#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221195.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221195_Fobs loop_ _publ_author_name 'Rofouei, Mohammad Kazem' 'Melardi, Mohammad Reza' 'Khalili Ghaydari, Hamid Reza' 'Barkhi, Mohammad' _publ_section_title ; trans-Bis[1,3-bis(2-methoxyphenyl)triazenido]dimethanolcadmium(II) ; _journal_coeditor_code SU2094 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m351 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.0333 _cell_length_b 13.1892 _cell_length_c 21.4784 _exptl_crystal_F_000 1416.00 _reflns_d_resolution_high 0.7110 _[local]_cod_data_source_file su2094Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cdn3m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 228.64 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10252.45 12352.14 370.00 o 4 0 0 4941.35 5599.47 208.59 o 6 0 0 3967.27 4620.89 132.32 o 8 0 0 4134.33 5089.27 153.06 o 10 0 0 3.67 -9.39 24.64 o 12 0 0 213.42 144.29 42.16 o 14 0 0 55.82 73.89 40.02 o 1 1 0 2468.28 2515.02 32.38 o 2 1 0 666.87 489.39 11.01 o 3 1 0 14049.03 16988.63 249.73 o 4 1 0 2066.52 2047.98 38.58 o 5 1 0 4821.97 6012.35 109.05 o 6 1 0 1854.61 1831.42 49.87 o 7 1 0 1905.46 2073.59 44.29 o 8 1 0 1166.67 1234.50 42.66 o 9 1 0 2722.54 2684.99 71.28 o 10 1 0 165.88 184.65 32.42 o 11 1 0 2032.30 2100.99 67.37 o 12 1 0 98.94 90.07 26.86 o 13 1 0 1955.26 1857.47 68.39 o 14 1 0 394.44 513.56 45.88 o 15 1 0 772.20 834.34 81.32 o 0 2 0 47490.12 50123.15 885.12 o 1 2 0 10948.28 12413.86 152.56 o 2 2 0 115.87 247.47 9.98 o 3 2 0 6339.23 6393.64 90.12 o 4 2 0 171.73 278.22 30.24 o 5 2 0 3185.58 3288.30 66.09 o 6 2 0 21.85 45.17 13.29 o 7 2 0 8978.12 9326.02 150.97 o 8 2 0 2418.10 3002.47 60.98 o 9 2 0 13.13 12.62 16.93 o 10 2 0 10.22 30.05 24.19 o 11 2 0 2.85 -12.78 20.66 o 12 2 0 110.12 124.05 28.71 o 13 2 0 162.05 180.25 33.22 o 14 2 0 56.63 -18.78 32.98 o 15 2 0 18.51 1.69 27.99 o 1 3 0 1715.13 2129.29 45.98 o 3 3 0 7102.63 6749.70 95.90 o 4 3 0 62.67 94.36 12.38 o 5 3 0 1020.52 1273.92 26.68 o 6 3 0 5939.34 5667.89 97.07 o 7 3 0 102.00 18.88 20.80 o 8 3 0 7173.33 7192.76 123.40 o 9 3 0 247.57 224.41 19.57 o 10 3 0 5675.05 5561.71 122.99 o 12 3 0 2252.96 1979.58 68.16 o 13 3 0 0.41 30.46 25.29 o 14 3 0 2407.03 2187.80 77.48 o 15 3 0 88.78 126.05 34.25 o 0 4 0 9241.71 8679.73 144.55 o 1 4 0 3284.50 4217.90 145.09 o 3 4 0 14199.97 13470.39 183.92 o 4 4 0 2078.36 2056.78 60.76 o 5 4 0 10518.84 11553.26 162.43 o 6 4 0 7436.05 6693.13 101.02 o 7 4 0 11162.26 12127.32 173.00 o 8 4 0 4892.43 3993.10 78.39 o 9 4 0 2152.03 2518.55 57.98 o 10 4 0 1247.05 1191.57 49.04 o 11 4 0 208.51 254.60 32.38 o 12 4 0 1.95 -2.76 22.59 o 13 4 0 2.67 -32.97 21.98 o 14 4 0 11.32 6.21 25.73 o 15 4 0 204.07 266.90 41.23 o 1 5 0 995.39 744.64 19.45 o 2 5 0 370.42 472.08 41.82 o 3 5 0 1436.92 1063.55 25.85 o 4 5 0 2687.12 2156.26 39.88 o 5 5 0 69.20 -6.54 32.66 o 6 5 0 250.51 375.36 33.13 o 7 5 0 2337.87 2140.79 43.13 o 8 5 0 641.10 738.30 31.09 o 9 5 0 2600.56 2216.44 54.25 o 10 5 0 985.00 1426.50 64.24 o 11 5 0 1092.65 984.19 50.78 o 12 5 0 502.34 623.03 44.20 o 13 5 0 757.41 653.16 47.28 o 14 5 0 21.80 41.32 28.15 o 0 6 0 11889.84 10003.96 248.68 o 1 6 0 704.45 875.98 34.34 o 2 6 0 14027.81 11833.11 163.85 o 4 6 0 7675.91 6396.60 96.51 o 5 6 0 158.08 268.38 21.28 o 6 6 0 9831.71 8890.12 131.86 o 7 6 0 38.96 30.93 11.46 o 8 6 0 409.18 400.72 25.76 o 9 6 0 1782.76 1699.63 47.71 o 10 6 0 4842.26 4438.23 106.05 o 11 6 0 153.39 170.52 36.83 o 12 6 0 116.32 60.92 32.50 o 13 6 0 62.33 46.02 26.76 o 14 6 0 95.26 95.70 39.23 o 1 7 0 247.78 239.82 34.92 o 2 7 0 113.86 87.58 35.67 o 3 7 0 2828.36 2671.09 58.20 o 4 7 0 1962.79 1610.72 58.50 o 5 7 0 3074.18 2792.22 51.60 o 6 7 0 846.45 769.59 33.01 o 7 7 0 8760.78 8176.75 125.53 o 8 7 0 4232.73 3847.56 70.18 o 9 7 0 1614.99 1569.47 47.07 o 10 7 0 908.36 791.29 36.62 o 11 7 0 996.06 928.37 49.74 o 12 7 0 67.61 117.94 28.73 o 13 7 0 638.61 679.80 49.05 o 14 7 0 382.06 345.57 41.68 o 0 8 0 4286.89 5597.76 567.89 o 1 8 0 9303.85 7685.38 125.37 o 2 8 0 3925.14 4069.86 74.69 o 3 8 0 12618.44 11602.21 183.35 o 4 8 0 1439.50 1787.98 74.83 o 5 8 0 3833.63 3577.43 63.20 o 6 8 0 169.67 154.16 15.87 o 7 8 0 17.80 -2.82 13.80 o 8 8 0 35.33 50.95 17.24 o 9 8 0 302.03 323.83 26.78 o 10 8 0 115.29 205.15 24.75 o 11 8 0 351.33 313.09 34.38 o 12 8 0 8.60 -5.96 23.48 o 13 8 0 27.70 -1.76 26.10 o 14 8 0 80.26 98.57 57.52 o 1 9 0 600.28 598.95 46.04 o 2 9 0 78.37 61.79 33.40 o 3 9 0 534.21 583.49 35.64 o 4 9 0 1764.81 1662.46 36.41 o 5 9 0 572.34 645.59 24.43 o 6 9 0 388.22 424.21 22.27 o 7 9 0 18.61 -1.03 12.48 o 8 9 0 3374.41 3082.85 91.25 o 9 9 0 286.18 477.64 30.75 o 10 9 0 3037.98 2768.47 111.26 o 11 9 0 3.19 114.01 49.97 o 12 9 0 610.20 454.14 50.02 o 13 9 0 179.94 274.31 45.54 o 0 10 0 2773.92 2814.26 99.85 o 1 10 0 4200.47 3795.80 86.52 o 2 10 0 3263.82 3709.32 72.38 o 3 10 0 7473.15 6886.89 119.84 o 4 10 0 2884.19 3275.23 79.94 o 5 10 0 3611.40 3524.84 73.87 o 6 10 0 1645.24 1545.71 44.61 o 7 10 0 1603.65 1599.02 46.90 o 8 10 0 665.68 740.05 61.64 o 9 10 0 808.28 797.71 44.93 o 10 10 0 658.47 684.97 44.00 o 11 10 0 348.41 272.04 57.83 o 12 10 0 42.68 108.80 35.00 o 13 10 0 1.82 0.54 31.97 o 1 11 0 6.51 -10.04 14.77 o 2 11 0 80.50 55.64 12.63 o 3 11 0 115.00 133.07 22.94 o 4 11 0 56.20 45.63 21.25 o 5 11 0 1673.60 1548.13 45.16 o 6 11 0 0.61 86.39 24.42 o 7 11 0 2669.13 2459.89 101.36 o 8 11 0 372.49 421.21 35.08 o 9 11 0 504.42 522.85 39.25 o 10 11 0 400.14 456.92 39.34 o 11 11 0 2602.32 2375.60 91.47 o 12 11 0 240.52 284.52 45.89 o 0 12 0 3121.17 2938.73 109.90 o 1 12 0 1.47 108.17 22.37 o 2 12 0 1558.60 1629.49 71.26 o 3 12 0 64.84 108.81 23.64 o 4 12 0 3584.42 3386.63 86.52 o 5 12 0 368.97 477.26 38.33 o 6 12 0 1765.77 1535.80 47.60 o 7 12 0 486.22 632.20 35.41 o 8 12 0 1380.98 1290.33 53.69 o 9 12 0 5.29 62.63 25.23 o 10 12 0 82.74 72.21 27.21 o 11 12 0 240.13 164.88 39.79 o 1 13 0 0.12 -29.71 18.56 o 2 13 0 101.24 54.64 30.15 o 3 13 0 56.29 119.29 25.42 o 4 13 0 121.89 189.33 28.45 o 5 13 0 611.87 599.54 41.53 o 6 13 0 748.45 657.15 52.33 o 7 13 0 1682.54 1620.17 67.35 o 8 13 0 464.56 619.44 62.91 o 9 13 0 128.18 103.33 32.72 o 10 13 0 212.61 208.20 43.40 o 11 13 0 387.30 378.65 61.28 o 0 14 0 484.11 697.72 93.22 o 1 14 0 4591.58 4289.07 160.47 o 2 14 0 117.00 192.61 31.30 o 3 14 0 2825.72 2701.41 109.28 o 4 14 0 409.60 359.21 36.13 o 5 14 0 1731.32 1733.04 63.46 o 6 14 0 31.47 57.01 25.66 o 7 14 0 880.67 909.32 51.40 o 8 14 0 199.75 242.59 57.54 o 9 14 0 479.94 476.71 61.86 o 10 14 0 79.87 1.89 31.56 o 1 15 0 22.90 25.59 26.90 o 2 15 0 2.10 6.67 22.02 o 3 15 0 74.04 61.24 31.40 o 4 15 0 1049.44 1047.91 62.78 o 5 15 0 6.59 55.79 25.89 o 6 15 0 886.19 791.86 50.63 o 7 15 0 26.13 58.06 27.16 o 8 15 0 266.48 294.70 56.15 o 9 15 0 102.14 56.47 35.23 o 0 16 0 2815.55 2403.46 222.96 o 1 16 0 1333.48 1256.52 65.46 o 2 16 0 758.82 947.82 54.76 o 3 16 0 886.25 913.69 76.71 o 4 16 0 425.10 384.97 63.09 o 5 16 0 294.54 435.14 51.85 o 6 16 0 295.19 294.45 37.81 o 7 16 0 385.24 388.71 49.74 o 1 17 0 95.34 93.68 45.34 o 2 17 0 12.54 11.52 26.29 o 3 17 0 1.16 11.24 26.13 o 4 17 0 13.47 31.96 27.71 o 5 17 0 478.00 393.83 48.70 o 6 17 0 50.87 109.05 32.53 o 0 18 0 966.69 987.62 84.98 o 1 18 0 106.11 238.43 52.03 o 2 18 0 990.96 862.75 57.78 o 3 18 0 115.07 152.63 33.77 o 1 0 1 42228.47 48244.45 875.17 o 3 0 1 1262.94 1446.18 28.86 o 4 0 1 7243.71 8377.77 152.19 o 5 0 1 27499.54 35022.64 510.69 o 6 0 1 4575.11 5350.78 90.67 o 7 0 1 8779.79 10734.46 226.67 o 8 0 1 2025.91 2273.34 61.34 o 9 0 1 155.27 188.34 25.10 o 10 0 1 268.11 273.73 29.81 o 11 0 1 575.74 636.37 41.95 o 12 0 1 1304.57 1337.40 55.88 o 13 0 1 580.88 617.70 45.92 o 14 0 1 656.08 700.39 50.64 o 15 0 1 60.15 79.39 31.83 o -15 1 1 153.06 133.84 33.10 o -14 1 1 1040.98 1118.99 70.48 o -13 1 1 199.67 221.66 33.82 o -12 1 1 1080.80 1108.57 54.73 o -11 1 1 1196.23 1196.22 50.85 o -10 1 1 2350.94 2517.78 87.20 o -9 1 1 2164.63 2255.59 64.23 o -8 1 1 2482.06 2794.67 70.11 o -7 1 1 2814.04 3233.14 62.00 o -6 1 1 7092.56 8541.92 134.97 o -5 1 1 7734.38 8991.97 140.10 o -4 1 1 979.52 1141.06 18.89 o -3 1 1 18590.66 21699.07 323.64 o -2 1 1 3770.18 4814.67 64.22 o -1 1 1 13917.39 17219.38 181.97 o 0 1 1 1714.48 1685.21 24.31 o 1 1 1 13357.57 16580.55 192.76 o 2 1 1 4125.23 5219.21 64.60 o 3 1 1 19512.25 23142.51 323.97 o 4 1 1 878.53 1040.46 24.07 o 5 1 1 7709.90 8916.69 139.88 o 6 1 1 6886.73 8264.30 134.25 o 7 1 1 2815.49 3226.55 74.20 o 8 1 1 2594.03 2814.50 61.79 o 9 1 1 2151.05 2245.91 63.67 o 10 1 1 2240.43 2270.52 68.16 o 11 1 1 1188.93 1146.23 51.20 o 12 1 1 1066.97 1047.68 53.79 o 13 1 1 174.12 208.92 33.21 o 14 1 1 1020.02 1077.58 60.38 o 15 1 1 138.37 103.20 32.36 o -15 2 1 170.56 141.45 35.57 o -14 2 1 153.41 194.73 34.19 o -13 2 1 334.94 370.02 39.30 o -12 2 1 275.22 344.49 35.61 o -11 2 1 1972.27 1905.77 64.88 o -10 2 1 126.49 149.60 25.40 o -9 2 1 1357.72 1391.08 39.54 o -8 2 1 3395.98 3494.35 67.19 o -7 2 1 2031.96 2359.49 51.28 o -6 2 1 7614.28 8684.49 140.52 o -5 2 1 3391.03 3875.68 60.45 o -4 2 1 5060.04 5348.64 68.61 o -3 2 1 6744.40 7768.21 118.47 o -2 2 1 5456.25 6409.95 92.52 o -1 2 1 8562.23 9406.76 113.25 o 0 2 1 18949.74 17708.77 252.85 o 1 2 1 7921.63 8782.69 122.45 o 2 2 1 5942.46 7030.45 93.01 o 3 2 1 6774.21 7790.62 108.17 o 4 2 1 4528.24 4779.22 74.16 o 5 2 1 3384.04 3860.09 68.02 o 6 2 1 7796.01 8878.54 157.01 o 7 2 1 2129.81 2560.08 52.04 o 8 2 1 3248.72 3224.31 65.68 o 9 2 1 1295.93 1238.23 46.34 o 10 2 1 76.52 77.21 21.80 o 11 2 1 1973.77 1976.95 65.04 o 12 2 1 305.85 309.67 35.62 o 13 2 1 346.10 290.18 36.57 o 14 2 1 148.89 136.43 31.68 o 15 2 1 161.74 161.53 51.47 o -15 3 1 959.81 883.88 59.53 o -14 3 1 16.02 58.01 27.31 o -13 3 1 1308.00 1279.54 61.92 o -12 3 1 306.41 369.63 41.61 o -11 3 1 4078.68 4051.01 100.17 o -10 3 1 103.03 202.34 27.78 o -9 3 1 3299.99 3327.28 68.66 o -8 3 1 1816.72 1871.85 45.41 o -7 3 1 2584.59 2662.88 62.79 o -6 3 1 1860.70 2152.90 39.73 o -5 3 1 3064.29 3043.87 52.29 o -4 3 1 6525.04 7262.19 104.64 o -3 3 1 6270.38 6432.56 92.87 o -2 3 1 6917.51 7007.96 100.46 o -1 3 1 2063.03 2511.88 57.69 o 0 3 1 5098.95 5047.68 70.49 o 1 3 1 1980.48 2491.95 63.07 o 2 3 1 7550.90 7544.22 111.45 o 3 3 1 6431.25 6637.19 93.18 o 4 3 1 6483.96 7369.38 104.68 o 5 3 1 3393.96 3395.52 53.02 o 6 3 1 1786.21 2061.98 56.44 o 7 3 1 2622.87 2607.54 54.92 o 8 3 1 1885.14 1861.22 45.18 o 9 3 1 3257.27 3225.52 67.77 o 10 3 1 107.68 203.78 47.37 o 11 3 1 4142.23 3804.75 112.20 o 12 3 1 289.65 380.99 38.01 o 13 3 1 1283.08 1274.06 61.71 o 14 3 1 17.37 103.99 29.95 o 15 3 1 992.39 871.23 58.05 o -15 4 1 579.29 541.28 50.04 o -14 4 1 105.86 121.52 30.96 o -13 4 1 378.60 323.02 38.30 o -12 4 1 231.87 294.13 34.79 o -11 4 1 1277.40 1290.73 52.91 o -10 4 1 520.90 749.22 42.90 o -9 4 1 852.76 912.39 32.82 o -8 4 1 4386.83 4499.08 84.71 o -7 4 1 3746.67 3482.64 59.25 o -6 4 1 4593.54 5171.30 85.80 o -5 4 1 4455.03 3992.30 63.37 o -4 4 1 8631.29 9430.29 135.22 o -3 4 1 6806.62 6021.64 88.04 o -2 4 1 12726.42 12505.29 159.51 o -1 4 1 7087.69 6444.55 88.41 o 1 4 1 6704.85 6085.08 97.77 o 2 4 1 13413.39 13137.35 191.74 o 3 4 1 6860.81 6104.73 88.30 o 4 4 1 9019.54 9757.00 135.61 o 5 4 1 4407.61 3803.62 62.74 o 6 4 1 4631.08 5190.69 81.27 o 7 4 1 3602.73 3229.32 66.63 o 8 4 1 4219.85 4301.60 84.01 o 9 4 1 829.04 862.08 33.07 o 10 4 1 606.50 793.51 44.56 o 11 4 1 1330.19 1262.78 52.38 o 12 4 1 234.05 275.32 34.48 o 13 4 1 356.02 345.31 39.21 o 14 4 1 93.57 38.49 28.54 o 15 4 1 559.63 487.69 47.87 o -14 5 1 426.33 349.75 41.34 o -13 5 1 290.70 297.34 36.97 o -12 5 1 807.04 726.45 46.96 o -11 5 1 319.25 396.18 36.86 o -10 5 1 3304.08 2885.20 79.67 o -9 5 1 82.77 169.15 20.33 o -8 5 1 2276.57 2016.06 42.54 o -7 5 1 1649.50 1457.49 34.06 o -6 5 1 2597.70 2379.51 45.35 o -5 5 1 6350.66 5864.16 89.50 o -4 5 1 3931.70 3846.81 60.39 o -3 5 1 6004.33 4671.74 71.12 o -2 5 1 2296.41 2182.72 68.17 o -1 5 1 1563.88 1527.17 28.04 o 0 5 1 1521.11 1816.61 81.95 o 1 5 1 1683.64 1639.02 42.46 o 2 5 1 2384.97 2296.09 48.08 o 3 5 1 5960.91 4668.90 71.23 o 4 5 1 3707.95 3532.68 59.60 o 5 5 1 6261.83 5767.25 89.11 o 6 5 1 2594.30 2330.99 66.94 o 7 5 1 1747.36 1506.27 34.63 o 8 5 1 2405.37 2082.98 50.67 o 9 5 1 53.79 94.73 23.45 o 10 5 1 3297.96 2960.77 136.93 o 11 5 1 372.06 413.54 39.99 o 12 5 1 828.25 734.85 47.38 o 13 5 1 285.84 293.73 36.49 o 14 5 1 400.47 337.86 40.62 o -14 6 1 332.25 264.38 38.56 o -13 6 1 19.23 -8.55 23.06 o -12 6 1 469.45 399.72 38.15 o -11 6 1 635.34 618.21 53.78 o -10 6 1 788.90 1005.69 50.12 o -9 6 1 580.14 700.42 39.52 o -8 6 1 1677.06 1497.95 36.15 o -7 6 1 212.98 299.99 18.47 o -6 6 1 727.90 800.08 62.21 o -5 6 1 10554.85 9687.72 140.15 o -4 6 1 2360.79 2513.19 46.17 o -3 6 1 17191.46 15266.95 211.20 o -2 6 1 584.77 992.69 76.21 o -1 6 1 21039.15 18559.58 246.32 o 0 6 1 1481.70 1361.36 71.29 o 1 6 1 20141.35 17855.12 271.68 o 2 6 1 645.95 1061.09 71.82 o 3 6 1 17322.69 15554.64 211.78 o 4 6 1 2543.54 2577.30 81.96 o 5 6 1 10573.15 9606.68 140.04 o 6 6 1 689.20 787.30 67.13 o 7 6 1 270.58 325.50 18.95 o 8 6 1 1700.09 1437.26 42.00 o 9 6 1 507.72 531.61 30.25 o 10 6 1 777.74 1046.45 48.43 o 11 6 1 611.73 615.09 42.77 o 12 6 1 433.67 350.16 37.90 o 13 6 1 16.93 4.64 24.20 o 14 6 1 337.16 242.19 37.45 o -14 7 1 572.47 625.38 50.64 o -13 7 1 364.40 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