#------------------------------------------------------------------------------ #$Date: 2016-04-03 03:58:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181130 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/09/2220901.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220901_Fobs loop_ _publ_author_name 'Yi, Shi-xu' 'Men, Jian' 'Wang, Yang' 'Xiao, Yong' 'Gao, Guo-wei' _publ_section_title ; 2,2'-Dimethyl-4,4'-(sulfonyldi-p-phenylene)dibut-3-yn-2-ol dihydrate ; _journal_coeditor_code RZ2282 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o212 _journal_volume 65 _journal_year 2009 _space_group_IT_number 38 _symmetry_space_group_name_Hall 'A 2 -2' _symmetry_space_group_name_H-M 'A m m 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.7507 _cell_length_b 10.9043 _cell_length_c 5.0915 _exptl_crystal_F_000 444.00 _reflns_d_resolution_high 0.8247 _cod_data_source_file rz2282Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MJ6 in Amm2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, z' 'x, -y, z' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -6 306.79 261.16 21.55 o 1 0 -6 8.57 0.01 12.85 o 2 0 -6 55.25 53.45 13.32 o 3 0 -6 305.60 260.10 21.06 o 4 0 -6 9.96 11.47 11.28 o 5 0 -6 97.59 48.74 15.31 o 0 2 -6 264.08 261.02 19.22 o 1 2 -6 6.25 8.39 12.66 o 2 2 -6 44.31 48.23 12.08 o 3 2 -6 100.72 89.39 14.58 o 0 1 -5 201.35 198.01 14.84 o 1 1 -5 5.00 0.00 11.27 o 2 1 -5 157.83 141.57 13.99 o 3 1 -5 354.29 299.77 18.49 o 4 1 -5 20.34 0.60 10.44 o 5 1 -5 54.84 73.98 10.47 o 6 1 -5 220.73 220.84 14.24 o 7 1 -5 120.38 102.72 12.16 o 8 1 -5 15.33 14.33 10.00 o 9 1 -5 27.86 9.36 10.97 o 10 1 -5 21.38 0.69 10.32 o 11 1 -5 66.19 73.34 11.30 o 12 1 -5 46.12 34.73 11.53 o 13 1 -5 15.62 13.23 10.59 o 0 3 -5 104.66 78.09 14.67 o 1 3 -5 360.76 345.34 18.61 o 2 3 -5 152.35 141.20 14.26 o 3 3 -5 206.74 205.20 14.95 o 4 3 -5 11.32 14.46 9.82 o 5 3 -5 68.68 83.88 11.69 o 6 3 -5 45.48 27.58 11.08 o 7 3 -5 50.56 62.26 10.92 o 8 3 -5 10.96 5.08 9.18 o 9 3 -5 72.90 55.91 12.38 o 10 3 -5 50.17 61.72 10.30 o 11 3 -5 131.96 117.92 13.30 o 12 3 -5 43.60 68.92 9.75 o 0 5 -5 171.52 160.44 14.71 o 1 5 -5 226.31 193.05 15.85 o 2 5 -5 208.32 187.55 15.85 o 3 5 -5 103.84 95.47 12.73 o 4 5 -5 31.28 29.65 10.03 o 5 5 -5 22.77 31.08 9.64 o 6 5 -5 70.79 95.08 11.85 o 7 5 -5 22.00 3.22 11.95 o 8 5 -5 37.95 29.56 11.43 o 9 5 -5 10.43 0.01 11.82 o 10 5 -5 86.69 81.16 13.92 o 0 7 -5 46.74 23.44 13.53 o 1 7 -5 22.28 10.43 10.59 o 2 7 -5 26.79 22.07 11.02 o 3 7 -5 74.72 72.67 12.62 o 4 7 -5 3.82 8.36 8.77 o 5 7 -5 13.43 32.30 9.61 o 0 0 -4 545.35 571.89 17.05 o 1 0 -4 223.73 212.75 12.06 o 2 0 -4 183.28 157.06 11.30 o 3 0 -4 93.21 58.23 10.27 o 4 0 -4 49.59 56.50 8.54 o 5 0 -4 21.78 18.77 8.10 o 6 0 -4 185.88 210.28 10.38 o 7 0 -4 117.37 150.80 9.99 o 8 0 -4 93.17 106.93 9.90 o 9 0 -4 67.02 65.17 9.75 o 10 0 -4 783.82 691.14 20.76 o 11 0 -4 76.55 72.63 10.10 o 12 0 -4 195.33 170.55 13.33 o 13 0 -4 115.36 108.83 11.02 o 14 0 -4 97.30 94.09 11.23 o 15 0 -4 11.22 8.39 8.78 o 16 0 -4 42.26 38.99 9.36 o 17 0 -4 1.79 0.01 8.05 o 18 0 -4 18.63 24.64 8.47 o 0 2 -4 170.21 171.19 12.97 o 1 2 -4 415.89 401.68 15.54 o 2 2 -4 39.65 32.10 9.95 o 3 2 -4 133.58 125.36 11.65 o 4 2 -4 88.38 92.80 9.87 o 5 2 -4 201.01 214.18 11.93 o 6 2 -4 154.87 179.23 11.19 o 7 2 -4 117.60 112.18 11.03 o 8 2 -4 104.23 127.93 9.38 o 9 2 -4 269.11 248.92 14.58 o 10 2 -4 81.62 54.37 10.85 o 5 4 -4 356.12 383.62 15.17 o 6 4 -4 660.60 663.82 19.96 o 7 4 -4 32.43 12.27 9.27 o 8 4 -4 152.41 123.28 11.26 o 9 4 -4 321.86 340.75 16.81 o 10 4 -4 86.49 85.90 11.77 o 11 4 -4 179.12 178.01 13.06 o 12 4 -4 178.29 175.70 13.10 o 13 4 -4 124.03 151.81 13.23 o 14 4 -4 74.91 72.01 12.62 o 15 4 -4 60.44 71.02 11.32 o 16 4 -4 212.50 227.87 16.57 o 0 6 -4 117.80 119.40 12.06 o 1 6 -4 187.91 177.88 13.48 o 2 6 -4 94.45 138.79 10.80 o 3 6 -4 85.61 82.49 9.87 o 4 6 -4 144.53 158.09 12.22 o 5 6 -4 79.80 62.46 10.59 o 6 6 -4 242.68 238.26 13.91 o 7 6 -4 29.41 14.12 9.73 o 8 6 -4 63.05 63.54 10.15 o 9 6 -4 135.59 133.19 12.86 o 10 6 -4 3.49 12.31 7.78 o 11 6 -4 55.99 66.99 10.39 o 12 6 -4 90.25 93.75 12.58 o 13 6 -4 74.91 76.45 11.37 o 14 6 -4 27.11 15.62 10.51 o 0 8 -4 45.21 48.67 9.85 o 1 8 -4 70.75 79.38 9.89 o 2 8 -4 0.19 0.01 8.63 o 3 8 -4 6.77 5.33 8.47 o 4 8 -4 2.75 0.01 8.56 o 5 8 -4 12.10 15.36 8.26 o 6 8 -4 29.87 30.90 9.69 o 7 8 -4 29.02 30.77 9.67 o 8 8 -4 16.37 20.59 9.67 o 9 8 -4 49.83 45.47 11.99 o 10 8 -4 91.93 107.67 12.01 o 0 10 -4 78.23 72.57 11.69 o 1 10 -4 31.42 15.54 11.12 o 0 1 -3 808.20 872.94 11.54 o 1 1 -3 458.09 488.93 12.58 o 2 1 -3 154.94 171.45 8.97 o 3 1 -3 260.02 280.27 10.57 o 4 1 -3 313.75 359.82 11.65 o 5 1 -3 9.98 19.59 5.79 o 6 1 -3 56.77 76.76 7.47 o 7 1 -3 61.52 68.14 7.51 o 8 1 -3 439.04 426.01 12.55 o 9 1 -3 903.94 1034.42 18.26 o 10 1 -3 292.88 299.40 12.44 o 11 1 -3 363.00 353.54 13.49 o 12 1 -3 7.77 9.07 7.77 o 13 1 -3 39.87 43.55 7.52 o 14 1 -3 13.84 9.57 7.01 o 15 1 -3 30.11 22.45 8.51 o 16 1 -3 63.65 68.49 8.54 o 17 1 -3 27.20 7.20 8.87 o 18 1 -3 19.13 19.50 8.48 o 19 1 -3 57.86 51.99 9.74 o 20 1 -3 33.64 31.66 8.52 o 0 3 -3 369.72 321.02 7.45 o 1 3 -3 118.53 115.67 8.31 o 2 3 -3 252.55 253.23 9.92 o 3 3 -3 580.10 641.24 15.05 o 4 3 -3 412.15 388.65 12.40 o 5 3 -3 190.48 242.31 11.80 o 6 3 -3 1846.82 1890.53 24.44 o 7 3 -3 0.86 0.81 7.43 o 8 3 -3 1027.37 1136.86 20.21 o 9 3 -3 1163.93 1232.75 21.55 o 10 3 -3 91.70 93.17 9.88 o 11 3 -3 81.56 98.46 9.86 o 12 3 -3 191.36 195.77 11.60 o 13 3 -3 44.40 53.31 7.54 o 14 3 -3 285.22 321.24 14.25 o 15 3 -3 25.70 29.49 8.13 o 16 3 -3 87.90 88.85 10.28 o 17 3 -3 21.09 30.10 8.42 o 18 3 -3 44.98 51.69 9.81 o 19 3 -3 46.61 62.78 9.89 o 20 3 -3 134.84 147.50 12.53 o 0 5 -3 127.20 125.99 6.20 o 1 5 -3 242.31 233.08 11.33 o 2 5 -3 42.97 45.23 7.53 o 3 5 -3 747.14 743.49 16.98 o 4 5 -3 126.59 140.15 8.82 o 5 5 -3 636.79 617.24 17.57 o 6 5 -3 1265.45 1224.84 23.98 o 7 5 -3 245.47 252.63 12.18 o 8 5 -3 818.18 864.61 20.57 o 9 5 -3 945.85 950.23 20.92 o 10 5 -3 316.53 286.75 14.78 o 11 5 -3 93.59 103.43 10.62 o 12 5 -3 87.90 81.28 10.40 o 13 5 -3 133.01 134.11 12.50 o 14 5 -3 229.97 246.02 15.15 o 15 5 -3 128.45 118.34 11.75 o 16 5 -3 20.79 37.14 8.20 o 17 5 -3 57.35 58.42 10.17 o 18 5 -3 15.50 22.65 9.10 o 0 7 -3 60.69 74.56 7.19 o 1 7 -3 40.97 36.49 9.11 o 2 7 -3 96.15 63.72 8.71 o 3 7 -3 30.21 29.52 7.43 o 4 7 -3 84.39 100.87 9.21 o 5 7 -3 21.52 34.15 6.75 o 6 7 -3 144.18 125.28 10.49 o 7 7 -3 0.67 1.91 7.36 o 8 7 -3 213.82 225.20 12.19 o 9 7 -3 227.85 217.14 12.99 o 10 7 -3 64.15 45.52 9.99 o 11 7 -3 31.81 38.76 8.52 o 12 7 -3 39.34 46.97 8.43 o 13 7 -3 11.32 4.01 9.40 o 14 7 -3 18.97 10.08 8.92 o 15 7 -3 5.93 18.10 6.16 o 16 7 -3 31.39 32.82 9.45 o 0 9 -3 64.78 60.80 10.17 o 1 9 -3 33.49 36.06 6.42 o 2 9 -3 58.04 57.25 9.62 o 3 9 -3 14.36 0.01 8.55 o 4 9 -3 39.73 55.29 8.15 o 5 9 -3 15.33 12.61 7.97 o 6 9 -3 12.85 0.01 8.39 o 7 9 -3 19.25 29.78 8.22 o 8 9 -3 45.19 54.58 9.25 o 9 9 -3 112.65 131.08 11.70 o 10 9 -3 90.85 100.14 11.66 o 11 9 -3 53.07 62.44 9.69 o 12 9 -3 7.22 21.71 8.68 o 13 9 -3 9.30 18.94 8.89 o 0 11 -3 0.94 0.01 9.63 o 1 11 -3 14.75 18.08 7.46 o 2 11 -3 6.01 0.01 8.09 o 3 11 -3 32.93 42.52 10.77 o 4 11 -3 17.29 9.79 9.64 o 5 11 -3 15.53 29.71 7.70 o 6 11 -3 15.89 9.66 9.66 o 0 0 -2 3176.93 4109.17 16.71 o 1 0 -2 1205.10 1673.35 10.63 o 2 0 -2 1857.62 2121.24 9.43 o 3 0 -2 41.44 33.23 4.15 o 4 0 -2 396.42 399.41 6.41 o 5 0 -2 3820.79 3897.60 18.16 o 6 0 -2 3623.91 4505.54 20.60 o 7 0 -2 5588.43 6419.52 25.38 o 8 0 -2 354.97 305.52 7.10 o 9 0 -2 85.67 73.01 5.05 o 10 0 -2 2005.14 2149.73 17.21 o 11 0 -2 256.19 242.75 7.29 o 12 0 -2 108.53 121.52 6.08 o 13 0 -2 303.41 316.19 8.31 o 14 0 -2 84.57 63.58 5.86 o 15 0 -2 203.64 213.67 7.97 o 16 0 -2 96.79 74.00 5.79 o 17 0 -2 45.39 49.06 5.60 o 18 0 -2 65.28 65.01 6.37 o 19 0 -2 201.39 237.22 9.22 o 20 0 -2 107.16 91.33 8.10 o 21 0 -2 55.60 55.57 7.64 o 22 0 -2 26.26 37.49 6.27 o 0 2 -2 449.94 464.18 6.91 o 1 2 -2 166.59 254.77 7.73 o 2 2 -2 627.23 646.61 10.65 o 3 2 -2 319.38 342.78 8.61 o 4 2 -2 333.00 293.13 7.79 o 5 2 -2 207.96 230.20 7.83 o 6 2 -2 3779.10 4012.63 19.23 o 7 2 -2 915.49 992.05 14.92 o 8 2 -2 282.73 275.26 8.90 o 9 2 -2 89.79 90.69 6.39 o 10 2 -2 398.81 415.18 11.43 o 11 2 -2 268.11 281.42 9.82 o 12 2 -2 197.33 194.88 8.90 o 13 2 -2 28.92 35.40 6.49 o 14 2 -2 128.00 123.94 8.78 o 15 2 -2 30.81 19.30 8.42 o 16 2 -2 219.87 199.27 11.89 o 17 2 -2 27.25 37.14 6.70 o 18 2 -2 95.72 85.31 9.38 o 19 2 -2 36.86 0.00 14.20 o 20 2 -2 91.76 77.90 10.76 o 21 2 -2 13.37 4.94 9.76 o 22 2 -2 59.11 83.37 10.12 o 0 4 -2 755.76 894.99 10.54 o 1 4 -2 2252.09 2387.40 21.68 o 2 4 -2 538.90 576.66 11.81 o 3 4 -2 1643.56 1642.48 18.58 o 4 4 -2 148.30 173.62 7.40 o 5 4 -2 74.46 79.00 6.21 o 6 4 -2 1007.00 1104.06 17.11 o 7 4 -2 41.31 55.80 6.55 o 8 4 -2 176.47 202.18 9.09 o 9 4 -2 1225.10 1130.92 18.92 o 10 4 -2 407.48 439.14 13.28 o 11 4 -2 1478.82 1368.29 22.21 o 12 4 -2 239.87 266.24 11.24 o 13 4 -2 402.34 427.49 13.16 o 14 4 -2 6.38 10.01 6.48 o 15 4 -2 11.41 14.61 5.79 o 16 4 -2 96.39 100.20 9.61 o 17 4 -2 168.92 167.28 10.92 o 18 4 -2 63.38 56.17 10.07 o 19 4 -2 61.95 78.13 10.32 o 20 4 -2 72.91 87.21 11.80 o 21 4 -2 50.46 69.38 11.23 o 0 6 -2 73.84 55.88 5.00 o 1 6 -2 613.42 625.58 14.53 o 2 6 -2 50.29 33.77 6.15 o 3 6 -2 628.08 665.38 13.93 o 4 6 -2 15.10 7.55 6.32 o 5 6 -2 275.40 295.54 10.93 o 6 6 -2 486.28 429.72 12.96 o 7 6 -2 78.81 81.70 7.88 o 8 6 -2 57.06 44.62 6.77 o 9 6 -2 524.67 589.50 15.22 o 10 6 -2 136.30 135.13 10.07 o 11 6 -2 716.88 741.68 17.88 o 12 6 -2 65.60 86.95 7.64 o 13 6 -2 68.70 66.18 7.88 o 14 6 -2 14.14 10.83 6.85 o 15 6 -2 21.44 17.97 8.53 o 16 6 -2 38.34 11.03 9.16 o 17 6 -2 84.47 96.82 9.39 o 18 6 -2 20.80 19.18 7.84 o 19 6 -2 31.03 50.27 9.11 o 0 8 -2 63.00 57.82 5.23 o 1 8 -2 53.13 53.94 6.80 o 2 8 -2 102.49 116.81 7.84 o 3 8 -2 22.73 25.69 6.54 o 4 8 -2 87.28 118.32 8.84 o 5 8 -2 103.13 103.57 9.75 o 6 8 -2 693.63 684.23 17.74 o 7 8 -2 423.00 418.54 17.03 o 8 8 -2 75.05 79.37 8.57 o 9 8 -2 4.48 5.19 6.63 o 10 8 -2 121.29 115.80 10.47 o 11 8 -2 7.58 9.99 6.46 o 12 8 -2 40.51 58.00 7.54 o 13 8 -2 35.68 50.53 8.75 o 14 8 -2 61.98 54.66 10.66 o 15 8 -2 13.75 8.98 9.05 o 16 8 -2 57.01 73.60 9.44 o 17 8 -2 0.31 0.01 7.71 o 0 10 -2 24.52 31.52 4.96 o 1 10 -2 17.26 15.52 7.48 o 2 10 -2 11.22 14.13 6.16 o 3 10 -2 5.46 10.39 5.44 o 4 10 -2 4.25 6.91 6.32 o 5 10 -2 146.36 153.75 10.41 o 6 10 -2 200.16 207.18 14.46 o 7 10 -2 192.82 157.92 14.28 o 8 10 -2 4.32 18.82 7.31 o 9 10 -2 10.37 0.01 8.60 o 10 10 -2 72.99 52.79 9.41 o 11 10 -2 12.08 6.00 9.19 o 12 10 -2 0.51 5.10 6.76 o 13 10 -2 10.69 12.80 7.48 o 0 12 -2 22.58 30.86 6.35 o 1 12 -2 26.22 42.35 7.96 o 2 12 -2 12.60 17.23 7.39 o 3 12 -2 30.76 31.00 10.27 o 4 12 -2 0.44 8.19 6.68 o 5 12 -2 5.94 0.01 9.43 o 6 12 -2 57.39 57.79 10.06 o 0 1 -1 2269.15 2194.02 9.32 o 1 1 -1 2275.37 2530.54 13.46 o 2 1 -1 2988.31 3234.04 16.02 o 3 1 -1 13921.39 15274.21 152.39 o 4 1 -1 8029.89 8472.28 118.16 o 5 1 -1 3175.27 3338.02 19.42 o 6 1 -1 140.45 122.48 5.22 o 7 1 -1 2672.07 2655.41 19.83 o 8 1 -1 1411.25 1535.95 16.24 o 9 1 -1 1410.22 1441.01 16.35 o 10 1 -1 1292.48 1241.27 16.81 o 11 1 -1 785.72 840.68 14.04 o 12 1 -1 172.86 174.40 7.94 o 13 1 -1 4.10 0.00 7.93 o 14 1 -1 767.83 733.73 17.29 o 15 1 -1 534.18 526.26 15.60 o 16 1 -1 73.48 61.02 10.69 o 17 1 -1 640.24 633.32 18.23 o 18 1 -1 83.23 86.11 11.60 o 19 1 -1 40.28 33.77 8.57 o 20 1 -1 124.40 157.78 9.05 o 21 1 -1 17.02 24.12 7.67 o 22 1 -1 57.99 69.78 10.36 o 23 1 -1 62.17 63.86 12.42 o 0 3 -1 3684.95 3986.68 15.60 o 1 3 -1 204.07 224.67 6.33 o 2 3 -1 3629.04 3782.46 14.23 o 3 3 -1 1185.38 1245.15 28.59 o 4 3 -1 1859.73 1942.76 16.28 o 5 3 -1 248.79 318.75 7.56 o 6 3 -1 1163.76 1218.52 14.08 o 7 3 -1 1085.57 1081.73 13.96 o 8 3 -1 139.82 155.83 6.33 o 9 3 -1 124.19 140.13 6.55 o 10 3 -1 43.72 50.98 5.40 o 11 3 -1 14.11 16.77 4.42 o 12 3 -1 127.28 120.80 7.69 o 13 3 -1 160.87 177.25 8.35 o 14 3 -1 544.60 551.83 14.07 o 15 3 -1 208.75 178.75 11.10 o 16 3 -1 450.83 486.81 14.63 o 17 3 -1 143.10 137.18 10.52 o 18 3 -1 51.33 49.94 8.27 o 19 3 -1 62.32 59.53 10.05 o 20 3 -1 183.41 188.97 13.04 o 21 3 -1 65.99 80.96 8.70 o 22 3 -1 5.64 11.15 6.84 o 23 3 -1 2.72 0.01 8.70 o 0 5 -1 5551.20 5396.64 22.82 o 1 5 -1 1379.30 1359.18 15.87 o 2 5 -1 462.23 468.78 9.49 o 3 5 -1 323.23 376.55 9.29 o 4 5 -1 343.91 471.03 10.46 o 5 5 -1 447.69 418.52 10.42 o 6 5 -1 36.09 45.37 5.35 o 7 5 -1 529.57 499.21 11.56 o 8 5 -1 497.96 475.47 11.41 o 9 5 -1 32.41 38.20 5.71 o 10 5 -1 121.56 123.19 7.81 o 11 5 -1 45.63 57.57 6.84 o 12 5 -1 193.05 188.80 9.91 o 13 5 -1 397.05 364.98 13.28 o 14 5 -1 386.26 400.94 13.73 o 15 5 -1 405.31 435.19 15.13 o 16 5 -1 295.27 311.58 14.34 o 17 5 -1 0.71 0.01 6.54 o 18 5 -1 15.71 36.20 6.71 o 19 5 -1 84.27 91.38 10.13 o 20 5 -1 271.94 304.21 15.84 o 21 5 -1 29.07 23.31 8.95 o 0 7 -1 459.77 456.18 8.90 o 1 7 -1 26.25 25.21 6.43 o 2 7 -1 310.98 332.17 9.97 o 3 7 -1 886.91 802.04 15.26 o 4 7 -1 71.67 77.32 7.13 o 5 7 -1 293.23 215.00 10.09 o 6 7 -1 136.89 117.23 8.23 o 7 7 -1 318.49 283.60 10.42 o 8 7 -1 134.84 155.37 8.84 o 9 7 -1 145.25 114.05 8.79 o 10 7 -1 77.87 86.87 8.48 o 11 7 -1 68.48 65.94 7.66 o 12 7 -1 58.78 72.23 8.20 o 13 7 -1 30.60 30.55 6.85 o 14 7 -1 230.74 243.54 13.44 o 15 7 -1 107.47 127.42 9.37 o 16 7 -1 15.05 0.01 7.99 o 17 7 -1 121.52 131.88 11.56 o 18 7 -1 20.92 25.54 7.43 o 19 7 -1 13.64 7.26 8.36 o 0 9 -1 142.75 144.34 7.28 o 1 9 -1 22.02 18.39 6.27 o 2 9 -1 120.90 122.01 10.41 o 3 9 -1 727.39 738.37 19.02 o 4 9 -1 396.86 367.56 15.01 o 5 9 -1 254.38 268.85 14.28 o 6 9 -1 31.12 34.80 7.17 o 7 9 -1 250.02 227.48 12.21 o 8 9 -1 71.96 75.66 8.86 o 9 9 -1 153.51 136.56 11.40 o 10 9 -1 76.02 89.40 8.93 o 11 9 -1 100.47 102.20 9.96 o 12 9 -1 22.47 21.28 8.33 o 13 9 -1 12.26 12.19 7.91 o 14 9 -1 99.46 101.94 11.16 o 15 9 -1 82.22 111.84 11.87 o 16 9 -1 27.62 18.53 11.21 o 17 9 -1 125.02 141.56 14.91 o 0 11 -1 56.32 69.94 6.39 o 1 11 -1 39.86 43.00 8.42 o 2 11 -1 32.71 35.92 7.81 o 3 11 -1 106.17 103.42 11.05 o 4 11 -1 40.03 41.90 7.88 o 5 11 -1 2.23 6.92 6.84 o 6 11 -1 12.53 0.01 8.20 o 7 11 -1 15.64 4.25 7.47 o 8 11 -1 36.89 44.44 8.86 o 9 11 -1 21.60 23.29 9.05 o 10 11 -1 14.97 20.75 7.94 o 11 11 -1 22.81 19.54 7.36 o 12 11 -1 3.48 1.49 8.20 o 0 13 -1 63.84 86.74 7.81 o 1 13 -1 10.00 8.36 9.25 o 1 0 0 1889.25 1540.24 15.78 o 2 0 0 1934.86 1732.81 8.18 o 3 0 0 1603.96 1354.09 6.29 o 4 0 0 1059.22 816.97 6.11 o 5 0 0 89.61 51.08 4.54 o 6 0 0 5271.89 4539.59 16.29 o 7 0 0 10.20 0.00 3.87 o 8 0 0 3025.01 2579.58 14.44 o 9 0 0 14.18 1.82 3.72 o 10 0 0 1088.49 1078.48 10.71 o 11 0 0 1337.57 938.13 11.81 o 12 0 0 5084.29 5287.21 25.98 o 13 0 0 308.27 209.01 8.99 o 14 0 0 1576.95 1486.75 15.66 o 15 0 0 5.23 4.14 4.86 o 16 0 0 32.10 37.20 5.23 o 17 0 0 719.66 671.62 12.90 o 18 0 0 144.16 140.14 7.82 o 19 0 0 1.53 0.01 5.29 o 20 0 0 720.37 738.85 15.69 o 21 0 0 79.52 92.14 7.92 o 22 0 0 103.17 115.63 9.07 o 23 0 0 0.01 0.01 6.40 o 0 2 0 22320.88 20267.14 114.46 o 1 2 0 1788.91 1671.45 7.60 o 2 2 0 510.04 526.37 4.62 o 3 2 0 4226.38 3540.90 12.34 o 4 2 0 144.12 131.85 3.51 o 5 2 0 3081.38 2942.83 12.99 o 6 2 0 206.78 279.92 4.95 o 7 2 0 974.82 993.94 8.65 o 8 2 0 2.84 9.33 2.51 o 9 2 0 215.34 179.47 4.82 o 10 2 0 97.97 104.14 4.36 o 11 2 0 589.85 505.17 8.41 o 12 2 0 675.82 607.08 9.60 o 13 2 0 305.90 324.57 7.59 o 14 2 0 149.71 126.14 6.22 o 15 2 0 308.10 297.67 8.12 o 16 2 0 8.90 0.01 5.61 o 17 2 0 1073.58 1011.73 15.14 o 18 2 0 9.23 4.68 5.53 o 19 2 0 10.17 0.01 5.65 o 20 2 0 57.42 48.03 7.34 o 21 2 0 53.84 55.67 7.14 o 22 2 0 24.04 24.48 6.23 o 23 2 0 6.35 4.80 5.20 o 0 4 0 7.00 8.96 2.84 o 1 4 0 569.13 488.47 6.28 o 2 4 0 78.46 99.05 3.52 o 3 4 0 186.11 181.28 4.25 o 4 4 0 2243.51 2157.15 13.29 o 5 4 0 1040.95 992.73 9.24 o 6 4 0 850.70 792.37 8.62 o 7 4 0 10.36 3.59 2.79 o 8 4 0 253.82 306.23 6.34 o 9 4 0 382.46 342.19 6.87 o 10 4 0 291.49 255.12 6.34 o 11 4 0 73.40 56.78 4.40 o 12 4 0 41.48 29.06 3.72 o 13 4 0 1.00 0.01 3.56 o 14 4 0 14.51 5.06 4.17 o 15 4 0 227.08 231.79 8.35 o 16 4 0 277.22 266.92 9.62 o 17 4 0 682.05 652.38 13.84 o 18 4 0 13.76 20.11 4.39 o 19 4 0 202.66 204.63 9.31 o 20 4 0 59.50 61.73 6.94 o 21 4 0 5.15 5.35 5.30 o 22 4 0 18.14 20.48 5.91 o 0 6 0 2347.40 2141.43 11.67 o 1 6 0 105.98 120.50 4.47 o 2 6 0 52.35 32.89 3.79 o 3 6 0 116.21 153.31 4.96 o 4 6 0 768.27 668.67 9.48 o 5 6 0 192.50 172.43 5.88 o 6 6 0 3.63 6.03 3.09 o 7 6 0 0.27 9.33 3.57 o 8 6 0 2.15 1.86 2.98 o 9 6 0 79.34 72.61 5.13 o 10 6 0 232.36 219.49 7.08 o 11 6 0 0.84 1.59 3.45 o 12 6 0 195.94 211.11 7.43 o 13 6 0 2.79 10.33 3.42 o 14 6 0 104.42 104.73 6.30 o 15 6 0 92.21 98.71 6.57 o 16 6 0 131.27 119.34 8.11 o 17 6 0 415.85 391.63 12.28 o 18 6 0 30.79 25.36 6.66 o 19 6 0 87.08 102.26 7.45 o 20 6 0 0.03 0.37 5.00 o 21 6 0 0.11 2.59 4.96 o 0 8 0 3309.84 3154.51 23.57 o 1 8 0 541.68 457.88 10.74 o 2 8 0 9.15 13.04 4.11 o 3 8 0 663.03 608.72 11.22 o 4 8 0 113.82 125.24 6.04 o 5 8 0 218.03 222.84 7.91 o 6 8 0 45.39 56.65 4.86 o 7 8 0 159.75 122.79 6.42 o 8 8 0 39.24 54.28 5.12 o 9 8 0 214.37 207.48 7.84 o 10 8 0 2.94 7.04 4.71 o 11 8 0 357.55 356.29 10.16 o 12 8 0 251.41 239.04 9.38 o 13 8 0 103.39 112.32 7.67 o 14 8 0 102.94 114.79 8.04 o 15 8 0 45.29 57.86 6.86 o 16 8 0 35.81 28.10 7.12 o 17 8 0 260.68 285.64 10.84 o 18 8 0 6.16 9.40 5.68 o 19 8 0 1.60 0.02 6.33 o 0 10 0 1866.22 1686.91 22.17 o 1 10 0 61.64 68.66 8.18 o 2 10 0 25.20 23.20 6.00 o 3 10 0 37.01 36.35 5.44 o 4 10 0 4.18 12.86 3.92 o 5 10 0 0.03 7.43 4.23 o 6 10 0 82.21 81.58 6.47 o 7 10 0 1.77 6.40 4.29 o 8 10 0 72.29 74.22 6.63 o 9 10 0 3.16 2.49 5.18 o 10 10 0 27.14 28.25 6.15 o 11 10 0 82.28 78.23 7.35 o 12 10 0 220.00 209.59 9.99 o 13 10 0 10.50 24.42 6.40 o 14 10 0 103.76 116.65 8.16 o 15 10 0 0.21 3.94 5.52 o 0 12 0 35.67 37.18 5.90 o 1 12 0 2.32 11.15 4.13 o 2 12 0 0.49 0.54 4.84 o 3 12 0 24.57 22.87 4.93 o 4 12 0 26.60 55.65 6.01 o 5 12 0 20.05 25.18 5.85 o 6 12 0 2.10 0.02 5.17 o 7 12 0 2.71 3.01 4.92 o 8 12 0 2.63 2.02 4.74 o 9 12 0 1.62 8.12 5.08 o 10 12 0 3.94 19.44 7.44 o 1 1 1 2238.81 2409.65 14.49 o 2 1 1 2979.19 3211.95 17.05 o 3 1 1 13902.15 16536.04 170.71 o 4 1 1 8103.03 8875.25 128.80 o 5 1 1 3222.19 3461.07 21.13 o 6 1 1 142.98 127.47 5.84 o 7 1 1 2716.85 2763.74 21.00 o 8 1 1 1427.49 1532.56 17.09 o 9 1 1 1401.15 1401.02 17.38 o 10 1 1 1309.93 1240.99 17.13 o 11 1 1 769.53 725.05 14.64 o 12 1 1 174.54 180.89 9.07 o 13 1 1 5.59 1.16 7.34 o 14 1 1 765.36 724.46 17.75 o 15 1 1 535.55 486.39 16.09 o 16 1 1 77.23 51.07 12.28 o 17 1 1 646.39 625.76 17.95 o 18 1 1 84.96 92.48 11.07 o 19 1 1 37.51 30.59 9.20 o 20 1 1 124.09 115.04 11.24 o 21 1 1 18.70 28.02 8.10 o 22 1 1 60.52 53.85 12.11 o 23 1 1 61.04 67.69 11.76 o 1 3 1 198.09 212.42 6.85 o 2 3 1 3580.48 3810.55 77.55 o 3 3 1 1203.53 1234.00 30.48 o 4 3 1 1826.72 1832.69 16.91 o 5 3 1 260.47 312.23 8.37 o 6 3 1 1138.64 1167.55 14.23 o 7 3 1 1096.55 1032.51 14.61 o 8 3 1 137.07 146.15 6.69 o 9 3 1 130.83 142.33 7.18 o 10 3 1 41.96 41.38 5.78 o 11 3 1 15.95 20.83 4.39 o 12 3 1 125.46 100.62 7.90 o 13 3 1 159.35 174.76 9.56 o 14 3 1 537.70 526.81 14.68 o 15 3 1 203.61 181.84 11.05 o 16 3 1 440.67 413.34 15.90 o 17 3 1 147.96 142.05 10.81 o 18 3 1 48.94 32.39 9.08 o 19 3 1 61.28 65.31 11.14 o 20 3 1 185.45 188.97 13.06 o 21 3 1 68.70 79.29 9.63 o 22 3 1 6.53 16.23 7.86 o 1 5 1 1354.47 1306.61 16.81 o 2 5 1 450.36 431.04 10.86 o 3 5 1 313.10 339.30 9.69 o 4 5 1 333.27 413.71 10.89 o 5 5 1 433.41 384.01 10.24 o 6 5 1 34.55 38.52 5.64 o 7 5 1 520.99 471.60 12.71 o 8 5 1 507.70 478.15 12.50 o 9 5 1 29.14 15.36 6.55 o 10 5 1 127.54 139.69 7.26 o 11 5 1 42.05 54.52 6.08 o 12 5 1 197.89 205.86 10.26 o 13 5 1 389.65 327.96 12.94 o 14 5 1 383.84 346.98 14.09 o 15 5 1 396.27 366.72 16.21 o 16 5 1 288.65 323.65 14.52 o 17 5 1 1.11 3.04 5.84 o 18 5 1 15.58 26.41 7.43 o 19 5 1 82.41 103.78 10.09 o 20 5 1 275.39 290.42 15.82 o 21 5 1 30.45 43.98 8.07 o 1 7 1 23.91 27.42 5.95 o 2 7 1 304.40 285.71 11.29 o 3 7 1 888.06 749.45 17.39 o 4 7 1 74.82 78.67 7.53 o 5 7 1 301.16 233.91 10.56 o 6 7 1 132.37 126.68 8.39 o 7 7 1 326.27 282.86 11.67 o 8 7 1 136.13 148.45 9.59 o 9 7 1 145.80 136.40 10.11 o 10 7 1 79.74 71.53 9.05 o 11 7 1 68.12 76.46 7.41 o 12 7 1 57.69 53.65 9.48 o 13 7 1 31.57 33.80 7.56 o 14 7 1 228.72 242.33 13.60 o 15 7 1 106.72 110.89 10.91 o 16 7 1 13.71 15.72 7.09 o 17 7 1 123.46 143.11 12.51 o 18 7 1 20.52 26.85 8.54 o 19 7 1 13.05 16.79 8.22 o 1 9 1 20.39 11.62 6.85 o 2 9 1 118.79 126.26 10.73 o 3 9 1 727.11 713.16 19.80 o 4 9 1 403.94 317.60 16.06 o 5 9 1 260.16 270.10 14.67 o 6 9 1 30.92 24.25 7.73 o 7 9 1 256.35 263.60 12.82 o 8 9 1 72.80 71.82 9.19 o 9 9 1 152.00 137.83 11.13 o 10 9 1 77.61 75.49 9.80 o 11 9 1 98.23 79.52 11.27 o 12 9 1 21.34 17.81 8.09 o 13 9 1 13.35 31.67 7.64 o 14 9 1 99.00 124.92 11.19 o 15 9 1 82.80 129.49 11.65 o 16 9 1 28.79 14.88 11.50 o 17 9 1 126.08 156.59 14.98 o 1 11 1 38.14 54.31 7.91 o 2 11 1 31.69 29.68 8.22 o 3 11 1 105.62 33.47 9.07 o 4 11 1 41.56 41.00 8.40 o 5 11 1 2.55 0.01 7.67 o 6 11 1 13.14 6.38 8.75 o 7 11 1 16.60 11.31 7.76 o 8 11 1 37.78 37.14 9.31 o 9 11 1 21.14 24.78 9.08 o 10 11 1 15.52 25.08 7.63 o 11 11 1 21.96 26.95 8.41 o 12 11 1 3.42 11.73 7.73 o 1 13 1 10.01 13.15 8.76 o 1 2 2 156.27 230.60 7.35 o 2 2 2 626.33 636.59 11.02 o 3 2 2 333.58 336.34 8.89 o 4 2 2 324.33 278.94 8.39 o 5 2 2 213.96 212.53 8.92 o 6 2 2 3766.77 4002.89 22.57 o 7 2 2 936.23 1000.77 15.69 o 8 2 2 282.75 278.92 9.33 o 9 2 2 85.74 75.30 6.80 o 10 2 2 409.16 408.54 12.19 o 11 2 2 265.87 255.62 11.07 o 12 2 2 193.86 172.08 9.95 o 13 2 2 29.63 32.63 6.11 o 14 2 2 128.96 122.94 9.35 o 15 2 2 32.49 24.69 8.28 o 16 2 2 213.54 216.75 11.46 o 17 2 2 28.38 19.32 8.24 o 18 2 2 95.62 81.57 10.87 o 19 2 2 37.95 29.00 10.55 o 20 2 2 93.16 78.86 11.77 o 21 2 2 13.94 0.01 11.22 o 22 2 2 59.31 28.35 14.18 o 1 4 2 2216.63 2288.89 22.95 o 2 4 2 528.01 541.23 12.42 o 3 4 2 1656.53 1634.01 20.17 o 4 4 2 139.74 161.43 7.31 o 5 4 2 71.54 66.29 6.95 o 6 4 2 1001.06 1087.63 17.38 o 7 4 2 40.28 56.33 6.98 o 8 4 2 172.65 200.58 9.67 o 9 4 2 1219.70 1103.68 20.04 o 10 4 2 406.40 429.58 13.63 o 11 4 2 1472.70 1369.09 22.30 o 12 4 2 233.14 246.72 12.13 o 13 4 2 393.11 378.93 14.25 o 14 4 2 7.75 13.51 6.63 o 15 4 2 12.50 17.90 6.43 o 16 4 2 92.07 88.12 9.99 o 17 4 2 171.06 161.68 12.14 o 18 4 2 62.17 55.62 10.24 o 19 4 2 59.67 62.31 9.85 o 20 4 2 72.91 85.67 10.95 o 21 4 2 49.13 52.99 12.27 o 1 6 2 600.28 578.74 14.45 o 2 6 2 49.59 36.71 6.56 o 3 6 2 632.29 645.20 15.12 o 4 6 2 15.22 21.89 5.94 o 5 6 2 273.79 323.15 11.36 o 6 6 2 485.04 418.68 14.07 o 7 6 2 82.79 102.65 7.34 o 8 6 2 57.65 33.72 7.64 o 9 6 2 521.80 537.15 16.64 o 10 6 2 138.73 116.85 10.58 o 11 6 2 713.78 698.02 19.03 o 12 6 2 63.12 55.05 8.89 o 13 6 2 65.33 64.25 7.93 o 14 6 2 15.72 23.29 5.96 o 15 6 2 22.01 29.76 7.04 o 16 6 2 36.15 25.11 9.54 o 17 6 2 85.33 98.79 10.22 o 18 6 2 20.76 37.17 7.77 o 19 6 2 30.45 35.69 10.43 o 1 8 2 56.32 37.60 7.90 o 2 8 2 103.93 75.00 9.19 o 3 8 2 24.10 28.04 6.79 o 4 8 2 87.37 118.67 9.40 o 5 8 2 103.88 104.98 9.76 o 6 8 2 691.39 689.00 18.58 o 7 8 2 429.78 427.62 16.18 o 8 8 2 75.98 86.91 8.55 o 9 8 2 4.29 16.94 6.19 o 10 8 2 125.42 144.45 11.03 o 11 8 2 8.15 6.06 6.78 o 12 8 2 40.19 34.37 8.57 o 13 8 2 37.60 46.27 7.98 o 14 8 2 62.23 87.57 9.28 o 15 8 2 13.81 8.91 8.91 o 16 8 2 55.37 62.14 10.89 o 17 8 2 0.21 0.01 7.91 o 1 10 2 17.56 11.17 8.14 o 2 10 2 12.20 0.01 8.37 o 3 10 2 5.00 0.01 7.46 o 4 10 2 4.89 0.01 7.74 o 5 10 2 145.37 139.01 11.13 o 6 10 2 199.40 224.82 14.82 o 7 10 2 195.00 193.64 13.95 o 8 10 2 4.85 16.03 7.45 o 9 10 2 9.57 15.08 6.89 o 10 10 2 75.11 60.63 10.35 o 11 10 2 11.91 19.97 7.12 o 12 10 2 0.62 6.37 6.67 o 13 10 2 11.11 11.62 7.35 o 1 12 2 25.15 26.65 9.05 o 2 12 2 12.12 3.39 9.53 o 3 12 2 31.44 47.37 10.61 o 4 12 2 0.35 0.01 8.33 o 5 12 2 5.78 15.09 7.73 o 6 12 2 57.30 50.24 10.80 o 1 1 3 468.48 509.55 12.93 o 2 1 3 161.81 180.54 10.11 o 3 1 3 269.07 286.34 10.73 o 4 1 3 306.55 340.56 12.08 o 5 1 3 8.21 21.61 6.32 o 6 1 3 51.77 62.95 8.15 o 7 1 3 61.40 67.75 7.86 o 8 1 3 429.99 404.54 13.05 o 9 1 3 903.45 1015.56 19.31 o 10 1 3 302.46 321.41 12.63 o 11 1 3 372.23 354.40 14.26 o 12 1 3 8.50 26.38 6.64 o 13 1 3 37.93 15.99 8.36 o 14 1 3 13.74 5.72 7.26 o 15 1 3 32.69 29.94 7.95 o 16 1 3 64.27 63.85 9.27 o 17 1 3 29.49 18.30 8.77 o 18 1 3 19.24 26.78 7.57 o 19 1 3 57.20 45.09 10.59 o 20 1 3 32.68 21.90 10.12 o 1 3 3 113.10 108.48 7.84 o 2 3 3 257.42 237.07 10.52 o 3 3 3 568.70 629.42 14.88 o 4 3 3 410.55 394.68 12.49 o 5 3 3 188.23 223.16 11.34 o 6 3 3 1852.32 1901.18 24.90 o 7 3 3 0.99 9.45 7.68 o 8 3 3 1020.61 1067.95 21.43 o 9 3 3 1150.21 1139.86 22.26 o 10 3 3 94.54 101.48 8.75 o 11 3 3 79.60 87.52 9.79 o 12 3 3 191.55 215.46 11.30 o 13 3 3 43.65 24.98 9.41 o 14 3 3 287.73 301.71 14.37 o 15 3 3 26.52 24.97 8.68 o 16 3 3 89.09 80.50 10.77 o 17 3 3 20.43 40.05 7.75 o 18 3 3 45.39 57.66 9.13 o 19 3 3 45.75 42.97 11.81 o 20 3 3 133.60 135.35 15.04 o 1 5 3 247.53 256.08 11.28 o 2 5 3 39.53 27.04 9.06 o 3 5 3 742.79 673.94 17.40 o 4 5 3 121.85 107.36 10.16 o 5 5 3 641.19 610.16 17.18 o 6 5 3 1266.48 1271.12 23.57 o 7 5 3 252.40 278.65 12.31 o 8 5 3 809.05 795.13 20.97 o 9 5 3 936.70 919.18 22.23 o 10 5 3 313.94 287.42 14.35 o 11 5 3 93.66 122.33 9.70 o 12 5 3 86.48 80.30 9.44 o 13 5 3 135.92 129.39 12.83 o 14 5 3 230.95 253.74 14.94 o 15 5 3 130.97 122.21 12.10 o 16 5 3 20.82 13.39 10.52 o 17 5 3 57.73 67.33 10.29 o 18 5 3 15.20 19.64 9.65 o 12 7 3 39.86 33.59 9.52 o 13 7 3 10.76 8.47 8.05 o 14 7 3 19.82 14.80 8.93 o 15 7 3 6.70 8.82 7.74 o 16 7 3 32.36 44.78 10.03 o