#------------------------------------------------------------------------------
#$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $
#$Revision: 697 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220918.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2220918_Fobs
loop_
_publ_author_name
'Sun, Weidong'
'Yao, Jin'
'Bai, Lifei'
'Wang, Xiaoming'
_publ_section_title
;
1-(2,3,4,6-Tetra-O-acetyl-\b-D-glucopyranosyl)-3-thioureidothiourea
monohydrate
;
_journal_coeditor_code SU2088
_journal_issue 2
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first o242
_journal_volume 65
_journal_year 2009
_space_group_IT_number 5
_symmetry_space_group_name_Hall 'C 2y'
_symmetry_space_group_name_H-M 'C 1 2 1'
_cell_angle_alpha 90.000
_cell_angle_beta 110.119
_cell_angle_gamma 90.000
_cell_length_a 22.2858
_cell_length_b 7.2005
_cell_length_c 15.8772
_exptl_crystal_F_000 1048.00
_reflns_d_resolution_high 0.8409
_[local]_cod_data_source_file su2088Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' A in C2'
_shelx_refln_list_code 4
_shelx_F_calc_maximum 210.12
_shelx_F_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 -8 0 46.64 55.17 26.45 o
2 -8 0 44.81 47.94 20.36 o
4 -8 0 33.33 35.33 18.32 o
6 -8 0 42.35 71.50 23.25 o
8 -8 0 182.40 235.29 35.49 o
1 -7 0 100.82 148.87 26.74 o
3 -7 0 465.83 433.96 37.42 o
5 -7 0 102.94 98.20 19.20 o
7 -7 0 55.86 78.28 17.51 o
9 -7 0 23.32 36.62 13.93 o
11 -7 0 40.55 72.08 17.42 o
13 -7 0 105.48 110.97 26.81 o
0 -6 0 872.54 803.29 40.27 o
2 -6 0 178.88 150.51 19.52 o
4 -6 0 287.48 245.10 23.54 o
6 -6 0 316.39 298.30 25.82 o
8 -6 0 97.13 94.94 14.35 o
10 -6 0 94.59 118.87 16.11 o
12 -6 0 308.98 357.50 29.63 o
14 -6 0 16.15 13.38 11.73 o
16 -6 0 122.74 128.00 27.81 o
1 -5 0 469.44 413.44 21.29 o
3 -5 0 139.55 127.50 12.71 o
5 -5 0 482.40 396.75 19.44 o
7 -5 0 102.24 98.30 12.95 o
9 -5 0 97.35 119.93 14.77 o
11 -5 0 102.71 110.96 14.69 o
13 -5 0 442.04 361.28 26.70 o
15 -5 0 137.53 147.23 27.50 o
17 -5 0 162.62 178.49 31.13 o
19 -5 0 12.55 23.32 17.42 o
0 -4 0 1413.81 1181.11 38.24 o
2 -4 0 1383.14 1440.68 29.63 o
4 -4 0 100.35 123.39 11.51 o
6 -4 0 932.80 871.52 25.94 o
8 -4 0 736.84 751.21 25.52 o
10 -4 0 106.22 148.76 14.38 o
12 -4 0 438.98 347.10 19.49 o
14 -4 0 349.89 333.10 25.01 o
16 -4 0 60.53 68.63 20.70 o
18 -4 0 96.30 117.61 25.64 o
20 -4 0 87.43 85.77 22.90 o
22 -4 0 74.98 86.97 24.90 o
1 -3 0 772.73 821.81 19.43 o
3 -3 0 3871.69 4260.95 114.57 o
5 -3 0 2946.58 3074.33 56.91 o
7 -3 0 11629.23 12556.55 207.06 o
9 -3 0 790.87 841.99 24.10 o
11 -3 0 217.34 205.84 14.11 o
13 -3 0 196.09 212.04 19.04 o
15 -3 0 326.38 325.21 32.78 o
17 -3 0 158.55 115.32 23.23 o
19 -3 0 242.73 221.66 31.75 o
21 -3 0 50.84 63.59 21.00 o
23 -3 0 43.03 44.89 23.96 o
0 -2 0 1754.59 1483.02 38.92 o
2 -2 0 18649.71 19384.92 100.05 o
4 -2 0 3444.85 3874.61 117.33 o
6 -2 0 1466.78 1498.00 25.99 o
8 -2 0 4429.14 4214.35 70.70 o
10 -2 0 3393.23 3224.23 55.40 o
12 -2 0 2410.07 2330.31 78.08 o
14 -2 0 192.40 172.34 23.44 o
16 -2 0 23.46 27.48 13.82 o
18 -2 0 767.79 691.78 44.08 o
20 -2 0 10.67 23.46 14.69 o
22 -2 0 12.21 28.36 30.20 o
24 -2 0 0.18 11.70 13.74 o
1 -1 0 10837.98 10232.01 117.55 o
3 -1 0 3072.41 3085.99 46.05 o
5 -1 0 32345.00 36559.62 734.09 o
7 -1 0 1601.63 1561.12 30.04 o
9 -1 0 4481.63 4870.82 111.08 o
11 -1 0 1866.60 2123.32 95.25 o
13 -1 0 611.08 626.03 33.44 o
15 -1 0 496.80 429.08 30.87 o
17 -1 0 798.44 775.00 43.36 o
19 -1 0 11.46 12.05 11.92 o
21 -1 0 208.31 212.02 30.91 o
23 -1 0 40.16 72.38 20.40 o
2 0 0 3975.10 3394.20 43.13 o
4 0 0 77.28 98.62 4.66 o
6 0 0 12099.43 12053.30 290.51 o
8 0 0 1293.46 1235.10 19.04 o
10 0 0 5204.13 6538.54 86.75 o
12 0 0 729.01 741.39 33.01 o
14 0 0 1108.24 1118.34 44.19 o
16 0 0 3.06 3.49 9.48 o
18 0 0 361.07 375.59 30.99 o
20 0 0 497.84 554.49 42.45 o
22 0 0 6.70 30.01 15.14 o
24 0 0 3.88 24.37 19.12 o
1 1 0 10793.24 11095.43 125.17 o
3 1 0 2998.31 3082.68 30.04 o
5 1 0 32461.69 37521.73 242.72 o
7 1 0 1562.14 1537.44 32.61 o
9 1 0 4527.00 4814.90 66.08 o
11 1 0 1831.45 1991.41 48.16 o
13 1 0 602.32 609.50 30.22 o
15 1 0 490.89 446.04 29.08 o
17 1 0 784.85 833.73 69.24 o
19 1 0 11.14 11.89 10.65 o
21 1 0 211.15 294.10 32.49 o
23 1 0 38.81 61.83 29.90 o
2 2 0 18423.11 21302.44 478.79 o
4 2 0 3409.95 4107.24 58.29 o
6 2 0 1438.84 1560.41 28.97 o
8 2 0 4459.55 4435.12 104.37 o
10 2 0 3363.21 3350.10 56.02 o
12 2 0 2364.81 2375.66 68.73 o
14 2 0 195.24 193.25 19.67 o
16 2 0 20.37 29.33 14.07 o
18 2 0 767.12 765.35 59.38 o
20 2 0 10.06 46.16 25.19 o
22 2 0 11.64 24.51 25.61 o
3 3 0 3811.74 4593.09 52.24 o
5 3 0 3000.16 3358.99 62.16 o
7 3 0 11561.55 13111.67 130.56 o
9 3 0 754.76 865.42 36.89 o
11 3 0 210.32 204.50 16.41 o
13 3 0 202.01 214.29 27.97 o
15 3 0 325.52 331.63 36.30 o
2 4 0 1395.07 1655.89 38.33 o
4 4 0 119.05 179.59 18.70 o
6 4 0 968.11 985.87 39.00 o
3 5 0 144.59 152.82 15.90 o
-8 -8 1 30.69 54.94 20.26 o
-6 -8 1 50.93 56.75 19.86 o
-4 -8 1 21.98 71.59 21.65 o
-2 -8 1 44.13 61.70 20.63 o
0 -8 1 27.99 54.72 19.65 o
2 -8 1 61.52 72.76 22.75 o
4 -8 1 10.21 37.02 17.57 o
6 -8 1 147.93 197.35 33.99 o
8 -8 1 27.24 61.01 27.88 o
-13 -7 1 67.41 86.32 23.96 o
-11 -7 1 86.99 105.51 20.26 o
-9 -7 1 379.64 414.59 33.46 o
-7 -7 1 126.54 142.54 22.01 o
-5 -7 1 27.71 72.76 17.18 o
-3 -7 1 50.81 48.60 18.40 o
-1 -7 1 89.97 89.43 21.91 o
1 -7 1 80.67 95.61 22.44 o
3 -7 1 133.25 136.24 27.18 o
5 -7 1 29.04 51.23 18.76 o
7 -7 1 127.29 142.73 22.32 o
9 -7 1 89.05 118.13 20.73 o
11 -7 1 79.00 102.92 23.99 o
13 -7 1 32.96 63.25 21.78 o
-18 -6 1 0.51 17.05 26.83 o
-16 -6 1 80.20 97.75 24.85 o
-14 -6 1 116.82 141.78 22.12 o
-12 -6 1 198.23 221.86 21.00 o
-10 -6 1 50.31 55.90 12.50 o
-8 -6 1 132.50 125.48 16.11 o
-6 -6 1 90.63 85.35 16.45 o
-4 -6 1 65.54 69.25 15.44 o
-2 -6 1 332.77 341.75 25.91 o
0 -6 1 102.48 93.94 21.11 o
2 -6 1 210.12 246.21 23.06 o
4 -6 1 244.01 205.92 22.26 o
6 -6 1 324.17 331.30 26.54 o
8 -6 1 193.99 158.92 20.76 o
10 -6 1 233.49 249.72 21.13 o
12 -6 1 43.00 42.20 13.84 o
14 -6 1 239.31 274.71 35.91 o
16 -6 1 41.71 77.31 23.40 o
-19 -5 1 77.60 88.13 25.60 o
-17 -5 1 280.93 277.89 36.46 o
-15 -5 1 219.76 211.08 23.94 o
-13 -5 1 289.01 286.97 25.53 o
-11 -5 1 42.59 60.63 12.38 o
-9 -5 1 190.14 182.71 16.90 o
-7 -5 1 804.80 747.82 27.37 o
-5 -5 1 165.77 219.20 16.24 o
-3 -5 1 931.16 957.83 34.86 o
-1 -5 1 487.56 440.63 19.47 o
1 -5 1 321.60 283.29 20.02 o
3 -5 1 716.33 682.05 36.38 o
5 -5 1 339.07 367.87 52.08 o
7 -5 1 192.44 206.95 16.94 o
9 -5 1 247.51 214.99 18.02 o
11 -5 1 306.81 303.51 20.52 o
13 -5 1 26.78 57.38 13.82 o
15 -5 1 15.12 17.37 15.40 o
17 -5 1 57.62 59.62 21.10 o
19 -5 1 85.94 89.67 25.49 o
-22 -4 1 123.55 124.28 26.53 o
-20 -4 1 9.20 32.97 14.95 o
-18 -4 1 38.94 50.59 17.26 o
-16 -4 1 1.14 8.81 12.18 o
-14 -4 1 122.73 125.52 18.02 o
-12 -4 1 1533.10 1449.03 37.08 o
-10 -4 1 385.01 353.07 18.50 o
-8 -4 1 355.95 370.60 18.35 o
-6 -4 1 582.04 493.38 19.87 o
-4 -4 1 1229.12 1171.31 34.42 o
-2 -4 1 1973.29 1827.52 74.76 o
0 -4 1 773.14 798.35 37.56 o
2 -4 1 913.57 958.62 32.55 o
4 -4 1 732.32 732.20 33.46 o
6 -4 1 413.71 423.76 18.69 o
8 -4 1 402.47 400.15 19.06 o
10 -4 1 387.04 341.88 18.80 o
12 -4 1 559.85 493.79 27.46 o
14 -4 1 46.36 53.69 17.01 o
16 -4 1 363.04 314.66 35.79 o
18 -4 1 35.15 25.05 15.96 o
20 -4 1 107.75 131.02 28.22 o
-23 -3 1 10.40 38.48 27.12 o
-21 -3 1 111.32 114.73 24.74 o
-19 -3 1 297.55 311.82 35.49 o
-17 -3 1 859.63 738.04 50.41 o
-15 -3 1 1385.91 1235.82 54.62 o
-13 -3 1 219.92 216.78 14.89 o
-11 -3 1 101.54 133.14 12.41 o
-9 -3 1 503.46 612.25 20.95 o
-7 -3 1 10448.48 10316.41 244.04 o
-5 -3 1 4447.18 4478.40 79.59 o
-3 -3 1 1998.51 1654.71 42.23 o
-1 -3 1 5557.67 6370.51 158.05 o
1 -3 1 68.12 62.17 6.87 o
3 -3 1 920.69 1073.18 32.26 o
5 -3 1 1479.19 1480.59 32.67 o
7 -3 1 527.80 444.06 17.36 o
9 -3 1 1307.18 1231.38 39.71 o
11 -3 1 579.79 600.42 21.26 o
13 -3 1 383.56 357.77 21.77 o
15 -3 1 75.99 71.30 25.02 o
17 -3 1 200.27 168.51 27.06 o
19 -3 1 255.93 262.45 34.48 o
21 -3 1 101.08 129.52 27.51 o
-24 -2 1 37.72 57.25 24.98 o
-22 -2 1 24.85 50.23 20.05 o
-20 -2 1 721.13 602.30 42.70 o
-18 -2 1 368.62 362.84 35.02 o
-16 -2 1 1970.15 1893.28 70.46 o
-14 -2 1 1183.22 1066.27 33.15 o
-12 -2 1 2465.92 2363.52 157.80 o
-10 -2 1 2382.18 2415.93 35.76 o
-8 -2 1 2951.82 3114.21 83.99 o
-6 -2 1 3564.30 4057.66 91.33 o
-4 -2 1 8028.73 8346.13 153.41 o
-2 -2 1 4388.96 4767.95 37.59 o
0 -2 1 14044.20 16168.96 369.14 o
2 -2 1 3085.01 3685.99 59.16 o
4 -2 1 7990.21 8811.65 107.20 o
6 -2 1 2153.61 2388.36 32.17 o
8 -2 1 3813.48 3845.87 42.29 o
10 -2 1 1304.28 1285.69 30.66 o
12 -2 1 134.03 125.55 13.48 o
14 -2 1 260.65 264.27 27.96 o
16 -2 1 2145.94 1987.71 95.39 o
18 -2 1 134.74 132.91 24.92 o
20 -2 1 94.22 101.49 23.42 o
22 -2 1 148.60 210.27 32.83 o
-25 -1 1 30.74 64.24 20.90 o
-23 -1 1 43.11 61.75 19.87 o
-21 -1 1 117.08 89.82 21.10 o
-19 -1 1 617.08 496.88 36.61 o
-17 -1 1 1322.90 1290.91 53.91 o
-15 -1 1 397.19 374.31 30.79 o
-13 -1 1 3126.94 3073.62 105.23 o
-11 -1 1 0.64 22.12 6.45 o
-9 -1 1 7378.01 8011.41 212.52 o
-7 -1 1 11718.12 15156.72 409.72 o
-5 -1 1 19017.29 21032.22 751.49 o
-3 -1 1 4580.72 4377.86 131.83 o
-1 -1 1 12343.60 11368.08 138.77 o
1 -1 1 6726.15 7090.54 93.82 o
3 -1 1 2331.15 2460.73 37.14 o
5 -1 1 1426.26 1445.66 24.50 o
7 -1 1 5270.52 5475.66 72.92 o
9 -1 1 3616.06 4010.77 54.49 o
11 -1 1 2523.47 2471.10 37.40 o
13 -1 1 707.97 631.49 34.68 o
15 -1 1 2131.89 2120.39 99.69 o
17 -1 1 627.75 646.59 46.71 o
19 -1 1 114.09 123.53 23.79 o
21 -1 1 434.05 401.57 53.83 o
23 -1 1 227.95 254.22 35.72 o
-24 0 1 17.56 31.13 16.63 o
-22 0 1 256.13 228.26 30.52 o
-20 0 1 477.22 507.05 36.58 o
-18 0 1 1498.55 1458.83 56.77 o
-16 0 1 112.09 112.07 19.16 o
-14 0 1 1532.35 1590.04 50.69 o
-12 0 1 5.19 5.16 4.58 o
-10 0 1 2256.41 3190.32 97.44 o
-8 0 1 20119.20 19750.80 527.66 o
-6 0 1 44148.35 44901.10 772.59 o
-4 0 1 10.79 1.03 3.29 o
-2 0 1 16052.42 18834.01 146.57 o
0 0 1 704.85 1.35 1.35 o
2 0 1 25.17 47.01 4.88 o
4 0 1 15.21 7.56 5.52 o
6 0 1 4.97 7.62 6.36 o
8 0 1 508.22 517.76 34.66 o
10 0 1 2437.95 2515.01 63.64 o
12 0 1 1314.54 1316.67 69.32 o
14 0 1 220.84 279.26 24.97 o
16 0 1 485.65 442.42 31.97 o
18 0 1 689.83 685.84 41.53 o
20 0 1 352.89 389.56 35.04 o
22 0 1 287.40 301.88 36.05 o
24 0 1 3.17 18.05 19.88 o
-25 1 1 31.16 17.35 25.10 o
-23 1 1 41.17 22.41 22.91 o
-21 1 1 112.54 108.83 33.27 o
-19 1 1 613.76 586.49 36.54 o
-17 1 1 1320.94 1277.81 49.08 o
-15 1 1 403.88 407.90 30.41 o
-13 1 1 3162.60 3116.65 71.73 o
-11 1 1 3.62 26.07 8.59 o
-9 1 1 7494.89 7939.42 79.80 o
-7 1 1 11684.18 15246.67 95.62 o
-5 1 1 19092.97 22449.37 186.20 o
-3 1 1 4635.11 4674.89 51.47 o
1 1 1 6760.31 7367.60 74.55 o
3 1 1 2300.96 2411.21 77.62 o
5 1 1 1480.88 1627.15 31.74 o
7 1 1 5303.17 5720.07 68.15 o
9 1 1 3590.50 4013.95 64.51 o
11 1 1 2538.64 2437.68 56.01 o
13 1 1 709.99 644.32 32.48 o
15 1 1 2111.23 2037.50 82.42 o
17 1 1 604.03 640.58 38.13 o
19 1 1 117.33 136.27 23.41 o
21 1 1 431.35 456.59 36.70 o
23 1 1 231.02 256.58 50.29 o
-20 2 1 718.38 686.93 59.72 o
-18 2 1 370.70 381.66 42.71 o
-16 2 1 1933.01 1744.64 81.54 o
-14 2 1 1207.38 1086.29 48.39 o
-12 2 1 2440.37 2619.78 52.31 o
-10 2 1 2442.70 2563.42 45.27 o
-8 2 1 2873.68 3181.96 42.82 o
-6 2 1 3588.79 4310.79 40.75 o
-4 2 1 8147.03 9087.40 79.85 o
2 2 1 3107.93 3949.98 64.86 o
4 2 1 7869.39 8716.43 100.83 o
6 2 1 2192.04 2537.97 59.22 o
8 2 1 3776.52 3984.53 102.60 o
10 2 1 1319.29 1375.34 70.17 o
12 2 1 138.66 110.70 15.52 o
14 2 1 269.45 290.19 23.17 o
16 2 1 2135.99 2114.36 62.79 o
18 2 1 137.67 165.50 23.15 o
20 2 1 88.62 90.30 31.76 o
22 2 1 147.98 201.66 44.64 o
-13 3 1 217.92 201.32 26.03 o
-11 3 1 104.16 142.68 12.90 o
-9 3 1 523.76 680.95 32.14 o
-7 3 1 10452.64 11276.81 103.61 o
-5 3 1 4524.10 4955.73 64.78 o
-3 3 1 1961.78 1954.92 41.78 o
1 3 1 67.14 58.32 8.78 o
3 3 1 949.61 1230.32 42.71 o
5 3 1 1437.03 1494.90 47.34 o
7 3 1 534.80 461.85 28.64 o
9 3 1 1289.44 1376.04 51.72 o
11 3 1 579.33 663.68 39.84 o
13 3 1 382.82 386.39 24.77 o
15 3 1 79.35 86.26 24.60 o
-6 4 1 576.49 548.45 25.86 o
-4 4 1 1245.04 1388.17 35.34 o
2 4 1 907.01 1030.60 32.33 o
4 4 1 725.22 756.93 38.24 o
6 4 1 422.13 472.30 30.91 o
8 4 1 405.04 455.37 31.33 o
-3 5 1 929.90 1139.31 34.24 o
1 5 1 322.22 315.83 21.98 o
3 5 1 717.45 772.76 44.05 o
0 6 1 96.53 135.90 18.99 o
-8 -8 2 70.23 82.98 19.37 o
-6 -8 2 43.05 75.62 22.39 o
-4 -8 2 17.81 20.55 17.77 o
-2 -8 2 16.53 54.48 20.38 o
0 -8 2 44.65 77.18 22.67 o
2 -8 2 27.19 65.00 21.23 o
4 -8 2 74.95 123.64 27.93 o
6 -8 2 230.50 337.97 41.40 o
-15 -7 2 8.72 5.13 12.37 o
-13 -7 2 22.93 27.88 18.24 o
-11 -7 2 54.88 62.95 17.18 o
-9 -7 2 259.36 261.82 28.08 o
-7 -7 2 461.20 452.29 33.09 o
-5 -7 2 15.28 19.41 11.64 o
-3 -7 2 132.33 125.17 26.86 o
-1 -7 2 63.02 77.91 21.23 o
1 -7 2 240.99 246.24 33.44 o
3 -7 2 28.89 36.76 17.13 o
5 -7 2 0.82 5.47 14.11 o
7 -7 2 127.59 131.81 21.68 o
9 -7 2 74.42 83.85 17.65 o
11 -7 2 38.26 61.40 21.47 o
13 -7 2 43.10 60.23 31.92 o
-18 -6 2 39.47 47.52 20.97 o
-16 -6 2 101.77 152.22 30.24 o
-14 -6 2 82.52 97.60 19.34 o
-12 -6 2 43.29 57.22 12.71 o
-10 -6 2 48.70 55.56 12.71 o
-8 -6 2 57.63 73.79 12.79 o
-6 -6 2 169.16 145.96 16.18 o
-4 -6 2 52.10 51.08 13.41 o
-2 -6 2 526.10 475.63 28.18 o
0 -6 2 235.65 220.81 28.93 o
2 -6 2 301.64 322.98 24.98 o
4 -6 2 269.32 257.22 23.71 o
6 -6 2 87.07 81.17 16.01 o
8 -6 2 100.29 112.55 18.65 o
10 -6 2 115.82 126.01 16.94 o
12 -6 2 84.50 101.52 19.17 o
14 -6 2 121.40 114.57 26.33 o
16 -6 2 21.12 22.71 17.26 o
-19 -5 2 39.01 64.67 21.33 o
-17 -5 2 4.43 21.20 16.31 o
-15 -5 2 371.05 375.25 28.91 o
-13 -5 2 77.13 106.36 14.84 o
-11 -5 2 654.24 604.98 31.19 o
-9 -5 2 444.72 410.39 21.89 o
-7 -5 2 855.68 782.76 37.68 o
-5 -5 2 68.49 50.11 12.53 o
-3 -5 2 281.57 307.01 21.17 o
-1 -5 2 542.13 499.00 24.11 o
1 -5 2 359.66 328.32 21.40 o
3 -5 2 1094.11 1056.09 48.50 o
5 -5 2 372.62 351.46 18.86 o
7 -5 2 76.83 86.96 12.83 o
9 -5 2 162.84 189.54 17.28 o
11 -5 2 70.97 69.96 14.86 o
13 -5 2 235.11 217.48 30.58 o
15 -5 2 110.83 114.52 25.99 o
17 -5 2 163.51 157.64 30.59 o
19 -5 2 49.86 74.43 24.05 o
-22 -4 2 42.72 89.42 22.28 o
-20 -4 2 34.02 60.51 19.12 o
-18 -4 2 359.36 370.58 38.41 o
-16 -4 2 1007.62 918.25 75.73 o
-14 -4 2 305.61 303.86 24.01 o
-12 -4 2 710.59 689.98 26.41 o
-10 -4 2 72.75 64.07 10.69 o
-8 -4 2 378.30 445.44 20.13 o
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1 1 12 456.09 456.72 50.20 o
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1 5 12 168.46 183.88 43.21 o
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2 -4 13 59.42 100.24 22.51 o
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1 -3 13 527.47 556.66 38.54 o
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5 -3 13 16.94 47.51 25.94 o
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0 -2 13 6.37 15.14 11.24 o
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-1 -1 13 335.44 402.63 33.24 o
1 -1 13 1409.37 1405.95 57.58 o
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0 0 13 1.90 -0.08 17.52 o
2 0 13 4105.11 3718.42 140.67 o
4 0 13 215.35 266.18 48.69 o
6 0 13 70.53 59.47 30.83 o
8 0 13 50.95 54.92 27.21 o
10 0 13 2.54 30.32 20.72 o
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1 1 13 1420.82 1222.32 81.88 o
3 1 13 222.70 218.59 44.22 o
5 1 13 253.40 304.84 52.48 o
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11 1 13 27.02 33.86 20.89 o
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0 2 13 6.32 4.72 18.36 o
2 2 13 255.00 228.19 44.56 o
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8 2 13 123.41 137.13 37.91 o
10 2 13 157.85 233.41 49.45 o
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1 3 13 525.87 531.26 57.11 o
3 3 13 200.59 205.28 43.80 o
5 3 13 18.15 54.08 25.27 o
7 3 13 265.69 301.81 52.56 o
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0 4 13 140.35 156.17 39.17 o
2 4 13 61.31 98.05 31.33 o
4 4 13 54.03 68.57 27.12 o
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1 5 13 253.99 266.68 50.88 o
3 5 13 58.66 106.05 35.21 o
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-1 -5 14 54.90 49.19 24.68 o
1 -5 14 3.79 23.42 24.09 o
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-10 -4 14 12.99 33.10 23.00 o
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0 -4 14 431.07 485.10 55.09 o
2 -4 14 55.18 66.80 27.88 o
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-11 -3 14 351.36 298.69 50.96 o
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-1 -3 14 46.19 69.92 18.91 o
1 -3 14 314.15 328.56 35.07 o
3 -3 14 73.02 106.13 34.62 o
5 -3 14 210.63 266.52 51.97 o
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-12 -2 14 78.65 80.53 29.99 o
-10 -2 14 552.69 520.57 55.26 o
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-2 -2 14 9.71 24.90 13.30 o
0 -2 14 32.76 51.66 16.85 o
2 -2 14 6.71 8.25 12.83 o
4 -2 14 321.04 305.94 51.55 o
6 -2 14 468.14 504.14 67.22 o
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-23 -1 14 4.09 24.85 23.42 o
-21 -1 14 81.14 86.85 30.66 o
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-5 -1 14 917.89 843.84 45.85 o
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-1 -1 14 771.87 774.86 44.86 o
1 -1 14 0.06 9.80 12.88 o
3 -1 14 291.58 277.13 49.87 o
5 -1 14 32.81 51.13 28.13 o
7 -1 14 53.59 43.13 27.38 o
9 -1 14 8.53 7.33 23.42 o
-22 0 14 67.33 48.69 28.39 o
-20 0 14 12.09 11.79 19.71 o
-18 0 14 14.13 29.73 20.30 o
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-12 0 14 12.90 22.49 16.85 o
-10 0 14 31.76 51.55 22.57 o
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-2 0 14 923.94 886.65 70.08 o
0 0 14 1195.25 1226.36 83.39 o
2 0 14 9.43 25.02 19.88 o
4 0 14 356.42 364.48 57.28 o
6 0 14 4.80 12.72 21.48 o
8 0 14 258.77 355.97 60.90 o
-23 1 14 4.00 22.91 23.50 o
-19 1 14 111.66 133.09 34.45 o
-17 1 14 164.57 216.23 40.85 o
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-5 1 14 913.04 822.54 66.12 o
-3 1 14 216.71 207.13 42.20 o
-1 1 14 765.74 741.01 65.79 o
1 1 14 0.39 12.89 19.71 o
3 1 14 295.21 268.03 51.21 o
5 1 14 30.88 24.60 23.42 o
7 1 14 55.23 65.28 28.81 o
9 1 14 8.25 27.46 18.03 o
-22 2 14 7.96 17.44 15.95 o
-20 2 14 6.86 -2.52 12.93 o
-18 2 14 63.73 43.17 18.18 o
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-12 2 14 78.66 85.50 30.41 o
-10 2 14 559.31 593.51 58.37 o
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-2 2 14 11.19 14.15 20.30 o
0 2 14 29.36 30.41 21.56 o
2 2 14 6.39 27.54 19.46 o
4 2 14 319.47 344.35 56.02 o
6 2 14 456.55 432.29 62.00 o
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-21 3 14 5.46 21.53 18.07 o
-19 3 14 18.52 16.39 15.80 o
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-15 3 14 172.60 130.56 36.81 o
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-11 3 14 360.35 332.39 52.90 o
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-5 3 14 389.04 426.64 58.63 o
-3 3 14 292.06 271.32 50.03 o
-1 3 14 48.83 58.63 27.29 o
1 3 14 309.66 275.36 50.88 o
3 3 14 74.57 114.14 34.03 o
5 3 14 206.72 265.84 51.72 o
7 3 14 131.82 177.31 43.55 o
-18 4 14 3.72 7.24 14.40 o
-16 4 14 33.76 50.43 21.59 o
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-12 4 14 72.17 136.46 40.18 o
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-2 4 14 3.74 27.21 23.08 o
0 4 14 435.26 402.13 59.22 o
2 4 14 53.72 93.50 31.50 o
4 4 14 31.39 70.84 29.90 o
-13 5 14 94.16 146.40 42.54 o
-11 5 14 33.90 38.49 26.03 o
-9 5 14 2.90 27.38 22.07 o
-7 5 14 19.77 36.05 24.60 o
-5 5 14 138.70 218.50 48.94 o
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-1 5 14 53.80 77.16 28.72 o
1 5 14 3.72 16.17 19.12 o
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-7 -5 15 16.91 22.07 19.79 o
-5 -5 15 38.88 78.08 30.58 o
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-12 -4 15 13.59 35.29 24.93 o
-10 -4 15 170.52 223.39 50.29 o
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-2 -4 15 17.90 55.68 26.11 o
0 -4 15 4.02 17.44 21.73 o
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-13 -3 15 179.72 181.19 44.39 o
-11 -3 15 241.82 285.89 52.56 o
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-3 -3 15 45.98 52.56 26.03 o
-1 -3 15 404.80 417.22 39.28 o
1 -3 15 183.35 180.51 42.03 o
3 -3 15 78.06 69.75 29.23 o
5 -3 15 87.69 112.37 39.51 o
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-2 -2 15 500.53 562.32 40.17 o
0 -2 15 273.04 326.07 34.99 o
2 -2 15 242.10 239.48 48.52 o
4 -2 15 26.63 69.32 29.73 o
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-21 -1 15 8.65 22.24 23.59 o
-19 -1 15 76.37 57.70 29.99 o
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1 -1 15 58.10 69.29 19.73 o
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5 -1 15 222.76 294.73 56.52 o
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-20 0 15 37.49 41.78 25.52 o
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-12 0 15 374.65 421.84 46.92 o
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0 0 15 36.46 64.94 28.64 o
2 0 15 1.91 4.89 17.44 o
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-17 1 15 328.29 419.15 50.71 o
-15 1 15 502.07 669.41 61.57 o
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-11 1 15 94.78 122.90 35.29 o
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-1 1 15 11.65 -9.86 17.35 o
1 1 15 55.33 92.74 33.53 o
3 1 15 46.38 41.19 30.32 o
5 1 15 230.24 229.54 51.55 o
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2 2 15 246.54 246.55 51.97 o
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-1 3 15 398.37 377.28 58.46 o
1 3 15 184.96 193.57 45.65 o
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2 4 15 31.32 20.30 20.13 o
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-1 -3 16 178.16 184.72 42.03 o
1 -3 16 34.70 41.27 25.94 o
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0 -2 16 600.66 615.21 44.48 o
2 -2 16 61.65 86.42 33.69 o
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-17 -1 16 144.30 153.81 42.62 o
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-1 -1 16 8.39 24.17 14.82 o
1 -1 16 140.53 126.60 39.76 o
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-12 0 16 36.85 63.85 26.20 o
-10 0 16 522.40 597.30 58.46 o
-8 0 16 256.75 300.63 48.43 o
-6 0 16 32.20 41.36 25.44 o
-4 0 16 22.35 19.79 21.65 o
-2 0 16 0.28 11.37 20.81 o
0 0 16 116.51 108.48 25.09 o
2 0 16 0.66 4.63 20.97 o
4 0 16 158.27 215.13 50.79 o
-17 1 16 144.80 143.28 38.07 o
-15 1 16 149.95 221.54 43.72 o
-13 1 16 64.37 42.96 22.83 o
-11 1 16 86.47 74.29 28.47 o
-9 1 16 162.83 157.77 40.10 o
-7 1 16 226.80 199.47 44.48 o
-5 1 16 298.08 327.08 53.66 o
-3 1 16 23.83 38.49 27.21 o
-1 1 16 10.07 20.05 21.56 o
1 1 16 139.01 150.86 42.96 o
3 1 16 132.09 107.31 38.24 o
5 1 16 368.46 412.07 68.40 o
-18 2 16 46.23 41.19 25.10 o
-16 2 16 105.53 93.84 33.02 o
-14 2 16 94.56 81.79 31.76 o
-12 2 16 13.93 15.75 18.70 o
-10 2 16 31.72 21.65 23.08 o
-8 2 16 107.96 113.13 36.81 o
-6 2 16 124.37 108.07 36.39 o
-4 2 16 32.75 56.10 27.46 o
-2 2 16 4.93 15.67 22.32 o
0 2 16 603.87 565.04 67.72 o
2 2 16 60.04 76.23 33.61 o
4 2 16 118.80 126.86 39.51 o
-17 3 16 165.51 188.01 47.51 o
-15 3 16 151.27 122.14 37.48 o
-13 3 16 55.27 75.89 31.59 o
-11 3 16 67.67 60.82 27.63 o
-9 3 16 152.48 163.33 44.64 o
-7 3 16 25.25 65.45 30.58 o
-5 3 16 389.32 360.18 59.81 o
-3 3 16 78.30 93.50 35.63 o
-1 3 16 178.02 147.07 41.53 o
1 3 16 35.63 62.00 25.69 o
-14 4 16 187.95 179.08 48.52 o
-12 4 16 137.21 189.02 48.35 o
-10 4 16 76.47 82.63 33.19 o
-8 4 16 12.14 18.53 21.90 o
-6 4 16 29.62 67.56 31.42 o
-4 4 16 10.72 17.35 20.05 o
-2 4 16 52.49 75.64 33.27 o
-13 -3 17 39.56 49.45 28.72 o
-11 -3 17 313.79 404.32 63.60 o
-9 -3 17 51.11 64.86 31.33 o
-7 -3 17 148.80 168.05 43.46 o
-5 -3 17 14.04 49.02 24.85 o
-3 -3 17 35.70 86.59 30.91 o
-16 -2 17 106.94 69.75 33.95 o
-14 -2 17 63.30 135.20 41.86 o
-12 -2 17 66.37 87.27 31.84 o
-10 -2 17 28.06 44.31 24.85 o
-8 -2 17 127.97 188.68 45.49 o
-6 -2 17 90.65 116.33 36.89 o
-4 -2 17 6.14 22.33 15.49 o
-2 -2 17 183.40 230.30 40.22 o
0 -2 17 76.65 77.16 32.85 o
-17 -1 17 57.20 67.89 31.76 o
-15 -1 17 9.13 7.50 20.47 o
-13 -1 17 18.08 39.08 26.03 o
-11 -1 17 34.94 59.30 28.05 o
-9 -1 17 158.13 158.78 40.85 o
-7 -1 17 125.22 149.20 28.39 o
-5 -1 17 9.79 12.06 13.30 o
-3 -1 17 202.36 229.85 33.17 o
-1 -1 17 409.05 397.26 41.20 o
1 -1 17 23.84 32.26 26.28 o
-18 0 17 1.69 5.22 21.65 o
-16 0 17 0.01 3.12 17.52 o
-14 0 17 6.15 4.30 16.51 o
-12 0 17 180.56 199.04 43.21 o
-10 0 17 289.71 225.16 44.73 o
-8 0 17 26.15 37.23 24.09 o
-6 0 17 775.14 707.06 68.31 o
-4 0 17 7.67 36.22 22.49 o
-2 0 17 189.88 224.01 33.10 o
0 0 17 8.00 51.81 19.87 o
2 0 17 26.20 42.12 28.98 o
-17 1 17 55.60 53.24 25.44 o
-15 1 17 9.40 25.78 21.23 o
-13 1 17 20.55 18.87 20.22 o
-11 1 17 34.14 34.54 24.26 o
-9 1 17 159.99 186.24 44.81 o
-7 1 17 123.39 139.58 41.11 o
-5 1 17 9.23 11.54 21.82 o
-3 1 17 204.48 248.07 52.73 o
-1 1 17 407.42 361.03 61.83 o
1 1 17 25.55 14.40 25.35 o
-16 2 17 107.27 119.95 38.16 o
-14 2 17 63.54 70.42 31.00 o
-12 2 17 64.05 93.92 33.95 o
-10 2 17 27.96 31.33 24.43 o
-8 2 17 128.44 166.11 44.05 o
-6 2 17 89.71 71.35 33.19 o
-4 2 17 6.49 19.88 23.00 o
-2 2 17 183.11 244.70 54.33 o
0 2 17 79.59 107.82 39.25 o
-13 3 17 37.06 50.37 28.05 o
-11 3 17 315.08 350.16 60.14 o
-9 3 17 49.60 77.92 34.96 o
-7 3 17 148.41 172.09 46.16 o
-5 3 17 15.31 41.11 29.06 o
-3 3 17 36.36 28.39 26.20 o
-12 -2 18 172.76 211.26 50.46 o
-10 -2 18 7.25 30.41 21.73 o
-8 -2 18 158.76 224.06 48.77 o
-6 -2 18 41.30 73.87 31.33 o
-4 -2 18 120.54 185.15 45.65 o
-15 -1 18 92.94 124.83 41.44 o
-13 -1 18 39.92 44.98 27.12 o
-11 -1 18 13.49 17.69 24.68 o
-9 -1 18 393.42 407.78 62.08 o
-7 -1 18 190.15 226.29 33.62 o
-5 -1 18 11.06 40.06 18.05 o
-3 -1 18 87.77 96.30 24.71 o
-16 0 18 2.14 5.39 19.54 o
-14 0 18 231.95 237.37 52.90 o
-12 0 18 123.11 164.84 30.03 o
-10 0 18 9.59 21.24 15.02 o
-8 0 18 94.62 84.10 25.78 o
-6 0 18 1.81 16.09 14.61 o
-4 0 18 25.73 57.13 19.41 o
-2 0 18 77.06 132.67 28.43 o
-15 1 18 94.45 143.53 40.18 o
-13 1 18 37.76 43.89 27.88 o
-11 1 18 13.03 20.89 22.32 o
-9 1 18 391.40 436.25 63.43 o
-7 1 18 196.57 226.00 50.71 o
-5 1 18 10.47 13.56 23.16 o
-3 1 18 85.04 117.59 40.60 o
-12 2 18 169.44 234.93 51.97 o
-10 2 18 8.29 8.25 23.42 o
-8 2 18 159.30 174.11 46.41 o
-6 2 18 43.74 52.22 30.07 o
-4 2 18 123.99 165.44 48.86 o