#------------------------------------------------------------------------------ #$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $ #$Revision: 717 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221258.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221258_Fobs loop_ _publ_author_name 'Benali-Cherif, Nourredine' 'Allouche, Fatima' 'Direm, Amani' 'Soudani, Kawther' _publ_section_title ; Hydrogen bonding in 2-carboxyanilinium dihydrogen phosphite at 100K ; _journal_coeditor_code BG2238 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o664 _journal_page_last o665 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.929 _cell_angle_beta 76.058 _cell_angle_gamma 86.814 _cell_length_a 4.8757 _cell_length_b 9.4597 _cell_length_c 10.0801 _exptl_crystal_F_000 228.00 _reflns_d_resolution_high 0.7107 _[local]_cod_data_source_file bg2238Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Final in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 136.08 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 35.80 37.67 0.45 o 2 0 0 3704.95 4232.55 32.88 o 3 0 0 650.52 643.05 5.32 o 4 0 0 0.09 0.94 0.64 o 5 0 0 86.12 90.49 2.44 o 6 0 0 70.63 73.75 2.15 o -6 1 0 87.53 95.02 2.31 o -5 1 0 4.90 5.00 1.35 o -4 1 0 390.59 391.99 4.28 o -3 1 0 110.61 116.69 1.20 o -2 1 0 0.17 -0.06 1.03 o -1 1 0 12.66 20.46 0.43 o 1 1 0 1258.93 1365.19 9.77 o 2 1 0 9.43 11.20 0.41 o 3 1 0 1007.18 1080.87 8.79 o 4 1 0 29.78 24.33 0.73 o 5 1 0 8.05 5.84 1.14 o 6 1 0 15.16 16.80 2.27 o -6 2 0 32.92 29.95 2.68 o -5 2 0 77.60 77.62 1.78 o -4 2 0 13.26 9.91 0.76 o -3 2 0 1079.48 1090.52 9.62 o -2 2 0 371.64 433.91 3.52 o -1 2 0 982.12 1028.91 8.30 o 0 2 0 2258.07 2677.56 24.98 o 1 2 0 100.34 92.44 1.04 o 2 2 0 0.32 1.40 0.35 o 3 2 0 336.87 347.72 2.98 o 4 2 0 5.66 5.18 0.58 o 5 2 0 59.73 54.05 2.10 o 6 2 0 36.36 29.68 1.92 o -6 3 0 78.93 76.75 3.43 o -5 3 0 21.33 18.47 1.45 o -4 3 0 824.22 837.44 11.16 o -3 3 0 47.59 37.93 0.82 o -2 3 0 520.47 557.18 4.55 o -1 3 0 9.71 7.88 0.43 o 0 3 0 1298.30 1337.38 11.81 o 1 3 0 34.53 24.06 0.46 o 2 3 0 20.94 24.08 0.47 o 3 3 0 89.57 93.44 1.05 o 4 3 0 125.33 126.78 1.49 o 5 3 0 31.87 25.52 0.98 o 6 3 0 26.88 26.44 2.10 o -6 4 0 83.21 81.29 5.50 o -5 4 0 72.89 67.29 2.71 o -4 4 0 108.33 107.43 2.82 o -3 4 0 155.29 153.13 2.03 o -2 4 0 460.22 418.59 3.63 o -1 4 0 841.66 902.67 7.46 o 0 4 0 1165.58 1364.95 12.71 o 1 4 0 474.05 479.36 4.14 o 2 4 0 102.90 118.04 1.20 o 3 4 0 252.10 247.05 2.27 o 4 4 0 71.74 70.22 1.07 o 5 4 0 8.30 5.71 0.92 o 6 4 0 12.36 12.49 2.45 o -6 5 0 14.55 16.92 2.05 o -5 5 0 285.85 303.17 4.47 o -4 5 0 0.63 1.51 1.05 o -3 5 0 246.51 245.06 3.68 o -2 5 0 7.06 6.79 0.57 o -1 5 0 15.55 20.51 0.63 o 0 5 0 4.60 4.68 0.51 o 1 5 0 1.00 0.47 0.55 o 2 5 0 226.31 243.17 2.39 o 3 5 0 192.52 187.38 1.82 o 4 5 0 19.21 15.94 0.88 o 5 5 0 40.59 35.75 1.38 o -5 6 0 40.32 41.35 2.13 o -4 6 0 391.86 413.15 6.53 o -3 6 0 46.73 41.82 1.23 o -2 6 0 756.03 801.02 7.22 o -1 6 0 259.91 259.72 4.52 o 0 6 0 419.95 464.94 4.97 o 1 6 0 629.54 622.28 5.89 o 2 6 0 1.41 2.53 0.61 o 3 6 0 214.82 217.21 2.39 o 4 6 0 81.30 81.66 1.46 o 5 6 0 3.63 2.93 1.10 o -5 7 0 154.27 163.85 4.71 o -4 7 0 14.56 14.20 1.34 o -3 7 0 108.47 112.70 2.04 o -2 7 0 0.00 0.80 0.70 o -1 7 0 51.38 53.46 1.03 o 0 7 0 95.47 87.85 2.12 o 1 7 0 21.85 26.23 1.70 o 2 7 0 185.44 176.05 3.11 o 3 7 0 21.83 18.17 0.96 o 4 7 0 101.09 100.16 1.78 o 5 7 0 2.65 1.05 1.33 o -5 8 0 65.19 56.68 3.16 o -4 8 0 4.83 4.25 1.57 o -3 8 0 132.08 125.42 3.61 o -2 8 0 2.81 2.00 0.73 o -1 8 0 66.85 60.29 1.44 o 0 8 0 1.34 0.23 0.82 o 1 8 0 35.59 29.32 1.42 o 2 8 0 3.07 3.24 1.16 o 3 8 0 72.57 68.20 2.61 o 4 8 0 18.18 15.53 2.38 o 5 8 0 15.28 12.51 2.58 o -4 9 0 3.86 1.71 1.77 o -3 9 0 8.99 4.13 1.49 o -2 9 0 138.79 122.37 1.54 o -1 9 0 68.63 67.31 1.55 o 0 9 0 2.96 1.53 1.02 o 1 9 0 2.24 1.96 1.11 o 2 9 0 371.82 379.56 5.65 o 3 9 0 7.31 5.84 1.45 o 4 9 0 102.71 91.59 2.81 o -4 10 0 6.13 3.39 2.04 o -3 10 0 3.65 4.87 1.64 o -2 10 0 2.39 2.27 1.03 o -1 10 0 105.74 110.19 3.57 o 0 10 0 77.31 76.16 1.58 o 1 10 0 768.00 805.00 12.88 o 2 10 0 71.62 74.39 1.98 o 3 10 0 36.07 27.64 4.13 o 4 10 0 66.80 68.08 4.73 o -3 11 0 110.29 124.76 4.90 o -2 11 0 103.41 97.75 1.67 o -1 11 0 76.89 73.56 2.88 o 0 11 0 26.84 28.39 1.69 o 1 11 0 139.42 140.02 5.63 o 2 11 0 5.45 5.25 1.58 o 3 11 0 43.57 44.65 2.18 o -2 12 0 43.74 38.99 5.96 o -1 12 0 147.84 159.44 3.14 o 0 12 0 1.62 0.73 1.85 o 1 12 0 273.75 280.60 4.78 o 2 12 0 124.50 134.88 5.88 o 0 13 0 124.54 136.30 3.48 o -2 -12 1 110.35 114.91 2.79 o -1 -12 1 36.79 35.02 2.77 o 0 -12 1 76.82 83.11 2.57 o 1 -12 1 9.61 10.56 1.91 o 2 -12 1 1.43 1.02 2.13 o -3 -11 1 0.02 -1.21 3.72 o -2 -11 1 0.01 1.06 1.79 o -1 -11 1 80.37 83.70 1.93 o 0 -11 1 40.77 42.79 1.64 o 1 -11 1 315.28 334.03 6.91 o 2 -11 1 184.09 198.52 5.25 o 3 -11 1 136.54 141.43 9.15 o -4 -10 1 9.55 12.18 2.41 o -3 -10 1 50.59 49.78 2.25 o -2 -10 1 125.75 132.06 3.39 o -1 -10 1 80.29 69.68 2.49 o 0 -10 1 14.56 15.55 1.24 o 1 -10 1 17.64 15.77 1.43 o 2 -10 1 69.71 70.36 2.08 o 3 -10 1 59.85 63.94 2.70 o 4 -10 1 75.70 69.59 2.89 o -4 -9 1 40.37 35.33 3.53 o -3 -9 1 47.74 47.84 3.51 o -2 -9 1 138.93 134.00 3.26 o -1 -9 1 7.05 4.86 1.18 o 0 -9 1 351.66 354.54 4.18 o 1 -9 1 0.06 0.30 0.99 o 2 -9 1 146.78 124.42 2.06 o 3 -9 1 0.02 0.72 1.59 o 4 -9 1 5.40 2.45 1.73 o -5 -8 1 1.35 2.63 1.68 o -4 -8 1 29.21 27.81 1.57 o -3 -8 1 212.79 211.93 3.38 o -2 -8 1 0.79 0.41 1.19 o -1 -8 1 712.82 719.52 8.92 o 0 -8 1 0.88 0.44 0.93 o 1 -8 1 33.78 27.67 0.90 o 2 -8 1 36.69 39.12 1.77 o 3 -8 1 2.03 3.56 1.87 o 4 -8 1 2.34 0.45 1.51 o 5 -8 1 118.20 124.67 3.22 o -5 -7 1 243.42 253.34 4.45 o -4 -7 1 36.90 31.16 1.32 o -3 -7 1 110.44 105.32 1.92 o -2 -7 1 61.23 54.03 1.66 o -1 -7 1 110.27 105.76 3.92 o 0 -7 1 1126.99 1130.17 11.24 o 1 -7 1 0.11 0.39 0.74 o 2 -7 1 712.03 653.54 7.34 o 3 -7 1 127.93 132.54 1.92 o 4 -7 1 1.01 1.45 1.35 o 5 -7 1 128.60 132.39 2.57 o -5 -6 1 0.09 -0.57 3.26 o -4 -6 1 1409.61 1504.93 20.26 o -3 -6 1 110.82 104.17 1.75 o -2 -6 1 808.99 803.41 7.94 o -1 -6 1 201.83 198.99 2.53 o 0 -6 1 4.65 1.65 0.66 o 1 -6 1 26.29 25.24 0.63 o 2 -6 1 115.21 110.97 2.30 o 3 -6 1 32.86 24.96 0.76 o 4 -6 1 120.59 123.34 2.11 o 5 -6 1 97.40 114.04 2.91 o -6 -5 1 1.57 1.88 2.65 o -5 -5 1 29.86 24.54 1.26 o -4 -5 1 83.69 83.64 1.47 o -3 -5 1 158.54 147.94 1.67 o -2 -5 1 3.79 2.43 0.56 o -1 -5 1 807.79 853.29 7.49 o 0 -5 1 65.70 64.00 1.17 o 1 -5 1 243.10 293.51 2.74 o 2 -5 1 44.06 34.82 0.76 o 3 -5 1 313.28 307.63 3.42 o 4 -5 1 85.44 75.71 1.67 o 5 -5 1 63.74 62.95 1.74 o 6 -5 1 100.80 110.62 2.69 o -6 -4 1 69.82 68.24 2.97 o -5 -4 1 38.83 33.08 1.33 o -4 -4 1 487.95 501.80 4.63 o -3 -4 1 40.02 39.92 0.81 o -2 -4 1 78.14 78.02 1.04 o -1 -4 1 230.91 222.88 2.62 o 0 -4 1 0.47 0.78 0.52 o 1 -4 1 432.59 439.18 5.29 o 2 -4 1 227.91 242.23 2.40 o 3 -4 1 551.08 565.93 5.09 o 4 -4 1 789.70 790.34 12.49 o 5 -4 1 11.42 11.58 1.56 o 6 -4 1 232.34 252.63 7.31 o -6 -3 1 150.92 151.61 5.04 o -5 -3 1 68.30 60.57 1.45 o -4 -3 1 412.33 417.97 4.63 o -3 -3 1 1.19 0.55 0.48 o -2 -3 1 51.60 47.52 0.74 o -1 -3 1 60.08 43.96 0.80 o 0 -3 1 5.83 3.01 0.36 o 1 -3 1 1127.01 1318.89 10.68 o 2 -3 1 17.63 14.19 0.51 o 3 -3 1 0.01 0.52 0.53 o 4 -3 1 0.72 0.58 0.84 o 5 -3 1 1.67 0.09 1.34 o 6 -3 1 46.03 46.20 2.33 o -6 -2 1 8.49 8.58 1.85 o -5 -2 1 216.08 211.96 3.53 o -4 -2 1 110.95 109.33 1.50 o -3 -2 1 99.94 84.37 1.11 o -2 -2 1 20.89 16.67 0.46 o -1 -2 1 987.58 957.36 7.20 o 0 -2 1 196.37 198.96 1.82 o 1 -2 1 2.06 3.45 0.33 o 2 -2 1 21.31 31.47 0.53 o 3 -2 1 518.97 517.52 4.51 o 4 -2 1 574.44 555.59 6.99 o 5 -2 1 135.70 142.03 2.33 o 6 -2 1 47.89 49.86 2.10 o -6 -1 1 11.85 11.59 2.58 o -5 -1 1 14.55 11.70 1.06 o -4 -1 1 78.02 73.06 0.99 o -3 -1 1 3.09 2.62 0.49 o -2 -1 1 552.31 617.00 5.38 o -1 -1 1 474.29 408.92 3.32 o 0 -1 1 845.46 943.92 7.50 o 1 -1 1 940.86 994.85 8.28 o 2 -1 1 97.23 103.36 1.06 o 3 -1 1 783.20 778.15 6.54 o 4 -1 1 5.88 5.98 0.99 o 5 -1 1 15.95 11.56 1.19 o 6 -1 1 138.81 143.16 2.72 o -6 0 1 204.38 205.90 5.78 o -5 0 1 150.27 148.40 2.73 o -4 0 1 257.40 251.97 3.02 o -3 0 1 537.00 523.63 5.01 o -2 0 1 266.87 275.84 2.48 o -1 0 1 1915.72 2113.22 16.18 o 1 0 1 875.26 943.92 7.64 o 2 0 1 2669.41 3071.57 24.18 o 3 0 1 135.92 131.02 1.73 o 4 0 1 287.41 296.40 2.92 o 5 0 1 10.00 10.35 1.38 o 6 0 1 31.24 24.32 2.10 o -6 1 1 0.03 -0.47 3.78 o -5 1 1 22.64 21.81 1.47 o -4 1 1 1.96 2.58 0.72 o -3 1 1 0.56 0.30 0.49 o -2 1 1 40.99 51.79 0.72 o -1 1 1 81.87 115.23 1.23 o 0 1 1 316.17 334.47 3.19 o 1 1 1 167.80 184.90 1.51 o 2 1 1 31.46 25.92 0.53 o 3 1 1 32.96 24.39 0.68 o 4 1 1 147.64 150.08 1.53 o 5 1 1 0.64 0.07 0.97 o 6 1 1 44.42 45.10 1.86 o -6 2 1 6.93 6.71 1.76 o -5 2 1 67.03 63.31 3.69 o -4 2 1 30.70 24.99 0.85 o -3 2 1 422.15 453.54 4.16 o -2 2 1 48.28 65.56 0.75 o -1 2 1 1202.43 1300.61 9.74 o 0 2 1 290.92 299.00 2.69 o 1 2 1 117.15 144.49 1.26 o 2 2 1 498.52 480.86 3.80 o 3 2 1 12.93 13.38 0.46 o 4 2 1 129.04 125.54 1.34 o 5 2 1 149.50 152.82 2.63 o 6 2 1 44.60 45.76 2.31 o -6 3 1 66.64 70.79 4.04 o -5 3 1 62.99 57.91 1.68 o -4 3 1 23.30 19.12 0.79 o -3 3 1 98.77 87.67 1.13 o -2 3 1 1015.88 1036.23 8.53 o -1 3 1 215.44 214.74 1.93 o 0 3 1 745.40 768.61 7.61 o 1 3 1 198.89 230.61 2.53 o 2 3 1 47.53 39.35 0.57 o 3 3 1 275.32 281.54 2.99 o 4 3 1 24.97 26.90 0.89 o 5 3 1 3.68 3.90 1.03 o 6 3 1 2.23 1.14 1.76 o -6 4 1 19.45 18.96 2.13 o -5 4 1 94.51 99.07 3.37 o -4 4 1 35.67 37.70 1.25 o -3 4 1 882.92 844.86 7.83 o -2 4 1 647.35 655.35 5.33 o -1 4 1 387.17 478.20 4.47 o 0 4 1 646.53 739.77 6.18 o 1 4 1 164.67 154.08 1.62 o 2 4 1 9.72 9.92 0.45 o 3 4 1 87.70 86.65 1.49 o 4 4 1 7.27 6.06 0.63 o 5 4 1 0.59 -0.11 2.75 o 6 4 1 108.06 113.20 2.45 o -6 5 1 34.60 35.03 3.32 o -5 5 1 115.67 124.63 3.00 o -4 5 1 8.63 7.58 1.25 o -3 5 1 29.57 32.41 0.80 o -2 5 1 22.63 22.66 0.69 o -1 5 1 114.05 111.96 1.59 o 0 5 1 258.77 319.64 3.65 o 1 5 1 17.57 18.97 0.59 o 2 5 1 119.40 116.94 2.04 o 3 5 1 9.07 7.12 0.55 o 4 5 1 29.64 26.14 0.71 o 5 5 1 218.70 221.61 2.37 o 6 5 1 10.17 6.37 3.00 o -5 6 1 235.13 251.78 5.07 o -4 6 1 100.08 102.04 1.87 o -3 6 1 780.30 772.35 7.72 o -2 6 1 1244.60 1281.12 12.24 o -1 6 1 64.78 81.07 1.32 o 0 6 1 704.44 758.72 8.35 o 1 6 1 266.83 255.88 3.11 o 2 6 1 101.96 97.57 1.59 o 3 6 1 205.40 205.94 2.62 o 4 6 1 4.61 4.31 0.76 o 5 6 1 308.30 323.58 4.02 o -5 7 1 9.51 10.77 1.90 o -4 7 1 28.53 25.03 2.03 o -3 7 1 0.02 0.99 0.84 o -2 7 1 122.36 117.52 1.81 o -1 7 1 125.33 117.20 2.32 o 0 7 1 31.75 43.52 1.26 o 1 7 1 108.53 107.95 1.73 o 2 7 1 770.11 796.09 9.15 o 3 7 1 1.11 -0.20 2.18 o 4 7 1 206.86 208.59 3.38 o 5 7 1 112.65 114.04 4.08 o -5 8 1 139.23 156.43 5.21 o -4 8 1 36.80 39.22 2.35 o -3 8 1 35.42 33.52 1.18 o -2 8 1 64.86 51.55 0.92 o -1 8 1 0.20 0.93 0.88 o 0 8 1 11.26 10.97 0.82 o 1 8 1 63.53 55.33 1.70 o 2 8 1 1.44 0.35 0.90 o 3 8 1 326.17 319.43 5.07 o 4 8 1 2.41 0.41 1.45 o 5 8 1 626.19 680.63 13.69 o -4 9 1 49.41 44.95 4.08 o -3 9 1 0.35 0.04 0.98 o -2 9 1 101.53 100.48 1.65 o -1 9 1 351.97 320.95 6.87 o 0 9 1 0.75 0.44 0.93 o 1 9 1 578.43 579.92 10.28 o 2 9 1 112.98 110.83 2.83 o 3 9 1 2.76 1.77 1.28 o 4 9 1 86.57 94.79 2.09 o 5 9 1 54.19 45.70 3.58 o -4 10 1 109.97 131.65 4.97 o -3 10 1 13.70 11.68 2.30 o -2 10 1 15.11 15.68 1.70 o -1 10 1 26.67 28.52 1.36 o 0 10 1 4.10 4.48 1.23 o 1 10 1 29.60 31.42 1.45 o 2 10 1 281.52 290.64 5.17 o 3 10 1 29.85 28.67 1.84 o 4 10 1 146.96 150.02 3.44 o -3 11 1 20.83 23.63 3.25 o -2 11 1 14.28 14.44 1.78 o -1 11 1 88.04 75.79 2.39 o 0 11 1 11.73 8.67 1.68 o 1 11 1 336.01 363.09 6.32 o 2 11 1 4.71 3.75 1.94 o 3 11 1 95.26 93.83 2.95 o -2 12 1 84.40 83.39 2.05 o -1 12 1 118.78 126.93 4.26 o 0 12 1 0.48 1.26 2.11 o 1 12 1 47.60 53.34 2.23 o 2 12 1 209.92 222.70 4.62 o -1 13 1 78.67 84.41 4.82 o 0 13 1 328.66 377.58 7.46 o 1 13 1 2.11 3.58 3.20 o -1 -12 2 0.31 -0.29 4.26 o 0 -12 2 43.83 45.69 1.96 o 1 -12 2 150.09 160.71 4.71 o 2 -12 2 55.05 54.82 3.06 o -2 -11 2 32.18 29.54 2.51 o -1 -11 2 147.94 155.51 2.60 o 0 -11 2 21.25 16.62 2.25 o 1 -11 2 223.31 243.06 4.62 o 2 -11 2 92.54 95.34 2.70 o 3 -11 2 82.97 84.48 3.16 o -3 -10 2 88.30 86.84 2.75 o -2 -10 2 5.43 2.56 1.66 o -1 -10 2 74.72 75.48 1.80 o 0 -10 2 384.91 402.13 5.50 o 1 -10 2 6.24 6.30 1.31 o 2 -10 2 217.07 221.39 3.31 o 3 -10 2 133.05 135.16 2.73 o 4 -10 2 9.07 7.58 2.31 o -4 -9 2 1.24 0.17 1.44 o -3 -9 2 75.92 65.50 6.19 o -2 -9 2 14.75 16.41 1.44 o -1 -9 2 3.62 2.90 1.17 o 0 -9 2 104.94 102.72 1.68 o 1 -9 2 6.87 4.55 0.99 o 2 -9 2 91.18 84.97 3.67 o 3 -9 2 13.35 8.65 1.55 o 4 -9 2 40.08 45.07 2.09 o -4 -8 2 70.59 69.56 2.09 o -3 -8 2 88.70 83.90 2.11 o -2 -8 2 10.61 7.74 1.06 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118.71 135.70 4.14 o -1 3 12 0.15 1.79 1.34 o 0 3 12 10.82 10.64 1.19 o 1 3 12 136.05 140.33 2.80 o 2 3 12 12.60 9.86 1.53 o 3 3 12 179.55 186.24 3.97 o 4 3 12 111.79 118.30 4.06 o -2 4 12 0.33 0.63 1.64 o -1 4 12 64.70 68.38 1.95 o 0 4 12 0.12 -0.33 3.45 o 1 4 12 313.56 328.88 4.02 o 2 4 12 0.51 -0.30 3.10 o 3 4 12 19.06 17.52 2.20 o 4 4 12 39.64 36.36 2.03 o -1 5 12 0.03 -0.55 3.76 o 0 5 12 33.03 31.70 1.64 o 1 5 12 191.20 194.22 3.94 o 2 5 12 211.17 211.14 4.52 o 3 5 12 27.02 24.16 2.43 o 4 5 12 64.89 60.34 2.90 o -1 6 12 0.53 0.64 1.26 o 0 6 12 43.39 45.55 1.44 o 1 6 12 108.31 110.36 1.78 o 2 6 12 4.46 5.72 1.62 o 3 6 12 82.87 85.47 3.09 o 4 6 12 83.81 84.99 3.76 o -1 7 12 82.47 83.44 2.34 o 0 7 12 61.37 64.16 1.62 o 1 7 12 39.59 39.34 1.46 o 2 7 12 146.43 145.37 2.59 o 3 7 12 6.68 6.99 1.55 o 0 8 12 202.36 206.90 2.79 o 1 8 12 35.22 37.62 1.57 o 2 8 12 27.43 28.51 1.53 o 3 8 12 3.63 3.67 1.65 o 1 9 12 166.91 172.47 3.48 o 2 9 12 24.84 28.89 1.78 o 1 -2 13 0.99 2.12 1.92 o 2 -2 13 68.26 78.41 2.81 o 0 -1 13 33.27 34.90 3.00 o 1 -1 13 11.66 12.95 2.08 o 2 -1 13 6.73 4.76 1.83 o 3 -1 13 0.49 -0.25 4.33 o 0 0 13 74.02 76.91 2.00 o 1 0 13 164.49 173.38 7.41 o 2 0 13 36.72 40.52 2.30 o 3 0 13 0.05 0.08 1.81 o -1 1 13 1.48 -0.17 4.55 o 0 1 13 206.28 229.88 3.69 o 1 1 13 23.23 24.42 3.52 o 2 1 13 5.31 4.36 1.77 o 3 1 13 37.17 37.18 2.07 o 4 1 13 5.47 5.24 2.31 o -1 2 13 7.60 8.13 1.62 o 0 2 13 0.30 0.51 1.38 o 1 2 13 17.36 14.40 2.08 o 2 2 13 0.28 1.47 1.66 o 3 2 13 8.76 10.30 1.80 o 4 2 13 79.26 78.91 4.73 o -1 3 13 1.10 0.34 1.51 o 0 3 13 194.90 206.72 4.98 o 1 3 13 49.33 55.04 2.00 o 2 3 13 3.62 3.74 1.53 o 3 3 13 28.58 28.38 2.23 o 4 3 13 33.44 34.06 2.49 o -1 4 13 40.22 40.03 1.84 o 0 4 13 23.46 24.12 1.57 o 1 4 13 4.06 3.10 1.29 o 2 4 13 7.67 6.36 1.64 o 3 4 13 57.21 55.45 2.52 o 4 4 13 20.35 18.77 2.42 o 0 5 13 15.36 12.76 1.48 o 1 5 13 16.18 15.24 1.44 o 2 5 13 15.74 14.34 1.79 o 3 5 13 31.78 33.32 2.03 o 0 6 13 29.32 28.04 1.61 o 1 6 13 5.62 4.33 1.35 o 2 6 13 6.04 4.39 1.73 o 3 6 13 59.56 65.01 3.76 o 1 7 13 146.09 149.96 3.02 o 2 7 13 21.96 14.76 2.27 o 1 1 14 52.61 53.25 2.75 o 2 1 14 46.23 50.17 2.32 o 1 2 14 9.32 9.06 2.30 o 2 2 14 0.60 1.92 2.16 o 1 3 14 0.44 1.14 2.05 o 2 3 14 65.05 58.87 2.73 o 1 4 14 0.35 0.46 2.68 o 2 4 14 25.76 25.71 2.23 o