#------------------------------------------------------------------------------ #$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $ #$Revision: 717 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221246.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221246_Fobs loop_ _publ_author_name 'Kia, Reza' 'Fun, Hoong-Kun' 'Kargar, Hadi' _publ_section_title ; N,N'-Bis(4-bromobenzylidene)-2,2-dimethylpropane-1,3-diamine ; _journal_coeditor_code AT2737 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o747 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.6687 _cell_length_b 7.7919 _cell_length_c 41.5932 _exptl_crystal_F_000 872.00 _reflns_d_resolution_high 0.5838 _[local]_cod_data_source_file at2737Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hk11m in P2(1)2(1)2(1) (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 255.94 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 29874.21 29564.54 1089.38 o 4 0 0 399.26 440.21 20.97 o 6 0 0 158.30 172.04 16.10 o 8 0 0 71.04 122.94 35.46 o 1 1 0 4893.00 4604.78 232.68 o 2 1 0 1480.98 1327.26 37.76 o 3 1 0 668.68 721.42 20.88 o 4 1 0 555.19 594.10 15.83 o 5 1 0 162.02 157.34 11.48 o 6 1 0 1717.93 1635.88 38.22 o 7 1 0 289.47 305.14 17.59 o 8 1 0 1442.57 1439.82 51.79 o 9 1 0 123.46 169.26 34.21 o 0 2 0 10113.61 9967.20 392.76 o 1 2 0 8417.05 8373.26 255.70 o 2 2 0 3211.83 3105.98 93.47 o 3 2 0 5809.38 5614.99 148.40 o 4 2 0 884.21 903.43 23.39 o 5 2 0 3.99 27.95 9.45 o 6 2 0 273.07 295.95 19.73 o 7 2 0 17.06 21.45 14.23 o 8 2 0 25.23 26.95 19.43 o 9 2 0 74.03 69.09 21.60 o 1 3 0 2679.43 2819.44 100.86 o 2 3 0 2028.46 1863.13 47.76 o 3 3 0 1408.97 1511.92 40.78 o 4 3 0 1549.62 1363.32 37.88 o 5 3 0 16.87 14.19 9.66 o 6 3 0 22.81 55.30 13.31 o 7 3 0 381.43 373.96 28.12 o 8 3 0 9.74 22.17 19.91 o 9 3 0 424.80 443.55 33.57 o 0 4 0 2903.07 3357.48 114.72 o 1 4 0 12765.74 13263.89 315.79 o 2 4 0 1413.44 1385.46 32.36 o 3 4 0 441.76 440.85 15.72 o 4 4 0 1942.93 1809.90 51.46 o 5 4 0 348.79 345.78 18.11 o 6 4 0 979.12 985.24 34.71 o 7 4 0 0.98 -13.85 15.59 o 8 4 0 64.44 59.15 26.59 o 9 4 0 6.85 42.39 30.29 o 1 5 0 1108.78 1142.12 29.34 o 2 5 0 3037.56 3120.99 78.95 o 3 5 0 889.00 927.64 27.31 o 4 5 0 749.28 725.25 25.71 o 5 5 0 233.60 233.41 15.90 o 6 5 0 570.48 562.55 24.94 o 7 5 0 141.46 167.56 20.05 o 8 5 0 8.76 24.82 25.51 o 9 5 0 49.27 24.44 30.02 o 0 6 0 2647.98 2622.11 102.65 o 1 6 0 11.81 11.14 5.33 o 2 6 0 404.98 364.48 15.48 o 3 6 0 4520.89 4446.01 108.88 o 4 6 0 666.14 637.40 22.91 o 5 6 0 2271.03 2249.70 64.59 o 6 6 0 13.32 13.45 17.15 o 7 6 0 312.82 277.82 29.91 o 8 6 0 4.18 -5.78 30.77 o 1 7 0 74.01 88.06 9.26 o 2 7 0 72.98 69.31 10.23 o 3 7 0 4638.82 4580.38 112.27 o 4 7 0 19.02 26.06 12.49 o 5 7 0 586.04 604.14 26.31 o 6 7 0 37.66 -4.38 22.87 o 7 7 0 1.05 -2.03 25.77 o 8 7 0 15.87 8.72 30.42 o 0 8 0 469.25 503.17 35.46 o 1 8 0 154.43 148.31 15.16 o 2 8 0 91.10 70.96 11.91 o 3 8 0 546.50 616.03 22.57 o 4 8 0 395.71 410.08 19.42 o 5 8 0 1039.19 1112.23 38.65 o 6 8 0 126.88 79.26 26.96 o 7 8 0 132.87 155.66 29.47 o 1 9 0 105.09 125.14 17.61 o 2 9 0 396.88 385.50 23.14 o 3 9 0 186.70 215.14 15.86 o 4 9 0 634.03 646.98 25.30 o 5 9 0 16.50 37.00 20.43 o 6 9 0 90.27 90.81 27.17 o 7 9 0 6.07 -18.22 29.18 o 0 10 0 51.87 45.48 23.65 o 1 10 0 262.14 337.50 22.85 o 2 10 0 374.24 408.14 25.13 o 3 10 0 84.60 126.28 21.07 o 4 10 0 646.37 624.11 45.37 o 5 10 0 181.58 187.38 24.00 o 6 10 0 171.24 161.61 29.54 o 1 11 0 4.49 30.78 26.32 o 2 11 0 86.90 94.70 28.13 o 3 11 0 71.37 57.66 25.34 o 4 11 0 109.12 105.43 43.00 o 5 11 0 68.82 46.43 39.60 o 0 12 0 104.39 120.81 42.95 o 1 12 0 278.38 206.38 32.12 o 2 12 0 41.48 27.72 33.68 o 3 12 0 143.46 104.48 28.01 o 4 12 0 1.72 11.65 39.23 o 1 13 0 2.30 -9.11 28.92 o 2 13 0 1.77 6.98 28.75 o 1 0 1 8713.03 9152.93 348.98 o 2 0 1 97.15 100.27 6.42 o 3 0 1 874.20 921.17 27.60 o 4 0 1 30.38 21.19 8.13 o 5 0 1 563.09 550.73 16.60 o 6 0 1 491.73 522.70 17.26 o 7 0 1 9.52 23.85 11.71 o 8 0 1 295.37 309.21 26.75 o 9 0 1 102.16 135.30 65.90 o -9 1 1 210.32 255.39 37.79 o -8 1 1 168.75 201.25 21.09 o -7 1 1 440.59 452.27 20.61 o -6 1 1 129.18 129.44 11.16 o -5 1 1 279.13 271.43 10.78 o -4 1 1 141.86 136.66 7.65 o -3 1 1 5090.48 4971.64 141.50 o -2 1 1 7007.35 6909.36 157.27 o -1 1 1 19348.29 18848.08 617.42 o 0 1 1 5706.69 5138.56 171.91 o 1 1 1 20393.38 19958.11 706.84 o 2 1 1 7183.07 6904.85 177.86 o 3 1 1 5900.72 5926.07 133.89 o 4 1 1 118.92 116.23 6.96 o 5 1 1 200.38 196.54 11.03 o 6 1 1 130.27 134.59 11.11 o 7 1 1 530.70 530.04 21.60 o 8 1 1 190.82 237.34 19.30 o 9 1 1 246.54 258.40 36.88 o -9 2 1 54.44 72.66 21.98 o -8 2 1 37.21 43.33 19.70 o -7 2 1 806.67 783.71 28.73 o -6 2 1 21.27 43.42 12.58 o -5 2 1 1757.11 1640.97 57.56 o -4 2 1 366.69 352.73 12.49 o -3 2 1 17.40 22.45 4.78 o -2 2 1 6142.05 6012.90 163.84 o -1 2 1 14372.26 14175.74 436.85 o 0 2 1 65505.65 60285.62 1830.79 o 1 2 1 15008.71 14971.11 451.53 o 2 2 1 6386.00 6334.50 193.38 o 3 2 1 35.28 43.45 7.52 o 4 2 1 404.53 361.85 12.57 o 5 2 1 1614.94 1560.48 43.69 o 6 2 1 22.35 21.59 12.54 o 7 2 1 726.04 699.62 26.60 o 8 2 1 15.14 18.72 19.17 o 9 2 1 70.40 44.82 24.08 o -9 3 1 10.79 1.64 21.00 o -8 3 1 336.66 341.53 26.16 o -7 3 1 202.62 206.35 18.31 o -6 3 1 821.59 791.58 31.71 o -5 3 1 301.78 332.45 16.63 o -4 3 1 238.01 234.00 11.18 o -3 3 1 4206.15 4018.84 88.30 o -2 3 1 381.81 417.99 24.73 o -1 3 1 7547.96 7782.51 236.45 o 0 3 1 123.93 152.09 7.02 o 1 3 1 7556.88 7787.02 238.86 o 2 3 1 740.86 763.30 24.56 o 3 3 1 4229.67 4089.71 108.03 o 4 3 1 300.05 286.30 12.80 o 5 3 1 325.67 361.65 15.54 o 6 3 1 998.45 1001.97 32.67 o 7 3 1 192.53 196.98 18.23 o 8 3 1 319.11 340.82 26.15 o 9 3 1 20.04 42.64 24.48 o -9 4 1 16.92 43.88 30.12 o -8 4 1 36.29 27.18 20.43 o -7 4 1 93.65 75.62 17.14 o -6 4 1 216.61 232.25 17.69 o -5 4 1 963.78 962.93 31.44 o -4 4 1 243.93 275.14 22.31 o -3 4 1 1964.19 1937.53 45.27 o -2 4 1 2186.67 2219.84 49.52 o -1 4 1 58.22 89.55 6.08 o 0 4 1 9089.27 9574.00 228.10 o 1 4 1 104.16 146.46 6.62 o 2 4 1 1911.58 1959.25 48.22 o 3 4 1 1669.35 1655.99 43.80 o 4 4 1 291.02 281.31 13.75 o 5 4 1 825.77 874.36 31.16 o 6 4 1 239.78 263.82 18.38 o 7 4 1 133.59 171.20 18.22 o 8 4 1 23.06 53.66 20.39 o 9 4 1 26.87 -2.13 29.66 o -9 5 1 13.76 40.17 30.60 o -8 5 1 91.28 109.88 27.33 o -7 5 1 99.79 102.51 22.72 o -6 5 1 723.13 735.25 33.09 o -5 5 1 322.40 345.88 18.42 o -4 5 1 2638.21 2598.48 71.35 o -3 5 1 965.90 937.55 27.52 o -2 5 1 3076.74 3043.91 83.70 o -1 5 1 99.83 115.11 7.24 o 0 5 1 3199.08 3295.19 80.09 o 1 5 1 149.81 172.08 7.98 o 2 5 1 3715.28 3672.82 91.59 o 3 5 1 1010.41 949.59 27.46 o 4 5 1 2654.33 2604.40 71.81 o 5 5 1 262.09 292.19 17.75 o 6 5 1 713.82 762.32 30.26 o 7 5 1 54.27 51.86 23.33 o 8 5 1 73.36 88.60 26.61 o 9 5 1 18.22 38.90 33.53 o -8 6 1 48.34 55.03 27.04 o -7 6 1 35.00 30.28 25.01 o -6 6 1 579.18 599.56 32.40 o -5 6 1 455.86 495.73 22.76 o -4 6 1 1169.85 1184.22 36.14 o -3 6 1 763.91 784.76 26.83 o -2 6 1 422.43 407.45 20.10 o -1 6 1 476.38 493.27 17.74 o 0 6 1 235.46 253.83 12.30 o 1 6 1 446.67 468.57 16.32 o 2 6 1 363.10 348.39 14.11 o 3 6 1 782.38 806.31 25.22 o 4 6 1 993.15 992.27 30.78 o 5 6 1 473.08 495.94 22.58 o 6 6 1 411.39 426.64 26.37 o 7 6 1 33.49 18.44 24.12 o 8 6 1 55.75 56.72 30.48 o -8 7 1 14.47 40.56 30.30 o -7 7 1 60.60 109.39 27.46 o -6 7 1 35.05 70.84 21.91 o -5 7 1 296.41 296.97 19.86 o -4 7 1 721.58 704.13 25.66 o -3 7 1 933.64 1019.95 31.18 o -2 7 1 1037.13 1080.62 32.23 o -1 7 1 1169.72 1169.37 34.54 o 0 7 1 181.19 213.11 15.37 o 1 7 1 1111.29 1098.70 34.15 o 2 7 1 969.83 987.22 30.94 o 3 7 1 1033.04 1075.85 31.22 o 4 7 1 756.88 753.56 26.12 o 5 7 1 302.87 363.50 23.60 o 6 7 1 40.74 37.14 18.29 o 7 7 1 48.32 66.47 26.70 o 8 7 1 12.40 39.70 30.55 o -7 8 1 15.23 24.81 27.10 o -6 8 1 90.78 66.25 30.99 o -5 8 1 445.86 479.20 24.28 o -4 8 1 472.91 485.37 20.95 o -3 8 1 790.00 816.09 26.59 o -2 8 1 199.61 202.09 13.98 o -1 8 1 304.05 311.01 18.98 o 0 8 1 115.22 150.69 15.69 o 1 8 1 289.08 282.68 17.96 o 2 8 1 265.38 254.17 14.77 o 3 8 1 830.76 831.96 27.11 o 4 8 1 556.01 564.62 23.53 o 5 8 1 519.46 557.21 25.17 o 6 8 1 143.29 149.99 22.91 o 7 8 1 23.82 29.76 26.62 o -7 9 1 63.13 43.56 30.39 o -6 9 1 261.17 262.57 31.55 o -5 9 1 100.41 91.92 21.35 o -4 9 1 572.14 611.48 25.44 o -3 9 1 355.68 374.04 18.32 o -2 9 1 768.49 801.92 35.17 o -1 9 1 4.60 -5.45 15.68 o 0 9 1 350.90 398.00 22.80 o 1 9 1 13.36 29.57 15.21 o 2 9 1 761.75 813.17 35.43 o 3 9 1 380.86 388.02 18.60 o 4 9 1 547.48 591.41 23.90 o 5 9 1 74.92 65.33 21.06 o 6 9 1 204.24 238.04 25.46 o 7 9 1 78.32 81.83 31.45 o -6 10 1 160.13 122.79 28.67 o -5 10 1 230.37 229.57 24.58 o -4 10 1 0.81 5.17 19.38 o -3 10 1 220.30 251.03 23.35 o -2 10 1 151.53 141.79 18.91 o -1 10 1 119.04 152.49 19.56 o 0 10 1 215.92 221.11 19.90 o 1 10 1 122.26 141.72 18.57 o 2 10 1 156.13 177.63 20.55 o 3 10 1 200.74 200.38 22.26 o 4 10 1 9.24 22.96 20.03 o 5 10 1 211.54 221.53 24.58 o 6 10 1 181.36 165.44 29.66 o -5 11 1 72.05 77.61 40.94 o -4 11 1 31.65 19.42 26.43 o -3 11 1 394.42 350.25 31.48 o -2 11 1 15.30 5.27 21.93 o -1 11 1 290.08 271.07 40.36 o 0 11 1 74.35 76.99 27.37 o 1 11 1 289.92 310.62 32.57 o 2 11 1 23.22 -18.92 24.82 o 3 11 1 393.58 381.75 40.28 o 4 11 1 38.48 37.74 26.11 o 5 11 1 109.33 119.66 49.15 o -4 12 1 41.83 29.96 40.39 o -3 12 1 68.60 34.93 26.90 o -2 12 1 121.02 127.48 27.24 o -1 12 1 10.96 28.63 26.10 o 0 12 1 199.61 216.08 34.50 o 1 12 1 8.44 34.92 28.01 o 2 12 1 143.80 107.80 26.72 o 3 12 1 52.93 53.46 26.78 o 4 12 1 40.78 19.77 38.50 o -2 13 1 52.87 25.07 61.47 o -1 13 1 103.07 96.01 30.93 o 0 13 1 58.76 33.05 29.06 o 1 13 1 87.99 91.47 30.09 o 2 13 1 49.04 7.24 29.14 o 1 0 2 374.41 396.18 14.29 o 2 0 2 1200.34 1349.87 34.71 o 3 0 2 2663.88 2763.80 74.79 o 4 0 2 3266.47 3390.90 69.49 o 5 0 2 679.08 657.27 18.48 o 6 0 2 656.48 693.53 20.65 o 7 0 2 1947.35 1903.59 44.50 o 8 0 2 14.40 34.98 22.32 o 9 0 2 293.26 313.38 38.01 o -9 1 2 29.42 40.93 31.54 o -8 1 2 130.18 125.70 19.47 o -7 1 2 39.01 45.87 13.86 o -6 1 2 62.28 54.70 10.27 o -5 1 2 414.16 416.28 14.60 o -4 1 2 888.57 823.57 21.83 o -3 1 2 4072.83 4005.24 98.68 o -2 1 2 8683.81 8308.16 251.84 o -1 1 2 60176.95 54001.27 1620.45 o 0 1 2 1920.72 1978.96 60.90 o 1 1 2 54823.42 50943.59 2298.37 o 2 1 2 9057.96 8666.73 240.85 o 3 1 2 4084.90 4074.38 98.15 o 4 1 2 945.87 904.03 22.24 o 5 1 2 432.21 415.41 14.97 o 6 1 2 93.62 83.63 10.51 o 7 1 2 44.70 53.82 14.21 o 8 1 2 125.70 169.53 18.88 o 9 1 2 41.26 31.60 30.24 o -9 2 2 87.50 68.46 21.62 o -8 2 2 323.42 326.21 24.75 o -7 2 2 248.09 273.99 18.03 o -6 2 2 559.60 580.43 23.17 o -5 2 2 545.26 521.86 22.33 o -4 2 2 216.76 201.84 10.60 o -3 2 2 2906.48 2770.16 71.61 o -2 2 2 2285.28 2436.88 64.33 o -1 2 2 1828.67 1770.02 57.11 o 0 2 2 23335.68 23483.23 824.07 o 1 2 2 1881.91 1912.14 52.39 o 2 2 2 2164.18 2257.80 69.61 o 3 2 2 3185.64 3004.74 76.88 o 4 2 2 300.66 300.17 15.60 o 5 2 2 637.07 608.09 21.41 o 6 2 2 591.40 603.53 23.17 o 7 2 2 329.80 347.55 18.26 o 8 2 2 308.97 320.18 24.85 o 9 2 2 96.42 96.61 25.16 o -9 3 2 9.60 32.69 20.95 o -8 3 2 291.24 275.76 25.08 o -7 3 2 278.45 263.76 19.66 o -6 3 2 84.95 79.19 14.40 o -5 3 2 1727.70 1585.72 49.64 o -4 3 2 828.26 759.44 21.37 o -3 3 2 1440.56 1425.79 34.72 o -2 3 2 7938.61 7802.01 203.87 o -1 3 2 108.47 122.43 8.49 o 0 3 2 15792.29 15754.17 444.52 o 1 3 2 38.11 44.31 8.57 o 2 3 2 9119.35 8821.60 195.74 o 3 3 2 1703.13 1650.00 44.19 o 4 3 2 664.24 678.81 20.13 o 5 3 2 1476.14 1410.84 40.42 o 6 3 2 103.10 136.98 15.31 o 7 3 2 241.93 246.51 19.51 o 8 3 2 309.68 344.24 27.43 o 9 3 2 11.82 17.70 24.01 o -9 4 2 8.18 17.13 26.19 o -8 4 2 222.45 239.41 24.43 o -7 4 2 354.95 366.26 21.86 o -6 4 2 262.84 265.89 17.47 o -5 4 2 1565.59 1451.84 44.50 o -4 4 2 171.63 185.77 10.64 o -3 4 2 2963.61 2891.23 71.84 o -2 4 2 2736.69 2787.07 66.03 o -1 4 2 3011.51 3273.40 79.17 o 0 4 2 3660.32 3640.00 87.82 o 1 4 2 3002.02 3233.17 82.53 o 2 4 2 2640.74 2689.62 63.69 o 3 4 2 3230.42 3132.17 72.86 o 4 4 2 159.58 181.08 12.85 o 5 4 2 1523.94 1427.19 48.16 o 6 4 2 184.10 194.68 17.21 o 7 4 2 390.61 395.78 22.49 o 8 4 2 211.51 219.65 24.17 o 9 4 2 20.97 44.33 30.16 o -8 5 2 47.68 29.39 26.25 o -7 5 2 152.01 166.55 24.15 o -6 5 2 677.30 659.20 31.16 o -5 5 2 830.17 860.37 30.80 o -4 5 2 1009.79 978.88 32.48 o -3 5 2 3948.18 3813.15 92.36 o -2 5 2 50.63 61.87 7.46 o -1 5 2 6123.41 6438.97 151.12 o 0 5 2 433.75 441.57 14.16 o 1 5 2 6135.50 6343.29 141.44 o 2 5 2 66.55 84.06 6.91 o 3 5 2 3593.03 3421.96 82.14 o 4 5 2 1143.55 1117.57 32.04 o 5 5 2 893.71 879.61 28.34 o 6 5 2 682.07 631.04 27.15 o 7 5 2 167.51 195.48 19.58 o 8 5 2 38.96 27.64 25.68 o -8 6 2 17.07 11.37 26.40 o -7 6 2 26.99 20.48 24.73 o -6 6 2 154.97 153.90 20.41 o -5 6 2 294.53 317.69 19.01 o -4 6 2 1688.29 1656.13 54.43 o -3 6 2 603.75 647.41 23.35 o -2 6 2 2638.25 2657.93 70.22 o -1 6 2 2447.21 2509.62 69.19 o 0 6 2 1065.13 1121.61 34.02 o 1 6 2 2553.84 2645.99 66.35 o 2 6 2 2456.02 2449.27 63.76 o 3 6 2 540.07 589.22 20.48 o 4 6 2 1958.07 1895.35 49.75 o 5 6 2 317.47 336.90 19.30 o 6 6 2 149.80 154.71 21.42 o 7 6 2 9.51 3.66 24.79 o 8 6 2 13.67 8.98 29.50 o -8 7 2 85.95 58.85 39.72 o -7 7 2 263.69 302.42 31.87 o -6 7 2 1096.82 1202.69 70.65 o -5 7 2 64.47 59.15 15.43 o -4 7 2 2265.85 2283.83 58.40 o -3 7 2 19.77 44.61 10.88 o -2 7 2 1214.49 1259.96 38.69 o -1 7 2 217.87 242.07 14.77 o 0 7 2 48.48 58.46 12.52 o 1 7 2 201.65 240.22 12.71 o 2 7 2 1498.17 1559.17 43.95 o 3 7 2 14.48 18.39 10.76 o 4 7 2 1985.45 1925.51 53.00 o 5 7 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