#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/11/2221115.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221115_Fobs loop_ _publ_author_name 'Yu, Zhong' 'Kuroda-Sowa, Takayoshi' 'Nabei, Atsuhiro' 'Maekawa, Masahiko' 'Okubo, Takashi' _publ_section_title ; {6,6'-Dimethoxy-2,2'-[naphthalene-2,3-diylbis(nitrilomethylidyne)]diphenolato}thiocyanatocobalt(III) diethyl ether dichloromethane solvate ; _journal_coeditor_code IS2372 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m257 _journal_page_last m258 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.462 _cell_angle_gamma 90.000 _cell_length_a 9.1935 _cell_length_b 13.3640 _cell_length_c 25.9096 _exptl_crystal_F_000 1448.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file is2372Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _CoLSCN_C4H10O_CH2Cl2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 228.38 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6241.10 6544.00 48.46 o 4 0 0 6893.58 6904.44 72.31 o 6 0 0 393.99 314.67 46.12 o 8 0 0 1619.61 1470.89 100.12 o 10 0 0 2052.74 1898.53 93.86 o 2 1 0 1515.09 1896.00 22.16 o 3 1 0 1773.50 1839.81 27.52 o 4 1 0 4397.25 4247.71 52.41 o 5 1 0 1141.53 977.82 34.70 o 6 1 0 1098.32 1099.06 43.79 o 7 1 0 242.19 256.82 35.27 o 8 1 0 4909.57 4952.17 174.71 o 9 1 0 423.05 423.10 38.66 o 10 1 0 1830.44 1900.29 67.45 o 11 1 0 834.08 890.53 115.07 o 0 2 0 919.92 1457.58 25.53 o 1 2 0 18804.80 20102.34 99.28 o 2 2 0 7647.95 8695.37 39.64 o 3 2 0 921.36 735.73 21.52 o 4 2 0 1.05 54.29 27.83 o 5 2 0 12680.39 13142.15 103.29 o 6 2 0 2361.27 2511.36 55.74 o 7 2 0 5777.04 5831.03 94.89 o 8 2 0 111.82 106.80 30.01 o 9 2 0 259.72 349.55 42.58 o 10 2 0 60.28 193.04 78.34 o 11 2 0 351.66 300.14 78.19 o 1 3 0 2307.09 2704.80 35.43 o 2 3 0 56.66 78.86 23.19 o 3 3 0 6568.58 6495.98 47.71 o 4 3 0 1083.72 1110.42 25.62 o 5 3 0 2880.12 2736.25 47.97 o 6 3 0 13.33 49.44 13.79 o 7 3 0 701.67 675.92 40.90 o 8 3 0 210.39 201.36 30.64 o 9 3 0 557.29 618.75 42.54 o 10 3 0 1566.44 1688.81 76.22 o 11 3 0 16.83 23.20 64.73 o 0 4 0 8662.99 8155.61 63.36 o 1 4 0 194.32 158.51 12.96 o 2 4 0 493.45 524.60 26.85 o 3 4 0 676.08 906.58 47.46 o 4 4 0 11725.02 11982.11 59.04 o 5 4 0 894.57 847.76 44.41 o 6 4 0 280.01 295.82 36.37 o 7 4 0 38.47 43.00 26.48 o 8 4 0 3208.12 3187.71 68.10 o 9 4 0 407.96 430.04 50.04 o 10 4 0 1.43 69.62 38.00 o 11 4 0 172.04 66.60 74.66 o 1 5 0 1446.46 1429.28 30.16 o 2 5 0 11336.65 11948.13 216.07 o 3 5 0 8505.58 8962.06 105.47 o 4 5 0 159.36 234.10 42.79 o 5 5 0 1031.97 1118.43 59.37 o 6 5 0 72.13 98.43 25.10 o 7 5 0 47.40 84.00 26.44 o 8 5 0 1585.94 1444.05 94.84 o 9 5 0 915.65 1025.09 72.43 o 10 5 0 1131.60 1241.47 73.34 o 11 5 0 830.39 1287.12 183.95 o 0 6 0 133.46 204.12 29.72 o 1 6 0 5748.71 6304.36 67.42 o 2 6 0 118.70 154.14 15.77 o 3 6 0 337.71 474.94 57.65 o 4 6 0 5818.27 5684.83 100.31 o 5 6 0 733.12 727.01 55.97 o 6 6 0 418.34 440.93 51.35 o 7 6 0 1598.28 1788.84 78.35 o 8 6 0 276.01 229.39 50.10 o 9 6 0 1171.49 1071.61 68.12 o 10 6 0 1.64 144.72 50.12 o 11 6 0 6.37 42.93 103.20 o 1 7 0 6441.96 5896.42 68.73 o 2 7 0 571.74 691.73 23.75 o 3 7 0 3335.47 3405.49 84.79 o 4 7 0 71.14 45.37 34.94 o 5 7 0 6983.83 6844.19 119.97 o 6 7 0 2025.74 1869.37 87.65 o 7 7 0 52.41 80.79 49.25 o 8 7 0 2.59 71.83 43.53 o 9 7 0 890.46 896.06 71.92 o 10 7 0 603.19 668.84 66.29 o 0 8 0 9133.91 9180.18 137.81 o 1 8 0 2201.04 2386.40 48.55 o 2 8 0 2678.20 2708.32 42.04 o 3 8 0 219.27 270.75 47.09 o 4 8 0 2160.61 2123.38 174.01 o 5 8 0 2333.54 2320.85 85.53 o 6 8 0 828.95 819.14 81.50 o 7 8 0 486.61 464.99 99.28 o 8 8 0 350.55 376.06 52.35 o 9 8 0 27.87 77.76 64.63 o 10 8 0 22.61 80.78 39.20 o 1 9 0 14.65 70.49 39.39 o 2 9 0 1234.27 1214.27 58.65 o 3 9 0 313.96 303.19 39.46 o 4 9 0 633.45 668.19 63.34 o 5 9 0 13.58 77.01 67.91 o 6 9 0 3767.46 3767.99 118.05 o 7 9 0 969.09 976.94 77.12 o 8 9 0 303.49 249.82 48.59 o 9 9 0 14.26 185.85 58.49 o 10 9 0 1538.28 1323.83 110.86 o 0 10 0 126.29 185.47 43.85 o 1 10 0 45.20 62.97 26.91 o 2 10 0 1364.43 1361.07 58.32 o 3 10 0 80.93 69.84 16.17 o 4 10 0 2956.00 3124.69 168.94 o 5 10 0 44.14 121.10 44.68 o 6 10 0 49.00 142.67 73.47 o 7 10 0 413.51 545.84 70.20 o 8 10 0 335.13 435.02 77.18 o 9 10 0 54.18 164.65 57.78 o 1 11 0 904.82 924.80 51.56 o 2 11 0 554.78 494.41 38.89 o 3 11 0 1024.99 893.61 47.15 o 4 11 0 885.43 970.42 99.83 o 5 11 0 461.00 508.90 65.57 o 6 11 0 27.60 80.18 74.58 o 7 11 0 773.61 861.30 88.99 o 8 11 0 315.40 207.44 62.22 o 9 11 0 156.61 248.48 53.92 o 0 12 0 154.15 190.91 53.49 o 1 12 0 17.48 94.36 41.66 o 2 12 0 413.57 480.52 43.42 o 3 12 0 4676.87 4482.82 125.45 o 4 12 0 43.87 198.76 66.81 o 5 12 0 1210.08 1155.07 86.05 o 6 12 0 574.73 606.49 74.77 o 7 12 0 243.94 271.73 61.75 o 8 12 0 191.21 217.71 57.12 o 1 13 0 2.40 72.17 31.40 o 2 13 0 758.95 761.50 71.50 o 3 13 0 521.72 629.01 98.48 o 4 13 0 1.28 180.90 71.91 o 5 13 0 29.22 89.23 54.84 o 6 13 0 552.66 621.57 78.60 o 7 13 0 599.43 631.79 71.89 o 0 14 0 4056.03 3749.07 122.71 o 1 14 0 53.71 79.10 35.40 o 2 14 0 266.26 271.12 57.40 o 3 14 0 496.00 505.93 68.44 o 4 14 0 3685.15 3999.53 164.23 o 5 14 0 2.73 107.39 62.64 o 6 14 0 0.33 86.12 56.74 o 7 14 0 311.51 345.36 88.51 o 1 15 0 233.75 377.61 55.52 o 2 15 0 2187.41 1965.36 100.33 o 3 15 0 1.81 151.21 62.29 o 4 15 0 1070.14 1239.54 91.68 o 5 15 0 861.62 900.93 126.92 o 6 15 0 277.01 235.89 86.77 o 0 16 0 14.17 10.16 143.76 o 1 16 0 32.36 166.56 55.54 o 2 16 0 289.91 267.70 54.70 o 3 16 0 324.32 329.76 56.60 o 4 16 0 0.61 153.76 62.66 o 1 17 0 1252.18 1343.53 133.46 o 2 17 0 18.85 167.53 125.62 o -9 0 1 3384.61 3266.61 109.17 o -7 0 1 836.58 869.34 69.47 o -5 0 1 4393.81 4474.66 129.71 o -3 0 1 17943.74 17916.97 117.15 o 3 0 1 933.17 1043.43 31.31 o 5 0 1 4955.00 5302.54 120.81 o 7 0 1 10393.52 10636.84 220.44 o 9 0 1 3737.28 3790.65 107.79 o -11 1 1 65.34 269.53 85.69 o -10 1 1 1618.47 1649.11 64.71 o -9 1 1 99.10 102.75 30.24 o -8 1 1 10.47 96.72 47.05 o -7 1 1 753.80 777.24 88.03 o -6 1 1 716.95 759.27 40.96 o -5 1 1 1223.47 1118.84 32.74 o -4 1 1 377.04 295.23 21.20 o -3 1 1 969.87 893.19 19.76 o -2 1 1 12.06 52.92 20.08 o 2 1 1 3667.36 4024.89 35.87 o 3 1 1 5903.92 5597.29 37.65 o 4 1 1 50.22 49.97 18.22 o 5 1 1 947.72 881.62 28.94 o 6 1 1 326.24 311.46 31.01 o 7 1 1 3715.49 3782.64 125.24 o 8 1 1 2189.84 2244.41 60.77 o 9 1 1 393.02 290.50 32.11 o 10 1 1 428.80 447.72 40.96 o 11 1 1 29.60 206.34 73.11 o -11 2 1 0.49 34.61 85.28 o -10 2 1 1677.76 1647.64 76.16 o -9 2 1 29.94 85.30 26.08 o -8 2 1 5.80 75.34 29.14 o -7 2 1 394.17 379.56 37.87 o -6 2 1 4142.10 4028.26 65.44 o -5 2 1 3649.10 3736.27 51.95 o -4 2 1 10747.19 10765.13 75.08 o -3 2 1 2792.51 2288.22 27.46 o -1 2 1 2714.71 2882.53 25.62 o 0 2 1 3471.36 3382.61 31.31 o 1 2 1 3934.63 4736.64 33.84 o 2 2 1 24325.67 24540.30 83.30 o 3 2 1 31.54 65.18 10.19 o 4 2 1 5017.27 4492.78 39.89 o 5 2 1 268.70 189.54 19.59 o 6 2 1 5970.01 6173.87 84.84 o 7 2 1 115.53 123.00 23.81 o 8 2 1 37.47 102.17 34.78 o 9 2 1 43.81 119.57 53.56 o 10 2 1 691.94 543.00 51.46 o 11 2 1 597.60 558.92 125.86 o -11 3 1 0.10 178.35 98.07 o -10 3 1 1318.68 1298.38 106.29 o -9 3 1 236.14 274.81 33.32 o -8 3 1 29.54 66.00 26.04 o -7 3 1 8.98 153.50 42.09 o -6 3 1 5106.68 5281.13 69.54 o -5 3 1 6480.43 6721.50 97.83 o -4 3 1 630.86 784.76 24.98 o -3 3 1 12.64 51.87 11.06 o -2 3 1 297.80 473.54 35.38 o -1 3 1 17539.48 16646.75 73.53 o 0 3 1 1737.22 1653.25 23.98 o 1 3 1 294.36 280.40 12.78 o 2 3 1 1939.74 1744.67 31.39 o 3 3 1 667.44 812.60 17.07 o 4 3 1 10686.87 10694.00 62.16 o 5 3 1 588.86 457.00 32.12 o 6 3 1 1283.19 1336.81 43.70 o 7 3 1 2259.35 2309.78 57.06 o 8 3 1 2866.86 2754.71 93.79 o 9 3 1 8.87 70.58 38.62 o 10 3 1 664.94 670.69 57.58 o 11 3 1 62.80 102.93 63.20 o -11 4 1 992.90 689.38 109.17 o -10 4 1 0.12 124.85 51.22 o -9 4 1 19.84 151.88 63.28 o -8 4 1 2497.43 2453.08 59.49 o -7 4 1 1566.82 1581.30 39.07 o -6 4 1 1923.20 1911.29 38.76 o -5 4 1 2514.12 2366.31 48.29 o -4 4 1 1425.79 1529.57 28.28 o -3 4 1 6660.77 7715.27 133.91 o -2 4 1 2205.31 1907.38 55.56 o -1 4 1 6173.87 5833.41 40.75 o 0 4 1 7096.94 6632.95 39.33 o 1 4 1 3666.59 3423.61 35.50 o 2 4 1 4711.92 5273.06 42.21 o 3 4 1 12291.94 12556.84 95.14 o 4 4 1 45.67 30.45 16.65 o 5 4 1 11426.74 11276.85 88.20 o 6 4 1 110.98 158.09 20.28 o 7 4 1 1241.43 1199.39 36.11 o 8 4 1 200.83 207.99 31.69 o 9 4 1 1328.92 1318.88 69.21 o 10 4 1 1.05 73.80 43.29 o 11 4 1 229.56 278.47 99.10 o -11 5 1 85.13 126.27 69.93 o -10 5 1 251.08 309.40 51.77 o -9 5 1 695.26 676.73 66.70 o -8 5 1 380.69 416.10 47.36 o -7 5 1 2471.73 2533.21 60.00 o -6 5 1 2458.68 2292.94 48.46 o -5 5 1 2681.26 2507.04 77.41 o -4 5 1 2831.61 2620.87 75.63 o -3 5 1 25.93 80.77 31.37 o -2 5 1 280.03 202.60 24.30 o -1 5 1 6188.30 5398.32 48.97 o 0 5 1 1617.31 1799.14 31.28 o 1 5 1 2820.52 2674.78 34.00 o 2 5 1 25.56 51.57 22.58 o 3 5 1 9974.75 9457.84 184.44 o 4 5 1 454.74 428.48 42.24 o 5 5 1 145.53 193.15 44.15 o 6 5 1 5756.37 5457.12 105.34 o 7 5 1 1239.15 1215.33 41.21 o 8 5 1 76.93 141.31 53.65 o 9 5 1 85.53 139.27 55.96 o 10 5 1 0.48 114.87 56.01 o 11 5 1 385.40 450.81 113.00 o -11 6 1 37.42 167.59 92.04 o -10 6 1 48.61 110.31 47.20 o -9 6 1 339.20 255.45 59.49 o -8 6 1 123.72 129.78 47.35 o -7 6 1 224.56 281.73 44.41 o -6 6 1 1225.72 1286.42 131.75 o -5 6 1 0.08 67.31 50.49 o -4 6 1 3215.91 3346.30 85.20 o -3 6 1 1130.89 1029.07 58.09 o -2 6 1 22164.57 23659.85 131.55 o -1 6 1 3952.16 4124.04 45.39 o 0 6 1 3885.32 3653.20 45.99 o 1 6 1 461.44 432.12 25.98 o 2 6 1 1904.04 2216.20 49.37 o 3 6 1 59.20 131.63 33.84 o 4 6 1 4084.64 3893.29 85.82 o 5 6 1 2125.93 2324.45 82.13 o 6 6 1 5.01 67.35 40.63 o 7 6 1 75.98 114.07 61.58 o 8 6 1 110.11 173.01 56.41 o 9 6 1 1406.83 1191.46 73.44 o 10 6 1 476.49 409.95 47.12 o 11 6 1 65.76 153.30 107.30 o -10 7 1 1084.47 960.32 72.74 o -9 7 1 0.26 56.97 52.81 o -8 7 1 744.33 763.51 108.97 o -7 7 1 56.21 132.99 46.98 o -6 7 1 165.94 149.62 41.94 o -5 7 1 0.77 82.32 79.19 o -4 7 1 2481.14 2363.06 90.76 o -3 7 1 2139.61 2114.03 104.04 o -2 7 1 60.18 37.37 15.26 o -1 7 1 2493.22 2138.25 49.99 o 0 7 1 1819.72 1900.63 37.45 o 1 7 1 276.14 201.47 22.06 o 2 7 1 1174.45 1158.63 27.67 o 3 7 1 2542.95 2404.49 87.75 o 4 7 1 1897.99 1970.61 74.37 o 5 7 1 1065.96 996.05 63.10 o 6 7 1 434.11 418.60 59.47 o 7 7 1 151.31 150.60 35.16 o 8 7 1 3282.60 3158.60 130.89 o 9 7 1 1051.59 1097.67 69.03 o 10 7 1 1.38 82.32 68.09 o -10 8 1 55.20 133.03 46.95 o -9 8 1 12.57 170.46 51.59 o -8 8 1 1417.76 1329.64 92.20 o -7 8 1 5.73 91.06 49.05 o -6 8 1 1136.98 1151.08 74.72 o -5 8 1 113.51 83.42 36.15 o -4 8 1 898.90 1020.07 67.89 o -3 8 1 2785.34 2713.97 82.78 o -2 8 1 689.79 770.01 30.98 o -1 8 1 1345.92 1464.78 57.28 o 0 8 1 2310.33 2223.63 54.65 o 1 8 1 1592.33 1629.99 41.52 o 2 8 1 1060.35 998.06 30.78 o 3 8 1 687.40 690.45 56.14 o 4 8 1 830.78 940.90 72.32 o 5 8 1 3.34 47.57 54.37 o 6 8 1 171.75 301.37 54.94 o 7 8 1 21.72 52.09 37.14 o 8 8 1 555.83 482.74 55.02 o 9 8 1 909.75 1014.02 75.16 o 10 8 1 39.40 75.79 60.77 o -10 9 1 427.15 468.07 61.40 o -9 9 1 1545.34 1599.87 90.11 o -8 9 1 19.61 78.21 45.51 o -7 9 1 173.83 168.40 54.13 o -6 9 1 62.65 130.16 52.58 o -5 9 1 1853.58 1884.79 92.09 o -4 9 1 77.97 164.71 43.33 o -3 9 1 649.86 673.94 44.79 o -2 9 1 1096.22 1099.53 34.85 o -1 9 1 1578.63 1523.94 49.30 o 0 9 1 0.71 70.25 35.41 o 1 9 1 837.96 834.27 45.28 o 2 9 1 1006.45 944.48 43.15 o 3 9 1 4424.90 3974.15 154.74 o 4 9 1 1.29 83.69 48.03 o 5 9 1 74.83 190.85 58.37 o 6 9 1 419.34 414.09 57.01 o 7 9 1 2769.13 2904.99 164.58 o 8 9 1 941.08 1050.23 82.46 o 9 9 1 17.12 134.62 63.84 o 10 9 1 544.85 554.17 79.99 o -9 10 1 533.86 460.94 60.24 o -8 10 1 34.98 170.24 62.81 o -7 10 1 2376.37 2371.44 119.71 o -6 10 1 1179.50 1387.98 91.42 o -5 10 1 598.90 529.45 67.14 o -4 10 1 1193.76 1182.57 89.14 o -3 10 1 57.42 84.73 26.15 o -2 10 1 58.52 75.42 18.36 o -1 10 1 147.37 192.03 48.10 o 0 10 1 13.73 131.37 63.29 o 1 10 1 3382.05 3435.13 119.27 o 2 10 1 2459.99 2437.33 56.15 o 3 10 1 144.24 140.69 18.49 o 4 10 1 103.90 117.66 39.78 o 5 10 1 1135.49 1036.25 76.97 o 6 10 1 449.52 344.96 55.58 o 7 10 1 122.50 168.91 53.50 o 8 10 1 420.10 511.97 60.93 o 9 10 1 542.23 512.02 102.64 o -9 11 1 134.08 156.80 58.66 o -8 11 1 60.28 167.65 61.90 o -7 11 1 1.14 -2.13 52.73 o -6 11 1 769.19 782.43 114.78 o -5 11 1 1481.05 1386.20 91.90 o -4 11 1 59.66 105.67 44.48 o -3 11 1 279.30 251.13 25.94 o -2 11 1 13.53 85.57 28.34 o -1 11 1 82.36 114.77 29.39 o 0 11 1 535.17 554.07 42.53 o 1 11 1 681.22 726.99 46.66 o 2 11 1 120.85 123.64 25.34 o 3 11 1 2.37 13.58 19.65 o 4 11 1 5165.38 5171.10 150.57 o 5 11 1 433.30 400.87 68.41 o 6 11 1 130.76 217.58 61.62 o 7 11 1 274.44 277.92 50.73 o 8 11 1 812.64 878.68 75.54 o 9 11 1 22.80 158.64 70.06 o -8 12 1 94.25 174.26 58.78 o -7 12 1 126.16 186.47 99.97 o -6 12 1 3525.39 3425.51 145.34 o -5 12 1 181.16 177.88 60.43 o -4 12 1 859.32 861.79 79.56 o -3 12 1 347.30 331.69 55.75 o -2 12 1 474.48 498.56 45.16 o -1 12 1 2.23 123.93 42.24 o 0 12 1 6975.53 6718.83 178.76 o 1 12 1 516.35 522.84 44.56 o 2 12 1 775.22 731.59 44.83 o 3 12 1 29.07 80.56 85.79 o 4 12 1 900.20 808.51 76.01 o 5 12 1 102.01 131.07 57.10 o 6 12 1 386.60 349.87 67.36 o 7 12 1 5.08 142.91 56.93 o 8 12 1 322.25 159.66 55.10 o -7 13 1 34.13 139.77 51.65 o -6 13 1 258.02 266.98 63.49 o -5 13 1 686.32 702.98 85.89 o -4 13 1 30.50 125.66 69.69 o -3 13 1 145.69 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