#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221111.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221111_Fobs loop_ _publ_author_name 'Cl\'ement, S\'ebastien' 'Guyard, Laurent' 'Knorr, Michael' 'D\"aschlein, Christian' 'Strohmann, Carsten' _publ_section_title ; 4,12-Bis(2,2-dibromovinyl)[2.2]paracyclophane ; _journal_coeditor_code IM2094 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o528 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.1545 _cell_length_b 8.3819 _cell_length_c 18.3350 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file im2094Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p in Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 317.68 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24917.69 29160.00 470.49 o 4 0 0 193.00 137.40 44.85 o 6 0 0 1041.38 1393.70 97.49 o 8 0 0 85037.31 86077.63 2370.94 o 10 0 0 856.55 722.99 84.84 o 12 0 0 579.34 614.84 91.62 o 14 0 0 17.91 -48.22 32.15 o 2 1 0 2053.32 2005.26 37.82 o 4 1 0 24467.72 26913.19 316.00 o 6 1 0 7263.94 7173.35 230.09 o 8 1 0 2485.21 2436.21 52.80 o 10 1 0 723.12 710.70 83.15 o 12 1 0 187.58 180.54 44.31 o 14 1 0 623.93 649.20 83.91 o 0 2 0 21917.69 22113.15 361.33 o 2 2 0 69685.80 76063.69 902.82 o 4 2 0 2480.64 2921.93 79.08 o 6 2 0 10735.93 11178.53 154.77 o 8 2 0 18479.99 18789.54 286.52 o 10 2 0 5415.22 5224.32 136.79 o 12 2 0 132.79 112.83 60.98 o 14 2 0 1072.94 985.39 106.20 o 2 3 0 9543.13 9749.22 130.20 o 4 3 0 26416.35 26856.82 361.73 o 6 3 0 2136.96 2020.03 49.75 o 8 3 0 141.99 198.64 23.45 o 10 3 0 2347.10 2383.72 147.34 o 12 3 0 6265.60 6493.82 563.12 o 14 3 0 598.95 627.36 100.01 o 0 4 0 275.31 386.54 35.21 o 2 4 0 58114.99 58762.51 670.46 o 4 4 0 45.28 68.95 13.19 o 6 4 0 37215.87 38136.88 458.30 o 8 4 0 144.15 136.63 33.14 o 10 4 0 17458.63 16865.36 469.15 o 12 4 0 413.60 295.54 75.88 o 14 4 0 1601.61 1680.87 132.71 o 2 5 0 5829.56 5984.98 101.26 o 4 5 0 567.66 637.60 46.03 o 6 5 0 5230.82 4920.88 144.07 o 8 5 0 6.66 15.92 32.64 o 10 5 0 9.75 72.14 74.61 o 12 5 0 3.43 -63.61 98.60 o 0 6 0 17891.81 17782.41 759.72 o 2 6 0 7529.88 7242.82 122.77 o 4 6 0 602.51 675.54 52.35 o 6 6 0 5455.98 5355.28 126.73 o 8 6 0 3616.76 3505.90 105.92 o 10 6 0 888.90 958.34 104.81 o 12 6 0 185.71 208.65 61.57 o 2 7 0 8040.97 7644.66 155.67 o 4 7 0 541.88 553.89 55.54 o 6 7 0 5313.29 5303.70 147.87 o 8 7 0 5.91 2.15 33.87 o 10 7 0 1015.21 1291.14 118.52 o 0 8 0 13426.51 13205.70 697.61 o 2 8 0 31.67 42.33 38.13 o 4 8 0 87.21 72.90 42.94 o 6 8 0 72.66 46.52 40.81 o 8 8 0 4802.50 5083.59 138.81 o 10 8 0 20.28 22.37 66.17 o 2 9 0 102.17 145.73 58.03 o 4 9 0 3332.69 3084.15 109.26 o 6 9 0 1.86 -46.08 30.72 o 8 9 0 578.80 623.26 48.82 o 0 10 0 2026.63 2249.11 173.23 o 2 10 0 100.07 133.65 49.22 o 4 10 0 19.44 122.83 39.68 o 1 1 1 294.33 370.10 8.78 o 2 1 1 9843.11 10813.99 97.41 o 3 1 1 740.54 837.55 16.36 o 4 1 1 100920.96 105421.11 860.76 o 5 1 1 1574.05 1498.11 25.87 o 6 1 1 1315.47 1262.31 25.10 o 7 1 1 5779.32 6042.04 73.66 o 8 1 1 1387.69 1293.21 29.21 o 9 1 1 375.69 416.61 33.45 o 10 1 1 2419.87 2250.22 64.36 o 11 1 1 591.89 545.96 40.72 o 12 1 1 12362.17 12505.57 180.97 o 13 1 1 528.05 566.02 45.36 o 14 1 1 278.07 248.81 43.11 o 15 1 1 263.69 255.86 31.82 o 0 2 1 95926.08 102054.90 1301.63 o 1 2 1 1964.03 2060.77 26.55 o 2 2 1 17125.29 17935.43 159.74 o 3 2 1 4374.93 4989.22 56.47 o 4 2 1 23.39 28.01 8.26 o 5 2 1 426.14 517.39 18.53 o 6 2 1 4748.97 4635.81 56.66 o 7 2 1 110.05 100.29 16.31 o 8 2 1 19015.54 19021.11 187.33 o 9 2 1 245.55 245.46 22.75 o 10 2 1 5303.11 5164.19 95.78 o 11 2 1 94.53 95.40 27.82 o 12 2 1 941.57 932.38 70.94 o 13 2 1 42.71 33.58 38.21 o 14 2 1 106.13 194.06 53.53 o 15 2 1 5.40 72.80 33.22 o 1 3 1 364.68 433.51 14.93 o 2 3 1 37528.02 39160.34 318.86 o 3 3 1 2154.35 2005.12 33.85 o 4 3 1 2456.98 2328.11 38.35 o 5 3 1 4888.09 4841.05 61.40 o 6 3 1 32150.45 32604.10 278.65 o 7 3 1 523.32 538.72 21.52 o 8 3 1 558.30 553.70 21.00 o 9 3 1 1064.48 1086.40 55.23 o 10 3 1 2941.76 2799.96 109.12 o 11 3 1 1195.70 1161.85 88.30 o 12 3 1 1494.87 1630.89 102.73 o 13 3 1 959.15 843.72 81.78 o 14 3 1 6523.66 5890.24 177.27 o 0 4 1 446.20 324.86 23.57 o 1 4 1 158.13 187.85 14.19 o 2 4 1 1766.21 1976.09 33.42 o 3 4 1 2122.05 2244.20 40.94 o 4 4 1 178.88 183.15 16.82 o 5 4 1 1448.83 1561.82 35.08 o 6 4 1 526.06 567.37 23.19 o 7 4 1 351.58 393.94 28.76 o 8 4 1 607.72 767.02 41.23 o 9 4 1 141.78 170.84 39.09 o 10 4 1 1174.02 1046.12 73.49 o 11 4 1 129.90 159.03 49.85 o 12 4 1 8.22 18.47 42.40 o 13 4 1 3.52 18.96 40.84 o 14 4 1 0.34 35.21 49.09 o 1 5 1 240.51 289.30 19.25 o 2 5 1 21453.20 21977.48 197.54 o 3 5 1 464.03 478.32 19.51 o 4 5 1 2296.90 2192.39 43.74 o 5 5 1 33.72 45.23 20.83 o 6 5 1 12647.07 12452.16 149.47 o 7 5 1 2588.77 2428.57 57.59 o 8 5 1 72.68 32.82 22.37 o 9 5 1 96.85 118.98 27.53 o 10 5 1 3622.60 3700.51 115.97 o 11 5 1 339.74 369.08 57.04 o 12 5 1 491.02 410.76 57.47 o 13 5 1 226.47 238.78 45.76 o 0 6 1 3921.65 3910.91 82.42 o 1 6 1 446.61 469.10 25.09 o 2 6 1 16772.78 17011.38 164.65 o 3 6 1 369.61 451.12 28.57 o 4 6 1 286.28 244.30 28.46 o 5 6 1 1248.84 1337.11 49.41 o 6 6 1 5245.85 5411.49 90.29 o 7 6 1 1693.27 1656.54 54.45 o 8 6 1 1146.88 1269.45 50.92 o 9 6 1 132.89 156.73 38.94 o 10 6 1 5201.26 5059.01 138.23 o 11 6 1 2.89 48.60 39.38 o 12 6 1 109.08 100.95 36.83 o 1 7 1 591.52 597.97 33.02 o 2 7 1 180.71 239.40 29.98 o 3 7 1 234.84 248.42 30.91 o 4 7 1 14306.14 14177.15 191.80 o 5 7 1 1796.74 1819.97 58.33 o 6 7 1 2.02 -37.77 25.43 o 7 7 1 95.24 109.42 29.31 o 8 7 1 482.64 458.63 47.08 o 9 7 1 82.43 42.10 32.61 o 10 7 1 680.15 656.10 62.34 o 11 7 1 153.85 129.91 35.58 o 0 8 1 3438.82 3228.87 126.76 o 1 8 1 104.81 108.86 25.94 o 2 8 1 380.38 330.76 35.28 o 3 8 1 359.12 351.88 36.46 o 4 8 1 89.85 80.33 29.16 o 5 8 1 574.64 665.50 44.63 o 6 8 1 748.47 775.75 47.34 o 7 8 1 41.51 21.11 26.54 o 8 8 1 705.16 630.55 41.73 o 9 8 1 319.04 428.06 33.12 o 10 8 1 196.30 260.11 34.15 o 1 9 1 3.21 -3.76 35.32 o 2 9 1 64.12 47.75 35.94 o 3 9 1 578.72 572.23 40.90 o 4 9 1 3441.98 3635.20 83.44 o 5 9 1 21.58 8.58 27.44 o 6 9 1 11.61 16.75 25.34 o 7 9 1 387.00 453.98 35.87 o 8 9 1 4.97 87.89 17.61 o 0 10 1 4558.63 4657.83 187.43 o 1 10 1 119.47 114.42 33.50 o 2 10 1 94.52 160.24 34.76 o 3 10 1 80.17 117.19 29.26 o 4 10 1 32.11 100.97 25.42 o 5 10 1 62.60 69.98 32.26 o 0 0 2 35692.43 37695.93 945.93 o 1 0 2 6476.08 6487.02 286.53 o 2 0 2 623.96 563.39 22.02 o 3 0 2 16836.23 17264.29 261.73 o 4 0 2 4230.59 4391.43 80.64 o 5 0 2 8219.69 8284.68 184.02 o 6 0 2 614.26 664.85 35.97 o 7 0 2 520.62 484.44 47.20 o 8 0 2 59920.35 60824.91 791.44 o 9 0 2 7936.69 7664.35 167.12 o 10 0 2 55.27 61.79 37.23 o 11 0 2 3480.96 3441.77 114.16 o 12 0 2 2377.04 2280.00 99.19 o 13 0 2 1383.48 1380.84 90.24 o 14 0 2 458.97 429.61 67.10 o 15 0 2 318.65 280.55 35.85 o 1 1 2 7236.43 7789.86 75.56 o 2 1 2 6674.77 6667.10 62.11 o 3 1 2 6465.03 6773.29 67.52 o 4 1 2 16514.95 16777.24 153.78 o 5 1 2 214.70 184.49 10.31 o 6 1 2 6285.30 6260.90 104.80 o 7 1 2 4275.13 4156.13 63.47 o 8 1 2 496.12 539.56 27.49 o 9 1 2 832.79 946.17 35.71 o 10 1 2 1548.45 1461.39 54.36 o 11 1 2 6.62 14.90 25.97 o 12 1 2 4466.93 4275.25 92.63 o 13 1 2 160.57 171.78 38.32 o 14 1 2 1231.25 1155.73 74.04 o 15 1 2 625.82 662.62 50.94 o 0 2 2 50941.95 54043.31 603.34 o 1 2 2 13503.92 14282.00 122.51 o 2 2 2 2561.89 2390.51 33.45 o 3 2 2 8279.41 8611.65 90.59 o 4 2 2 2588.49 2926.98 37.84 o 5 2 2 1432.08 1423.90 28.91 o 6 2 2 5545.73 5470.68 65.64 o 7 2 2 9288.40 9198.43 115.31 o 8 2 2 9992.79 10048.04 113.56 o 9 2 2 3197.22 3301.39 64.85 o 10 2 2 6436.07 6229.99 107.43 o 11 2 2 981.50 958.87 55.71 o 12 2 2 8.35 9.67 37.59 o 13 2 2 366.37 341.02 51.75 o 14 2 2 501.29 500.90 55.75 o 15 2 2 685.57 690.44 58.35 o 1 3 2 7095.53 7203.59 71.88 o 2 3 2 812.18 709.74 21.36 o 3 3 2 79.17 114.25 13.09 o 4 3 2 20489.55 21094.83 195.31 o 5 3 2 21.54 17.81 12.27 o 6 3 2 3036.40 3062.18 48.63 o 7 3 2 4601.09 4592.27 61.52 o 8 3 2 1227.73 1269.20 58.10 o 9 3 2 2433.05 2385.94 57.58 o 10 3 2 91.12 52.47 40.48 o 11 3 2 123.32 104.43 46.45 o 12 3 2 1286.16 1478.20 91.37 o 13 3 2 3.34 -1.52 46.39 o 14 3 2 67.45 39.79 38.50 o 0 4 2 6408.66 6827.98 103.92 o 1 4 2 8897.15 8540.74 87.23 o 2 4 2 48530.90 50174.97 409.00 o 3 4 2 31.52 50.81 14.37 o 4 4 2 1206.86 1220.37 32.46 o 5 4 2 728.84 784.08 27.92 o 6 4 2 9746.73 9353.73 116.73 o 7 4 2 8448.38 8354.05 109.65 o 8 4 2 31.95 45.04 19.12 o 9 4 2 3863.82 3819.94 86.44 o 10 4 2 15330.72 15214.75 377.36 o 11 4 2 0.24 17.18 42.24 o 12 4 2 136.97 146.31 49.57 o 13 4 2 6.65 -30.92 32.28 o 14 4 2 1280.93 1388.02 86.13 o 1 5 2 254.75 249.69 18.59 o 2 5 2 7007.94 7012.37 80.45 o 3 5 2 1950.07 1929.36 41.96 o 4 5 2 898.73 896.17 31.40 o 5 5 2 880.09 910.70 33.88 o 6 5 2 12854.12 12481.77 149.89 o 7 5 2 158.20 172.97 27.00 o 8 5 2 1711.15 1579.86 49.26 o 9 5 2 545.11 547.51 43.65 o 10 5 2 607.43 679.83 64.64 o 11 5 2 583.92 547.92 61.81 o 12 5 2 0.99 21.80 46.60 o 13 5 2 139.76 174.29 38.69 o 0 6 2 4567.55 4486.46 90.05 o 1 6 2 3321.23 3195.99 52.54 o 2 6 2 1123.18 1022.69 30.49 o 3 6 2 29.84 35.55 17.94 o 4 6 2 1528.85 1504.23 47.31 o 5 6 2 17.09 15.43 23.13 o 6 6 2 2462.01 2401.55 60.40 o 7 6 2 803.69 887.44 44.04 o 8 6 2 2960.81 2860.28 67.71 o 9 6 2 3189.31 3092.23 82.29 o 10 6 2 960.17 1041.49 76.03 o 11 6 2 44.57 92.72 39.77 o 12 6 2 169.60 179.52 39.72 o 1 7 2 923.75 997.68 39.49 o 2 7 2 2867.38 2887.94 64.65 o 3 7 2 334.10 419.93 35.04 o 4 7 2 32.97 23.00 26.99 o 5 7 2 1054.10 1021.76 47.98 o 6 7 2 2760.74 2686.51 67.62 o 7 7 2 9.78 70.65 30.71 o 8 7 2 44.14 130.42 25.25 o 9 7 2 631.90 696.51 47.71 o 10 7 2 1074.07 1133.70 78.39 o 11 7 2 367.87 377.19 49.96 o 0 8 2 12115.96 12029.45 243.85 o 1 8 2 956.93 1051.34 52.52 o 2 8 2 399.39 424.11 37.53 o 3 8 2 608.53 657.01 42.89 o 4 8 2 88.71 95.91 29.71 o 5 8 2 598.92 697.29 45.12 o 6 8 2 79.52 125.19 31.63 o 7 8 2 564.12 690.04 45.82 o 8 8 2 6805.67 7022.19 126.80 o 9 8 2 328.43 360.48 32.20 o 10 8 2 242.84 279.50 42.85 o 1 9 2 60.41 63.48 36.17 o 2 9 2 240.19 265.16 33.82 o 3 9 2 131.12 162.88 35.36 o 4 9 2 2972.76 2715.56 74.58 o 5 9 2 377.39 416.10 39.07 o 6 9 2 11.91 56.82 24.63 o 7 9 2 222.95 254.14 29.20 o 8 9 2 243.04 316.26 34.37 o 0 10 2 103.57 250.59 57.95 o 1 10 2 58.07 124.32 34.95 o 2 10 2 609.60 636.06 51.49 o 3 10 2 318.41 452.11 44.28 o 4 10 2 70.02 92.55 28.35 o 5 10 2 53.20 187.53 35.79 o 1 1 3 47457.24 49802.76 407.15 o 2 1 3 1547.41 1533.41 23.72 o 3 1 3 26676.09 28719.84 236.97 o 4 1 3 62282.19 65914.13 547.40 o 5 1 3 15742.95 15948.79 151.79 o 6 1 3 59.52 64.65 9.67 o 7 1 3 8729.83 8556.22 110.68 o 8 1 3 1606.16 1757.30 44.59 o 9 1 3 5830.83 5786.69 98.42 o 10 1 3 160.95 147.39 29.12 o 11 1 3 2438.18 2366.02 70.42 o 12 1 3 10551.55 10369.72 159.16 o 13 1 3 2397.44 2353.06 82.51 o 14 1 3 0.01 19.82 29.33 o 15 1 3 1145.06 1297.36 95.70 o 0 2 3 36572.33 38481.40 436.64 o 1 2 3 602.52 570.60 14.57 o 2 2 3 27894.76 28869.73 237.72 o 3 2 3 8304.82 8257.19 83.23 o 4 2 3 6841.82 7842.82 79.25 o 5 2 3 3710.95 3598.41 46.67 o 6 2 3 4644.74 4440.47 60.71 o 7 2 3 711.46 686.68 22.23 o 8 2 3 15763.58 16186.27 172.09 o 9 2 3 447.24 475.64 30.63 o 10 2 3 4065.50 3891.73 81.86 o 11 2 3 504.08 543.30 47.22 o 12 2 3 1073.14 959.44 71.13 o 13 2 3 322.15 274.23 50.98 o 14 2 3 94.41 144.79 40.89 o 15 2 3 224.65 240.68 36.48 o 1 3 3 1023.03 1123.14 22.83 o 2 3 3 19660.14 20241.72 175.09 o 3 3 3 42036.04 43679.47 375.64 o 4 3 3 176.12 211.35 16.70 o 5 3 3 19842.95 19938.46 189.89 o 6 3 3 24501.95 25462.56 232.13 o 7 3 3 4.97 1.95 15.07 o 8 3 3 1030.91 1042.32 49.27 o 9 3 3 6.73 21.45 19.80 o 10 3 3 4537.90 4398.45 118.40 o 11 3 3 5448.95 5378.26 161.50 o 12 3 3 119.88 131.19 44.40 o 13 3 3 1982.80 1926.72 97.87 o 14 3 3 1065.79 1010.25 79.90 o 0 4 3 4242.12 4257.60 75.63 o 1 4 3 1258.44 1360.69 28.39 o 2 4 3 1925.50 2112.04 35.17 o 3 4 3 54.01 64.92 15.72 o 4 4 3 1456.05 1534.88 35.87 o 5 4 3 37.49 47.32 15.88 o 6 4 3 84.28 104.87 18.62 o 7 4 3 716.82 696.48 34.53 o 8 4 3 1391.44 1456.06 49.93 o 9 4 3 24.24 41.69 26.94 o 10 4 3 277.87 214.29 49.20 o 11 4 3 848.89 857.19 71.90 o 12 4 3 150.51 121.63 46.05 o 13 4 3 4.61 -11.25 49.06 o 14 4 3 31.50 65.17 31.86 o 1 5 3 101.68 136.64 16.46 o 2 5 3 7073.49 6580.34 83.63 o 3 5 3 11804.84 11677.80 127.81 o 4 5 3 630.37 681.99 30.13 o 5 5 3 12543.49 12196.90 134.95 o 6 5 3 12143.23 11873.94 144.57 o 7 5 3 213.05 242.28 28.31 o 8 5 3 10.67 -0.66 17.20 o 9 5 3 155.00 216.23 35.86 o 10 5 3 3192.49 3113.46 109.38 o 11 5 3 3244.41 3132.98 113.18 o 12 5 3 0.19 -9.82 32.77 o 13 5 3 1657.20 1627.60 92.15 o 0 6 3 3516.61 3340.95 76.37 o 1 6 3 2018.92 1948.81 41.59 o 2 6 3 6138.94 5789.47 82.09 o 3 6 3 263.30 263.49 25.58 o 4 6 3 58.11 95.20 25.19 o 5 6 3 640.05 668.59 38.66 o 6 6 3 2716.74 2866.25 64.76 o 7 6 3 550.17 542.11 38.01 o 8 6 3 1480.54 1490.94 51.55 o 9 6 3 769.21 863.19 53.20 o 10 6 3 5032.36 4892.35 117.13 o 11 6 3 7.78 -53.60 35.73 o 12 6 3 71.83 55.52 35.61 o 1 7 3 3177.32 3262.27 62.96 o 2 7 3 35.83 51.61 19.73 o 3 7 3 3362.12 3215.28 69.34 o 4 7 3 5825.36 5492.36 114.32 o 5 7 3 949.88 1031.74 47.85 o 6 7 3 229.90 196.24 32.21 o 7 7 3 1947.01 1855.87 61.42 o 8 7 3 699.85 687.10 46.92 o 9 7 3 1434.93 1486.60 64.39 o 10 7 3 289.16 217.90 45.85 o 11 7 3 183.68 233.06 41.10 o 0 8 3 20.03 3.06 33.47 o 1 8 3 612.44 594.79 43.82 o 2 8 3 639.22 660.73 42.16 o 3 8 3 56.38 49.86 28.08 o 4 8 3 306.24 311.33 35.70 o 5 8 3 64.43 43.61 29.88 o 6 8 3 264.86 259.34 35.23 o 7 8 3 402.28 446.39 39.10 o 8 8 3 443.96 407.44 38.48 o 9 8 3 263.27 293.92 37.67 o 10 8 3 95.26 132.38 61.22 o 1 9 3 1995.65 2152.38 80.05 o 2 9 3 55.88 117.53 30.53 o 3 9 3 183.61 254.36 37.59 o 4 9 3 2241.24 2493.12 69.79 o 5 9 3 775.78 737.02 46.30 o 6 9 3 1.25 3.41 22.72 o 7 9 3 429.97 577.44 37.98 o 8 9 3 17.12 72.73 34.77 o 0 10 3 2077.50 2011.34 111.60 o 1 10 3 117.03 113.50 40.83 o 2 10 3 47.85 91.30 29.97 o 3 10 3 509.62 552.86 45.63 o 4 10 3 91.91 110.84 23.42 o 5 10 3 329.41 484.77 38.50 o 0 0 4 53076.08 55105.22 1307.71 o 1 0 4 38789.52 42123.97 576.22 o 2 0 4 2410.57 2528.03 72.61 o 3 0 4 29200.13 27523.41 571.83 o 4 0 4 2823.87 3018.77 77.19 o 5 0 4 23292.83 23857.67 328.14 o 6 0 4 1014.66 1397.48 53.14 o 7 0 4 9711.08 10092.64 171.66 o 8 0 4 9494.37 9761.79 171.48 o 9 0 4 8909.73 8699.91 161.03 o 10 0 4 1038.00 898.88 67.20 o 11 0 4 3995.31 3663.03 118.00 o 12 0 4 1539.69 1449.09 86.73 o 13 0 4 1450.14 1547.58 83.57 o 14 0 4 1123.09 1037.67 100.10 o 15 0 4 117.12 138.47 36.84 o 1 1 4 22532.70 23433.60 200.50 o 2 1 4 16985.26 18477.88 158.27 o 3 1 4 120.29 138.33 12.52 o 4 1 4 17054.67 18000.81 165.77 o 5 1 4 945.38 1021.22 23.01 o 6 1 4 7208.09 7503.21 108.65 o 7 1 4 4359.34 4262.02 71.46 o 8 1 4 1806.99 1853.73 47.31 o 9 1 4 4446.89 4237.51 73.05 o 10 1 4 135.51 90.60 27.83 o 11 1 4 1307.86 1228.66 54.87 o 12 1 4 894.83 875.07 57.48 o 13 1 4 232.70 224.80 37.74 o 14 1 4 181.99 261.80 33.49 o 15 1 4 54.42 15.27 53.99 o 0 2 4 8496.78 8217.18 109.99 o 1 2 4 36122.64 37369.66 317.19 o 2 2 4 8854.30 9531.97 90.41 o 3 2 4 2781.69 2616.64 39.38 o 4 2 4 1813.02 2110.40 34.02 o 5 2 4 4438.63 4602.01 56.55 o 6 2 4 1388.84 1375.84 29.49 o 7 2 4 9827.65 9514.43 112.42 o 8 2 4 2734.28 2874.40 59.39 o 9 2 4 8901.29 8774.69 165.05 o 10 2 4 324.24 379.15 44.11 o 11 2 4 2555.10 2495.32 87.48 o 12 2 4 345.99 371.46 41.48 o 13 2 4 19.50 27.71 38.28 o 14 2 4 20.94 25.47 46.55 o 15 2 4 1675.52 1704.60 89.00 o 1 3 4 12330.87 12342.11 114.15 o 2 3 4 832.27 720.44 20.17 o 3 3 4 1.47 1.54 11.52 o 4 3 4 4156.44 3831.19 54.63 o 5 3 4 84.07 98.49 15.91 o 6 3 4 627.35 610.17 21.21 o 7 3 4 2739.72 2534.04 51.55 o 8 3 4 168.57 189.19 20.64 o 9 3 4 1136.90 1224.58 48.61 o 10 3 4 267.45 269.09 35.06 o 11 3 4 8.78 -18.59 38.41 o 12 3 4 1275.95 1353.53 82.37 o 13 3 4 24.40 17.50 36.74 o 14 3 4 312.77 288.18 58.95 o 0 4 4 451.08 392.00 31.43 o 1 4 4 32457.95 33350.53 280.54 o 2 4 4 10122.78 9962.04 100.55 o 3 4 4 885.24 947.92 30.19 o 4 4 4 112.04 134.79 17.97 o 5 4 4 215.47 229.43 20.76 o 6 4 4 5884.28 5885.86 80.07 o 7 4 4 13271.23 12550.29 139.69 o 8 4 4 519.02 582.43 31.72 o 9 4 4 4548.40 4490.25 97.40 o 10 4 4 3641.13 3573.45 95.52 o 11 4 4 339.32 294.18 55.11 o 12 4 4 901.66 820.34 73.07 o 13 4 4 502.61 612.44 65.43 o 14 4 4 129.19 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1 9 11 84.54 95.34 40.03 o 2 9 11 2.21 37.08 31.48 o 3 9 11 576.39 623.22 54.02 o 4 9 11 2306.22 2452.82 93.25 o 0 0 12 25033.34 24512.81 458.05 o 1 0 12 17633.16 17910.53 250.69 o 2 0 12 1077.33 1170.95 47.78 o 3 0 12 4680.96 5008.14 103.55 o 4 0 12 69.78 110.97 40.77 o 5 0 12 6143.64 6125.52 122.95 o 6 0 12 478.33 576.01 47.53 o 7 0 12 17042.36 16886.81 283.07 o 8 0 12 8318.98 8520.26 181.40 o 9 0 12 389.72 363.74 59.20 o 10 0 12 1088.30 981.49 74.59 o 11 0 12 0.31 18.59 49.72 o 12 0 12 582.63 897.08 99.00 o 13 0 12 498.26 609.55 103.57 o 1 1 12 5954.97 6125.30 90.04 o 2 1 12 3638.86 3605.55 65.94 o 3 1 12 3640.14 3624.81 71.01 o 4 1 12 4755.61 4587.54 74.74 o 5 1 12 753.59 784.04 40.70 o 6 1 12 374.41 391.51 28.77 o 7 1 12 39.69 50.52 26.44 o 8 1 12 3.00 7.23 31.21 o 9 1 12 1140.62 1159.66 57.45 o 10 1 12 577.78 563.92 50.39 o 11 1 12 763.50 771.43 57.87 o 12 1 12 1115.21 1218.97 75.47 o 13 1 12 127.60 104.40 36.36 o 0 2 12 14451.63 13523.11 230.01 o 1 2 12 5565.85 5312.52 87.52 o 2 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