#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/10/2221019.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221019_Fobs loop_ _publ_author_name 'Imhof, Wolfgang' _publ_section_title ; (2,6-Diisopropylphenyl)(2-thienylmethylene)amine ; _journal_coeditor_code BT2882 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o593 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.651 _cell_angle_gamma 90.000 _cell_length_a 10.0877 _cell_length_b 14.2750 _cell_length_c 11.4503 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.9114 _[local]_cod_data_source_file bt2882Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tt302 in P2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 157.91 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.23 0.18 0.17 o 2 0 0 105.12 90.71 1.38 o 3 0 0 867.60 790.63 28.48 o 4 0 0 343.58 304.92 6.86 o 5 0 0 442.66 407.41 15.01 o 6 0 0 0.05 0.83 0.43 o 7 0 0 5.86 4.46 0.38 o 8 0 0 93.70 91.54 3.92 o 9 0 0 0.74 -1.37 1.37 o 10 0 0 49.24 53.39 4.01 o 1 1 0 3488.20 3405.65 176.90 o 2 1 0 200.81 159.35 2.48 o 3 1 0 2088.92 2072.80 67.98 o 4 1 0 222.70 211.92 7.15 o 5 1 0 103.44 110.14 3.49 o 6 1 0 485.50 439.99 8.60 o 7 1 0 138.41 139.22 3.06 o 8 1 0 521.18 519.97 17.33 o 9 1 0 154.16 149.24 3.90 o 10 1 0 5.41 6.44 0.87 o 0 2 0 486.85 465.64 3.15 o 1 2 0 683.47 662.04 8.86 o 2 2 0 529.07 548.63 9.03 o 3 2 0 172.42 152.81 7.80 o 4 2 0 35.13 34.43 2.60 o 5 2 0 96.22 100.36 2.14 o 6 2 0 246.82 227.44 12.42 o 7 2 0 212.41 193.85 5.35 o 8 2 0 138.51 131.45 3.32 o 9 2 0 235.17 221.67 9.53 o 10 2 0 137.21 136.10 2.85 o 1 3 0 7525.39 7882.91 204.59 o 2 3 0 1469.07 1429.75 42.59 o 3 3 0 533.19 460.90 14.69 o 4 3 0 388.27 334.45 10.00 o 5 3 0 538.61 537.56 20.01 o 6 3 0 222.39 206.91 7.37 o 7 3 0 99.54 94.67 2.16 o 8 3 0 56.40 52.28 2.56 o 9 3 0 162.87 166.43 4.08 o 10 3 0 126.94 140.18 2.93 o 0 4 0 6678.86 7236.44 17.61 o 1 4 0 236.08 219.56 2.24 o 2 4 0 3132.85 3113.84 39.14 o 3 4 0 298.02 287.48 6.15 o 4 4 0 955.51 967.67 31.05 o 5 4 0 322.27 317.73 3.77 o 6 4 0 231.94 244.86 3.68 o 7 4 0 225.27 225.47 9.42 o 8 4 0 207.24 204.04 5.73 o 9 4 0 108.30 110.07 2.53 o 10 4 0 12.04 11.37 0.70 o 1 5 0 19.12 15.39 0.59 o 2 5 0 331.21 326.66 3.17 o 3 5 0 3760.96 3955.67 95.19 o 4 5 0 917.14 973.21 6.23 o 5 5 0 742.80 688.49 17.40 o 6 5 0 174.12 168.94 3.94 o 7 5 0 197.65 194.54 4.88 o 8 5 0 28.04 29.83 1.14 o 9 5 0 68.60 66.62 1.72 o 0 6 0 95.14 93.53 2.56 o 1 6 0 2964.04 3187.42 11.75 o 2 6 0 273.94 303.27 3.94 o 3 6 0 264.62 327.73 5.80 o 4 6 0 406.93 396.69 8.25 o 5 6 0 67.17 78.48 6.11 o 6 6 0 49.67 51.52 2.74 o 7 6 0 134.84 154.43 3.56 o 8 6 0 34.22 38.49 1.08 o 9 6 0 147.80 151.62 4.16 o 1 7 0 161.18 144.31 4.61 o 2 7 0 47.99 39.86 1.05 o 3 7 0 67.94 73.09 1.59 o 4 7 0 542.03 508.11 12.33 o 5 7 0 118.37 119.85 2.77 o 6 7 0 117.66 113.05 4.76 o 7 7 0 368.72 353.97 5.34 o 8 7 0 30.41 32.13 1.41 o 9 7 0 37.15 44.17 1.22 o 0 8 0 1118.76 1207.14 10.12 o 1 8 0 405.24 422.73 7.82 o 2 8 0 596.97 616.43 5.40 o 3 8 0 183.17 190.81 3.25 o 4 8 0 271.87 281.08 4.36 o 5 8 0 201.16 190.77 3.59 o 6 8 0 95.19 90.41 2.01 o 7 8 0 114.52 106.09 2.30 o 8 8 0 73.25 73.64 2.17 o 1 9 0 5.48 5.36 0.44 o 2 9 0 631.44 689.31 6.03 o 3 9 0 271.78 269.20 4.01 o 4 9 0 49.04 49.33 1.42 o 5 9 0 327.14 329.64 4.93 o 6 9 0 13.16 11.55 0.58 o 7 9 0 12.85 14.31 0.63 o 8 9 0 47.19 50.31 1.49 o 0 10 0 354.44 369.06 6.56 o 1 10 0 305.10 321.07 4.33 o 2 10 0 337.05 344.95 4.60 o 3 10 0 60.24 57.12 1.57 o 4 10 0 6.18 8.77 0.46 o 5 10 0 23.44 21.09 0.64 o 6 10 0 258.49 238.89 4.71 o 7 10 0 104.05 113.40 5.08 o 8 10 0 1.48 -0.04 1.34 o 1 11 0 147.06 145.18 5.65 o 2 11 0 465.46 458.29 5.56 o 3 11 0 62.85 59.25 1.74 o 4 11 0 82.24 76.73 2.01 o 5 11 0 308.23 304.14 5.36 o 6 11 0 76.86 78.08 2.21 o 7 11 0 73.20 68.04 1.89 o 0 12 0 480.80 481.31 8.43 o 1 12 0 890.78 957.02 8.42 o 2 12 0 96.20 96.10 2.38 o 3 12 0 124.83 134.16 3.60 o 4 12 0 61.18 55.18 1.51 o 5 12 0 23.40 26.04 0.78 o 6 12 0 36.62 36.35 1.03 o 1 13 0 344.43 354.34 5.51 o 2 13 0 26.38 28.85 1.22 o 3 13 0 144.87 142.70 3.82 o 4 13 0 150.45 152.78 5.53 o 5 13 0 69.10 73.44 3.98 o 0 14 0 1282.50 1308.52 15.48 o 1 14 0 95.45 99.37 2.40 o 2 14 0 35.19 34.07 0.99 o 3 14 0 55.54 56.66 3.87 o 4 14 0 50.95 52.33 2.28 o 1 15 0 27.93 27.60 0.81 o 2 15 0 7.88 8.43 1.35 o 3 15 0 60.12 52.96 1.34 o -10 0 1 15.19 12.07 0.95 o -9 0 1 120.71 138.26 5.12 o -8 0 1 533.01 505.80 8.45 o -7 0 1 298.59 303.99 6.10 o -6 0 1 713.77 638.30 7.78 o -5 0 1 23.31 21.64 0.79 o -4 0 1 733.25 738.82 6.52 o -3 0 1 24.57 17.68 0.65 o -2 0 1 24935.50 26878.30 133.69 o -1 0 1 272.18 239.17 1.99 o 0 0 1 1046.84 1066.90 3.72 o 1 0 1 24.98 26.59 0.97 o 2 0 1 5412.63 5260.17 14.28 o 3 0 1 2.89 3.91 0.29 o 4 0 1 1702.61 1550.92 10.17 o 5 0 1 21.03 18.33 0.69 o 6 0 1 31.92 30.35 1.27 o 7 0 1 0.15 1.97 0.51 o 8 0 1 19.56 19.17 0.90 o 9 0 1 104.58 106.87 3.53 o 10 0 1 296.67 302.74 8.61 o -10 1 1 58.38 60.69 2.39 o -9 1 1 127.89 133.10 5.12 o -8 1 1 69.50 65.86 2.49 o -7 1 1 171.55 159.57 4.53 o -6 1 1 12.57 13.92 0.54 o -5 1 1 121.70 106.50 2.91 o -4 1 1 2410.57 2338.76 11.72 o -3 1 1 1209.07 1173.65 7.08 o -2 1 1 11472.39 11686.71 82.24 o -1 1 1 265.90 257.05 2.20 o 0 1 1 3574.24 3581.99 8.19 o 1 1 1 99.73 102.65 1.64 o 2 1 1 1064.91 1075.42 6.21 o 3 1 1 182.09 167.53 2.98 o 4 1 1 78.24 73.87 2.42 o 5 1 1 888.29 875.12 8.61 o 6 1 1 89.93 83.15 3.19 o 7 1 1 426.55 437.69 7.50 o 8 1 1 104.35 98.15 2.96 o 9 1 1 92.50 89.55 3.31 o 10 1 1 108.21 104.67 3.84 o -10 2 1 140.91 148.38 5.61 o -9 2 1 9.33 11.96 0.85 o -8 2 1 261.57 271.28 6.33 o -7 2 1 198.13 202.34 5.10 o -6 2 1 180.10 185.48 4.30 o -5 2 1 427.99 388.76 5.39 o -4 2 1 678.00 708.27 6.38 o -3 2 1 1479.83 1354.90 7.93 o -2 2 1 1118.30 988.12 5.69 o -1 2 1 1659.90 1576.72 6.58 o 0 2 1 90.09 83.86 1.49 o 1 2 1 7971.82 7699.13 16.20 o 2 2 1 978.64 913.91 5.98 o 3 2 1 1228.12 1216.29 8.09 o 4 2 1 276.40 277.29 4.41 o 5 2 1 60.66 53.43 1.68 o 6 2 1 246.76 241.16 5.17 o 7 2 1 135.70 125.46 4.30 o 8 2 1 480.25 514.58 8.91 o 9 2 1 66.69 62.44 2.36 o 10 2 1 13.37 12.52 1.00 o -10 3 1 22.54 23.17 1.11 o -9 3 1 7.65 7.89 0.84 o -8 3 1 289.10 303.58 6.69 o -7 3 1 345.69 347.81 6.69 o -6 3 1 385.77 368.41 6.06 o -5 3 1 752.36 784.63 7.91 o -4 3 1 127.09 134.08 3.06 o -3 3 1 396.11 354.33 4.35 o -2 3 1 291.68 276.03 3.41 o -1 3 1 2347.24 2373.67 9.36 o 0 3 1 3326.18 3404.46 10.81 o 1 3 1 1712.85 1639.37 7.72 o 2 3 1 23.44 15.59 0.67 o 3 3 1 1000.95 1026.12 7.69 o 4 3 1 886.65 920.84 8.32 o 5 3 1 949.99 920.09 9.09 o 6 3 1 34.70 27.33 1.11 o 7 3 1 55.19 58.72 2.22 o 8 3 1 137.29 139.69 5.04 o 9 3 1 204.47 232.18 6.50 o -10 4 1 9.71 10.12 0.95 o -9 4 1 178.89 182.15 5.87 o -8 4 1 118.64 127.16 4.52 o -7 4 1 407.04 420.67 7.35 o -6 4 1 275.49 282.63 5.60 o -5 4 1 17.70 16.03 0.85 o -4 4 1 1519.67 1550.92 10.49 o -3 4 1 22.94 16.62 0.59 o -2 4 1 288.81 262.62 3.60 o -1 4 1 2095.72 2029.40 9.38 o 0 4 1 834.99 821.89 5.91 o 1 4 1 218.37 192.77 3.08 o 2 4 1 36.23 46.15 1.22 o 3 4 1 74.10 94.49 2.57 o 4 4 1 2257.03 2301.99 13.64 o 5 4 1 104.82 102.79 3.37 o 6 4 1 40.51 40.15 1.89 o 7 4 1 46.74 41.46 1.76 o 8 4 1 162.57 160.17 5.40 o 9 4 1 22.41 22.72 1.06 o -10 5 1 51.30 51.26 2.08 o -9 5 1 26.24 27.24 1.29 o -8 5 1 60.80 60.90 2.59 o -7 5 1 27.41 25.62 1.12 o -6 5 1 756.73 768.01 9.24 o -5 5 1 138.54 161.18 4.01 o -4 5 1 663.95 662.07 7.26 o -3 5 1 708.96 687.27 6.73 o -2 5 1 738.13 781.55 6.71 o -1 5 1 685.32 767.58 6.41 o 0 5 1 357.91 342.03 4.27 o 1 5 1 694.98 730.56 6.48 o 2 5 1 1252.72 1343.43 9.13 o 3 5 1 99.64 136.01 3.38 o 4 5 1 46.96 44.94 1.60 o 5 5 1 97.06 96.82 3.44 o 6 5 1 120.38 129.50 4.17 o 7 5 1 552.44 550.34 8.82 o 8 5 1 85.84 82.28 3.10 o 9 5 1 188.00 200.80 6.89 o -9 6 1 46.80 43.12 1.79 o -8 6 1 88.03 93.88 3.06 o -7 6 1 300.76 271.78 6.33 o -6 6 1 50.66 57.68 2.14 o -5 6 1 385.34 376.30 6.30 o -4 6 1 302.04 339.19 5.50 o -3 6 1 1107.46 1058.33 8.93 o -2 6 1 1.59 1.37 0.33 o -1 6 1 12.07 11.46 0.58 o 0 6 1 249.98 228.59 3.87 o 1 6 1 2569.45 2777.95 13.67 o 2 6 1 496.21 525.88 6.27 o 3 6 1 2117.79 2266.00 13.52 o 4 6 1 85.13 79.68 3.05 o 5 6 1 321.38 304.49 5.96 o 6 6 1 144.90 140.21 4.55 o 7 6 1 11.61 13.32 0.81 o 8 6 1 3.66 3.21 0.78 o 9 6 1 6.07 7.31 0.95 o -9 7 1 43.34 45.68 1.90 o -8 7 1 96.77 108.46 3.38 o -7 7 1 21.50 21.09 0.94 o -6 7 1 78.15 75.98 2.45 o -5 7 1 432.80 428.41 7.07 o -4 7 1 356.30 350.21 5.91 o -3 7 1 410.11 431.80 6.21 o -2 7 1 1240.07 1292.63 10.18 o -1 7 1 786.33 842.97 7.95 o 0 7 1 415.05 432.23 5.68 o 1 7 1 956.43 1069.32 8.97 o 2 7 1 210.84 242.77 4.52 o 3 7 1 130.62 140.44 3.74 o 4 7 1 119.23 118.03 3.80 o 5 7 1 385.53 413.48 7.12 o 6 7 1 344.34 355.89 7.25 o 7 7 1 88.37 87.94 2.96 o 8 7 1 123.85 125.53 3.82 o -9 8 1 52.74 56.45 1.86 o -8 8 1 23.14 23.63 1.04 o -7 8 1 53.57 55.37 2.09 o -6 8 1 207.95 199.54 5.66 o -5 8 1 110.13 118.29 4.08 o -4 8 1 291.59 287.84 5.65 o -3 8 1 182.85 178.23 4.44 o -2 8 1 15.17 16.41 0.73 o -1 8 1 143.89 166.44 3.96 o 0 8 1 799.31 802.34 8.48 o 1 8 1 54.27 64.96 2.54 o 2 8 1 909.98 907.72 9.28 o 3 8 1 627.53 649.49 8.28 o 4 8 1 278.04 295.36 6.01 o 5 8 1 141.10 136.30 4.48 o 6 8 1 47.50 43.91 1.64 o 7 8 1 147.32 148.60 5.41 o 8 8 1 21.71 25.31 1.12 o -8 9 1 28.61 32.74 1.37 o -7 9 1 8.43 8.51 0.82 o -6 9 1 176.67 169.16 5.33 o -5 9 1 348.89 358.99 7.12 o -4 9 1 26.94 28.32 1.23 o -3 9 1 300.52 318.31 6.09 o -2 9 1 101.26 104.00 3.57 o -1 9 1 532.70 535.68 7.32 o 0 9 1 640.17 659.96 8.13 o 1 9 1 93.35 103.21 3.47 o 2 9 1 308.88 336.89 6.11 o 3 9 1 67.44 66.34 2.22 o 4 9 1 102.96 103.99 4.00 o 5 9 1 70.68 70.43 2.51 o 6 9 1 129.24 143.94 5.22 o 7 9 1 84.77 85.87 3.24 o 8 9 1 31.05 32.11 1.16 o -8 10 1 132.35 126.29 4.03 o -7 10 1 315.96 331.52 8.24 o -6 10 1 158.74 146.02 5.36 o -5 10 1 57.72 62.70 2.50 o -4 10 1 327.83 305.91 6.72 o -3 10 1 55.15 53.23 2.18 o -2 10 1 236.82 229.73 5.43 o -1 10 1 59.97 62.78 2.23 o 0 10 1 214.29 217.45 5.16 o 1 10 1 535.02 521.31 7.80 o 2 10 1 256.31 252.54 5.70 o 3 10 1 525.69 527.18 8.43 o 4 10 1 291.40 297.96 6.78 o 5 10 1 219.01 216.63 6.15 o 6 10 1 67.21 71.22 2.95 o 7 10 1 3.47 4.47 0.87 o -7 11 1 216.65 210.86 6.81 o -6 11 1 72.56 79.05 3.03 o -5 11 1 65.13 62.03 2.22 o -4 11 1 94.05 102.50 3.11 o -3 11 1 966.42 1000.14 11.90 o -2 11 1 691.63 699.42 9.72 o -1 11 1 1325.87 1318.10 13.06 o 0 11 1 777.83 828.10 10.33 o 1 11 1 57.77 58.33 2.35 o 2 11 1 59.70 60.43 2.39 o 3 11 1 54.13 52.92 2.36 o 4 11 1 126.68 126.78 4.71 o 5 11 1 18.18 16.75 0.91 o 6 11 1 28.68 24.29 1.09 o 7 11 1 36.52 39.77 1.77 o -6 12 1 35.09 37.96 1.63 o -5 12 1 25.99 25.14 1.07 o -4 12 1 410.28 413.51 8.51 o -3 12 1 33.48 35.08 1.36 o -2 12 1 125.09 129.00 4.75 o -1 12 1 512.27 499.93 8.59 o 0 12 1 182.60 177.60 5.57 o 1 12 1 358.77 368.41 7.37 o 2 12 1 355.19 372.33 7.74 o 3 12 1 57.36 54.23 2.07 o 4 12 1 111.49 121.82 3.58 o 5 12 1 29.88 29.46 1.43 o 6 12 1 18.91 16.93 1.05 o -6 13 1 43.43 42.17 1.61 o -5 13 1 46.50 53.91 2.00 o -4 13 1 10.48 9.95 0.86 o -3 13 1 191.63 204.58 6.35 o -2 13 1 159.26 176.65 5.67 o -1 13 1 481.62 506.82 9.04 o 0 13 1 69.56 69.29 2.98 o 1 13 1 173.47 175.65 5.77 o 2 13 1 173.14 169.70 5.67 o 3 13 1 74.91 70.86 3.02 o 4 13 1 100.38 101.47 3.44 o 5 13 1 212.72 194.46 6.78 o -4 14 1 1.26 -1.01 1.77 o -3 14 1 36.29 34.27 1.20 o -2 14 1 510.59 497.04 9.90 o -1 14 1 187.29 190.31 6.36 o 0 14 1 44.96 48.25 1.90 o 1 14 1 219.20 218.37 6.81 o 2 14 1 68.62 61.83 2.95 o 3 14 1 210.75 209.00 6.66 o 4 14 1 24.37 27.41 1.21 o -3 15 1 1.72 -0.53 1.57 o -2 15 1 91.38 94.37 3.73 o -1 15 1 31.83 31.72 1.25 o 0 15 1 39.85 41.18 1.75 o 1 15 1 34.81 33.53 1.38 o 2 15 1 29.45 23.88 1.13 o -10 0 2 66.69 65.85 2.42 o -9 0 2 373.03 378.47 7.97 o -8 0 2 310.93 300.24 6.66 o -7 0 2 19.77 21.96 0.96 o -6 0 2 663.04 682.92 7.82 o -5 0 2 0.91 1.43 0.34 o -4 0 2 1744.47 1643.16 9.78 o -3 0 2 2404.21 2311.33 10.03 o -2 0 2 87.23 85.13 1.81 o -1 0 2 1662.22 1677.09 6.78 o 0 0 2 717.71 730.72 4.42 o 1 0 2 206.00 195.56 2.63 o 2 0 2 69.20 70.69 1.94 o 3 0 2 892.89 934.09 7.34 o 4 0 2 409.76 352.06 5.13 o 5 0 2 270.31 314.07 5.45 o 6 0 2 1.17 -0.20 0.83 o 7 0 2 0.04 0.60 1.29 o 8 0 2 219.72 206.70 6.13 o 9 0 2 824.81 782.75 12.43 o -10 1 2 81.98 84.45 3.29 o -9 1 2 145.00 153.21 5.28 o -8 1 2 616.38 652.42 9.38 o -7 1 2 178.20 182.90 4.62 o -6 1 2 74.34 64.01 1.84 o -5 1 2 240.55 236.68 4.33 o -4 1 2 256.75 246.28 3.75 o -3 1 2 1544.04 1434.20 7.84 o -2 1 2 5315.47 4813.19 13.07 o -1 1 2 3333.80 3163.17 9.49 o 0 1 2 4102.80 4196.72 11.00 o 1 1 2 5094.12 4822.78 13.03 o 2 1 2 510.64 480.39 4.69 o 3 1 2 429.73 392.35 4.91 o 4 1 2 30.14 22.48 0.97 o 5 1 2 331.59 319.55 5.50 o 6 1 2 16.39 17.57 0.64 o 7 1 2 16.97 15.52 0.74 o 8 1 2 177.53 178.26 5.58 o 9 1 2 100.85 96.21 3.43 o -10 2 2 18.66 18.95 0.97 o -9 2 2 50.21 56.52 2.12 o -8 2 2 396.78 401.37 7.53 o -7 2 2 411.01 419.54 7.00 o -6 2 2 391.95 397.39 6.13 o -5 2 2 830.60 785.05 7.68 o -4 2 2 341.65 345.37 4.60 o -3 2 2 5221.56 4792.88 15.30 o -2 2 2 889.68 835.22 5.72 o -1 2 2 9607.45 9860.01 19.43 o 0 2 2 91.95 87.43 1.76 o 1 2 2 20297.18 18543.66 125.23 o 2 2 2 148.02 148.90 2.81 o 3 2 2 998.48 987.06 7.81 o 4 2 2 349.24 363.28 5.37 o 5 2 2 419.49 405.32 6.19 o 6 2 2 16.09 18.51 0.70 o 7 2 2 137.29 140.30 4.55 o 8 2 2 85.28 65.93 2.84 o 9 2 2 13.11 14.24 1.03 o -10 3 2 41.56 39.88 1.62 o -9 3 2 138.56 155.75 5.43 o -8 3 2 211.31 225.91 5.77 o -7 3 2 43.30 51.81 2.03 o -6 3 2 117.37 108.24 3.46 o -5 3 2 576.34 550.06 6.62 o -4 3 2 751.63 733.57 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188.56 178.42 5.01 o -6 5 2 436.23 440.91 6.99 o -5 5 2 21.39 21.44 0.71 o -4 5 2 554.64 564.92 6.71 o -3 5 2 106.64 100.42 2.74 o -2 5 2 166.70 156.90 3.21 o -1 5 2 847.47 868.25 7.07 o 0 5 2 2930.22 2952.88 13.21 o 1 5 2 744.83 749.02 6.80 o 2 5 2 323.49 350.57 4.96 o 3 5 2 614.43 607.82 6.96 o 4 5 2 12.49 16.16 0.65 o 5 5 2 310.05 321.68 5.97 o 6 5 2 103.12 105.73 3.95 o 7 5 2 41.28 36.56 1.39 o 8 5 2 185.35 184.35 6.02 o 9 5 2 30.94 29.69 1.21 o -10 6 2 54.14 55.43 2.16 o -9 6 2 27.51 29.05 1.19 o -8 6 2 309.83 309.41 7.21 o -7 6 2 115.90 119.96 4.30 o -6 6 2 392.39 388.23 6.90 o -5 6 2 110.19 107.69 3.54 o -4 6 2 73.82 70.59 2.65 o -3 6 2 831.67 819.67 8.09 o -2 6 2 190.78 212.29 3.98 o -1 6 2 619.33 668.58 6.86 o 0 6 2 409.92 465.12 5.71 o 1 6 2 1218.66 1318.17 9.66 o 2 6 2 79.80 85.19 2.76 o 3 6 2 317.94 295.59 5.14 o 4 6 2 159.64 163.25 4.25 o 5 6 2 612.88 655.44 8.75 o 6 6 2 81.22 88.42 2.73 o 7 6 2 165.03 177.80 5.57 o 8 6 2 64.89 60.63 2.85 o -9 7 2 49.86 51.50 1.90 o -8 7 2 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