#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/10/2221030.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221030_Fobs loop_ _publ_author_name 'Hong, Zhe' _publ_section_title ; Bis[4-chloro-2-(iminomethyl)phenolato]nickel(II) ; _journal_coeditor_code CI2768 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m273 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.864 _cell_angle_gamma 90.000 _cell_length_a 15.7751 _cell_length_b 5.6846 _cell_length_c 7.8944 _exptl_crystal_F_000 372.00 _reflns_d_resolution_high 0.7831 _[local]_cod_data_source_file ci2768Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21c in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 187.34 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1068.64 1092.43 25.43 o 3 0 0 1428.79 1449.57 23.03 o 4 0 0 924.28 878.49 14.48 o 5 0 0 1403.83 1470.09 23.79 o 6 0 0 145.60 141.64 8.84 o 7 0 0 4677.03 4731.15 74.06 o 8 0 0 7.65 7.19 1.50 o 9 0 0 4352.85 4279.06 91.28 o 10 0 0 60.30 64.37 3.60 o 11 0 0 1328.15 1357.74 23.77 o 12 0 0 1019.24 1017.50 27.04 o 13 0 0 239.38 239.61 10.38 o 14 0 0 15.33 20.19 3.88 o 15 0 0 2.07 -1.40 2.65 o 17 0 0 5.03 7.06 3.53 o 18 0 0 277.94 298.99 13.90 o 19 0 0 34.13 38.11 5.97 o 20 0 0 10.80 5.94 4.33 o 1 1 0 474.59 523.40 12.22 o 2 1 0 287.34 343.83 8.05 o 3 1 0 2245.69 2281.01 24.74 o 4 1 0 1106.63 1140.75 18.10 o 5 1 0 2036.79 2060.85 23.99 o 6 1 0 83.16 72.14 1.59 o 7 1 0 800.18 874.88 10.27 o 8 1 0 725.06 819.78 13.53 o 9 1 0 7.10 7.29 0.85 o 10 1 0 205.03 207.67 4.47 o 11 1 0 75.26 77.84 2.13 o 12 1 0 397.02 384.73 9.19 o 13 1 0 515.04 497.80 11.55 o 14 1 0 28.71 27.84 2.96 o 15 1 0 3.12 7.41 2.42 o 16 1 0 1.24 4.50 2.43 o 17 1 0 9.76 8.29 2.76 o 18 1 0 20.25 30.10 3.84 o 19 1 0 29.38 26.90 3.96 o 0 2 0 555.53 677.22 11.91 o 1 2 0 720.30 749.69 10.47 o 2 2 0 1241.92 1371.73 37.24 o 3 2 0 1302.04 1311.82 15.75 o 4 2 0 452.68 445.90 7.49 o 5 2 0 2059.63 2138.96 52.16 o 6 2 0 4795.30 5081.29 78.84 o 7 2 0 315.94 299.59 5.63 o 8 2 0 447.55 385.00 8.40 o 9 2 0 499.24 483.06 6.78 o 10 2 0 935.43 854.80 26.52 o 11 2 0 462.24 434.09 6.75 o 12 2 0 530.54 517.83 7.83 o 13 2 0 672.69 652.05 9.50 o 14 2 0 315.33 313.83 11.34 o 15 2 0 263.73 255.83 8.26 o 16 2 0 26.01 25.18 3.39 o 17 2 0 148.48 154.73 11.81 o 18 2 0 51.09 61.61 6.06 o 19 2 0 7.48 6.49 3.10 o 1 3 0 22.56 25.30 1.48 o 2 3 0 729.99 841.63 14.62 o 3 3 0 51.53 53.99 1.91 o 4 3 0 162.45 175.36 3.16 o 5 3 0 0.09 -0.33 0.72 o 6 3 0 9.26 9.32 1.21 o 7 3 0 11.58 11.90 1.11 o 8 3 0 121.51 120.59 4.26 o 9 3 0 6.41 5.95 1.11 o 10 3 0 24.16 22.68 1.70 o 11 3 0 84.33 78.90 2.79 o 12 3 0 1.95 0.06 1.18 o 13 3 0 5.09 3.93 1.48 o 14 3 0 10.08 9.30 2.57 o 15 3 0 8.97 8.41 2.66 o 16 3 0 18.13 19.16 7.62 o 17 3 0 21.73 36.07 11.82 o 18 3 0 1.47 5.27 2.98 o 0 4 0 89.40 83.76 4.08 o 1 4 0 1493.39 1605.39 19.58 o 2 4 0 595.97 617.65 21.67 o 3 4 0 1465.36 1488.88 31.42 o 4 4 0 1554.33 1584.43 23.08 o 5 4 0 468.70 458.57 8.86 o 6 4 0 379.56 388.93 13.92 o 7 4 0 222.14 219.25 11.74 o 8 4 0 1169.14 1152.29 17.87 o 9 4 0 3.69 0.77 3.07 o 10 4 0 70.34 68.31 4.10 o 11 4 0 31.55 31.09 3.12 o 12 4 0 38.49 49.80 3.81 o 13 4 0 173.65 162.20 14.50 o 14 4 0 59.40 50.06 6.97 o 1 5 0 0.00 -2.31 1.54 o 2 5 0 15.07 14.94 2.35 o 3 5 0 19.49 24.16 2.63 o 4 5 0 759.27 807.15 14.19 o 5 5 0 21.47 27.77 2.81 o 6 5 0 0.34 0.51 2.15 o 7 5 0 12.31 17.21 2.56 o 8 5 0 31.22 35.31 5.33 o 9 5 0 46.30 41.01 3.87 o 10 5 0 30.02 30.85 3.68 o 11 5 0 28.87 25.69 3.52 o 12 5 0 15.23 6.83 2.85 o 13 5 0 25.19 21.73 3.98 o 14 5 0 9.72 17.92 3.51 o 0 6 0 294.13 278.59 13.90 o 1 6 0 116.19 119.63 15.39 o 2 6 0 226.62 242.09 11.60 o 3 6 0 79.44 84.87 4.65 o 4 6 0 61.72 62.30 4.06 o 5 6 0 59.74 55.85 3.91 o 6 6 0 33.81 38.87 6.19 o 7 6 0 199.52 200.12 14.32 o 8 6 0 96.79 102.78 5.77 o 9 6 0 281.40 292.94 9.82 o 10 6 0 194.42 196.14 12.28 o 11 6 0 111.43 103.21 6.74 o 1 7 0 0.65 3.05 3.76 o 2 7 0 1.57 4.28 4.33 o 3 7 0 0.92 1.60 3.55 o 4 7 0 8.86 10.49 3.10 o 5 7 0 5.68 5.79 3.17 o -19 1 1 0.72 1.00 2.65 o -18 1 1 194.81 209.93 11.13 o -17 1 1 32.60 32.11 3.86 o -16 1 1 129.36 136.48 6.52 o -15 1 1 137.47 141.89 5.86 o -14 1 1 38.46 37.20 3.32 o -13 1 1 156.49 142.26 5.31 o -12 1 1 288.00 298.24 5.47 o -11 1 1 2318.91 2276.18 23.48 o -10 1 1 275.31 276.30 4.15 o -9 1 1 2377.46 2432.38 24.67 o -8 1 1 245.14 214.61 3.37 o -7 1 1 156.26 124.83 2.58 o -6 1 1 2934.36 3076.34 34.41 o -5 1 1 729.76 766.25 7.45 o -4 1 1 2589.40 2668.24 23.63 o -3 1 1 571.99 600.60 9.51 o -2 1 1 3879.06 4116.81 70.45 o -1 1 1 201.67 241.02 32.05 o 0 1 1 15282.59 16391.99 253.38 o 1 1 1 5993.16 6300.51 86.25 o 2 1 1 81.90 85.30 1.74 o 3 1 1 2600.96 2557.70 25.02 o 4 1 1 5.21 5.47 0.49 o 5 1 1 2516.58 2390.32 44.37 o 6 1 1 1909.54 1940.76 28.33 o 7 1 1 2547.58 2501.99 27.70 o 8 1 1 158.04 112.20 5.07 o 9 1 1 757.85 679.17 8.91 o 10 1 1 1063.79 1012.06 16.08 o 11 1 1 218.45 208.05 4.77 o 12 1 1 1645.34 1639.35 22.50 o 13 1 1 36.91 37.04 2.40 o 14 1 1 66.16 69.56 3.18 o 15 1 1 82.98 78.36 11.16 o 16 1 1 164.32 174.94 10.11 o 17 1 1 93.08 102.47 5.73 o 18 1 1 67.07 73.74 6.97 o 19 1 1 73.62 82.91 5.64 o -19 2 1 1.52 0.48 2.67 o -18 2 1 8.30 10.11 3.08 o -17 2 1 5.28 6.52 2.75 o -16 2 1 118.08 110.66 5.63 o -15 2 1 7.98 18.19 2.96 o -14 2 1 65.02 72.08 3.47 o -13 2 1 476.76 454.28 8.93 o -12 2 1 47.36 42.48 2.63 o -11 2 1 1.28 0.85 0.95 o -10 2 1 123.68 133.71 2.93 o -9 2 1 174.86 166.59 4.01 o -8 2 1 297.04 310.45 6.38 o -7 2 1 990.92 1002.99 11.22 o -6 2 1 66.92 56.80 2.10 o -5 2 1 1102.17 1140.72 32.32 o -4 2 1 527.65 614.40 15.67 o -3 2 1 435.05 461.45 5.90 o -2 2 1 352.72 412.61 9.17 o -1 2 1 3175.21 3462.63 45.02 o 0 2 1 1598.26 1869.52 51.79 o 1 2 1 417.15 492.05 18.52 o 2 2 1 1766.62 1837.07 20.89 o 3 2 1 0.09 0.39 0.51 o 4 2 1 711.46 733.05 8.14 o 5 2 1 2.00 3.81 0.73 o 6 2 1 618.49 642.46 9.60 o 7 2 1 8.73 6.19 0.96 o 8 2 1 1182.65 1238.36 16.65 o 9 2 1 182.20 161.43 3.50 o 10 2 1 74.34 65.98 2.35 o 11 2 1 216.87 217.89 6.80 o 12 2 1 8.15 7.74 1.81 o 13 2 1 8.35 9.09 1.77 o 14 2 1 64.39 65.99 4.47 o 15 2 1 100.92 96.47 6.69 o 16 2 1 4.35 5.14 2.58 o 17 2 1 101.75 112.66 6.02 o 18 2 1 1.30 2.60 2.82 o 19 2 1 2.62 1.53 2.90 o -18 3 1 0.91 1.66 2.66 o -17 3 1 251.29 260.99 8.94 o -16 3 1 49.20 52.98 4.21 o -15 3 1 137.44 137.83 6.71 o -14 3 1 360.58 349.65 7.89 o -13 3 1 127.49 114.27 4.22 o -12 3 1 402.90 410.20 6.96 o -11 3 1 10.33 8.08 1.57 o -10 3 1 433.18 421.33 7.44 o -9 3 1 2.25 3.40 0.90 o -8 3 1 1200.19 1217.09 30.75 o -7 3 1 1028.91 1043.98 31.40 o -6 3 1 947.42 988.78 16.12 o -5 3 1 3160.73 3301.95 75.17 o -4 3 1 81.11 68.68 2.09 o -3 3 1 1966.25 2053.76 40.81 o -2 3 1 385.28 479.02 7.26 o -1 3 1 2519.06 2778.91 31.23 o 0 3 1 3.30 6.49 0.99 o 1 3 1 555.09 581.58 12.01 o 2 3 1 3555.40 3792.91 42.20 o 3 3 1 838.93 885.42 11.33 o 4 3 1 3314.45 3347.12 37.58 o 5 3 1 284.15 279.90 5.13 o 6 3 1 1939.49 1959.82 23.02 o 7 3 1 166.90 158.88 3.11 o 8 3 1 521.24 508.68 6.72 o 9 3 1 396.57 384.36 6.25 o 10 3 1 156.56 154.32 3.92 o 11 3 1 469.16 464.71 8.37 o 12 3 1 4.31 0.80 1.23 o 13 3 1 499.46 530.36 9.79 o 14 3 1 154.38 151.96 7.99 o 15 3 1 161.77 166.95 7.10 o 16 3 1 21.44 24.12 3.38 o 17 3 1 51.47 59.73 6.17 o 18 3 1 83.60 99.02 6.08 o -15 4 1 3.67 8.77 4.58 o -14 4 1 27.60 28.68 5.24 o -13 4 1 32.26 28.96 3.28 o -12 4 1 20.34 19.30 2.90 o -11 4 1 14.57 19.10 3.63 o -10 4 1 120.78 126.73 9.36 o -9 4 1 71.99 74.57 4.34 o -8 4 1 14.62 14.84 2.24 o -7 4 1 373.75 392.09 8.28 o -6 4 1 13.57 12.73 2.09 o -5 4 1 100.40 103.49 4.90 o -4 4 1 132.49 132.59 4.43 o -3 4 1 141.94 155.01 3.85 o -2 4 1 1.52 0.16 1.17 o -1 4 1 168.98 170.74 4.77 o 0 4 1 41.43 45.06 3.06 o 1 4 1 6.42 10.43 1.76 o 2 4 1 8.87 5.18 1.58 o 3 4 1 0.41 -0.22 1.43 o 4 4 1 711.58 698.57 13.01 o 5 4 1 44.70 45.93 2.81 o 6 4 1 146.20 146.06 4.51 o 7 4 1 2.99 3.95 2.10 o 8 4 1 278.26 289.34 13.03 o 9 4 1 5.75 3.74 2.16 o 10 4 1 52.99 47.56 6.04 o 11 4 1 69.42 68.64 4.37 o 12 4 1 0.47 1.36 2.64 o 13 4 1 7.09 10.45 3.67 o 14 4 1 2.61 4.58 3.28 o 15 4 1 12.94 13.17 4.09 o -14 5 1 60.25 62.39 7.51 o -13 5 1 105.86 110.00 10.88 o -12 5 1 115.98 117.05 6.50 o -11 5 1 159.08 153.52 6.58 o -10 5 1 169.60 173.52 10.32 o -9 5 1 134.83 137.65 9.94 o -8 5 1 228.41 233.23 7.31 o -7 5 1 341.35 350.23 8.31 o -6 5 1 55.39 56.35 3.92 o -5 5 1 116.56 117.70 7.19 o -4 5 1 677.14 689.31 12.73 o -3 5 1 729.12 809.87 14.24 o -2 5 1 394.02 389.39 12.96 o -1 5 1 273.43 282.44 7.00 o 0 5 1 294.87 295.01 7.16 o 1 5 1 179.67 193.43 5.69 o 2 5 1 132.37 130.65 4.63 o 3 5 1 248.97 249.29 6.49 o 4 5 1 671.35 671.69 25.43 o 5 5 1 409.38 409.79 8.86 o 6 5 1 48.01 53.81 3.42 o 7 5 1 222.61 212.81 7.43 o 8 5 1 468.29 459.55 11.79 o 9 5 1 142.65 152.00 6.40 o 10 5 1 32.56 38.35 3.80 o 11 5 1 92.14 101.57 5.56 o 12 5 1 123.27 119.60 6.04 o 13 5 1 93.79 96.47 5.59 o 14 5 1 80.58 95.61 7.79 o -11 6 1 0.31 -1.53 2.71 o -10 6 1 0.10 -2.83 2.60 o -9 6 1 12.53 15.43 3.56 o -8 6 1 0.01 2.76 2.55 o -7 6 1 1.45 5.23 2.48 o -6 6 1 4.04 2.75 2.20 o -5 6 1 24.01 30.42 3.36 o -4 6 1 92.14 104.08 6.90 o -3 6 1 57.76 68.42 6.62 o -2 6 1 75.51 89.83 6.29 o -1 6 1 24.29 19.71 2.93 o 0 6 1 14.89 21.44 3.52 o 1 6 1 0.02 0.39 2.70 o 2 6 1 0.02 1.58 2.12 o 3 6 1 13.45 9.83 2.46 o 4 6 1 4.08 3.13 2.72 o 5 6 1 0.59 2.33 3.40 o 6 6 1 8.59 11.07 4.47 o 7 6 1 1.30 2.54 2.67 o 8 6 1 18.51 18.91 7.23 o 9 6 1 4.00 4.15 3.00 o 10 6 1 9.83 12.13 3.32 o 11 6 1 0.07 1.79 2.84 o -5 7 1 29.22 37.66 7.89 o -4 7 1 49.33 63.78 7.41 o -3 7 1 25.32 27.69 4.93 o -2 7 1 145.56 144.29 7.99 o -1 7 1 132.71 143.52 8.05 o 0 7 1 131.56 137.23 19.46 o 1 7 1 165.14 183.23 6.84 o 2 7 1 248.76 273.99 8.29 o 3 7 1 148.45 166.61 9.10 o 4 7 1 1.25 0.90 3.57 o -19 0 2 0.77 2.41 4.02 o -18 0 2 92.13 90.79 8.03 o -17 0 2 235.85 247.68 12.30 o -16 0 2 15.93 17.85 4.40 o -15 0 2 640.59 641.41 20.79 o -14 0 2 1.65 1.64 2.69 o -13 0 2 701.03 670.06 21.47 o -12 0 2 17.77 19.27 2.33 o -11 0 2 1350.89 1399.42 25.08 o -10 0 2 483.75 480.61 16.99 o -9 0 2 514.15 549.69 11.32 o -8 0 2 1814.24 1698.94 28.74 o -7 0 2 1282.12 1541.66 29.13 o -6 0 2 4448.61 4354.86 68.73 o -5 0 2 28.26 29.22 1.90 o -4 0 2 1656.19 1680.84 40.21 o -3 0 2 268.43 268.60 5.62 o -2 0 2 160.45 181.23 6.08 o 0 0 2 5786.25 6121.79 139.31 o 1 0 2 35094.68 34319.50 668.48 o 2 0 2 22.18 21.95 1.35 o 3 0 2 6245.39 5981.49 126.98 o 4 0 2 613.02 576.74 13.40 o 5 0 2 1227.73 1117.23 26.37 o 6 0 2 2387.78 2327.42 52.05 o 7 0 2 923.02 862.22 21.76 o 8 0 2 2723.36 2613.59 58.86 o 9 0 2 325.45 318.49 11.04 o 10 0 2 2344.88 2231.25 51.84 o 11 0 2 113.29 105.85 6.53 o 12 0 2 2097.09 2029.54 48.66 o 13 0 2 269.06 265.84 11.11 o 14 0 2 227.84 226.05 10.45 o 15 0 2 27.50 25.12 4.54 o 16 0 2 27.61 26.06 4.65 o 17 0 2 165.63 185.81 10.20 o 18 0 2 9.62 8.10 4.09 o 19 0 2 140.93 142.21 9.99 o -19 1 2 28.09 26.05 3.94 o -18 1 2 83.07 76.88 5.28 o -17 1 2 34.66 39.08 4.30 o -16 1 2 71.56 68.18 4.63 o -15 1 2 0.96 1.13 1.67 o -14 1 2 16.03 12.87 1.68 o -13 1 2 490.64 452.38 7.73 o -12 1 2 576.55 541.21 9.76 o -11 1 2 351.25 335.89 5.98 o -10 1 2 507.53 511.64 7.80 o -9 1 2 196.88 192.05 3.26 o -8 1 2 7.18 5.98 0.81 o -7 1 2 1161.11 1300.84 13.74 o -6 1 2 79.54 93.67 1.96 o -5 1 2 301.81 298.09 4.60 o -4 1 2 278.12 271.99 3.65 o -3 1 2 744.40 753.01 9.18 o -2 1 2 504.74 490.22 6.16 o -1 1 2 2736.56 2922.96 53.82 o 0 1 2 8031.27 8212.49 287.98 o 1 1 2 6012.12 6378.64 284.43 o 2 1 2 50.11 49.93 3.65 o 3 1 2 117.60 115.42 2.15 o 4 1 2 12.18 10.80 1.22 o 5 1 2 474.42 474.25 7.43 o 6 1 2 2171.48 2080.62 27.42 o 7 1 2 1.99 0.01 0.96 o 8 1 2 276.78 254.17 5.01 o 9 1 2 2.99 2.77 1.09 o 10 1 2 1.60 1.87 3.00 o 11 1 2 67.35 64.82 3.83 o 12 1 2 76.71 77.02 3.22 o 13 1 2 149.55 151.20 10.77 o 14 1 2 1.92 -0.76 1.80 o 15 1 2 98.89 100.39 3.92 o 16 1 2 6.41 7.29 2.62 o 17 1 2 1.07 8.02 5.47 o 18 1 2 4.71 7.17 2.95 o 19 1 2 10.04 16.11 3.51 o -19 2 2 32.50 41.65 4.45 o -18 2 2 22.62 23.83 3.72 o -17 2 2 73.45 72.61 5.82 o -16 2 2 71.71 77.35 4.88 o -15 2 2 31.34 41.63 3.59 o -14 2 2 232.17 230.19 6.15 o -13 2 2 34.18 27.65 3.05 o -12 2 2 518.21 498.83 10.55 o -11 2 2 683.20 698.32 10.22 o -10 2 2 711.42 715.37 8.84 o -9 2 2 640.78 662.01 10.11 o -8 2 2 820.60 842.03 10.94 o -7 2 2 1518.29 1508.23 15.44 o -6 2 2 1094.68 1135.75 12.34 o -5 2 2 4344.56 4544.07 59.40 o -4 2 2 1279.98 1308.76 30.04 o -3 2 2 1713.46 1734.09 38.77 o -2 2 2 2850.53 3017.62 123.12 o -1 2 2 2135.09 2219.46 49.30 o 0 2 2 1229.54 1225.94 22.03 o 1 2 2 240.58 269.69 18.27 o 2 2 2 996.38 1001.07 15.26 o 3 2 2 182.57 171.19 2.88 o 4 2 2 768.53 729.32 8.24 o 5 2 2 296.01 272.11 3.89 o 6 2 2 1492.50 1505.59 15.76 o 7 2 2 1373.89 1393.67 14.78 o 8 2 2 16.45 10.29 1.22 o 9 2 2 241.40 227.17 5.54 o 10 2 2 288.50 270.22 6.86 o 11 2 2 369.36 356.40 7.11 o 12 2 2 77.52 82.74 3.45 o 13 2 2 258.09 268.68 6.37 o 14 2 2 365.54 368.93 8.67 o 15 2 2 209.62 210.09 6.63 o 16 2 2 133.85 137.41 6.36 o 17 2 2 63.81 71.66 5.09 o 18 2 2 140.43 169.03 8.03 o -18 3 2 0.30 0.86 2.76 o -17 3 2 1.77 2.47 2.74 o -16 3 2 9.65 12.98 2.46 o -15 3 2 7.47 7.30 2.14 o -14 3 2 4.00 7.28 2.02 o -13 3 2 12.31 15.59 2.21 o -12 3 2 0.49 0.91 1.35 o -11 3 2 23.69 24.28 1.73 o -10 3 2 0.60 0.32 0.87 o -9 3 2 330.20 330.45 5.33 o -8 3 2 20.64 23.83 1.33 o -7 3 2 294.97 302.27 6.81 o -6 3 2 43.72 51.06 2.80 o -5 3 2 61.18 69.08 1.91 o -4 3 2 0.42 0.34 0.90 o -3 3 2 286.19 273.70 8.76 o -2 3 2 69.49 79.24 4.18 o -1 3 2 436.69 499.01 13.39 o 0 3 2 88.20 85.35 3.01 o 1 3 2 155.83 160.73 4.02 o 2 3 2 3.03 3.65 1.01 o 3 3 2 130.45 143.25 3.24 o 4 3 2 223.42 212.79 7.14 o 5 3 2 21.37 19.83 1.23 o 6 3 2 16.61 18.20 1.24 o 7 3 2 75.63 77.14 2.58 o 8 3 2 16.88 17.53 1.55 o 9 3 2 1.26 2.49 1.18 o 10 3 2 14.89 17.61 1.70 o 11 3 2 1.16 -0.20 1.28 o 12 3 2 78.08 66.15 3.24 o 13 3 2 8.41 7.39 1.84 o 14 3 2 22.90 24.84 2.58 o 15 3 2 0.57 0.16 1.89 o 16 3 2 4.07 10.70 2.18 o 17 3 2 5.82 5.93 2.96 o -16 4 2 155.42 152.59 10.27 o -15 4 2 16.80 8.63 4.72 o -14 4 2 272.58 265.51 12.16 o -13 4 2 103.07 101.76 5.51 o -12 4 2 196.27 208.34 7.33 o -11 4 2 36.80 42.86 2.22 o -10 4 2 35.48 38.80 2.09 o -9 4 2 41.87 50.05 3.20 o -8 4 2 63.02 60.80 3.43 o -7 4 2 1053.41 1085.92 27.46 o -6 4 2 85.15 79.90 3.59 o -5 4 2 726.29 740.00 21.22 o -4 4 2 267.83 270.23 6.30 o -3 4 2 463.58 457.43 12.07 o -2 4 2 489.21 496.78 9.28 o -1 4 2 261.10 244.54 5.90 o 0 4 2 549.43 586.61 8.63 o 1 4 2 80.54 84.57 2.79 o 2 4 2 1443.95 1534.55 18.94 o 3 4 2 603.43 606.49 10.93 o 4 4 2 2151.99 2173.74 35.19 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