#------------------------------------------------------------------------------ #$Date: 2016-04-03 03:59:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181131 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/10/2221052.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221052_Fobs loop_ _publ_author_name 'Maliha, Bushra' 'Tariq, Muhammad Ilyas' 'Tahir, M. Nawaz' 'Hussain, Ishtiaq' 'Siddiqui, Hamid Latif' _publ_section_title ; 3-[(Methylcarbamoyl)amino]-1H-isoindolium chloride ; _journal_coeditor_code EZ2156 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o448 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.484 _cell_angle_beta 69.997 _cell_angle_gamma 74.613 _cell_length_a 7.1171 _cell_length_b 7.7900 _cell_length_c 10.3033 _exptl_crystal_F_000 236.00 _reflns_d_resolution_high 0.7686 _cod_data_source_file ez2156Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BM51_sad in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 76.78 77.83 0.88 o 3 0 0 205.07 198.43 1.97 o 4 0 0 10.95 19.86 0.55 o 5 0 0 240.43 245.30 2.94 o 6 0 0 2.69 1.99 0.39 o 7 0 0 0.24 0.24 0.36 o 8 0 0 10.48 11.28 1.03 o -8 1 0 51.90 52.05 1.71 o -7 1 0 154.33 156.16 2.84 o -6 1 0 176.96 177.87 3.23 o -5 1 0 0.06 0.30 0.21 o -4 1 0 252.80 254.46 2.63 o -3 1 0 1064.71 1074.77 8.88 o -2 1 0 846.15 871.80 7.75 o -1 1 0 1618.05 1644.70 12.67 o 1 1 0 76.64 57.43 2.98 o 2 1 0 2966.05 3095.19 20.52 o 3 1 0 62.18 58.79 0.86 o 4 1 0 32.20 39.79 0.78 o 5 1 0 50.19 60.02 1.10 o 6 1 0 0.29 -0.18 0.25 o 7 1 0 18.01 18.08 1.09 o 8 1 0 68.41 70.12 2.14 o -7 2 0 1.36 0.90 0.50 o -6 2 0 301.95 312.15 4.79 o -5 2 0 1.56 0.67 0.26 o -4 2 0 209.52 203.11 2.31 o -3 2 0 73.23 77.42 1.54 o -2 2 0 589.73 628.37 5.92 o -1 2 0 1278.66 1406.54 10.83 o 0 2 0 3177.21 3270.13 53.56 o 1 2 0 17.91 24.33 0.46 o 2 2 0 6.47 8.22 0.28 o 3 2 0 878.52 887.68 6.85 o 4 2 0 9.78 6.50 0.38 o 5 2 0 1.84 0.53 0.19 o 6 2 0 148.50 149.57 2.85 o 7 2 0 42.39 40.04 1.45 o 8 2 0 43.81 46.44 1.71 o -7 3 0 10.35 11.22 1.21 o -6 3 0 0.29 1.10 0.46 o -5 3 0 1.86 1.17 0.46 o -4 3 0 240.77 231.80 3.16 o -3 3 0 677.87 742.40 6.66 o -2 3 0 339.48 360.83 3.23 o -1 3 0 415.82 514.56 4.51 o 0 3 0 22.56 19.86 0.54 o 1 3 0 68.75 69.64 0.96 o 2 3 0 771.29 773.49 6.55 o 3 3 0 115.84 107.80 1.27 o 4 3 0 39.82 40.11 0.82 o 5 3 0 77.21 78.91 1.31 o 6 3 0 142.43 137.67 2.35 o 7 3 0 50.64 56.51 1.73 o 8 3 0 19.65 19.38 1.44 o -6 4 0 183.92 179.79 5.85 o -5 4 0 20.40 19.26 1.27 o -4 4 0 21.32 15.46 0.91 o -3 4 0 30.80 33.27 0.90 o -2 4 0 419.54 425.98 3.85 o -1 4 0 324.76 341.34 3.61 o 0 4 0 137.58 154.32 2.60 o 1 4 0 96.47 117.38 2.28 o 2 4 0 22.65 35.10 0.93 o 3 4 0 1462.94 1498.69 12.33 o 4 4 0 636.56 601.51 5.68 o 5 4 0 1.07 1.60 0.27 o 6 4 0 16.76 17.31 0.93 o 7 4 0 8.60 7.76 0.92 o 8 4 0 42.68 45.23 2.01 o -6 5 0 3.85 2.42 0.88 o -5 5 0 178.41 169.68 7.78 o -4 5 0 3.83 4.78 1.44 o -3 5 0 54.74 55.29 3.41 o -2 5 0 1.36 1.37 0.30 o -1 5 0 39.42 36.67 0.93 o 0 5 0 400.65 388.76 4.28 o 1 5 0 318.52 301.23 7.01 o 2 5 0 248.10 279.46 3.05 o 3 5 0 1.66 1.35 0.26 o 4 5 0 67.70 64.83 1.24 o 5 5 0 296.24 304.14 4.48 o 6 5 0 298.49 302.28 5.33 o 7 5 0 0.06 0.35 0.46 o 8 5 0 63.37 64.46 2.46 o -5 6 0 0.22 0.08 0.67 o -4 6 0 33.26 34.74 2.11 o -3 6 0 140.93 138.89 3.37 o -2 6 0 35.63 39.91 1.22 o -1 6 0 7.23 8.11 0.63 o 0 6 0 276.38 273.78 3.54 o 1 6 0 2.37 2.22 0.37 o 2 6 0 1117.36 1077.72 11.69 o 3 6 0 472.51 501.48 6.72 o 4 6 0 118.74 114.86 2.12 o 5 6 0 0.07 0.57 0.37 o 6 6 0 75.59 78.95 2.45 o 7 6 0 42.01 42.46 2.43 o 8 6 0 44.12 41.32 2.07 o -4 7 0 16.05 16.13 1.78 o -3 7 0 0.01 -0.22 0.53 o -2 7 0 31.84 33.44 1.61 o -1 7 0 9.78 8.41 1.07 o 0 7 0 431.59 427.73 5.14 o 1 7 0 885.26 903.33 9.01 o 2 7 0 75.18 78.50 2.14 o 3 7 0 15.92 15.46 1.01 o 4 7 0 190.98 200.36 3.65 o 5 7 0 52.82 52.35 1.84 o 6 7 0 121.22 119.82 4.03 o 7 7 0 103.74 109.48 3.96 o -3 8 0 44.22 34.93 3.30 o -2 8 0 96.16 95.54 2.59 o -1 8 0 5.61 7.49 0.84 o 0 8 0 41.47 38.45 1.36 o 1 8 0 111.45 112.19 2.32 o 2 8 0 213.16 218.42 3.73 o 3 8 0 582.29 572.56 7.66 o 4 8 0 87.15 85.81 2.82 o 5 8 0 5.97 5.12 1.07 o 6 8 0 52.10 47.30 2.65 o 7 8 0 12.11 7.80 1.95 o -1 9 0 129.59 133.84 4.67 o 0 9 0 251.63 273.95 4.77 o 1 9 0 0.03 0.23 0.39 o 2 9 0 0.01 0.40 0.38 o 3 9 0 9.56 8.61 1.06 o 4 9 0 131.69 134.52 3.86 o 5 9 0 7.96 5.87 1.23 o 2 10 0 46.49 53.89 2.09 o 3 10 0 23.26 20.07 1.65 o -3 -10 1 25.58 21.18 1.73 o -2 -10 1 173.07 183.48 4.12 o -5 -9 1 52.82 50.05 2.16 o -4 -9 1 0.51 0.81 0.59 o -3 -9 1 3.70 3.95 0.75 o -2 -9 1 29.51 32.00 1.36 o -1 -9 1 219.47 226.63 3.77 o 0 -9 1 54.31 58.90 2.08 o 1 -9 1 2.80 1.64 0.77 o -6 -8 1 0.42 -0.01 0.93 o -5 -8 1 75.32 74.48 2.72 o -4 -8 1 305.25 308.37 5.29 o -3 -8 1 25.44 28.12 1.46 o -2 -8 1 8.29 6.07 0.76 o -1 -8 1 33.92 29.72 1.20 o 0 -8 1 4.11 2.38 0.46 o 1 -8 1 28.16 29.67 1.95 o 2 -8 1 93.38 95.46 2.91 o 3 -8 1 2.81 4.20 1.09 o -7 -7 1 191.36 212.78 5.97 o -6 -7 1 126.55 133.40 4.37 o -5 -7 1 31.55 31.10 1.73 o -4 -7 1 7.08 6.27 0.69 o -3 -7 1 7.51 6.88 0.76 o -2 -7 1 122.82 120.36 2.63 o -1 -7 1 131.27 142.82 2.90 o 0 -7 1 27.66 23.79 1.01 o 1 -7 1 65.47 67.09 1.68 o 2 -7 1 121.51 126.85 3.29 o 3 -7 1 18.84 20.20 1.56 o 4 -7 1 14.89 12.54 1.55 o -7 -6 1 25.92 25.71 3.21 o -6 -6 1 174.07 172.14 3.90 o -5 -6 1 18.73 18.54 1.09 o -4 -6 1 318.47 321.54 3.86 o -3 -6 1 176.22 166.94 3.05 o -2 -6 1 115.03 109.65 2.67 o -1 -6 1 152.68 159.76 2.87 o 0 -6 1 19.23 19.05 0.83 o 1 -6 1 226.33 239.39 3.29 o 2 -6 1 261.36 233.23 3.30 o 3 -6 1 308.27 282.23 4.97 o 4 -6 1 135.52 145.38 4.32 o 5 -6 1 28.87 28.59 1.95 o -8 -5 1 343.34 354.44 9.27 o -7 -5 1 342.11 353.13 6.40 o -6 -5 1 0.07 0.20 0.44 o -5 -5 1 3.05 2.37 0.43 o -4 -5 1 51.54 59.78 1.88 o -3 -5 1 6.71 6.56 0.53 o -2 -5 1 82.44 70.41 1.24 o -1 -5 1 231.80 253.31 3.63 o 0 -5 1 12.65 12.60 0.73 o 1 -5 1 11.36 14.67 0.93 o 2 -5 1 636.88 627.87 5.87 o 3 -5 1 1.13 2.06 0.38 o 4 -5 1 49.72 46.54 3.01 o 5 -5 1 214.50 198.94 4.28 o 6 -5 1 80.46 85.17 4.52 o -8 -4 1 18.50 15.01 2.26 o -7 -4 1 95.47 89.90 2.77 o -6 -4 1 271.95 265.00 4.95 o -5 -4 1 43.05 40.86 1.05 o -4 -4 1 310.66 320.38 3.57 o -3 -4 1 62.29 75.61 1.23 o -2 -4 1 218.58 262.53 2.84 o -1 -4 1 42.62 42.32 1.30 o 0 -4 1 603.07 634.43 6.95 o 1 -4 1 9.59 14.59 0.48 o 2 -4 1 3.15 2.55 0.24 o 3 -4 1 30.62 26.87 0.72 o 4 -4 1 307.00 296.18 4.23 o 5 -4 1 97.02 99.07 2.30 o 6 -4 1 22.35 20.01 1.38 o -8 -3 1 32.89 33.84 1.85 o -7 -3 1 223.68 235.05 4.79 o -6 -3 1 1.13 1.06 0.36 o -5 -3 1 33.40 31.19 0.84 o -4 -3 1 331.17 332.48 3.25 o -3 -3 1 44.70 51.24 0.96 o -2 -3 1 684.61 708.01 5.26 o -1 -3 1 319.90 360.98 3.67 o 0 -3 1 957.47 1071.06 10.64 o 1 -3 1 109.95 88.57 1.01 o 2 -3 1 977.10 1035.10 7.33 o 3 -3 1 121.94 137.97 1.67 o 4 -3 1 117.41 126.82 2.07 o 5 -3 1 260.43 257.34 3.55 o 6 -3 1 2.78 2.83 0.63 o 7 -3 1 27.02 25.63 1.47 o -8 -2 1 1.30 1.68 0.65 o -7 -2 1 1.36 0.63 0.42 o -6 -2 1 149.34 146.59 2.81 o -5 -2 1 272.41 282.16 3.03 o -4 -2 1 288.31 282.32 2.84 o -3 -2 1 401.29 405.75 3.81 o -2 -2 1 267.32 290.84 2.51 o -1 -2 1 549.11 538.01 4.93 o 0 -2 1 1034.66 1111.59 9.63 o 1 -2 1 3.71 5.19 0.20 o 2 -2 1 522.88 522.80 3.87 o 3 -2 1 154.41 214.83 2.32 o 4 -2 1 150.62 156.16 1.87 o 5 -2 1 65.04 63.08 1.39 o 6 -2 1 0.22 0.24 0.29 o 7 -2 1 308.09 328.92 5.13 o -8 -1 1 61.73 62.75 4.60 o -7 -1 1 39.60 43.31 1.59 o -6 -1 1 3.87 4.94 0.71 o -5 -1 1 16.26 16.89 0.65 o -4 -1 1 1721.79 1812.64 14.58 o -3 -1 1 277.63 258.19 2.64 o -2 -1 1 13.86 8.71 0.31 o -1 -1 1 2.10 1.77 0.14 o 0 -1 1 14.42 1.24 0.17 o 1 -1 1 26.25 37.87 0.38 o 2 -1 1 739.29 781.20 4.84 o 3 -1 1 42.59 43.96 0.67 o 4 -1 1 28.35 19.96 0.54 o 5 -1 1 114.60 113.37 1.93 o 6 -1 1 9.08 7.29 0.71 o 7 -1 1 24.75 25.22 1.25 o 8 -1 1 1.32 0.87 0.44 o -8 0 1 6.07 5.26 0.85 o -7 0 1 70.69 76.79 2.38 o -6 0 1 447.64 453.96 6.12 o -5 0 1 52.45 53.55 1.20 o -4 0 1 27.81 23.04 0.85 o -3 0 1 77.36 66.32 1.22 o -2 0 1 1978.82 2060.67 17.53 o -1 0 1 1092.28 1084.38 9.31 o 1 0 1 122.62 23.08 0.89 o 2 0 1 2302.48 2384.21 16.99 o 3 0 1 203.94 212.82 1.84 o 4 0 1 156.37 168.31 1.82 o 5 0 1 45.10 50.20 1.17 o 6 0 1 84.47 79.54 1.67 o 7 0 1 233.62 254.10 3.69 o 8 0 1 215.46 217.60 4.00 o -7 1 1 236.52 240.90 3.83 o -6 1 1 173.25 172.13 3.26 o -5 1 1 543.44 564.60 5.69 o -4 1 1 159.26 158.95 2.32 o -3 1 1 307.98 312.12 3.49 o -2 1 1 0.39 0.46 0.12 o -1 1 1 8.54 3.75 0.20 o 0 1 1 706.20 418.45 8.46 o 1 1 1 226.61 125.96 5.95 o 2 1 1 1482.98 1546.08 10.40 o 3 1 1 272.07 288.43 2.21 o 4 1 1 421.11 400.97 3.49 o 5 1 1 206.88 197.94 2.58 o 6 1 1 31.75 29.62 0.97 o 7 1 1 0.09 0.04 0.30 o 8 1 1 158.94 160.94 3.27 o -7 2 1 354.92 370.66 6.64 o -6 2 1 100.90 107.03 2.56 o -5 2 1 4.72 3.19 0.44 o -4 2 1 0.45 0.98 0.22 o -3 2 1 196.49 180.70 2.70 o -2 2 1 118.64 104.64 1.56 o -1 2 1 155.62 155.70 1.90 o 0 2 1 259.54 249.65 2.28 o 1 2 1 2.18 9.66 0.43 o 2 2 1 0.08 1.44 0.21 o 3 2 1 110.56 99.81 1.10 o 4 2 1 88.16 85.85 1.17 o 5 2 1 3.73 3.53 0.34 o 6 2 1 780.94 789.04 8.02 o 7 2 1 69.01 75.07 1.76 o 8 2 1 7.46 5.72 0.74 o -7 3 1 6.17 2.79 1.33 o -6 3 1 17.55 19.39 2.06 o -5 3 1 519.68 505.99 7.71 o -4 3 1 45.50 48.52 1.79 o -3 3 1 7.40 9.98 0.59 o -2 3 1 169.74 159.78 2.68 o -1 3 1 475.38 609.56 5.28 o 0 3 1 1322.09 1306.36 15.31 o 1 3 1 127.37 136.85 1.74 o 2 3 1 136.81 145.30 1.67 o 3 3 1 334.87 330.27 2.97 o 4 3 1 76.08 74.41 1.27 o 5 3 1 270.98 288.16 3.73 o 6 3 1 0.02 0.14 0.23 o 7 3 1 85.09 83.55 1.84 o 8 3 1 71.03 72.53 2.07 o -6 4 1 7.33 6.48 0.87 o -5 4 1 1.31 1.71 0.57 o -4 4 1 0.11 0.32 0.30 o -3 4 1 561.14 542.93 5.92 o -2 4 1 0.10 2.25 0.34 o -1 4 1 152.03 158.29 2.01 o 0 4 1 437.85 437.73 4.45 o 1 4 1 47.85 39.24 0.81 o 2 4 1 1104.91 1093.01 9.10 o 3 4 1 5.83 6.29 0.38 o 4 4 1 262.43 281.82 2.89 o 5 4 1 47.63 48.11 1.09 o 6 4 1 207.55 207.40 3.02 o 7 4 1 3.70 4.86 0.64 o 8 4 1 36.60 35.02 2.14 o -5 5 1 34.30 31.80 3.41 o -4 5 1 100.90 94.25 2.85 o -3 5 1 0.20 0.22 0.29 o -2 5 1 429.80 392.67 5.24 o -1 5 1 70.89 64.81 1.59 o 0 5 1 152.75 136.25 2.09 o 1 5 1 41.37 46.44 0.99 o 2 5 1 107.23 118.17 1.68 o 3 5 1 141.90 149.01 2.03 o 4 5 1 0.47 0.61 0.31 o 5 5 1 81.66 91.79 1.85 o 6 5 1 83.20 84.91 2.08 o 7 5 1 7.34 6.12 1.16 o 8 5 1 124.07 127.35 3.97 o -5 6 1 0.15 -0.62 0.93 o -4 6 1 102.39 99.09 3.64 o -3 6 1 369.75 344.97 6.07 o -2 6 1 5.43 5.88 0.60 o -1 6 1 43.78 31.83 1.05 o 0 6 1 697.69 669.65 6.89 o 1 6 1 10.76 9.70 0.63 o 2 6 1 59.97 54.93 1.54 o 3 6 1 47.92 47.87 1.44 o 4 6 1 0.87 1.00 0.31 o 5 6 1 24.03 23.55 1.02 o 6 6 1 1.43 0.77 0.52 o 7 6 1 2.28 1.82 0.62 o 8 6 1 20.93 14.77 1.35 o -4 7 1 2.03 5.45 1.64 o -3 7 1 6.40 6.17 0.97 o -2 7 1 178.29 179.35 4.09 o -1 7 1 453.11 432.49 5.32 o 0 7 1 16.43 12.47 0.81 o 1 7 1 136.46 141.07 2.45 o 2 7 1 8.07 6.05 0.78 o 3 7 1 62.61 67.26 1.98 o 4 7 1 251.30 253.91 4.91 o 5 7 1 46.09 42.34 2.19 o 6 7 1 104.27 107.86 3.71 o 7 7 1 22.09 20.82 2.22 o -2 8 1 1.88 2.07 0.75 o -1 8 1 0.07 0.41 0.39 o 0 8 1 181.94 187.79 3.20 o 1 8 1 0.28 0.34 0.34 o 2 8 1 5.10 4.68 0.60 o 3 8 1 60.03 59.76 1.63 o 4 8 1 60.59 60.19 2.31 o 5 8 1 4.93 3.85 0.97 o 6 8 1 104.66 107.56 6.65 o 7 8 1 0.63 1.65 0.88 o -1 9 1 1.05 1.69 0.76 o 0 9 1 11.13 12.20 1.45 o 1 9 1 8.26 6.62 0.76 o 2 9 1 15.22 14.65 1.01 o 3 9 1 7.21 6.34 0.80 o 4 9 1 0.33 0.30 0.45 o 5 9 1 4.86 4.36 1.13 o 6 9 1 114.93 126.18 6.47 o 2 10 1 3.85 3.93 0.85 o 3 10 1 108.90 109.78 2.93 o -2 -10 2 152.71 162.68 7.44 o -5 -9 2 19.89 16.91 2.63 o -4 -9 2 112.66 125.93 5.01 o -3 -9 2 55.84 63.94 2.35 o -2 -9 2 116.36 107.56 2.91 o -1 -9 2 13.78 11.29 1.06 o 0 -9 2 16.76 17.00 1.26 o 1 -9 2 11.88 8.60 1.41 o -6 -8 2 84.36 83.00 3.68 o -5 -8 2 19.82 20.22 1.65 o -4 -8 2 20.73 20.21 1.22 o -3 -8 2 6.89 5.01 0.73 o -2 -8 2 63.87 63.44 2.04 o -1 -8 2 79.06 80.88 2.34 o 0 -8 2 32.84 29.28 1.89 o 1 -8 2 10.98 12.23 1.03 o 2 -8 2 157.94 173.77 4.02 o 3 -8 2 100.65 103.85 3.92 o -7 -7 2 53.59 43.77 3.63 o -6 -7 2 20.34 19.95 1.90 o -5 -7 2 70.07 65.87 2.48 o -4 -7 2 100.71 103.15 3.37 o -3 -7 2 14.45 13.21 0.91 o -2 -7 2 389.77 391.23 5.65 o -1 -7 2 492.52 490.62 6.55 o 0 -7 2 170.43 175.86 2.85 o 1 -7 2 228.24 232.40 3.85 o 2 -7 2 0.04 -0.31 0.36 o 3 -7 2 2.11 1.60 0.87 o 4 -7 2 17.44 16.24 3.30 o -7 -6 2 5.14 4.18 0.88 o -6 -6 2 0.21 -0.16 0.41 o -5 -6 2 264.42 260.27 3.88 o -4 -6 2 47.46 44.31 1.33 o -3 -6 2 22.43 26.01 1.27 o -2 -6 2 201.22 187.32 3.27 o -1 -6 2 4.66 8.56 0.72 o 0 -6 2 502.10 476.96 6.09 o 1 -6 2 661.54 651.61 7.37 o 2 -6 2 538.12 546.41 6.71 o 3 -6 2 10.42 10.37 0.95 o 4 -6 2 62.40 64.58 2.16 o 5 -6 2 33.35 27.56 2.02 o -7 -5 2 42.35 40.73 3.54 o -6 -5 2 181.47 186.85 3.63 o -5 -5 2 4.84 5.37 0.59 o -4 -5 2 353.48 344.27 4.35 o -3 -5 2 55.36 55.79 1.23 o -2 -5 2 103.70 115.99 2.03 o -1 -5 2 383.82 408.67 5.60 o 0 -5 2 1282.57 1274.98 13.72 o 1 -5 2 113.84 121.49 1.96 o 2 -5 2 17.52 17.59 0.70 o 3 -5 2 7.23 5.87 0.68 o 4 -5 2 4.51 6.50 0.77 o 5 -5 2 130.28 126.15 3.20 o 6 -5 2 49.77 57.24 2.63 o -8 -4 2 3.58 2.11 0.98 o -7 -4 2 1.13 1.09 0.57 o -6 -4 2 141.82 149.10 3.11 o 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2.48 o 0 -2 2 876.23 940.83 8.31 o 1 -2 2 28.09 20.18 0.37 o 2 -2 2 167.31 171.20 1.38 o 3 -2 2 454.92 477.76 3.29 o 4 -2 2 0.01 0.48 0.26 o 5 -2 2 526.35 550.27 5.87 o 6 -2 2 185.89 174.88 2.76 o 7 -2 2 1.48 1.43 0.49 o 8 -2 2 21.02 20.23 1.42 o -7 -1 2 6.80 5.68 0.76 o -6 -1 2 115.06 118.54 2.59 o -5 -1 2 186.02 184.38 2.74 o -4 -1 2 78.89 100.02 1.58 o -3 -1 2 7.16 10.24 0.45 o -2 -1 2 112.62 118.87 1.64 o -1 -1 2 986.19 972.13 9.54 o 0 -1 2 493.39 581.47 4.35 o 1 -1 2 57.51 40.48 0.45 o 2 -1 2 1807.63 1751.97 17.53 o 3 -1 2 733.59 762.80 5.25 o 4 -1 2 511.51 492.57 4.17 o 5 -1 2 22.86 18.22 0.69 o 6 -1 2 9.07 6.95 0.56 o 7 -1 2 1.66 2.04 0.43 o 8 -1 2 210.84 205.57 3.35 o -7 0 2 135.56 136.98 5.26 o -6 0 2 34.89 37.70 1.68 o -5 0 2 2.02 2.05 0.35 o -4 0 2 13.14 8.05 0.55 o -3 0 2 140.63 148.02 2.09 o -2 0 2 21.32 26.80 0.67 o -1 0 2 12.02 11.97 0.42 o 0 0 2 2428.54 2397.46 22.24 o 1 0 2 44.81 51.25 1.10 o 2 0 2 4251.26 4430.31 85.82 o 3 0 2 398.66 465.94 3.68 o 4 0 2 158.66 157.04 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5.03 o 6 -1 9 99.75 101.07 3.75 o 7 -1 9 19.19 14.75 1.30 o 8 -1 9 67.88 66.19 2.70 o -4 0 9 0.02 0.86 0.77 o -3 0 9 53.10 58.52 4.59 o -2 0 9 51.44 46.74 2.00 o -1 0 9 31.23 23.30 1.69 o 0 0 9 29.31 25.89 1.52 o 1 0 9 297.23 290.89 5.64 o 2 0 9 63.37 64.05 1.62 o 3 0 9 116.35 124.34 2.10 o 4 0 9 18.97 19.42 0.82 o 5 0 9 25.98 30.71 1.96 o 6 0 9 144.51 153.92 4.77 o 7 0 9 212.57 207.85 5.89 o 8 0 9 0.00 0.41 0.42 o -3 1 9 1.02 0.77 0.65 o -2 1 9 173.39 148.01 4.51 o -1 1 9 68.19 72.00 4.12 o 0 1 9 0.36 0.11 0.45 o 1 1 9 163.79 172.11 4.03 o 2 1 9 56.33 53.00 2.07 o 3 1 9 184.73 177.75 2.75 o 4 1 9 241.54 235.90 3.98 o 5 1 9 12.43 10.62 2.15 o 6 1 9 0.17 0.30 0.55 o 7 1 9 3.17 2.97 1.02 o 8 1 9 81.28 80.41 5.45 o -3 2 9 57.90 58.25 2.51 o -2 2 9 65.81 70.36 2.53 o -1 2 9 0.23 -0.14 0.44 o 0 2 9 128.80 120.30 3.60 o 1 2 9 124.42 121.89 3.34 o 2 2 9 61.99 62.66 3.01 o 3 2 9 125.24 124.80 2.30 o 4 2 9 356.33 370.61 6.06 o 5 2 9 26.61 24.76 1.20 o 6 2 9 22.72 22.11 2.88 o 7 2 9 17.18 15.72 1.76 o 8 2 9 4.09 2.90 0.54 o -2 3 9 26.40 26.95 1.78 o -1 3 9 207.81 207.95 5.48 o 0 3 9 4.88 2.64 1.26 o 1 3 9 13.00 11.54 1.97 o 2 3 9 266.51 268.37 11.23 o 3 3 9 57.55 55.03 1.56 o 4 3 9 5.71 6.19 0.80 o 5 3 9 19.47 19.67 1.19 o 6 3 9 129.39 127.77 6.38 o 7 3 9 53.44 52.76 1.86 o 8 3 9 49.43 51.24 2.03 o -2 4 9 8.91 6.50 2.06 o -1 4 9 9.07 8.02 1.28 o 0 4 9 69.46 68.38 2.85 o 1 4 9 337.64 330.59 6.89 o 2 4 9 12.02 9.81 1.10 o 3 4 9 168.23 184.76 4.59 o 4 4 9 53.39 51.03 3.12 o 5 4 9 121.22 126.94 3.09 o 6 4 9 5.59 5.09 0.61 o 7 4 9 7.59 7.24 0.90 o 8 4 9 0.57 1.47 0.64 o -1 5 9 124.34 135.87 4.63 o 0 5 9 5.49 5.67 1.10 o 1 5 9 121.45 124.85 3.95 o 2 5 9 288.82 298.72 6.44 o 3 5 9 26.08 27.42 1.63 o 4 5 9 68.04 73.85 2.47 o 5 5 9 29.50 32.09 1.75 o 6 5 9 55.34 53.06 3.86 o 7 5 9 102.94 113.38 3.78 o 0 6 9 5.67 6.33 1.22 o 1 6 9 61.56 56.68 2.77 o 2 6 9 22.33 19.59 1.67 o 3 6 9 112.67 121.03 3.74 o 4 6 9 266.39 267.17 7.58 o 5 6 9 1.12 2.12 0.60 o 6 6 9 10.02 10.49 1.17 o 7 6 9 38.20 40.14 1.75 o 2 7 9 30.77 30.90 3.23 o 3 7 9 29.86 29.51 2.04 o 4 7 9 9.27 7.94 1.21 o 5 7 9 50.09 54.47 2.43 o 6 7 9 36.20 37.75 2.92 o -1 -6 10 206.86 221.72 6.16 o 0 -6 10 3.84 3.11 0.98 o 1 -6 10 43.90 35.73 2.13 o 2 -6 10 1.63 2.72 0.88 o 3 -6 10 82.73 71.86 4.12 o -2 -5 10 0.56 0.07 0.79 o -1 -5 10 125.08 135.31 4.46 o 0 -5 10 80.92 73.61 4.25 o 1 -5 10 9.52 7.35 1.48 o 2 -5 10 2.49 1.75 0.69 o 3 -5 10 17.06 19.63 2.13 o 4 -5 10 25.46 29.68 2.44 o -3 -4 10 118.75 98.31 5.72 o -2 -4 10 9.77 9.97 1.52 o -1 -4 10 48.08 49.57 4.12 o 0 -4 10 8.53 8.32 1.19 o 1 -4 10 180.52 174.29 4.67 o 2 -4 10 1.99 2.05 0.78 o 3 -4 10 130.59 129.28 4.92 o 4 -4 10 3.24 1.99 0.93 o 5 -4 10 12.75 13.16 1.55 o -3 -3 10 17.54 16.88 2.24 o -2 -3 10 14.87 16.30 1.72 o -1 -3 10 30.34 31.75 2.03 o 0 -3 10 65.55 62.73 2.58 o 1 -3 10 43.07 39.60 1.90 o 2 -3 10 9.95 9.63 1.06 o 3 -3 10 388.34 409.49 10.28 o 4 -3 10 62.96 63.45 2.11 o 5 -3 10 34.94 38.80 1.84 o 6 -3 10 12.74 12.11 1.09 o -3 -2 10 114.01 123.75 4.51 o -2 -2 10 5.29 6.66 1.24 o -1 -2 10 27.64 28.63 2.00 o 0 -2 10 138.10 137.13 3.92 o 1 -2 10 24.47 23.40 2.30 o 2 -2 10 409.37 416.16 7.28 o 3 -2 10 158.81 168.49 3.90 o 4 -2 10 172.62 174.60 3.18 o 5 -2 10 48.76 51.16 1.92 o 6 -2 10 24.22 23.45 1.21 o 7 -2 10 8.13 6.21 0.77 o -3 -1 10 33.80 34.00 2.49 o -2 -1 10 63.63 60.47 2.88 o -1 -1 10 136.77 142.82 6.53 o 0 -1 10 19.77 17.59 1.46 o 1 -1 10 157.88 156.72 3.93 o 2 -1 10 401.37 412.44 7.14 o 3 -1 10 320.83 330.65 5.94 o 4 -1 10 20.94 18.40 2.28 o 5 -1 10 2.29 1.13 0.40 o 6 -1 10 0.78 0.85 1.00 o 7 -1 10 16.50 14.01 5.05 o -3 0 10 25.38 27.86 2.30 o -2 0 10 0.34 0.27 0.67 o -1 0 10 115.63 119.40 3.87 o 0 0 10 119.39 117.06 7.84 o 1 0 10 375.91 373.25 7.03 o 2 0 10 4.04 3.30 0.64 o 3 0 10 135.07 147.74 3.37 o 4 0 10 166.76 170.15 3.34 o 5 0 10 40.74 37.67 2.30 o 6 0 10 35.31 36.16 3.41 o 7 0 10 137.83 126.43 4.60 o -2 1 10 78.21 75.01 3.27 o -1 1 10 58.42 59.05 2.69 o 0 1 10 179.53 158.94 4.34 o 1 1 10 278.55 271.75 5.72 o 2 1 10 57.93 58.01 2.04 o 3 1 10 90.49 90.49 1.88 o 4 1 10 3.62 3.37 0.52 o 5 1 10 6.59 5.05 0.62 o 6 1 10 109.72 119.13 7.75 o 7 1 10 7.80 9.51 3.48 o 8 1 10 1.54 0.66 1.42 o -2 2 10 106.09 131.94 4.57 o -1 2 10 41.06 36.66 2.22 o 0 2 10 97.50 95.58 4.96 o 1 2 10 37.87 36.14 2.64 o 2 2 10 4.84 4.81 1.13 o 3 2 10 42.84 43.35 1.33 o 4 2 10 25.47 26.87 1.24 o 5 2 10 34.75 37.26 1.77 o 6 2 10 74.18 80.23 5.09 o 7 2 10 52.74 53.16 4.43 o 8 2 10 38.86 34.07 3.99 o -1 3 10 13.58 14.37 2.15 o 0 3 10 3.19 1.83 0.75 o 1 3 10 146.29 148.50 8.00 o 2 3 10 25.75 26.68 1.54 o 3 3 10 48.58 42.79 1.72 o 4 3 10 0.75 1.21 0.49 o 5 3 10 27.97 26.69 1.25 o 6 3 10 168.59 172.78 7.93 o 7 3 10 26.91 32.34 3.72 o 8 3 10 0.06 0.04 0.45 o -1 4 10 77.73 75.56 3.35 o 0 4 10 6.07 7.29 1.24 o 1 4 10 19.28 17.04 2.48 o 2 4 10 1.02 0.85 0.59 o 3 4 10 37.85 41.01 1.82 o 4 4 10 211.91 225.17 4.58 o 5 4 10 39.50 42.09 2.48 o 6 4 10 3.74 3.34 0.71 o 7 4 10 10.43 11.75 1.95 o 0 5 10 47.15 47.28 2.65 o 1 5 10 42.17 38.85 2.59 o 2 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1.80 o -2 -1 11 0.08 -0.54 0.70 o -1 -1 11 29.28 30.97 2.13 o 0 -1 11 34.33 37.32 2.86 o 1 -1 11 150.70 159.51 4.21 o 2 -1 11 2.89 2.80 1.15 o 3 -1 11 293.41 295.79 7.38 o 4 -1 11 17.99 14.02 0.99 o 5 -1 11 1.78 2.07 0.59 o 6 -1 11 75.40 77.65 3.80 o 7 -1 11 26.08 22.59 3.28 o -2 0 11 31.37 29.37 2.30 o -1 0 11 28.28 25.94 2.39 o 0 0 11 1.04 0.82 0.59 o 1 0 11 30.29 25.09 2.33 o 2 0 11 1.77 1.50 0.53 o 3 0 11 80.76 82.76 2.55 o 4 0 11 0.05 0.48 0.39 o 5 0 11 4.22 3.32 0.71 o 6 0 11 89.03 94.33 3.93 o 7 0 11 8.79 9.74 3.32 o -1 1 11 25.79 26.32 2.07 o 0 1 11 73.46 72.05 2.91 o 1 1 11 0.05 0.14 0.53 o 2 1 11 17.79 17.03 1.26 o 3 1 11 22.91 23.84 1.95 o 4 1 11 51.46 56.11 1.88 o 5 1 11 93.24 94.85 3.19 o 6 1 11 3.35 5.98 1.99 o 7 1 11 23.55 16.88 2.92 o -1 2 11 11.80 13.68 2.04 o 0 2 11 26.80 20.40 1.77 o 1 2 11 46.19 48.02 2.27 o 2 2 11 1.33 2.33 0.86 o 3 2 11 173.11 181.19 3.95 o 4 2 11 0.92 0.84 0.47 o 5 2 11 9.15 7.97 1.06 o 6 2 11 151.56 157.19 4.39 o 7 2 11 10.43 8.51 2.17 o 0 3 11 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277.89 279.42 7.40 o 6 -1 12 54.65 57.90 2.53 o 0 0 12 27.54 24.10 2.59 o 1 0 12 146.74 150.53 4.24 o 2 0 12 55.11 54.35 2.21 o 3 0 12 185.97 188.64 6.25 o 4 0 12 146.28 151.10 3.62 o 5 0 12 74.64 75.94 3.10 o 6 0 12 53.41 54.49 2.22 o 0 1 12 8.08 6.51 1.17 o 1 1 12 14.12 11.65 1.35 o 2 1 12 19.79 19.96 1.44 o 3 1 12 308.72 315.84 8.90 o 4 1 12 6.87 9.44 1.33 o 5 1 12 157.81 155.33 4.92 o 6 1 12 48.71 45.10 2.04 o 0 2 12 75.06 80.37 3.34 o 1 2 12 67.87 67.47 2.83 o 2 2 12 229.40 232.56 5.34 o 3 2 12 49.20 51.83 3.15 o 4 2 12 34.59 39.25 2.53 o 6 2 12 3.12 2.30 0.75 o 1 3 12 11.88 10.45 1.42 o 2 3 12 29.89 29.68 1.85 o 3 3 12 69.27 72.88 3.90 o 4 3 12 8.36 9.75 1.55 o 6 3 12 13.35 11.47 1.42 o 2 4 12 8.33 6.88 3.01 o 3 4 12 39.02 38.38 3.37 o 4 4 12 16.50 15.82 1.95 o 5 4 12 51.25 57.99 3.28 o 2 -2 13 9.48 8.68 1.73 o 3 -2 13 34.47 29.02 2.48 o 1 -1 13 5.09 4.30 1.42 o 2 -1 13 86.00 94.90 4.65 o 3 -1 13 17.12 15.90 1.99 o 2 0 13 5.57 3.85 1.33 o 3 0 13 57.51 55.38 3.37 o 4 0 13 0.82 1.64 0.97 o 5 0 13 76.68 72.70 3.37 o 2 1 13 3.68 4.78 0.93 o 3 1 13 0.01 0.97 0.89 o 4 1 13 2.20 0.66 0.80 o 3 2 13 5.06 2.66 1.24 o 4 2 13 12.78 12.14 1.73 o