4 0 411.95 412.75 6.81 o 6 4 0 556.47 537.76 14.43 o 7 4 0 5.68 5.28 1.20 o 8 4 0 47.70 43.24 4.03 o 1 5 0 2.79 6.43 0.61 o 2 5 0 750.05 743.05 10.54 o 3 5 0 349.14 311.16 4.34 o 4 5 0 24.56 29.76 1.04 o 5 5 0 34.36 32.34 3.04 o 6 5 0 0.25 0.25 0.72 o 7 5 0 76.18 76.86 3.44 o 0 6 0 1.26 1.04 0.56 o 1 6 0 815.61 843.15 13.71 o 2 6 0 92.53 104.87 2.36 o 3 6 0 45.15 52.36 1.18 o 4 6 0 286.90 304.70 5.02 o 5 6 0 253.27 240.00 4.39 o 6 6 0 47.44 41.82 2.43 o 7 6 0 1.28 1.11 0.94 o 1 7 0 638.71 755.89 12.51 o 2 7 0 357.07 349.64 8.48 o 3 7 0 3.79 3.18 0.46 o 4 7 0 619.58 648.85 11.23 o 5 7 0 125.45 123.09 2.79 o 6 7 0 142.30 143.89 4.96 o 7 7 0 9.13 8.50 1.89 o 0 8 0 221.06 251.55 8.38 o 1 8 0 441.16 452.34 7.99 o 2 8 0 62.57 48.61 1.59 o 3 8 0 27.32 27.43 1.20 o 4 8 0 48.74 43.85 1.70 o 5 8 0 129.09 119.41 6.03 o 6 8 0 64.54 60.54 3.07 o 7 8 0 5.04 5.75 1.50 o 1 9 0 368.97 370.03 16.69 o 2 9 0 31.54 29.64 1.29 o 3 9 0 80.09 81.93 2.33 o 4 9 0 236.20 237.12 5.10 o 5 9 0 2.48 2.54 0.82 o 6 9 0 17.23 14.73 1.83 o 0 10 0 482.88 491.77 15.39 o 1 10 0 121.56 126.82 3.79 o 2 10 0 202.36 206.46 4.47 o 3 10 0 8.98 9.80 1.20 o 4 10 0 306.56 323.95 6.63 o 5 10 0 35.09 39.11 2.92 o 6 10 0 41.40 43.27 2.89 o 1 11 0 77.57 73.88 8.16 o 2 11 0 561.45 581.02 12.75 o 3 11 0 2.98 2.86 0.68 o 4 11 0 1.24 1.39 0.83 o 5 11 0 11.52 11.30 1.23 o 6 11 0 4.16 8.97 1.75 o 0 12 0 56.57 58.69 3.67 o 1 12 0 13.55 20.05 1.85 o 2 12 0 51.72 41.18 2.17 o 3 12 0 32.40 35.33 2.20 o 4 12 0 8.13 9.01 1.33 o 5 12 0 9.71 10.31 1.26 o 1 13 0 125.98 113.45 3.99 o 2 13 0 96.26 99.20 3.70 o 3 13 0 36.83 43.41 2.35 o 4 13 0 18.02 16.28 1.79 o 0 14 0 80.91 73.37 4.56 o 1 14 0 0.38 1.41 0.80 o 2 14 0 0.05 1.57 0.81 o 3 14 0 66.22 79.95 3.40 o 4 14 0 10.80 16.09 2.37 o 1 15 0 0.04 0.97 0.92 o 2 15 0 13.07 19.55 2.24 o 3 15 0 7.91 10.10 1.95 o 0 16 0 0.24 0.16 1.11 o 1 16 0 50.88 52.33 2.90 o -7 0 1 76.98 74.90 3.25 o -5 0 1 849.10 805.66 17.27 o -3 0 1 4634.68 4700.72 126.15 o -1 0 1 614.96 707.65 13.67 o 1 0 1 1474.28 1356.83 21.52 o 3 0 1 608.05 601.68 10.02 o 5 0 1 171.32 171.99 4.82 o 7 0 1 109.17 107.28 6.10 o -8 1 1 2.36 1.99 1.04 o -7 1 1 19.52 20.72 1.29 o -6 1 1 31.78 32.77 3.20 o -5 1 1 859.55 853.44 17.48 o -4 1 1 15.01 19.96 1.05 o -3 1 1 234.19 278.65 6.04 o -2 1 1 768.01 755.60 12.09 o -1 1 1 1300.29 1321.98 38.88 o 0 1 1 412.35 417.64 6.75 o 1 1 1 3458.49 3310.99 65.87 o 2 1 1 196.03 180.69 2.54 o 3 1 1 132.04 130.18 1.85 o 4 1 1 1749.28 1832.30 27.25 o 5 1 1 2.72 2.84 0.47 o 6 1 1 180.18 172.71 5.54 o 7 1 1 10.81 15.28 1.76 o 8 1 1 67.58 70.77 3.65 o -8 2 1 185.30 200.13 6.89 o -7 2 1 29.22 30.62 1.46 o -6 2 1 62.84 52.69 1.83 o -5 2 1 84.62 84.42 2.45 o -4 2 1 558.91 574.32 8.51 o -3 2 1 147.89 159.81 2.75 o -2 2 1 0.72 0.30 0.15 o -1 2 1 1013.86 1005.02 19.55 o 0 2 1 2597.25 2505.41 62.44 o 1 2 1 2.11 7.35 0.80 o 2 2 1 950.04 939.49 10.69 o 3 2 1 574.79 619.42 7.30 o 4 2 1 0.84 0.45 0.24 o 5 2 1 53.32 54.01 1.51 o 6 2 1 833.58 852.02 19.36 o 7 2 1 59.24 58.86 3.07 o 8 2 1 2.50 4.70 1.19 o -8 3 1 5.87 5.60 1.37 o -7 3 1 34.75 35.23 1.84 o -6 3 1 184.46 182.99 3.84 o -5 3 1 352.12 342.62 17.85 o -4 3 1 39.69 37.98 1.10 o -3 3 1 2.81 4.00 0.29 o -2 3 1 2490.45 2511.19 84.86 o -1 3 1 7114.95 6492.63 173.04 o 0 3 1 110.63 85.16 1.44 o 1 3 1 31.52 32.52 0.80 o 2 3 1 12.96 10.89 0.41 o 3 3 1 102.59 97.58 1.95 o 4 3 1 438.59 455.70 5.66 o 5 3 1 153.03 151.29 3.03 o 6 3 1 0.25 1.01 0.75 o 7 3 1 11.12 9.37 1.43 o 8 3 1 36.76 36.51 2.76 o -8 4 1 7.46 11.55 2.37 o -7 4 1 144.17 146.43 5.08 o -6 4 1 47.27 46.36 2.29 o -5 4 1 144.56 153.54 3.64 o -4 4 1 81.12 81.37 1.82 o -3 4 1 209.35 191.73 4.04 o -2 4 1 1.56 1.27 0.35 o -1 4 1 208.06 204.86 3.67 o 0 4 1 1346.36 1392.95 24.08 o 1 4 1 1089.77 1083.65 17.45 o 2 4 1 2015.39 2129.82 26.27 o 3 4 1 591.24 630.96 7.52 o 4 4 1 123.95 135.07 2.23 o 5 4 1 205.46 203.60 3.83 o 6 4 1 20.30 20.59 2.05 o 7 4 1 26.62 27.05 3.77 o -7 5 1 0.04 2.02 0.89 o -6 5 1 149.65 142.70 4.52 o -5 5 1 55.12 53.49 2.65 o -4 5 1 202.28 199.41 3.55 o -3 5 1 66.10 69.44 1.97 o -2 5 1 369.18 380.11 7.30 o -1 5 1 57.56 72.73 1.70 o 0 5 1 1621.86 1674.57 26.38 o 1 5 1 367.25 420.93 7.24 o 2 5 1 676.44 692.68 10.02 o 3 5 1 123.30 121.62 1.92 o 4 5 1 42.11 39.03 1.15 o 5 5 1 20.51 19.51 1.64 o 6 5 1 0.31 1.77 0.80 o 7 5 1 0.24 -1.43 1.37 o -7 6 1 0.02 0.02 0.81 o -6 6 1 45.15 39.80 2.36 o -5 6 1 10.99 8.24 1.18 o -4 6 1 356.65 382.42 9.01 o -3 6 1 136.57 135.78 2.56 o -2 6 1 1112.66 1127.67 18.09 o -1 6 1 62.57 71.85 1.78 o 0 6 1 4339.63 4425.65 103.74 o 1 6 1 1125.02 1197.63 23.47 o 2 6 1 184.87 168.21 3.02 o 3 6 1 0.55 1.15 0.41 o 4 6 1 35.53 41.12 1.43 o 5 6 1 23.07 23.07 1.10 o 6 6 1 108.84 103.81 6.43 o 7 6 1 54.24 55.10 4.78 o -7 7 1 141.89 142.72 5.27 o -6 7 1 0.00 0.77 0.80 o -5 7 1 13.96 14.24 1.47 o -4 7 1 22.03 20.07 1.16 o -3 7 1 5.96 6.09 0.68 o -2 7 1 132.94 123.99 3.43 o -1 7 1 527.13 491.50 8.46 o 0 7 1 0.95 2.23 0.44 o 1 7 1 510.48 521.58 10.95 o 2 7 1 105.26 111.09 2.61 o 3 7 1 773.19 753.31 11.61 o 4 7 1 10.07 8.97 1.29 o 5 7 1 316.13 313.87 6.42 o 6 7 1 41.70 41.14 2.52 o 7 7 1 3.36 1.71 1.76 o -7 8 1 16.64 18.79 2.11 o -6 8 1 11.44 9.97 2.00 o -5 8 1 68.43 70.59 2.98 o -4 8 1 837.78 819.24 14.32 o -3 8 1 607.45 592.39 10.34 o -2 8 1 20.58 15.32 0.93 o -1 8 1 170.78 174.44 3.67 o 0 8 1 52.97 50.92 1.97 o 1 8 1 226.97 204.55 5.11 o 2 8 1 49.37 42.00 1.79 o 3 8 1 101.32 93.36 2.18 o 4 8 1 231.85 226.27 5.60 o 5 8 1 67.33 68.63 2.36 o 6 8 1 0.23 1.56 1.04 o 7 8 1 10.65 12.46 1.88 o -6 9 1 35.42 35.78 3.27 o -5 9 1 50.02 42.15 3.65 o -4 9 1 16.38 18.34 1.74 o -3 9 1 32.17 26.59 2.14 o -2 9 1 348.46 367.05 6.86 o -1 9 1 138.42 124.56 2.97 o 0 9 1 290.37 269.35 11.33 o 1 9 1 9.64 9.61 1.02 o 2 9 1 108.87 102.73 3.90 o 3 9 1 52.70 50.98 1.57 o 4 9 1 430.62 442.39 7.28 o 5 9 1 273.45 288.53 8.07 o 6 9 1 17.05 15.05 1.83 o -6 10 1 1.81 0.71 1.42 o -5 10 1 181.88 175.61 4.36 o -4 10 1 30.99 25.93 1.50 o -3 10 1 224.67 228.57 5.86 o -2 10 1 1.36 1.36 0.73 o -1 10 1 153.95 138.62 3.33 o 0 10 1 16.79 21.66 1.43 o 1 10 1 259.34 260.61 6.51 o 2 10 1 329.62 333.60 13.39 o 3 10 1 120.49 117.00 2.70 o 4 10 1 0.43 0.51 0.61 o 5 10 1 51.67 48.73 2.09 o 6 10 1 71.88 63.46 3.37 o -6 11 1 20.94 25.62 3.30 o -5 11 1 184.44 180.54 4.58 o -4 11 1 19.82 21.42 3.27 o -3 11 1 0.06 0.50 0.52 o -2 11 1 20.30 20.80 1.31 o -1 11 1 384.09 374.44 8.82 o 0 11 1 12.31 12.44 1.26 o 1 11 1 78.81 72.50 2.81 o 2 11 1 159.07 158.32 4.67 o 3 11 1 27.78 27.47 1.42 o 4 11 1 144.65 142.39 3.87 o 5 11 1 0.32 1.37 0.72 o -5 12 1 16.53 16.61 1.74 o -4 12 1 44.41 44.74 2.06 o -3 12 1 4.47 3.21 0.69 o -2 12 1 13.02 12.18 1.11 o -1 12 1 74.11 71.77 5.55 o 0 12 1 2.00 1.70 0.67 o 1 12 1 0.34 0.57 0.60 o 2 12 1 190.26 204.64 7.99 o 3 12 1 211.65 213.41 7.87 o 4 12 1 9.68 10.53 1.85 o 5 12 1 7.31 8.85 1.21 o -4 13 1 9.35 12.95 1.32 o -3 13 1 70.92 66.37 4.05 o -2 13 1 253.31 248.72 6.78 o -1 13 1 78.08 85.35 3.37 o 0 13 1 1.31 2.91 0.83 o 1 13 1 1.48 1.55 0.68 o 2 13 1 57.46 52.28 6.73 o 3 13 1 61.06 62.93 3.10 o 4 13 1 114.46 132.55 6.44 o -4 14 1 14.34 17.64 1.77 o -3 14 1 32.04 35.10 2.25 o -2 14 1 4.76 4.35 1.06 o -1 14 1 23.20 23.01 2.26 o 0 14 1 20.03 18.84 1.83 o 1 14 1 1.66 2.57 1.21 o 2 14 1 10.00 10.73 1.39 o 3 14 1 38.49 35.90 5.68 o 4 14 1 1.57 3.20 1.26 o -3 15 1 3.61 6.85 1.71 o -2 15 1 18.30 17.24 1.79 o -1 15 1 18.70 25.40 2.57 o 0 15 1 6.81 8.26 1.48 o 1 15 1 0.29 -0.43 0.82 o 2 15 1 38.94 35.23 3.17 o 0 16 1 3.06 1.48 1.04 o -8 0 2 123.53 136.22 5.09 o -6 0 2 34.16 34.62 2.89 o -4 0 2 156.57 154.25 6.10 o -2 0 2 2285.26 2375.84 45.22 o 2 0 2 307.31 304.31 6.73 o 4 0 2 108.35 103.87 2.81 o 6 0 2 47.57 51.89 3.87 o 8 0 2 110.92 118.03 6.93 o -8 1 2 36.95 44.42 2.23 o -7 1 2 7.01 8.31 0.94 o -6 1 2 41.68 44.05 1.89 o -5 1 2 205.28 197.88 5.42 o -4 1 2 51.10 40.96 3.93 o -3 1 2 570.27 598.83 14.70 o -2 1 2 2095.63 2143.64 28.92 o -1 1 2 439.57 439.62 6.28 o 0 1 2 1074.69 1158.68 15.76 o 1 1 2 15067.10 13571.35 185.05 o 2 1 2 55.38 62.50 1.39 o 3 1 2 25.08 23.09 0.58 o 4 1 2 335.05 352.45 6.37 o 5 1 2 352.93 361.74 6.01 o 6 1 2 2.85 2.75 0.86 o 7 1 2 19.77 21.09 2.04 o -8 2 2 28.71 27.71 1.95 o -7 2 2 229.60 230.24 5.54 o -6 2 2 162.63 158.59 4.04 o -5 2 2 0.64 0.28 0.65 o -4 2 2 195.10 217.44 5.89 o -3 2 2 1013.20 1128.24 18.15 o -2 2 2 529.74 580.07 8.59 o -1 2 2 2347.84 2435.12 32.73 o 0 2 2 450.83 482.02 13.75 o 1 2 2 317.03 335.15 4.92 o 2 2 2 394.76 428.93 6.48 o 3 2 2 190.83 163.92 3.04 o 4 2 2 92.38 101.97 3.33 o 5 2 2 16.38 16.19 0.91 o 6 2 2 9.52 13.04 1.56 o 7 2 2 7.80 8.41 1.37 o -7 3 2 1.35 -0.25 0.86 o -6 3 2 14.31 14.22 1.51 o -5 3 2 310.37 307.42 6.25 o -4 3 2 597.15 567.40 16.23 o -3 3 2 10.41 17.09 0.59 o -2 3 2 261.18 277.16 4.24 o -1 3 2 743.96 722.00 10.11 o 0 3 2 1104.03 1096.90 15.14 o 1 3 2 307.26 324.88 7.05 o 2 3 2 326.77 320.10 4.37 o 3 3 2 400.30 445.05 5.44 o 4 3 2 573.53 615.52 8.29 o 5 3 2 1.81 1.69 0.57 o 6 3 2 479.41 461.11 11.62 o 7 3 2 235.07 242.05 10.69 o -7 4 2 10.40 13.40 1.64 o -6 4 2 0.04 1.29 0.86 o -5 4 2 70.76 73.25 2.93 o -4 4 2 0.98 1.09 0.75 o -3 4 2 1142.11 1206.76 16.74 o -2 4 2 533.11 523.19 7.60 o -1 4 2 413.27 424.15 7.12 o 0 4 2 310.19 294.98 4.43 o 1 4 2 31.08 29.74 0.81 o 2 4 2 870.39 839.44 13.92 o 3 4 2 210.00 216.40 3.35 o 4 4 2 108.65 102.05 1.99 o 5 4 2 68.03 70.51 1.89 o 6 4 2 181.77 181.47 6.69 o 7 4 2 29.30 30.59 2.48 o -7 5 2 6.03 3.95 1.24 o -6 5 2 4.60 4.20 1.08 o -5 5 2 767.59 767.21 16.54 o -4 5 2 32.47 31.60 1.31 o -3 5 2 245.54 238.51 3.92 o -2 5 2 186.67 203.85 3.25 o -1 5 2 78.52 72.21 1.73 o 0 5 2 30.74 30.19 0.82 o 1 5 2 66.94 53.04 2.91 o 2 5 2 31.35 33.45 1.20 o 3 5 2 99.49 116.29 2.35 o 4 5 2 34.57 37.69 2.17 o 5 5 2 315.73 328.70 9.77 o 6 5 2 5.69 5.43 1.68 o 7 5 2 29.35 25.28 2.30 o -7 6 2 121.20 123.37 4.57 o -6 6 2 38.52 41.87 2.37 o -5 6 2 9.12 9.83 1.31 o -4 6 2 223.99 214.68 4.69 o -3 6 2 799.01 782.44 11.29 o -2 6 2 94.82 78.52 1.74 o -1 6 2 67.41 58.32 1.60 o 0 6 2 29.28 32.49 0.89 o 1 6 2 64.77 64.62 1.72 o 2 6 2 24.60 24.56 1.07 o 3 6 2 958.04 973.90 14.08 o 4 6 2 50.67 42.99 2.59 o 5 6 2 72.63 70.34 2.00 o 6 6 2 9.91 12.15 1.58 o 7 6 2 97.34 97.36 6.49 o -7 7 2 0.92 2.79 1.21 o -6 7 2 96.86 89.86 3.66 o -5 7 2 55.85 48.89 2.49 o -4 7 2 117.49 96.96 2.67 o -3 7 2 11.79 12.63 0.76 o -2 7 2 160.69 156.23 4.27 o -1 7 2 235.95 281.28 7.21 o 0 7 2 653.20 683.43 9.89 o 1 7 2 88.15 92.60 2.26 o 2 7 2 402.38 412.18 7.51 o 3 7 2 12.22 12.38 0.90 o 4 7 2 243.09 237.34 4.33 o 5 7 2 58.43 60.66 1.88 o 6 7 2 88.44 80.04 5.44 o 7 7 2 0.29 0.41 1.53 o -7 8 2 101.10 100.81 5.86 o -6 8 2 111.64 114.82 4.32 o -5 8 2 0.01 0.90 0.82 o -4 8 2 0.34 0.86 0.54 o -3 8 2 19.19 16.75 1.53 o -2 8 2 50.84 47.38 1.68 o -1 8 2 46.79 42.58 2.37 o 0 8 2 50.98 58.01 2.97 o 1 8 2 102.17 97.42 4.18 o 2 8 2 50.12 57.20 1.81 o 3 8 2 31.39 29.28 1.54 o 4 8 2 116.55 114.91 2.65 o 5 8 2 19.52 19.20 1.37 o 6 8 2 102.83 113.13 6.69 o -6 9 2 5.34 6.18 1.39 o -5 9 2 167.96 168.15 16.36 o -4 9 2 61.59 56.35 2.08 o -3 9 2 150.55 146.29 3.61 o -2 9 2 83.51 76.25 3.32 o -1 9 2 609.90 608.69 29.15 o 0 9 2 245.07 255.31 5.07 o 1 9 2 206.93 212.48 7.57 o 2 9 2 56.93 59.86 1.92 o 3 9 2 55.24 52.37 1.88 o 4 9 2 18.35 19.75 1.27 o 5 9 2 245.94 258.27 5.80 o 6 9 2 0.47 0.33 0.68 o -6 10 2 2.47 3.78 1.28 o -5 10 2 3.21 3.74 1.21 o -4 10 2 114.75 107.17 3.13 o -3 10 2 54.69 51.33 2.00 o -2 10 2 44.61 42.78 3.11 o -1 10 2 364.81 379.81 7.19 o 0 10 2 62.90 62.53 2.48 o 1 10 2 34.98 38.04 1.91 o 2 10 2 1000.48 1009.03 48.74 o 3 10 2 259.24 257.89 5.48 o 4 10 2 12.33 14.20 1.15 o 5 10 2 7.81 9.93 1.80 o 6 10 2 1.81 1.95 0.89 o -5 11 2 0.48 0.78 1.00 o -4 11 2 97.12 98.45 3.84 o -3 11 2 38.09 35.27 2.01 o -2 11 2 2.77 3.26 0.67 o -1 11 2 34.73 30.32 1.44 o 0 11 2 9.56 10.62 1.21 o 1 11 2 37.56 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