#------------------------------------------------------------------------------ #$Date: 2016-04-03 03:57:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181129 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/08/2220896.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220896_Fobs loop_ _publ_author_name 'Khawar Rauf, M.' 'Bolte, Michael' 'Badshah, Amin' _publ_section_title ; 1-(4-Chlorophenyl)-3-(2,4-dichlorobenzoyl)thiourea ; _journal_coeditor_code RK2121 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o260 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.919 _cell_angle_beta 98.005 _cell_angle_gamma 101.330 _cell_length_a 5.9674 _cell_length_b 9.6577 _cell_length_c 13.9585 _exptl_crystal_F_000 364.00 _reflns_d_resolution_high 0.7803 _cod_data_source_file rk2121Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rauf40 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 96.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1051.50 883.50 74.12 o 2 0 0 9365.12 9387.75 201.01 o 3 0 0 169.25 154.87 5.83 o 4 0 0 559.03 513.03 16.69 o 5 0 0 233.99 223.72 9.25 o 6 0 0 5.23 5.86 0.84 o 7 0 0 17.39 20.29 1.03 o -7 1 0 2.76 3.05 1.19 o -6 1 0 715.50 742.93 31.59 o -5 1 0 7.07 10.08 1.09 o -4 1 0 139.89 128.93 4.10 o -3 1 0 745.27 733.15 8.26 o -2 1 0 411.72 391.11 13.19 o -1 1 0 424.41 363.10 24.48 o 1 1 0 30.30 26.48 1.15 o 2 1 0 153.24 154.27 4.02 o 3 1 0 223.79 216.11 6.06 o 4 1 0 646.51 612.95 24.95 o 5 1 0 401.50 404.62 14.81 o 6 1 0 17.38 19.66 0.90 o 7 1 0 1.06 1.06 1.25 o -7 2 0 39.46 37.74 2.00 o -6 2 0 404.91 424.71 15.49 o -5 2 0 179.36 193.71 8.07 o -4 2 0 546.32 494.35 22.39 o -3 2 0 1635.56 1581.76 163.99 o -2 2 0 12.54 10.51 1.50 o -1 2 0 555.79 519.12 13.72 o 0 2 0 3898.53 4248.59 158.93 o 1 2 0 1398.43 1417.51 15.94 o 2 2 0 746.33 705.79 14.35 o 3 2 0 2.23 3.44 0.71 o 4 2 0 56.38 46.81 1.31 o 5 2 0 105.05 98.97 3.90 o 6 2 0 1.64 3.07 0.98 o 7 2 0 8.49 9.32 1.17 o -7 3 0 19.15 21.10 1.27 o -6 3 0 200.89 206.88 9.26 o -5 3 0 216.95 213.74 7.50 o -4 3 0 644.56 673.27 59.80 o -3 3 0 331.48 333.11 11.46 o -2 3 0 587.06 640.66 17.88 o -1 3 0 277.51 248.00 8.36 o 0 3 0 273.39 314.18 3.79 o 1 3 0 417.32 422.28 2.98 o 2 3 0 148.18 153.88 6.30 o 3 3 0 204.07 190.87 5.92 o 4 3 0 7.67 9.22 2.39 o 5 3 0 13.99 12.20 0.71 o 6 3 0 243.47 238.92 6.28 o -7 4 0 14.67 13.15 1.10 o -6 4 0 249.06 251.41 5.41 o -5 4 0 3.90 0.98 1.43 o -4 4 0 648.43 632.21 25.58 o -3 4 0 201.52 220.83 6.46 o -2 4 0 2342.04 2430.79 21.29 o -1 4 0 340.53 328.98 3.21 o 0 4 0 705.93 642.22 8.36 o 1 4 0 504.65 442.55 35.84 o 2 4 0 303.36 293.81 5.73 o 3 4 0 131.29 125.01 1.91 o 4 4 0 201.36 196.80 1.55 o 5 4 0 51.51 49.18 1.97 o 6 4 0 59.31 53.14 0.98 o -7 5 0 42.70 44.76 2.08 o -6 5 0 13.50 14.35 1.18 o -5 5 0 56.63 59.20 5.04 o -4 5 0 429.05 427.02 4.62 o -3 5 0 329.34 316.59 2.32 o -2 5 0 3443.56 3466.78 32.56 o -1 5 0 143.32 135.47 2.89 o 0 5 0 2127.85 1900.13 63.66 o 1 5 0 7.09 12.54 3.36 o 2 5 0 548.83 551.93 7.03 o 3 5 0 56.89 52.59 1.55 o 4 5 0 329.58 336.34 3.60 o 5 5 0 0.00 -0.12 0.77 o 6 5 0 124.11 117.11 2.70 o -7 6 0 21.88 22.78 1.60 o -6 6 0 0.92 1.00 0.93 o -5 6 0 4.74 8.17 0.99 o -4 6 0 14.04 13.45 1.00 o -3 6 0 51.08 60.93 1.14 o -2 6 0 498.04 530.32 21.85 o -1 6 0 42.92 41.17 1.76 o 0 6 0 131.59 120.43 1.38 o 1 6 0 657.17 677.22 26.77 o 2 6 0 23.47 28.02 1.20 o 3 6 0 565.78 599.87 14.87 o 4 6 0 142.97 141.44 8.47 o 5 6 0 75.65 79.31 1.42 o -6 7 0 284.88 303.31 11.74 o -5 7 0 75.87 74.21 4.05 o -4 7 0 54.54 51.86 1.20 o -3 7 0 24.73 26.66 1.04 o -2 7 0 611.59 586.77 5.38 o -1 7 0 0.37 0.35 0.67 o 0 7 0 1529.53 1576.43 14.30 o 1 7 0 328.54 318.99 8.51 o 2 7 0 146.42 147.29 2.97 o 3 7 0 144.56 145.50 5.31 o 4 7 0 67.49 64.22 1.22 o 5 7 0 0.59 -0.35 0.95 o -6 8 0 21.57 27.62 1.10 o -5 8 0 512.66 537.14 11.67 o -4 8 0 82.22 87.38 2.08 o -3 8 0 683.38 664.78 7.56 o -2 8 0 35.63 36.70 1.26 o -1 8 0 29.73 28.49 1.54 o 0 8 0 32.19 35.20 2.43 o 1 8 0 3.62 5.08 1.18 o 2 8 0 21.48 20.47 0.77 o 3 8 0 53.03 56.76 1.12 o 4 8 0 0.16 1.64 0.93 o -6 9 0 33.95 33.09 1.15 o -5 9 0 0.00 1.77 0.84 o -4 9 0 19.13 24.04 0.87 o -3 9 0 76.09 81.61 2.45 o -2 9 0 389.31 419.98 24.41 o -1 9 0 554.66 542.20 7.80 o 0 9 0 171.94 172.36 6.05 o 1 9 0 120.61 121.20 3.69 o 2 9 0 37.57 38.25 1.17 o 3 9 0 5.68 5.21 0.84 o -5 10 0 21.09 20.30 1.11 o -4 10 0 199.74 203.66 4.06 o -3 10 0 9.88 13.35 1.11 o -2 10 0 540.83 527.55 3.58 o -1 10 0 70.51 71.45 2.99 o 0 10 0 126.45 127.61 3.90 o 1 10 0 38.27 31.75 0.89 o 2 10 0 0.52 0.94 0.71 o 3 10 0 0.85 2.75 1.05 o -4 11 0 0.00 -0.21 0.99 o -3 11 0 28.73 30.21 1.17 o -2 11 0 53.65 48.30 3.42 o -1 11 0 44.58 36.03 1.35 o 0 11 0 0.14 0.25 1.22 o 1 11 0 46.22 48.13 2.01 o -3 12 0 0.70 2.36 1.24 o -2 12 0 84.42 80.81 3.45 o -1 12 0 156.44 140.03 4.49 o 0 12 0 84.00 78.21 3.60 o 0 -12 1 64.03 66.08 2.48 o 1 -12 1 1.49 4.12 1.13 o 2 -12 1 9.08 12.26 1.07 o 3 -12 1 72.73 66.96 1.64 o -2 -11 1 18.00 22.08 0.99 o -1 -11 1 9.43 8.22 0.79 o 0 -11 1 65.84 72.73 2.83 o 1 -11 1 118.62 116.93 3.17 o 2 -11 1 2.93 4.34 1.40 o 3 -11 1 9.49 10.87 1.39 o 4 -11 1 102.77 105.83 3.34 o -3 -10 1 48.94 44.78 1.29 o -2 -10 1 0.01 1.24 0.68 o -1 -10 1 7.67 8.93 0.81 o 0 -10 1 358.06 343.03 7.22 o 1 -10 1 43.12 40.85 1.29 o 2 -10 1 594.81 558.83 4.20 o 3 -10 1 34.55 38.91 3.76 o 4 -10 1 188.12 176.71 2.23 o 5 -10 1 27.27 28.99 1.03 o -4 -9 1 0.21 0.11 1.18 o -3 -9 1 42.46 44.47 0.96 o -2 -9 1 136.48 149.52 2.43 o -1 -9 1 6.12 6.76 0.79 o 0 -9 1 104.15 99.33 2.61 o 1 -9 1 6.25 6.19 0.96 o 2 -9 1 198.80 189.67 3.95 o 3 -9 1 24.52 23.50 1.04 o 4 -9 1 19.21 16.89 1.56 o 5 -9 1 1.24 2.22 1.93 o 6 -9 1 14.82 16.58 1.31 o -4 -8 1 281.48 276.42 4.05 o -3 -8 1 132.66 137.22 2.60 o -2 -8 1 31.42 31.01 1.30 o -1 -8 1 781.88 802.22 28.72 o 0 -8 1 145.52 147.52 3.64 o 1 -8 1 4.84 3.70 0.86 o 2 -8 1 185.15 193.31 2.97 o 3 -8 1 308.12 293.83 6.25 o 4 -8 1 87.50 85.15 2.83 o 5 -8 1 420.46 408.65 9.08 o 6 -8 1 116.26 125.25 2.98 o -5 -7 1 27.73 26.86 0.93 o -4 -7 1 53.09 48.85 0.99 o -3 -7 1 276.50 285.55 2.24 o -2 -7 1 129.08 123.34 1.84 o -1 -7 1 612.04 608.23 22.34 o 0 -7 1 874.39 836.28 13.13 o 1 -7 1 7.44 5.34 1.00 o 2 -7 1 391.14 391.11 11.17 o 3 -7 1 6.87 7.18 1.35 o 4 -7 1 206.16 198.20 6.76 o 5 -7 1 77.40 74.60 3.50 o 6 -7 1 1.78 1.40 0.97 o -5 -6 1 1.42 2.17 0.94 o -4 -6 1 13.25 12.58 0.91 o -3 -6 1 30.16 30.24 0.97 o -2 -6 1 4.41 4.83 0.63 o -1 -6 1 234.05 255.80 2.65 o 0 -6 1 29.67 29.58 1.06 o 1 -6 1 131.09 120.87 3.02 o 2 -6 1 28.93 19.23 0.91 o 3 -6 1 123.89 135.57 3.63 o 4 -6 1 758.50 777.81 18.88 o 5 -6 1 2.25 2.86 0.79 o 6 -6 1 214.68 220.48 9.35 o 7 -6 1 28.90 32.83 1.11 o -6 -5 1 140.08 140.36 6.45 o -5 -5 1 3.61 3.80 0.88 o -4 -5 1 109.72 115.86 1.64 o -3 -5 1 1.12 1.89 0.69 o -2 -5 1 299.34 349.69 11.01 o -1 -5 1 249.00 228.26 5.37 o 0 -5 1 273.41 274.46 9.96 o 1 -5 1 313.78 278.28 9.72 o 2 -5 1 68.60 93.70 2.68 o 3 -5 1 810.46 822.75 20.56 o 4 -5 1 27.27 29.14 1.61 o 5 -5 1 10.72 10.67 1.05 o 6 -5 1 12.94 11.78 1.06 o 7 -5 1 13.83 17.62 1.15 o -6 -4 1 4.69 5.50 0.82 o -5 -4 1 323.64 303.59 7.30 o -4 -4 1 1019.45 1009.40 26.37 o -3 -4 1 302.33 278.86 3.61 o -2 -4 1 1328.30 1348.51 26.81 o -1 -4 1 294.80 348.66 3.26 o 0 -4 1 3100.96 3107.95 96.20 o 1 -4 1 1201.39 1302.06 30.23 o 2 -4 1 6.59 3.03 0.84 o 3 -4 1 145.17 159.93 5.41 o 4 -4 1 7.35 9.29 2.44 o 5 -4 1 2.37 3.20 1.97 o 6 -4 1 204.70 197.04 5.38 o 7 -4 1 53.42 60.75 3.15 o -6 -3 1 312.02 269.49 31.58 o -5 -3 1 45.40 43.68 2.06 o -4 -3 1 230.54 239.99 1.80 o -3 -3 1 0.78 2.22 0.86 o -2 -3 1 205.98 244.09 8.46 o -1 -3 1 409.36 387.14 5.55 o 0 -3 1 415.63 389.77 10.39 o 1 -3 1 2893.01 2874.45 72.42 o 2 -3 1 1406.82 1468.89 24.97 o 3 -3 1 893.88 741.40 20.37 o 4 -3 1 43.58 38.98 1.39 o 5 -3 1 1477.72 1497.21 64.19 o 6 -3 1 4.70 5.10 0.96 o 7 -3 1 157.40 172.96 6.52 o -7 -2 1 44.31 42.82 2.54 o -6 -2 1 12.65 14.68 1.46 o -5 -2 1 283.73 282.69 9.07 o -4 -2 1 14.33 15.15 0.81 o -3 -2 1 1459.69 1434.41 29.62 o -2 -2 1 1240.31 1228.25 22.17 o -1 -2 1 3285.99 3268.29 64.99 o 0 -2 1 63.84 48.39 1.67 o 1 -2 1 1324.28 1182.42 10.05 o 2 -2 1 1239.96 1146.09 71.38 o 3 -2 1 123.93 128.89 6.09 o 4 -2 1 0.07 0.27 0.91 o 5 -2 1 557.60 582.68 26.86 o 6 -2 1 9.96 11.89 0.95 o 7 -2 1 247.34 236.42 6.02 o -7 -1 1 131.75 120.25 3.98 o -6 -1 1 2.21 2.39 0.85 o -5 -1 1 267.07 249.87 7.42 o -4 -1 1 31.31 34.62 1.31 o -3 -1 1 1674.65 1632.43 30.57 o -2 -1 1 18.62 20.11 0.90 o -1 -1 1 2977.29 2735.29 167.00 o 1 -1 1 3.88 3.75 1.42 o 2 -1 1 1351.27 1235.69 32.44 o 3 -1 1 249.38 281.27 2.25 o 4 -1 1 212.69 196.00 12.16 o 5 -1 1 7.48 7.87 1.59 o 6 -1 1 371.95 387.59 12.59 o 7 -1 1 0.33 1.84 1.15 o -7 0 1 268.99 269.42 14.58 o -6 0 1 557.31 558.96 25.82 o -5 0 1 163.39 160.64 2.76 o -4 0 1 139.41 149.26 6.64 o -3 0 1 531.14 440.57 27.04 o -2 0 1 52.92 51.92 2.74 o -1 0 1 137.21 129.41 3.43 o 1 0 1 2324.80 2218.20 32.49 o 2 0 1 46.77 45.29 2.43 o 3 0 1 232.05 236.47 4.96 o 4 0 1 153.74 145.79 7.21 o 5 0 1 47.40 49.45 2.50 o 6 0 1 10.66 9.30 0.94 o 7 0 1 104.38 104.71 3.66 o -7 1 1 17.44 20.57 1.25 o -6 1 1 179.59 182.09 10.84 o -5 1 1 440.54 449.17 22.07 o -4 1 1 97.76 82.53 4.56 o -3 1 1 44.54 61.36 1.37 o -2 1 1 3587.74 3075.92 72.41 o -1 1 1 2074.67 1870.22 10.85 o 1 1 1 110.55 102.79 3.84 o 2 1 1 393.18 403.29 8.37 o 3 1 1 102.38 112.43 2.78 o 4 1 1 782.69 773.83 21.28 o 5 1 1 644.72 656.90 17.55 o 6 1 1 11.83 13.80 1.17 o 7 1 1 174.76 159.08 9.79 o -7 2 1 58.22 55.28 2.10 o -6 2 1 61.35 64.05 3.88 o -5 2 1 5.74 8.99 1.15 o -4 2 1 29.63 36.14 1.29 o -3 2 1 99.20 74.01 1.83 o -2 2 1 1100.01 1086.04 12.97 o -1 2 1 8089.35 8203.69 220.15 o 0 2 1 1524.03 1532.89 133.84 o 1 2 1 5546.86 5686.75 118.70 o 2 2 1 11.27 12.14 2.21 o 3 2 1 3639.22 3579.91 54.91 o 4 2 1 8.66 6.96 0.62 o 5 2 1 350.29 313.00 14.33 o 6 2 1 88.42 84.37 1.97 o -7 3 1 35.94 33.15 2.38 o -6 3 1 0.17 1.43 0.86 o -5 3 1 375.21 385.07 14.10 o -4 3 1 663.45 687.83 45.66 o -3 3 1 566.33 611.83 32.76 o -2 3 1 40.93 28.90 1.06 o -1 3 1 6.66 8.52 0.74 o 0 3 1 764.98 693.14 35.34 o 1 3 1 499.23 519.92 21.89 o 2 3 1 33.25 46.30 0.96 o 3 3 1 2.41 3.14 0.70 o 4 3 1 144.96 148.22 7.57 o 5 3 1 0.27 0.27 0.69 o 6 3 1 435.14 408.27 16.89 o -7 4 1 271.95 273.80 14.59 o -6 4 1 8.24 8.54 1.07 o -5 4 1 770.75 727.26 24.60 o -4 4 1 9.59 8.83 0.90 o -3 4 1 308.44 266.53 2.89 o -2 4 1 4.68 5.15 1.05 o -1 4 1 173.53 167.16 2.96 o 0 4 1 533.33 528.01 14.62 o 1 4 1 268.26 314.02 6.59 o 2 4 1 8.32 6.76 0.78 o 3 4 1 5.31 5.13 0.73 o 4 4 1 9.40 10.19 0.97 o 5 4 1 4.61 4.51 0.96 o 6 4 1 42.19 41.88 2.07 o -7 5 1 54.80 55.90 2.19 o -6 5 1 3.32 3.01 0.96 o -5 5 1 327.75 305.67 5.75 o -4 5 1 195.92 170.48 6.67 o -3 5 1 19.02 16.63 1.01 o -2 5 1 911.97 971.18 23.24 o -1 5 1 55.63 49.57 0.89 o 0 5 1 151.82 148.41 2.45 o 1 5 1 173.81 159.16 5.03 o 2 5 1 106.58 109.95 3.83 o 3 5 1 421.65 444.08 7.72 o 4 5 1 7.64 6.67 0.79 o 5 5 1 0.01 0.28 0.70 o 6 5 1 35.72 31.48 0.97 o -7 6 1 68.38 70.04 2.12 o -6 6 1 34.29 28.44 1.12 o -5 6 1 358.83 339.16 6.49 o -4 6 1 94.04 92.66 3.27 o -3 6 1 754.33 793.02 22.38 o -2 6 1 8.80 6.96 0.91 o -1 6 1 340.98 323.16 10.12 o 0 6 1 925.38 1008.22 21.77 o 1 6 1 192.57 243.42 3.77 o 2 6 1 546.74 545.57 6.36 o 3 6 1 332.78 344.63 5.93 o 4 6 1 596.62 574.13 32.82 o 5 6 1 250.24 257.08 6.79 o -7 7 1 13.16 12.16 1.28 o -6 7 1 128.29 126.69 3.05 o -5 7 1 17.30 14.70 1.05 o -4 7 1 5.45 3.40 1.18 o -3 7 1 398.29 411.93 6.05 o -2 7 1 267.24 263.00 8.61 o -1 7 1 435.47 417.27 7.78 o 0 7 1 380.49 380.32 11.23 o 1 7 1 614.51 593.17 14.99 o 2 7 1 0.22 0.15 0.64 o 3 7 1 40.91 45.64 1.27 o 4 7 1 1.07 2.10 0.92 o 5 7 1 4.38 6.89 0.97 o -6 8 1 24.30 27.84 0.92 o -5 8 1 5.70 5.70 0.72 o -4 8 1 147.01 141.20 1.43 o -3 8 1 351.72 379.94 11.46 o -2 8 1 361.26 342.54 7.07 o -1 8 1 1093.06 1097.03 21.27 o 0 8 1 10.86 11.49 1.76 o 1 8 1 113.84 110.03 2.82 o 2 8 1 283.39 291.97 6.79 o 3 8 1 86.73 75.67 1.99 o 4 8 1 138.54 147.39 1.86 o -6 9 1 6.86 7.87 0.96 o -5 9 1 248.46 245.37 4.28 o -4 9 1 1.03 2.34 0.73 o -3 9 1 37.81 36.51 1.31 o -2 9 1 12.41 13.89 0.98 o -1 9 1 51.54 52.57 0.98 o 0 9 1 93.37 91.73 1.22 o 1 9 1 56.79 63.01 1.97 o 2 9 1 115.23 109.00 1.44 o 3 9 1 10.14 9.12 0.94 o -5 10 1 17.36 18.25 1.41 o -4 10 1 276.61 273.21 7.80 o -3 10 1 27.71 29.54 1.25 o -2 10 1 147.87 149.07 4.56 o -1 10 1 23.46 25.55 0.96 o 0 10 1 124.30 112.30 2.46 o 1 10 1 61.01 60.87 2.11 o 2 10 1 11.36 9.74 1.00 o -4 11 1 18.47 16.26 0.96 o -3 11 1 0.77 0.76 2.35 o -2 11 1 45.69 41.67 1.90 o -1 11 1 31.43 25.94 0.96 o 0 11 1 30.28 29.78 1.50 o 1 11 1 2.74 1.06 0.73 o -3 12 1 0.22 -0.51 1.22 o -2 12 1 98.63 106.46 1.91 o -1 12 1 98.30 92.17 2.94 o 0 -12 2 107.79 103.91 3.88 o 1 -12 2 238.59 226.65 12.73 o 2 -12 2 47.50 46.02 4.85 o 3 -12 2 121.49 128.17 13.96 o -2 -11 2 109.87 101.21 2.39 o -1 -11 2 71.46 72.40 3.24 o 0 -11 2 347.11 345.19 14.61 o 1 -11 2 142.09 145.86 1.96 o 2 -11 2 96.76 91.05 1.62 o 3 -11 2 3.27 4.78 3.11 o 4 -11 2 13.53 21.87 2.12 o -3 -10 2 5.96 6.04 0.88 o -2 -10 2 1.00 1.13 0.90 o -1 -10 2 75.02 70.43 2.73 o 0 -10 2 0.09 1.63 0.86 o 1 -10 2 32.36 32.81 1.37 o 2 -10 2 14.65 16.00 1.32 o 3 -10 2 159.96 167.35 9.52 o 4 -10 2 20.47 23.52 1.12 o 5 -10 2 98.75 113.15 2.79 o -4 -9 2 10.83 9.19 1.04 o -3 -9 2 0.03 0.31 0.76 o -2 -9 2 99.53 97.65 1.96 o -1 -9 2 268.60 295.90 7.31 o 0 -9 2 15.35 15.19 1.01 o 1 -9 2 349.95 347.34 13.88 o 2 -9 2 72.76 72.11 2.69 o 3 -9 2 10.31 10.68 1.07 o 4 -9 2 141.03 142.79 1.57 o 5 -9 2 11.41 15.64 1.16 o 6 -9 2 65.66 65.06 1.95 o -4 -8 2 4.93 4.96 0.83 o -3 -8 2 103.76 111.91 2.49 o -2 -8 2 0.56 0.99 0.74 o -1 -8 2 99.26 102.29 5.30 o 0 -8 2 0.16 0.88 0.73 o 1 -8 2 129.11 120.68 2.39 o 2 -8 2 126.24 122.52 1.71 o 3 -8 2 112.99 111.49 5.39 o 4 -8 2 55.22 61.80 1.12 o 5 -8 2 36.00 39.68 1.19 o 6 -8 2 167.30 173.35 8.80 o -5 -7 2 155.05 143.15 1.57 o -4 -7 2 20.77 23.19 0.99 o -3 -7 2 19.51 19.49 0.83 o -2 -7 2 256.36 260.65 4.97 o -1 -7 2 143.41 147.26 3.67 o 0 -7 2 785.53 753.44 19.41 o 1 -7 2 1307.94 1293.03 59.15 o 2 -7 2 229.61 252.39 5.14 o 3 -7 2 674.33 691.86 15.49 o 4 -7 2 19.04 20.86 1.05 o 5 -7 2 9.92 13.46 1.26 o 6 -7 2 84.31 89.12 2.31 o -5 -6 2 80.42 80.24 2.77 o -4 -6 2 25.46 26.83 1.02 o -3 -6 2 333.51 335.78 9.19 o -2 -6 2 610.37 612.63 10.13 o -1 -6 2 44.67 42.33 1.37 o 0 -6 2 261.82 257.16 1.92 o 1 -6 2 252.52 253.68 10.01 o 2 -6 2 0.94 1.19 0.74 o 3 -6 2 199.57 201.46 4.04 o 4 -6 2 617.58 586.49 12.24 o 5 -6 2 211.87 219.38 7.70 o 6 -6 2 41.07 46.33 4.36 o 7 -6 2 78.83 69.76 1.41 o -6 -5 2 65.74 60.76 1.01 o -5 -5 2 35.43 39.46 1.56 o -4 -5 2 94.12 95.83 2.47 o -3 -5 2 121.22 122.36 2.66 o -2 -5 2 802.78 841.96 19.92 o -1 -5 2 26.46 32.01 0.93 o 0 -5 2 436.71 449.95 3.30 o 1 -5 2 764.84 844.02 18.43 o 2 -5 2 73.07 65.45 1.72 o 3 -5 2 641.00 680.59 9.85 o 4 -5 2 174.21 180.64 3.51 o 5 -5 2 240.31 236.67 16.21 o 6 -5 2 332.29 326.93 10.58 o 7 -5 2 1.04 1.21 0.99 o -6 -4 2 81.54 75.39 5.55 o -5 -4 2 25.47 24.08 1.43 o -4 -4 2 115.98 116.35 1.88 o -3 -4 2 91.21 98.98 3.78 o -2 -4 2 804.91 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