#------------------------------------------------------------------------------ #$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $ #$Revision: 717 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221392.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221392_Fobs loop_ _publ_author_name 'Sharif, Shahzad' 'Tahir, M. Nawaz' 'Khan, Islam Ullah' 'Ahmad, Sarfraz' 'Salariya, Manan Ayub' _publ_section_title ; Methyl 2-(2-amino-1,3-thiazol-4-yl)-2-[(Z)-methoxycarbonylmethoxyimino]ethanoate ; _journal_coeditor_code HK2639 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o713 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 120.016 _cell_angle_gamma 90.000 _cell_length_a 12.2395 _cell_length_b 5.7500 _cell_length_c 19.8865 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.8351 _[local]_cod_data_source_file hk2639Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SHEHZAD3_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 157.18 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 232.70 173.50 10.94 o 3 0 0 17822.27 17549.59 341.55 o 4 0 0 91.88 88.70 14.45 o 5 0 0 7448.37 7668.18 212.31 o 6 0 0 717.76 758.47 47.34 o 7 0 0 13.39 -18.24 18.24 o 8 0 0 288.41 296.78 36.94 o 9 0 0 821.32 811.75 67.03 o 10 0 0 0.06 -19.82 30.37 o 11 0 0 100.81 54.97 37.88 o 12 0 0 56.87 110.96 47.74 o 1 1 0 427.98 463.88 9.36 o 2 1 0 1867.81 1828.09 28.47 o 3 1 0 6.42 4.38 6.57 o 4 1 0 2419.77 2553.41 46.45 o 5 1 0 0.33 -7.67 8.63 o 6 1 0 209.29 181.15 16.00 o 7 1 0 44.89 12.99 13.67 o 8 1 0 119.65 108.35 18.42 o 9 1 0 144.35 118.94 21.22 o 10 1 0 23.23 19.55 19.48 o 11 1 0 34.75 37.89 22.44 o 12 1 0 21.46 4.68 32.94 o 0 2 0 2095.05 2105.61 124.57 o 1 2 0 526.45 523.89 24.31 o 2 2 0 1141.20 1169.29 23.92 o 3 2 0 2606.75 2424.82 44.67 o 4 2 0 357.63 359.79 16.84 o 5 2 0 184.82 177.69 13.62 o 6 2 0 245.24 268.88 23.59 o 7 2 0 294.22 302.50 20.86 o 8 2 0 204.96 203.43 21.64 o 9 2 0 227.87 197.60 24.73 o 10 2 0 163.30 202.53 29.81 o 11 2 0 14.36 8.81 23.49 o 12 2 0 25.38 131.70 47.84 o 1 3 0 120.03 141.31 13.17 o 2 3 0 327.20 343.37 12.84 o 3 3 0 78.66 84.97 9.59 o 4 3 0 452.91 517.35 19.07 o 5 3 0 28.45 32.40 9.91 o 6 3 0 191.74 184.31 15.49 o 7 3 0 0.50 1.26 12.33 o 8 3 0 0.80 -5.46 17.49 o 9 3 0 44.69 49.52 30.38 o 10 3 0 19.62 55.80 28.76 o 11 3 0 135.28 149.02 36.44 o 0 4 0 421.50 475.17 71.17 o 1 4 0 598.13 553.36 25.07 o 2 4 0 117.04 120.59 22.09 o 3 4 0 408.65 412.48 15.38 o 4 4 0 131.39 101.64 12.03 o 5 4 0 102.52 111.92 17.06 o 6 4 0 56.60 57.62 21.21 o 7 4 0 29.63 22.66 23.43 o 8 4 0 28.04 48.07 29.42 o 9 4 0 98.73 75.81 28.50 o 10 4 0 241.68 276.89 42.15 o 1 5 0 0.02 4.00 20.22 o 2 5 0 2.71 -6.75 13.59 o 3 5 0 112.59 62.71 28.08 o 4 5 0 179.99 160.40 20.40 o 5 5 0 56.63 53.91 30.10 o 6 5 0 15.08 -6.23 18.71 o 7 5 0 135.17 173.02 27.93 o 8 5 0 18.65 33.96 26.58 o 0 6 0 1.14 13.09 54.67 o 1 6 0 176.32 101.01 45.04 o 2 6 0 164.22 175.37 29.97 o 3 6 0 52.87 10.44 26.08 o 4 6 0 7.29 9.47 22.28 o 5 6 0 11.12 -4.12 16.23 o 6 6 0 23.88 -4.53 18.86 o -12 1 1 18.51 14.00 32.39 o -11 1 1 160.64 157.12 26.26 o -10 1 1 42.40 7.82 17.31 o -9 1 1 93.03 118.20 20.93 o -8 1 1 1134.09 1074.57 54.15 o -7 1 1 0.04 -11.94 11.94 o -6 1 1 1660.14 1726.14 45.80 o -5 1 1 2087.58 2106.62 42.50 o -4 1 1 43.74 46.73 9.24 o -3 1 1 6818.47 6406.87 88.97 o -2 1 1 1608.29 1508.71 25.12 o -1 1 1 1.22 3.49 2.91 o 0 1 1 17667.18 17163.74 261.39 o 1 1 1 41.10 43.42 4.19 o 2 1 1 16.31 4.46 5.25 o 3 1 1 753.54 699.89 18.18 o 4 1 1 69.37 55.84 10.74 o 5 1 1 203.37 187.80 15.39 o 6 1 1 372.57 348.01 23.54 o 7 1 1 240.99 252.87 21.30 o 8 1 1 448.49 447.65 43.95 o 9 1 1 745.61 814.21 41.14 o 10 1 1 2.26 -18.73 18.73 o 11 1 1 130.58 122.47 48.50 o 12 1 1 36.25 2.07 32.71 o -12 2 1 0.11 -2.76 24.91 o -11 2 1 17.26 37.35 24.54 o -10 2 1 10.48 -11.98 19.80 o -9 2 1 177.73 194.02 23.82 o -8 2 1 0.97 15.00 15.21 o -7 2 1 121.69 90.15 14.71 o -6 2 1 874.94 822.32 27.17 o -5 2 1 2.61 0.98 8.39 o -4 2 1 58.28 51.01 11.27 o -3 2 1 53.67 63.34 9.01 o -2 2 1 171.86 177.99 8.74 o -1 2 1 3025.51 2973.02 65.88 o 0 2 1 0.06 -1.66 7.12 o 1 2 1 3563.76 3505.47 57.56 o 2 2 1 1372.85 1466.51 27.02 o 3 2 1 1455.58 1526.11 32.10 o 4 2 1 23.62 9.22 8.22 o 5 2 1 392.48 420.28 20.66 o 6 2 1 839.74 862.62 31.86 o 7 2 1 94.14 81.84 15.46 o 8 2 1 390.83 393.75 28.65 o 9 2 1 4.90 -8.26 17.18 o 10 2 1 26.71 6.84 24.78 o 11 2 1 40.74 102.33 35.64 o -11 3 1 71.95 32.95 28.89 o -10 3 1 252.07 256.63 38.53 o -9 3 1 293.59 236.91 33.22 o -8 3 1 538.85 567.77 33.73 o -7 3 1 3.54 -5.91 10.90 o -6 3 1 1338.74 1332.71 36.39 o -5 3 1 574.32 603.92 21.10 o -4 3 1 7.68 10.81 7.14 o -3 3 1 2715.11 2627.96 51.13 o -2 3 1 460.95 461.05 30.06 o -1 3 1 1681.68 1593.51 45.79 o 0 3 1 1.20 10.37 18.59 o 1 3 1 616.31 657.64 27.02 o 2 3 1 305.49 294.41 12.52 o 3 3 1 24.73 11.43 8.27 o 4 3 1 371.28 322.88 15.16 o 5 3 1 47.56 57.33 11.43 o 6 3 1 0.49 -7.46 10.68 o 7 3 1 305.84 318.19 29.95 o 8 3 1 32.83 46.41 21.06 o 9 3 1 4.20 -3.23 25.00 o 10 3 1 365.97 469.96 64.04 o 11 3 1 38.10 89.30 35.70 o -10 4 1 2.88 47.56 30.80 o -9 4 1 3.94 18.98 25.66 o -8 4 1 186.75 105.24 26.79 o -7 4 1 141.67 148.15 25.03 o -6 4 1 6.41 21.56 27.35 o -5 4 1 0.04 -7.92 11.14 o -4 4 1 0.15 -5.53 8.55 o -3 4 1 716.98 726.64 23.53 o -2 4 1 226.15 234.48 46.13 o -1 4 1 0.03 11.96 11.37 o 0 4 1 226.70 258.02 24.49 o 1 4 1 1.35 -11.59 13.48 o 2 4 1 34.88 46.32 14.14 o 3 4 1 0.34 -7.54 7.54 o 4 4 1 13.52 5.79 9.91 o 5 4 1 0.12 16.59 17.28 o 6 4 1 5.63 -15.77 16.80 o 7 4 1 0.72 6.60 25.05 o 8 4 1 6.66 -0.94 23.98 o 9 4 1 10.51 -3.87 24.86 o 10 4 1 0.45 20.08 29.51 o -9 5 1 2.02 3.40 26.26 o -8 5 1 57.29 35.57 25.48 o -7 5 1 15.91 24.39 20.50 o -6 5 1 21.82 30.15 18.93 o -5 5 1 44.51 43.69 18.08 o -4 5 1 214.19 203.23 41.57 o -3 5 1 388.32 346.36 37.65 o -2 5 1 38.85 44.98 14.67 o -1 5 1 68.26 117.55 39.24 o 0 5 1 98.82 147.04 40.28 o 1 5 1 413.08 380.72 24.32 o 2 5 1 154.79 69.30 35.18 o 3 5 1 80.51 91.49 30.04 o 4 5 1 489.77 447.39 37.68 o 5 5 1 0.80 5.69 17.23 o 6 5 1 49.27 -1.59 22.01 o 7 5 1 199.74 169.03 32.17 o 8 5 1 0.08 3.39 24.57 o -6 6 1 1.06 8.06 18.21 o -5 6 1 83.09 53.72 18.24 o -4 6 1 109.69 84.45 27.73 o -3 6 1 3.88 -13.02 22.94 o -2 6 1 0.62 -15.86 19.82 o -1 6 1 58.01 -1.62 38.14 o 0 6 1 10.26 -16.67 34.32 o 1 6 1 29.26 69.55 42.74 o 2 6 1 7.88 12.53 37.43 o 3 6 1 0.51 52.60 32.15 o 4 6 1 84.67 70.33 28.97 o 5 6 1 33.47 23.04 19.94 o -13 0 2 33.68 79.76 46.47 o -12 0 2 92.22 156.53 47.59 o -11 0 2 677.60 715.08 103.59 o -10 0 2 355.74 386.05 51.36 o -9 0 2 161.45 191.93 38.60 o -8 0 2 236.94 206.10 31.50 o -7 0 2 143.73 122.04 25.39 o -6 0 2 806.32 846.25 66.08 o -5 0 2 2611.04 2842.70 80.50 o -4 0 2 454.86 490.55 27.08 o -3 0 2 1478.23 1774.03 40.10 o -2 0 2 28.00 13.44 7.05 o -1 0 2 20.28 15.21 10.39 o 1 0 2 530.39 549.44 30.70 o 2 0 2 14.72 25.07 22.54 o 3 0 2 84.48 71.14 14.04 o 4 0 2 1315.98 1368.81 99.27 o 5 0 2 188.17 285.38 29.11 o 6 0 2 133.55 129.41 26.45 o 7 0 2 204.27 183.58 24.10 o 8 0 2 733.27 634.25 39.79 o 9 0 2 1240.16 1218.67 94.32 o 10 0 2 0.84 39.31 45.73 o 11 0 2 74.70 112.40 46.27 o 12 0 2 10.20 -38.61 38.61 o -13 1 2 28.37 84.98 38.27 o -12 1 2 6.63 22.03 26.26 o -11 1 2 93.57 97.49 23.69 o -10 1 2 1.30 -1.38 17.38 o -9 1 2 370.36 306.95 31.94 o -8 1 2 33.81 29.77 16.17 o -7 1 2 506.30 548.70 29.70 o -6 1 2 131.55 144.70 15.79 o -5 1 2 146.18 170.47 13.05 o -4 1 2 175.68 171.25 11.89 o -3 1 2 1007.87 976.26 19.48 o -2 1 2 153.75 129.80 9.50 o -1 1 2 1827.11 1760.81 24.85 o 0 1 2 40.09 51.88 4.18 o 1 1 2 1.71 -0.87 3.00 o 2 1 2 2227.15 2311.55 33.08 o 3 1 2 1640.77 1713.38 31.22 o 4 1 2 49.90 59.03 11.66 o 5 1 2 68.11 79.89 12.52 o 6 1 2 44.63 22.75 12.98 o 7 1 2 241.62 266.52 31.25 o 8 1 2 913.92 892.75 40.33 o 9 1 2 4.77 -9.89 16.23 o 10 1 2 1.15 -15.05 24.09 o 11 1 2 22.55 15.97 32.76 o -12 2 2 0.38 22.89 25.19 o -11 2 2 149.46 155.08 34.83 o -10 2 2 74.45 71.31 20.97 o -9 2 2 1447.13 1462.55 55.17 o -8 2 2 1525.99 1489.61 45.63 o -7 2 2 13.04 25.06 12.11 o -6 2 2 2338.84 2364.48 60.89 o -5 2 2 0.90 7.51 8.26 o -4 2 2 377.50 452.86 24.08 o -3 2 2 1967.65 1961.64 39.92 o -2 2 2 6.81 -7.08 7.08 o -1 2 2 385.52 382.71 13.28 o 0 2 2 6346.14 6505.85 101.75 o 1 2 2 565.73 547.74 15.17 o 2 2 2 34.91 18.90 6.78 o 3 2 2 3015.61 2828.29 55.44 o 4 2 2 612.22 567.88 21.58 o 5 2 2 426.35 466.33 29.16 o 6 2 2 1024.10 1048.11 36.15 o 7 2 2 291.59 307.56 29.39 o 8 2 2 402.46 433.29 31.19 o 9 2 2 75.35 62.78 23.26 o 10 2 2 100.89 100.22 27.24 o 11 2 2 158.85 162.30 60.37 o -11 3 2 0.02 -14.66 25.33 o -10 3 2 7.59 -7.44 23.19 o -9 3 2 58.63 66.06 21.48 o -8 3 2 5.61 -6.41 15.87 o -7 3 2 6.42 -7.37 9.15 o -6 3 2 0.06 -8.06 12.57 o -5 3 2 1.29 1.88 8.34 o -4 3 2 52.75 42.59 8.28 o -3 3 2 247.39 255.77 12.43 o -2 3 2 2.50 -14.05 14.05 o -1 3 2 14.82 19.68 8.01 o 0 3 2 402.51 387.21 20.07 o 1 3 2 216.66 191.25 20.27 o 2 3 2 385.79 405.15 13.65 o 3 3 2 10.81 9.89 7.38 o 4 3 2 23.14 24.24 8.86 o 5 3 2 90.17 86.72 13.09 o 6 3 2 15.03 6.39 12.75 o 7 3 2 2.16 12.23 17.92 o 8 3 2 6.09 -3.83 18.99 o 9 3 2 49.80 43.37 27.04 o 10 3 2 82.41 70.62 32.36 o -10 4 2 33.67 -8.37 32.88 o -9 4 2 24.41 10.59 23.89 o -8 4 2 68.70 86.60 24.77 o -7 4 2 307.52 285.89 35.00 o -6 4 2 12.75 21.30 17.13 o -5 4 2 0.78 5.41 9.98 o -4 4 2 0.09 -1.07 7.87 o -3 4 2 2.49 14.51 8.54 o -2 4 2 437.69 418.28 22.36 o -1 4 2 205.38 225.78 24.57 o 0 4 2 50.23 46.30 11.90 o 1 4 2 226.83 232.97 19.97 o 2 4 2 196.81 197.23 18.55 o 3 4 2 34.09 28.90 9.58 o 4 4 2 556.36 557.10 24.52 o 5 4 2 30.21 12.16 18.82 o 6 4 2 64.78 110.04 26.48 o 7 4 2 0.22 18.03 23.15 o 8 4 2 108.89 112.00 30.84 o 9 4 2 15.09 11.87 27.86 o -9 5 2 2.47 2.67 25.16 o -8 5 2 271.49 270.38 32.77 o -7 5 2 333.05 349.22 35.71 o -6 5 2 0.84 6.51 19.35 o -5 5 2 26.89 30.49 16.86 o -4 5 2 102.64 120.13 20.73 o -3 5 2 229.63 236.54 28.02 o -2 5 2 350.40 257.89 56.78 o -1 5 2 90.50 53.71 33.84 o 0 5 2 197.92 196.26 21.98 o 1 5 2 115.41 167.47 19.78 o 2 5 2 31.98 28.27 21.18 o 3 5 2 195.22 236.62 20.40 o 4 5 2 21.19 0.10 19.93 o 5 5 2 55.38 74.91 22.52 o 6 5 2 29.26 63.86 31.16 o 7 5 2 47.27 62.03 32.57 o 8 5 2 62.32 95.61 29.18 o -6 6 2 0.36 21.70 18.11 o -5 6 2 4.60 6.84 16.06 o -4 6 2 210.29 224.95 28.98 o -3 6 2 26.08 -3.77 62.37 o -2 6 2 8.67 26.58 51.59 o -1 6 2 3.80 0.48 49.41 o 0 6 2 2.60 57.46 41.65 o 1 6 2 316.62 289.74 56.07 o 2 6 2 49.56 88.05 48.93 o 3 6 2 24.65 18.42 51.49 o 4 6 2 221.18 210.24 46.01 o 5 6 2 2.39 15.08 19.42 o -13 1 3 17.33 -3.30 26.31 o -12 1 3 10.79 38.55 22.22 o -11 1 3 86.01 104.96 24.20 o -10 1 3 190.33 168.37 31.03 o -9 1 3 212.88 248.53 25.38 o -8 1 3 0.05 -4.81 14.14 o -7 1 3 61.37 89.30 16.10 o -6 1 3 112.29 150.16 21.24 o -5 1 3 112.60 116.00 11.92 o -4 1 3 513.24 504.89 16.24 o -3 1 3 8443.70 8290.22 108.10 o -2 1 3 1578.70 1418.28 22.27 o -1 1 3 1.36 0.37 4.64 o 0 1 3 6796.65 6575.41 84.87 o 1 1 3 2385.23 2561.69 34.12 o 2 1 3 1.37 3.29 5.76 o 3 1 3 1241.65 1208.61 26.62 o 4 1 3 1367.31 1288.72 31.95 o 5 1 3 1259.04 1236.58 32.52 o 6 1 3 95.27 58.73 15.10 o 7 1 3 17.10 14.10 13.69 o 8 1 3 1189.30 1106.82 45.54 o 9 1 3 317.16 328.23 34.00 o 10 1 3 23.96 9.52 26.01 o 11 1 3 160.24 201.88 45.04 o -12 2 3 8.89 36.63 26.17 o -11 2 3 315.81 300.89 35.65 o -10 2 3 54.85 68.55 20.33 o -9 2 3 779.76 762.16 35.00 o -8 2 3 58.14 88.54 16.83 o -7 2 3 311.47 333.90 19.89 o -6 2 3 367.88 337.48 22.36 o -5 2 3 3.84 4.71 8.42 o -4 2 3 640.52 669.82 20.95 o -3 2 3 785.03 765.19 23.53 o -2 2 3 324.05 328.84 9.53 o -1 2 3 319.63 333.12 11.40 o 0 2 3 277.23 312.19 11.18 o 1 2 3 922.81 961.60 20.23 o 2 2 3 916.91 912.69 25.08 o 3 2 3 25.04 22.64 6.64 o 4 2 3 214.64 208.50 15.48 o 5 2 3 35.84 58.05 13.14 o 6 2 3 17.72 30.89 13.27 o 7 2 3 12.87 15.32 15.63 o 8 2 3 112.42 99.37 25.45 o 9 2 3 12.10 14.54 21.03 o 10 2 3 55.82 16.42 30.00 o 11 2 3 7.51 48.81 49.14 o -12 3 3 30.63 56.54 32.43 o -11 3 3 88.79 87.28 31.57 o -10 3 3 81.75 84.12 26.38 o -9 3 3 134.37 115.80 24.17 o -8 3 3 166.94 186.93 20.08 o -7 3 3 485.52 481.03 23.93 o -6 3 3 183.47 161.26 14.14 o -5 3 3 674.74 704.06 27.04 o -4 3 3 22.48 17.93 7.48 o -3 3 3 18.53 28.84 7.68 o -2 3 3 1797.22 1634.01 44.93 o -1 3 3 245.37 248.39 12.11 o 0 3 3 1880.72 1857.35 51.66 o 1 3 3 1023.39 1020.85 29.00 o 2 3 3 313.01 297.22 13.89 o 3 3 3 943.04 934.72 29.88 o 4 3 3 8.29 -6.12 9.22 o 5 3 3 12.49 8.30 10.97 o 6 3 3 502.13 498.08 34.17 o 7 3 3 168.10 148.47 29.09 o 8 3 3 67.92 37.62 29.91 o 9 3 3 18.29 -30.03 30.63 o 10 3 3 0.14 -51.39 60.92 o -11 4 3 9.54 -19.48 27.96 o -10 4 3 17.76 27.57 25.14 o -9 4 3 1.44 -20.47 20.47 o -8 4 3 338.68 335.49 38.23 o -7 4 3 171.60 141.44 24.15 o -6 4 3 3.81 -4.81 15.34 o -5 4 3 349.93 332.15 17.29 o -4 4 3 0.16 1.85 8.02 o -3 4 3 357.59 354.86 18.12 o -2 4 3 261.19 312.12 14.83 o -1 4 3 0.01 -10.32 10.32 o 0 4 3 533.60 555.02 34.83 o 1 4 3 460.42 451.18 36.96 o 2 4 3 92.83 82.65 13.05 o 3 4 3 148.29 148.72 13.79 o 4 4 3 0.33 4.49 13.95 o 5 4 3 6.83 -0.81 18.38 o 6 4 3 108.93 103.14 26.88 o 7 4 3 164.81 122.45 28.59 o 8 4 3 0.45 25.50 24.82 o 9 4 3 0.80 3.12 27.89 o -9 5 3 14.59 44.84 25.28 o -8 5 3 21.59 5.52 22.05 o -7 5 3 285.61 243.42 29.49 o -6 5 3 2.15 -0.69 17.02 o -5 5 3 32.65 -5.16 19.86 o -4 5 3 418.27 432.54 38.09 o -3 5 3 0.02 2.93 9.92 o -2 5 3 424.87 424.06 49.01 o -1 5 3 329.42 368.83 61.83 o 0 5 3 18.88 1.02 14.17 o 1 5 3 549.98 520.04 39.96 o 2 5 3 21.80 15.56 21.53 o 3 5 3 4.23 -7.38 15.30 o 4 5 3 285.42 251.99 28.51 o 5 5 3 0.86 8.25 20.38 o 6 5 3 34.56 12.44 24.96 o 7 5 3 8.91 30.02 26.03 o -6 6 3 38.82 39.22 20.83 o -5 6 3 0.00 4.84 25.35 o -4 6 3 17.32 27.36 21.62 o -3 6 3 2.14 6.23 17.97 o -2 6 3 66.32 92.48 34.13 o -1 6 3 0.55 18.42 32.57 o 0 6 3 0.37 10.97 21.23 o 1 6 3 340.42 379.79 38.86 o 2 6 3 2.30 -17.78 26.52 o 3 6 3 12.44 0.18 31.38 o 4 6 3 104.24 73.04 20.10 o 5 6 3 14.37 -2.02 19.93 o -13 0 4 23.76 42.89 40.30 o -12 0 4 389.04 443.19 116.74 o -11 0 4 5.43 9.84 32.78 o -10 0 4 544.32 545.26 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