#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/10/2221008.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221008_Fobs loop_ _publ_author_name 'Roopan, S. Mohana' 'Hathwar, Venkatesha R.' 'Kumar, A. Sudheer' 'Malathi, N.' 'Khan, F. Nawaz' _publ_section_title ; N-Phenylnicotinamide ; _journal_coeditor_code BT2869 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o571 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.746 _cell_angle_gamma 90.000 _cell_length_a 18.7316 _cell_length_b 5.2766 _cell_length_c 20.2482 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.8258 _[local]_cod_data_source_file bt2869Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nqo_m in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 410.26 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5657.77 5859.71 55.40 o 4 0 0 103.33 93.16 18.18 o 6 0 0 450.30 400.36 19.49 o 8 0 0 43.46 31.60 10.59 o 10 0 0 4714.51 4752.07 82.92 o 12 0 0 621.97 620.00 33.05 o 14 0 0 1758.14 1698.79 58.46 o 16 0 0 43.41 20.26 16.71 o 18 0 0 1379.86 1328.81 99.00 o 20 0 0 141.30 157.34 25.87 o 22 0 0 153.52 137.98 49.73 o 1 1 0 1614.35 1530.22 18.68 o 3 1 0 4031.89 3987.41 28.27 o 5 1 0 319.48 259.07 7.92 o 7 1 0 3207.64 3275.68 29.15 o 9 1 0 15.25 8.78 5.10 o 11 1 0 210.25 198.71 10.71 o 13 1 0 46.70 56.67 10.85 o 15 1 0 583.25 537.10 25.38 o 17 1 0 338.79 354.18 24.74 o 19 1 0 588.86 555.99 35.02 o 21 1 0 7.62 25.03 13.82 o 0 2 0 1938.35 1757.59 32.02 o 2 2 0 552.93 583.77 13.82 o 4 2 0 541.86 510.38 11.43 o 6 2 0 1550.29 1571.83 20.74 o 8 2 0 1962.25 2123.65 27.99 o 10 2 0 418.28 422.40 15.42 o 12 2 0 761.54 801.51 27.45 o 14 2 0 54.32 56.32 14.48 o 16 2 0 135.24 93.89 17.92 o 18 2 0 7.37 13.64 17.12 o 20 2 0 21.83 7.82 15.95 o 1 3 0 0.27 0.00 3.79 o 3 3 0 198.23 218.41 8.96 o 5 3 0 1078.75 1234.52 28.72 o 7 3 0 64.10 83.08 8.84 o 9 3 0 50.52 51.64 7.94 o 11 3 0 20.11 24.30 9.11 o 13 3 0 173.16 170.34 19.54 o 15 3 0 174.17 181.14 20.57 o 17 3 0 47.34 21.06 21.48 o 19 3 0 123.10 158.17 35.01 o 0 4 0 1.04 6.98 12.28 o 2 4 0 513.10 481.67 20.20 o 4 4 0 1394.83 1450.65 35.35 o 6 4 0 0.25 0.00 6.75 o 8 4 0 74.77 70.35 10.07 o 10 4 0 2.19 6.48 8.87 o 12 4 0 300.26 328.42 22.65 o 14 4 0 301.55 283.56 26.29 o 16 4 0 287.42 295.17 36.07 o 1 5 0 89.43 87.32 14.11 o 3 5 0 542.75 585.87 30.42 o 5 5 0 489.37 535.14 28.74 o 7 5 0 32.65 26.30 11.20 o 9 5 0 11.43 8.25 9.92 o 11 5 0 212.93 202.42 31.00 o 13 5 0 8.66 0.00 14.72 o 0 6 0 32.78 0.00 16.24 o 2 6 0 25.46 36.12 14.03 o 4 6 0 7.49 10.08 13.04 o 6 6 0 1.41 1.53 16.85 o -21 1 1 79.81 98.62 19.15 o -19 1 1 0.46 5.77 12.49 o -17 1 1 796.22 778.50 31.50 o -15 1 1 108.22 103.66 13.75 o -13 1 1 98.06 102.84 12.15 o -11 1 1 1162.10 1100.49 23.34 o -9 1 1 47.37 29.06 5.66 o -7 1 1 8233.08 8377.25 52.05 o -5 1 1 1900.11 1927.43 20.75 o -3 1 1 5520.67 5332.13 34.23 o -1 1 1 3162.42 3387.00 24.83 o 1 1 1 2925.55 2824.99 26.45 o 3 1 1 2094.21 2232.26 24.65 o 5 1 1 616.69 578.43 11.35 o 7 1 1 9.50 2.18 3.78 o 9 1 1 648.16 646.01 17.49 o 11 1 1 124.68 136.00 9.66 o 13 1 1 282.78 262.71 17.63 o 15 1 1 185.69 190.24 17.00 o 17 1 1 0.01 9.97 12.78 o 19 1 1 32.00 49.93 16.51 o 21 1 1 24.68 24.35 15.45 o -20 2 1 47.27 103.49 20.44 o -18 2 1 10.99 34.01 15.90 o -16 2 1 125.23 128.84 19.18 o -14 2 1 508.56 533.24 31.05 o -12 2 1 30.13 22.56 6.69 o -10 2 1 201.26 223.96 10.00 o -8 2 1 665.50 621.19 16.34 o -6 2 1 577.07 588.54 13.82 o -4 2 1 2684.84 2818.08 29.46 o -2 2 1 4390.81 4690.28 45.92 o 0 2 1 0.32 0.00 3.49 o 2 2 1 185.62 187.30 9.66 o 4 2 1 2535.88 2560.10 34.92 o 6 2 1 572.72 584.22 15.95 o 8 2 1 503.89 543.62 14.20 o 10 2 1 205.47 192.03 11.12 o 12 2 1 874.66 871.76 36.69 o 14 2 1 345.64 346.74 25.98 o 16 2 1 175.81 176.65 22.13 o 18 2 1 40.51 40.52 16.61 o 20 2 1 128.29 150.34 22.80 o -19 3 1 43.74 27.64 18.42 o -17 3 1 24.86 7.43 12.80 o -15 3 1 180.01 162.35 29.04 o -13 3 1 105.74 86.06 21.73 o -11 3 1 71.76 98.03 12.27 o -9 3 1 168.67 178.78 12.32 o -7 3 1 51.55 60.87 7.85 o -5 3 1 291.79 292.60 14.21 o -3 3 1 786.09 801.49 18.19 o -1 3 1 5.59 7.16 4.23 o 1 3 1 148.14 139.17 8.03 o 3 3 1 5.15 11.42 5.66 o 5 3 1 1486.03 1574.06 32.87 o 7 3 1 0.14 7.23 6.22 o 9 3 1 2.39 3.89 7.03 o 11 3 1 377.42 378.63 21.53 o 13 3 1 111.00 118.99 20.35 o 15 3 1 0.95 32.37 13.56 o 17 3 1 15.77 4.51 14.20 o 19 3 1 212.70 239.72 29.45 o -16 4 1 2.99 7.74 20.95 o -14 4 1 73.95 54.81 15.74 o -12 4 1 36.55 26.25 10.39 o -10 4 1 47.39 41.79 9.76 o -8 4 1 137.10 128.00 12.08 o -6 4 1 664.58 633.41 23.92 o -4 4 1 137.84 130.33 11.56 o -2 4 1 17.31 9.74 7.84 o 0 4 1 744.21 732.28 29.74 o 2 4 1 105.77 114.50 10.83 o 4 4 1 340.33 311.88 17.08 o 6 4 1 26.95 13.19 7.54 o 8 4 1 14.97 15.84 7.46 o 10 4 1 160.67 160.95 20.34 o 12 4 1 21.67 33.85 11.07 o 14 4 1 21.31 35.05 15.84 o 16 4 1 1.13 0.00 24.03 o -13 5 1 9.94 0.00 11.28 o -11 5 1 90.23 102.94 14.95 o -9 5 1 65.72 63.16 16.24 o -7 5 1 82.25 68.51 13.21 o -5 5 1 285.13 276.04 21.32 o -3 5 1 2693.82 2693.94 64.26 o -1 5 1 424.84 495.84 28.26 o 1 5 1 297.41 398.27 28.71 o 3 5 1 331.12 320.35 23.24 o 5 5 1 13.39 28.62 11.22 o 7 5 1 2.25 0.00 8.27 o 9 5 1 172.27 185.11 18.25 o 11 5 1 89.81 78.88 23.35 o 13 5 1 9.22 0.00 11.72 o -6 6 1 14.10 20.59 17.34 o -4 6 1 1.36 0.00 12.81 o -2 6 1 2.08 0.00 12.06 o 0 6 1 644.24 719.62 37.55 o 2 6 1 139.11 112.92 16.48 o 4 6 1 16.43 39.66 14.08 o 6 6 1 21.04 3.49 19.88 o -22 0 2 115.04 169.12 54.16 o -20 0 2 1673.41 1724.99 71.25 o -18 0 2 999.39 996.52 50.61 o -16 0 2 2005.93 1979.56 66.88 o -14 0 2 89.57 95.04 18.26 o -12 0 2 186.34 195.85 19.49 o -10 0 2 50.25 22.09 10.72 o -8 0 2 3078.35 3012.71 35.11 o -6 0 2 1061.79 1102.83 19.62 o -4 0 2 663.60 608.88 18.40 o -2 0 2 0.98 0.00 6.32 o 0 0 2 4302.34 4249.14 57.19 o 2 0 2 15494.59 14782.06 122.70 o 4 0 2 17450.20 17596.67 111.20 o 6 0 2 0.27 4.23 4.49 o 8 0 2 1120.55 1104.86 21.75 o 10 0 2 87.23 98.30 15.29 o 12 0 2 572.71 550.36 32.89 o 14 0 2 1976.98 1919.56 64.39 o 16 0 2 2919.92 3063.08 86.95 o 18 0 2 8.38 16.82 18.89 o 20 0 2 40.30 49.90 20.14 o -21 1 2 322.41 302.51 23.94 o -19 1 2 39.47 38.85 11.24 o -17 1 2 67.10 98.28 13.28 o -15 1 2 15.40 12.45 10.52 o -13 1 2 405.23 423.60 20.22 o -11 1 2 132.57 137.12 9.33 o -9 1 2 1927.13 1946.66 27.52 o -7 1 2 234.80 235.88 8.24 o -5 1 2 1920.87 1978.40 21.33 o -3 1 2 26004.98 26828.81 110.32 o -1 1 2 28221.73 28796.78 159.47 o 1 1 2 3258.38 3276.80 29.63 o 3 1 2 66.41 42.84 5.10 o 5 1 2 1811.52 1819.12 20.89 o 7 1 2 745.55 727.74 14.35 o 9 1 2 2429.27 2739.87 28.94 o 11 1 2 4.35 8.20 7.51 o 13 1 2 19.52 25.07 10.14 o 15 1 2 128.97 125.21 15.09 o 17 1 2 1391.52 1428.84 66.22 o 19 1 2 1.21 29.87 15.18 o 21 1 2 36.46 62.00 18.57 o -20 2 2 5.00 55.22 23.78 o -18 2 2 7.25 0.00 12.91 o -16 2 2 307.65 310.00 27.43 o -14 2 2 49.93 47.25 13.43 o -12 2 2 468.59 409.32 16.34 o -10 2 2 258.37 286.01 11.36 o -8 2 2 27.85 37.86 6.88 o -6 2 2 1270.43 1423.54 22.14 o -4 2 2 25.68 34.78 5.15 o -2 2 2 825.14 801.42 15.74 o 0 2 2 5.45 6.25 3.45 o 2 2 2 8796.60 9762.50 73.14 o 4 2 2 627.06 685.16 18.35 o 6 2 2 137.52 149.77 9.63 o 8 2 2 520.33 493.45 13.58 o 10 2 2 220.11 220.15 15.27 o 12 2 2 18.65 21.10 12.96 o 14 2 2 4.03 32.18 13.05 o 16 2 2 54.52 68.91 16.42 o 18 2 2 0.34 41.59 16.18 o 20 2 2 43.22 82.04 20.10 o -19 3 2 25.53 64.21 23.77 o -17 3 2 118.61 76.27 17.46 o -15 3 2 63.24 50.71 13.99 o -13 3 2 435.58 425.97 23.31 o -11 3 2 2.74 7.44 8.03 o -9 3 2 40.84 43.44 7.83 o -7 3 2 1396.65 1384.02 31.17 o -5 3 2 1371.77 1413.56 25.00 o -3 3 2 40.20 45.46 5.62 o -1 3 2 13.25 30.35 5.14 o 1 3 2 1533.33 1654.90 25.39 o 3 3 2 1770.96 1816.62 34.80 o 5 3 2 926.18 973.42 29.78 o 7 3 2 60.56 65.03 8.47 o 9 3 2 176.69 154.43 12.12 o 11 3 2 33.16 37.23 10.24 o 13 3 2 1157.47 1143.07 47.54 o 15 3 2 144.70 141.52 20.32 o 17 3 2 21.56 13.76 15.36 o -16 4 2 209.29 134.23 24.44 o -14 4 2 0.53 6.55 11.75 o -12 4 2 142.54 124.89 14.65 o -10 4 2 373.70 404.66 23.56 o -8 4 2 52.03 47.00 9.24 o -6 4 2 1031.90 1027.06 30.17 o -4 4 2 1481.67 1420.04 36.82 o -2 4 2 1026.41 993.50 35.07 o 0 4 2 796.57 819.79 25.88 o 2 4 2 888.44 833.31 26.74 o 4 4 2 17.15 16.88 7.11 o 6 4 2 706.40 696.28 26.00 o 8 4 2 71.07 64.01 10.33 o 10 4 2 7.24 7.60 9.30 o 12 4 2 1041.38 947.22 38.39 o 14 4 2 0.85 11.30 12.85 o 16 4 2 231.70 227.70 27.37 o -13 5 2 39.90 34.16 12.15 o -11 5 2 169.55 227.06 19.96 o -9 5 2 28.72 19.13 10.19 o -7 5 2 106.33 90.68 14.46 o -5 5 2 456.62 462.21 26.95 o -3 5 2 385.81 319.18 23.22 o -1 5 2 624.92 552.43 29.92 o 1 5 2 200.46 216.29 19.87 o 3 5 2 26.10 39.78 12.01 o 5 5 2 381.16 419.07 26.29 o 7 5 2 83.63 96.58 12.44 o 9 5 2 140.50 139.97 16.55 o 11 5 2 0.00 4.81 17.43 o 13 5 2 337.50 281.14 28.41 o -6 6 2 28.08 69.30 15.59 o -4 6 2 65.01 57.57 15.70 o -2 6 2 143.58 168.97 20.30 o 0 6 2 207.85 202.72 21.50 o 2 6 2 8.77 26.94 13.43 o 4 6 2 136.47 159.14 19.33 o 6 6 2 30.17 37.22 14.11 o -21 1 3 2.24 23.92 13.11 o -19 1 3 178.72 180.44 15.36 o -17 1 3 62.20 71.01 15.05 o -15 1 3 2.48 4.72 10.08 o -13 1 3 112.05 114.97 12.08 o -11 1 3 90.92 95.07 8.41 o -9 1 3 292.82 342.10 10.63 o -7 1 3 3673.83 3674.38 32.45 o -5 1 3 20922.09 21223.71 95.56 o -3 1 3 1113.42 1181.20 14.29 o -1 1 3 739.70 651.18 11.18 o 1 1 3 431.68 377.25 8.36 o 3 1 3 3379.53 3356.51 26.07 o 5 1 3 629.51 590.34 12.48 o 7 1 3 2791.34 3041.69 31.19 o 9 1 3 855.67 868.42 16.86 o 11 1 3 61.78 86.28 10.78 o 13 1 3 4045.12 3968.68 64.40 o 15 1 3 338.58 360.39 22.38 o 17 1 3 339.90 366.37 29.67 o 19 1 3 36.97 60.21 17.36 o -20 2 3 31.46 42.04 16.77 o -18 2 3 106.33 77.11 16.15 o -16 2 3 622.94 637.64 40.66 o -14 2 3 58.75 101.32 25.35 o -12 2 3 2.62 0.00 5.65 o -10 2 3 280.97 291.11 11.52 o -8 2 3 1412.98 1480.77 24.37 o -6 2 3 512.63 520.96 13.71 o -4 2 3 1915.40 1881.95 25.07 o -2 2 3 6.06 5.12 3.83 o 0 2 3 177.61 177.87 7.63 o 2 2 3 3684.29 4014.11 44.56 o 4 2 3 3115.55 3037.28 39.51 o 6 2 3 431.07 504.38 16.83 o 8 2 3 0.26 4.78 4.29 o 10 2 3 1561.55 1578.48 41.54 o 12 2 3 300.20 297.74 24.18 o 14 2 3 17.35 34.01 14.73 o 16 2 3 10.94 48.34 26.15 o 18 2 3 3.18 8.19 13.28 o 20 2 3 19.27 42.84 16.56 o -19 3 3 35.45 46.01 15.93 o -17 3 3 0.21 0.00 19.13 o -15 3 3 259.46 295.94 24.73 o -13 3 3 2.54 0.00 9.53 o -11 3 3 2.34 8.29 8.95 o -9 3 3 121.10 151.94 11.63 o -7 3 3 45.45 36.47 7.09 o -5 3 3 1619.71 1537.49 26.77 o -3 3 3 1.70 7.93 4.21 o -1 3 3 693.75 746.25 17.99 o 1 3 3 1387.93 1424.94 30.50 o 3 3 3 1192.21 1208.11 28.85 o 5 3 3 90.69 96.29 11.25 o 7 3 3 11.49 21.08 6.69 o 9 3 3 39.63 75.74 12.29 o 11 3 3 50.30 10.56 11.84 o 13 3 3 12.22 17.65 11.67 o 15 3 3 112.01 100.74 31.58 o 17 3 3 45.54 61.38 22.78 o -16 4 3 0.01 0.00 12.88 o -14 4 3 53.74 43.52 13.72 o -12 4 3 8.06 3.40 10.41 o -10 4 3 11.52 23.59 8.64 o -8 4 3 588.02 527.73 22.68 o -6 4 3 3.53 15.53 7.39 o -4 4 3 764.80 769.73 25.48 o -2 4 3 639.40 625.78 30.35 o 0 4 3 715.08 724.98 24.95 o 2 4 3 361.03 353.11 18.05 o 4 4 3 79.64 76.12 10.29 o 6 4 3 91.04 80.31 10.22 o 8 4 3 97.68 113.06 11.92 o 10 4 3 137.72 160.35 16.33 o 12 4 3 16.52 24.43 10.76 o 14 4 3 521.96 525.50 53.75 o 16 4 3 46.44 60.61 18.85 o -13 5 3 44.99 44.16 12.90 o -11 5 3 13.89 8.09 12.76 o -9 5 3 310.61 325.67 23.15 o -7 5 3 227.37 232.65 20.06 o -5 5 3 257.60 319.49 22.69 o -3 5 3 107.14 172.52 16.01 o -1 5 3 2898.08 2950.97 69.11 o 1 5 3 293.09 286.89 22.46 o 3 5 3 261.37 254.76 18.64 o 5 5 3 165.16 185.24 25.77 o 7 5 3 69.74 69.00 11.62 o 9 5 3 237.70 184.78 18.60 o 11 5 3 17.43 24.57 11.88 o -6 6 3 74.03 62.60 15.38 o -4 6 3 140.36 182.64 24.65 o -2 6 3 43.87 30.23 12.81 o 0 6 3 2.29 23.89 13.27 o 2 6 3 123.44 135.10 27.30 o 4 6 3 26.60 45.57 14.45 o 6 6 3 106.45 142.45 19.92 o -22 0 4 391.42 414.72 42.35 o -20 0 4 2.56 5.17 12.94 o -18 0 4 778.33 840.38 45.82 o -16 0 4 46.91 37.17 14.06 o -14 0 4 855.21 799.56 39.10 o -12 0 4 269.19 290.30 22.64 o -10 0 4 0.46 5.37 7.26 o -8 0 4 2624.10 2481.33 36.22 o -6 0 4 5557.66 5785.86 54.69 o -4 0 4 168313.78 150334.27 5141.33 o -2 0 4 5014.73 5133.50 56.81 o 0 0 4 1947.51 1726.98 22.80 o 2 0 4 60.99 48.14 9.68 o 4 0 4 49.72 39.97 21.95 o 6 0 4 16820.42 17889.80 126.76 o 8 0 4 11369.36 12467.77 103.07 o 10 0 4 328.32 307.94 24.40 o 12 0 4 89.23 76.04 17.43 o 14 0 4 289.47 263.32 38.08 o 16 0 4 436.70 403.18 34.47 o 18 0 4 410.74 385.55 36.75 o 20 0 4 9.16 41.50 28.13 o -21 1 4 108.92 146.71 30.33 o -19 1 4 357.10 380.25 23.37 o -17 1 4 11.03 17.68 12.23 o -15 1 4 10.94 11.42 8.57 o -13 1 4 1.20 1.60 7.32 o -11 1 4 1464.88 1500.29 27.97 o -9 1 4 325.07 332.69 10.80 o -7 1 4 0.12 1.73 4.95 o -5 1 4 30.64 22.41 4.53 o -3 1 4 4958.47 4861.23 34.48 o -1 1 4 8511.00 8614.41 49.08 o 1 1 4 88.68 58.55 5.12 o 3 1 4 1971.37 1978.83 22.22 o 5 1 4 19.80 16.00 4.80 o 7 1 4 515.09 569.55 14.06 o 9 1 4 132.31 116.59 7.81 o 11 1 4 24.98 7.80 14.47 o 13 1 4 587.57 591.76 26.16 o 15 1 4 401.27 403.21 39.18 o 17 1 4 2.12 18.28 14.68 o 19 1 4 2.46 23.97 16.02 o -20 2 4 45.20 43.85 14.93 o -18 2 4 7.05 10.89 13.44 o -16 2 4 302.32 330.52 29.98 o -14 2 4 230.93 228.24 22.05 o -12 2 4 472.37 490.13 21.28 o -10 2 4 155.43 158.94 9.05 o -8 2 4 136.58 131.91 7.97 o -6 2 4 186.54 210.56 9.19 o -4 2 4 1395.23 1548.96 23.09 o -2 2 4 63.31 77.02 6.09 o 0 2 4 4967.33 5183.99 41.94 o 2 2 4 1002.16 970.70 21.95 o 4 2 4 2995.36 2985.28 40.03 o 6 2 4 598.75 590.57 18.55 o 8 2 4 17.01 26.76 6.46 o 10 2 4 23.28 21.43 9.07 o 12 2 4 255.11 248.11 32.22 o 14 2 4 1214.43 1188.05 48.00 o 16 2 4 9.23 10.70 15.60 o 18 2 4 235.24 278.47 28.46 o -19 3 4 166.13 160.30 44.84 o -17 3 4 165.80 180.25 21.30 o -15 3 4 45.40 30.79 15.75 o -13 3 4 9.25 6.67 8.57 o -11 3 4 1.63 6.54 7.82 o -9 3 4 184.81 194.67 12.92 o -7 3 4 927.93 879.35 20.97 o -5 3 4 153.27 146.79 9.03 o -3 3 4 289.43 269.35 11.38 o -1 3 4 861.72 870.71 19.54 o 1 3 4 1818.68 2008.84 45.13 o 3 3 4 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