#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:01:46 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181135 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/14/2221417.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221417_Fobs loop_ _publ_author_name 'Akriche, Samah' 'Rzaigui, Mohamed' _publ_section_title ; 2-Amino-3-nitropyridinium hydrogen oxalate ; _journal_coeditor_code KJ2116 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o793 _journal_volume 65 _journal_year 2009 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.2683 _cell_length_b 6.9205 _cell_length_c 8.8067 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7583 _cod_data_source_file kj2116Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cad4 in P c 21 n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -11 0.86 3.27 2.08 o 4 0 -11 6.49 4.97 2.57 o 6 0 -11 28.30 34.01 3.28 o 0 1 -11 23.29 30.08 2.10 o 1 1 -11 35.29 44.56 5.37 o 2 1 -11 15.47 15.93 1.85 o 3 1 -11 2.78 0.32 2.38 o 4 1 -11 0.23 -1.32 2.10 o 5 1 -11 15.09 17.34 1.92 o 6 1 -11 13.55 17.40 3.64 o 1 2 -11 4.67 7.06 1.65 o 2 2 -11 4.86 7.46 2.94 o 3 2 -11 2.74 2.13 1.87 o 4 2 -11 14.01 18.86 1.90 o 0 0 -10 11.08 7.93 1.94 o 2 0 -10 19.01 19.65 2.38 o 4 0 -10 36.66 33.43 2.67 o 6 0 -10 50.26 56.48 3.27 o 8 0 -10 51.92 56.46 3.43 o 10 0 -10 20.31 21.16 2.88 o 1 1 -10 4.16 5.37 2.62 o 2 1 -10 0.13 1.80 1.60 o 3 1 -10 3.06 1.67 1.59 o 4 1 -10 18.15 18.92 1.79 o 5 1 -10 0.99 2.65 2.01 o 6 1 -10 13.00 12.84 1.68 o 7 1 -10 68.69 76.12 2.74 o 8 1 -10 26.10 33.39 2.11 o 9 1 -10 8.94 8.76 1.74 o 10 1 -10 14.58 15.29 2.81 o 0 2 -10 11.36 11.63 1.66 o 1 2 -10 0.11 1.15 1.97 o 2 2 -10 18.71 23.43 5.74 o 3 2 -10 3.91 3.06 1.86 o 4 2 -10 12.98 13.41 1.67 o 5 2 -10 21.39 18.81 3.41 o 6 2 -10 5.98 3.21 1.89 o 7 2 -10 59.42 65.73 4.87 o 8 2 -10 12.49 11.97 1.94 o 9 2 -10 16.95 20.64 4.36 o 1 3 -10 20.43 17.96 2.13 o 2 3 -10 3.86 0.81 2.18 o 3 3 -10 16.45 15.86 1.74 o 4 3 -10 2.61 1.08 2.11 o 5 3 -10 37.11 34.93 3.01 o 6 3 -10 9.88 10.02 1.82 o 7 3 -10 0.08 2.40 2.55 o 0 4 -10 20.02 25.95 3.12 o 1 4 -10 1.76 0.65 1.76 o 2 4 -10 7.60 7.85 1.88 o 3 4 -10 3.48 3.56 3.14 o 4 4 -10 0.74 -1.29 2.40 o 5 4 -10 1.81 4.01 1.97 o 2 0 -9 67.85 65.39 3.10 o 4 0 -9 137.67 147.19 4.43 o 6 0 -9 61.03 61.64 3.22 o 8 0 -9 119.55 126.32 4.28 o 10 0 -9 86.45 93.65 4.13 o 12 0 -9 47.87 53.47 3.63 o 0 1 -9 129.61 130.49 2.85 o 1 1 -9 26.02 24.08 2.85 o 2 1 -9 16.59 15.14 2.40 o 3 1 -9 118.78 105.23 5.42 o 4 1 -9 79.63 77.16 2.67 o 5 1 -9 26.01 25.76 1.79 o 6 1 -9 40.73 39.37 2.87 o 7 1 -9 28.55 25.91 2.14 o 8 1 -9 27.55 29.54 1.91 o 9 1 -9 70.21 72.04 2.64 o 10 1 -9 15.15 15.76 1.94 o 11 1 -9 0.88 1.38 2.56 o 12 1 -9 8.14 7.63 1.77 o 1 2 -9 57.62 53.98 2.10 o 2 2 -9 31.87 27.14 2.45 o 3 2 -9 50.89 51.78 3.30 o 4 2 -9 8.47 9.65 1.41 o 5 2 -9 26.34 27.28 2.19 o 6 2 -9 12.82 14.11 1.58 o 7 2 -9 29.02 31.95 2.01 o 8 2 -9 20.11 21.03 1.88 o 9 2 -9 41.46 50.01 2.31 o 10 2 -9 1.83 0.39 1.87 o 11 2 -9 11.54 15.00 1.89 o 0 3 -9 55.27 55.14 2.21 o 1 3 -9 10.83 11.54 1.45 o 2 3 -9 25.85 25.33 1.79 o 3 3 -9 8.06 8.79 1.49 o 4 3 -9 19.70 18.51 1.68 o 5 3 -9 3.27 -1.34 2.22 o 6 3 -9 13.92 15.62 2.44 o 7 3 -9 10.91 11.37 1.75 o 8 3 -9 36.29 40.81 2.19 o 9 3 -9 18.96 18.81 2.82 o 10 3 -9 15.38 19.84 2.01 o 1 4 -9 24.61 26.36 2.43 o 2 4 -9 5.16 4.38 1.57 o 3 4 -9 24.78 22.88 1.96 o 4 4 -9 9.84 8.52 3.95 o 5 4 -9 5.23 6.14 1.59 o 6 4 -9 7.01 8.98 1.75 o 7 4 -9 6.61 7.19 1.71 o 8 4 -9 1.69 -2.30 2.52 o 9 4 -9 9.92 10.04 1.93 o 0 5 -9 16.25 14.33 2.03 o 1 5 -9 7.72 6.63 1.77 o 2 5 -9 1.79 2.47 1.51 o 3 5 -9 5.70 5.02 3.06 o 4 5 -9 11.99 11.99 1.84 o 5 5 -9 25.40 24.16 2.34 o 6 5 -9 3.78 5.09 1.79 o 0 0 -8 356.82 339.85 5.57 o 2 0 -8 597.38 584.02 7.25 o 4 0 -8 169.33 152.56 4.03 o 6 0 -8 94.28 84.33 3.30 o 8 0 -8 82.42 81.35 3.38 o 10 0 -8 30.68 29.55 2.74 o 12 0 -8 12.00 9.83 2.53 o 14 0 -8 50.42 60.52 3.60 o 1 1 -8 49.05 42.40 1.74 o 2 1 -8 108.82 106.63 2.44 o 3 1 -8 271.80 255.95 4.13 o 4 1 -8 72.26 65.82 2.70 o 5 1 -8 263.75 253.92 3.69 o 6 1 -8 19.75 19.56 1.49 o 7 1 -8 21.42 22.75 1.50 o 8 1 -8 13.45 13.98 1.57 o 9 1 -8 5.51 6.87 1.83 o 10 1 -8 39.48 37.73 2.09 o 11 1 -8 42.50 43.99 2.19 o 12 1 -8 16.44 22.07 1.81 o 13 1 -8 28.67 30.20 2.19 o 14 1 -8 1.07 3.84 1.80 o 0 2 -8 206.85 192.69 3.19 o 1 2 -8 0.42 1.23 2.13 o 2 2 -8 84.64 86.49 2.32 o 3 2 -8 317.13 324.05 4.12 o 4 2 -8 10.25 11.50 1.41 o 5 2 -8 153.47 141.70 3.00 o 6 2 -8 12.00 12.98 2.03 o 7 2 -8 65.27 63.73 5.30 o 8 2 -8 10.09 12.06 1.52 o 9 2 -8 28.66 34.93 2.07 o 10 2 -8 0.38 -1.56 2.08 o 11 2 -8 59.26 59.27 2.45 o 12 2 -8 8.04 7.79 1.69 o 13 2 -8 15.96 20.67 1.99 o 1 3 -8 93.21 90.25 3.32 o 2 3 -8 135.50 128.16 2.86 o 3 3 -8 76.41 73.49 2.37 o 4 3 -8 117.82 112.86 2.79 o 5 3 -8 31.19 31.77 1.81 o 6 3 -8 38.74 42.01 1.96 o 7 3 -8 13.58 15.32 1.79 o 8 3 -8 11.92 10.39 1.62 o 9 3 -8 8.90 11.77 1.50 o 10 3 -8 6.96 6.98 1.96 o 11 3 -8 2.52 4.34 1.89 o 12 3 -8 0.38 -1.92 3.32 o 13 3 -8 14.46 16.29 1.98 o 0 4 -8 0.30 1.03 1.27 o 1 4 -8 16.34 16.52 1.60 o 2 4 -8 30.93 30.50 1.83 o 3 4 -8 63.59 58.85 4.04 o 4 4 -8 65.54 63.66 2.87 o 5 4 -8 14.55 13.10 1.72 o 6 4 -8 31.26 32.49 2.74 o 7 4 -8 13.27 11.50 1.71 o 8 4 -8 23.60 22.16 2.93 o 9 4 -8 3.83 2.67 1.57 o 10 4 -8 7.15 5.93 1.70 o 11 4 -8 10.64 10.43 1.83 o 1 5 -8 34.81 34.36 2.10 o 2 5 -8 16.85 13.48 1.87 o 3 5 -8 42.45 39.82 2.21 o 4 5 -8 2.95 5.20 1.65 o 5 5 -8 13.50 8.94 1.79 o 6 5 -8 2.72 4.64 1.78 o 7 5 -8 6.57 2.22 4.57 o 8 5 -8 6.99 6.85 1.75 o 9 5 -8 3.09 1.69 1.88 o 0 6 -8 15.33 14.71 1.89 o 1 6 -8 5.74 4.47 1.65 o 2 6 -8 8.74 7.16 1.69 o 3 6 -8 8.98 6.75 3.46 o 4 6 -8 12.04 8.52 1.94 o 5 6 -8 8.80 10.27 1.78 o 6 6 -8 14.45 14.47 2.04 o 2 0 -7 170.63 157.91 3.52 o 4 0 -7 1092.00 1069.44 11.31 o 6 0 -7 329.32 308.50 5.29 o 8 0 -7 229.98 227.78 4.84 o 10 0 -7 265.45 281.28 5.74 o 12 0 -7 60.16 56.29 3.11 o 14 0 -7 3.91 5.79 2.32 o 16 0 -7 0.90 6.39 2.32 o 0 1 -7 2.13 1.92 1.57 o 1 1 -7 129.70 117.91 2.30 o 2 1 -7 73.57 71.34 1.90 o 3 1 -7 238.05 234.40 3.16 o 4 1 -7 491.97 465.15 4.45 o 5 1 -7 397.49 372.32 6.55 o 6 1 -7 33.24 29.11 1.54 o 7 1 -7 60.18 55.93 1.94 o 8 1 -7 14.90 17.32 3.65 o 9 1 -7 8.98 11.97 1.34 o 10 1 -7 28.68 31.91 1.77 o 11 1 -7 52.60 48.24 2.08 o 12 1 -7 13.09 11.16 1.56 o 13 1 -7 80.24 85.23 3.12 o 14 1 -7 2.84 1.92 1.83 o 15 1 -7 18.85 19.50 1.97 o 1 2 -7 137.80 138.52 2.60 o 2 2 -7 8.68 9.36 1.15 o 3 2 -7 466.11 439.20 5.43 o 4 2 -7 12.73 13.69 1.39 o 5 2 -7 299.22 308.21 4.99 o 6 2 -7 143.50 135.18 2.72 o 7 2 -7 26.56 27.24 1.63 o 8 2 -7 40.31 39.54 3.77 o 9 2 -7 93.77 94.88 2.52 o 10 2 -7 0.51 3.27 1.52 o 11 2 -7 54.02 52.20 2.20 o 12 2 -7 32.64 30.36 2.00 o 13 2 -7 3.27 4.90 2.36 o 14 2 -7 14.72 14.38 1.92 o 15 2 -7 0.52 0.69 2.78 o 0 3 -7 248.67 235.78 3.39 o 1 3 -7 22.61 21.10 2.64 o 2 3 -7 109.15 112.17 4.53 o 3 3 -7 73.94 75.36 2.21 o 4 3 -7 282.17 275.76 3.80 o 5 3 -7 6.46 5.84 1.34 o 6 3 -7 65.66 61.44 2.14 o 7 3 -7 85.69 84.38 2.40 o 8 3 -7 71.48 68.51 2.29 o 9 3 -7 81.02 81.72 3.80 o 10 3 -7 50.06 52.45 2.31 o 11 3 -7 3.23 0.25 2.22 o 12 3 -7 14.97 10.82 1.82 o 13 3 -7 2.08 0.53 2.35 o 14 3 -7 34.40 39.36 2.30 o 1 4 -7 56.85 52.55 2.01 o 2 4 -7 72.50 68.39 2.22 o 3 4 -7 29.12 25.66 1.74 o 4 4 -7 224.53 214.03 3.65 o 5 4 -7 114.17 113.60 2.87 o 6 4 -7 0.09 1.59 2.80 o 7 4 -7 0.31 0.61 1.94 o 8 4 -7 19.52 18.99 1.81 o 9 4 -7 2.38 4.31 1.39 o 10 4 -7 76.02 77.14 2.70 o 11 4 -7 5.43 6.11 2.80 o 12 4 -7 8.64 10.71 2.59 o 13 4 -7 21.75 23.43 2.09 o 0 5 -7 23.92 22.81 1.70 o 1 5 -7 55.56 52.83 2.22 o 2 5 -7 18.76 19.03 1.71 o 3 5 -7 72.92 74.97 4.49 o 4 5 -7 3.45 4.44 2.23 o 5 5 -7 105.70 106.18 2.93 o 6 5 -7 0.34 -0.72 2.05 o 7 5 -7 5.67 5.31 1.56 o 8 5 -7 7.16 3.23 1.98 o 9 5 -7 0.40 -1.21 2.77 o 10 5 -7 16.60 16.36 1.93 o 11 5 -7 10.30 13.96 3.35 o 1 6 -7 15.14 14.90 1.80 o 2 6 -7 0.25 1.03 2.11 o 3 6 -7 68.91 64.05 2.63 o 4 6 -7 30.72 27.96 2.34 o 5 6 -7 1.24 2.09 1.85 o 6 6 -7 9.19 9.44 2.20 o 7 6 -7 8.59 6.90 2.85 o 8 6 -7 0.85 1.55 1.78 o 9 6 -7 2.11 -1.09 3.22 o 0 7 -7 41.13 40.01 2.42 o 1 7 -7 4.96 5.87 1.74 o 2 7 -7 9.70 10.79 1.83 o 3 7 -7 6.25 5.87 1.80 o 4 7 -7 20.45 21.49 2.24 o 0 0 -6 1529.83 1500.81 13.62 o 2 0 -6 719.39 735.88 7.42 o 4 0 -6 157.00 172.32 3.51 o 6 0 -6 71.88 63.30 2.44 o 8 0 -6 181.02 176.78 3.99 o 10 0 -6 311.67 317.90 5.66 o 12 0 -6 46.94 45.85 2.78 o 14 0 -6 63.58 64.01 3.27 o 16 0 -6 42.43 45.48 3.28 o 1 1 -6 120.52 123.17 2.11 o 2 1 -6 165.83 169.56 2.91 o 3 1 -6 165.42 162.00 2.40 o 4 1 -6 41.78 40.00 2.70 o 5 1 -6 101.88 108.58 2.15 o 6 1 -6 1.15 2.09 1.07 o 7 1 -6 44.70 41.80 4.15 o 8 1 -6 0.30 0.17 1.46 o 9 1 -6 686.29 658.89 7.67 o 10 1 -6 338.92 336.00 4.19 o 11 1 -6 2.25 3.97 1.70 o 12 1 -6 29.03 30.68 1.71 o 13 1 -6 76.37 73.91 2.42 o 14 1 -6 15.10 13.58 1.58 o 15 1 -6 6.20 6.41 2.87 o 16 1 -6 30.05 33.62 2.73 o 17 1 -6 38.14 51.32 2.67 o 0 2 -6 75.00 76.04 1.84 o 1 2 -6 280.46 286.27 3.24 o 2 2 -6 139.82 134.05 2.26 o 3 2 -6 162.14 148.70 2.44 o 4 2 -6 71.99 67.64 1.81 o 5 2 -6 215.86 218.83 3.01 o 6 2 -6 33.92 36.51 1.55 o 7 2 -6 67.73 70.37 1.95 o 8 2 -6 5.13 8.20 1.39 o 9 2 -6 579.33 578.19 5.33 o 10 2 -6 20.48 20.40 2.14 o 11 2 -6 14.70 12.63 1.57 o 12 2 -6 0.85 -0.05 2.60 o 13 2 -6 4.86 2.43 2.44 o 14 2 -6 10.52 11.78 1.64 o 15 2 -6 56.90 59.98 2.59 o 16 2 -6 13.75 16.40 3.95 o 1 3 -6 8.54 7.32 1.13 o 2 3 -6 111.78 115.32 2.29 o 3 3 -6 45.99 46.98 1.62 o 4 3 -6 51.81 56.98 1.82 o 5 3 -6 107.66 100.11 2.32 o 6 3 -6 92.92 89.26 4.28 o 7 3 -6 22.81 24.01 2.06 o 8 3 -6 184.13 191.42 3.96 o 9 3 -6 0.18 1.50 1.70 o 10 3 -6 161.93 162.81 3.29 o 11 3 -6 46.37 45.20 2.03 o 12 3 -6 23.06 21.92 1.74 o 13 3 -6 2.32 -0.73 1.79 o 14 3 -6 1.69 2.12 3.37 o 15 3 -6 19.17 16.46 2.05 o 0 4 -6 1.13 2.59 2.07 o 1 4 -6 67.16 70.29 2.06 o 2 4 -6 201.13 201.21 3.19 o 3 4 -6 28.42 29.03 1.57 o 4 4 -6 2.01 2.15 1.41 o 5 4 -6 25.75 26.22 1.56 o 6 4 -6 28.36 31.31 1.63 o 7 4 -6 29.36 30.10 1.80 o 8 4 -6 57.42 53.07 3.30 o 9 4 -6 19.66 21.64 1.72 o 10 4 -6 43.83 49.10 3.34 o 11 4 -6 13.13 17.29 2.23 o 12 4 -6 21.43 24.10 1.95 o 13 4 -6 13.34 13.18 2.34 o 14 4 -6 0.42 1.67 2.27 o 1 5 -6 178.27 177.46 3.32 o 2 5 -6 5.63 6.92 1.60 o 3 5 -6 0.96 3.67 1.76 o 4 5 -6 20.44 19.38 1.69 o 5 5 -6 8.65 9.24 1.92 o 6 5 -6 4.76 4.25 2.79 o 7 5 -6 9.57 9.45 1.54 o 8 5 -6 33.94 35.78 2.51 o 9 5 -6 116.25 116.69 3.15 o 10 5 -6 4.40 2.33 2.26 o 11 5 -6 32.54 30.73 2.14 o 12 5 -6 2.15 0.78 1.98 o 13 5 -6 1.39 3.11 1.99 o 0 6 -6 22.55 21.72 1.79 o 1 6 -6 7.00 8.22 1.50 o 2 6 -6 42.68 43.87 2.12 o 3 6 -6 44.80 48.80 3.42 o 4 6 -6 9.72 8.97 1.59 o 5 6 -6 10.89 12.05 1.97 o 6 6 -6 9.39 10.24 1.73 o 7 6 -6 0.04 1.41 1.74 o 8 6 -6 8.04 10.49 2.64 o 9 6 -6 39.71 34.07 4.46 o 10 6 -6 15.64 9.97 2.08 o 11 6 -6 6.53 8.04 1.90 o 1 7 -6 7.31 6.29 3.01 o 2 7 -6 23.18 26.11 2.19 o 3 7 -6 0.81 2.57 1.77 o 4 7 -6 4.12 4.51 3.10 o 5 7 -6 6.10 3.60 4.31 o 6 7 -6 18.65 21.54 2.44 o 7 7 -6 4.63 4.75 2.14 o 2 0 -5 243.87 247.75 3.60 o 4 0 -5 15.54 21.38 1.52 o 6 0 -5 122.48 122.63 2.91 o 8 0 -5 869.76 878.96 8.76 o 10 0 -5 358.77 334.02 5.50 o 12 0 -5 0.56 0.36 1.50 o 14 0 -5 158.72 170.19 4.66 o 16 0 -5 79.18 78.75 3.82 o 18 0 -5 32.86 40.62 3.35 o 0 1 -5 865.65 896.64 5.89 o 1 1 -5 876.07 935.26 12.70 o 2 1 -5 202.67 199.23 2.35 o 3 1 -5 288.78 288.98 3.22 o 4 1 -5 315.61 318.06 3.05 o 5 1 -5 41.01 47.89 1.36 o 6 1 -5 144.42 139.85 2.21 o 7 1 -5 37.96 34.54 1.37 o 8 1 -5 165.31 144.02 2.45 o 9 1 -5 352.09 330.83 3.67 o 10 1 -5 61.28 67.30 2.43 o 11 1 -5 42.88 49.72 1.85 o 12 1 -5 1.92 2.65 1.55 o 13 1 -5 14.93 14.11 1.47 o 14 1 -5 37.01 40.07 2.80 o 15 1 -5 6.03 5.05 1.52 o 16 1 -5 23.74 24.56 1.90 o 17 1 -5 30.66 32.35 3.86 o 18 1 -5 11.80 12.31 1.94 o 1 2 -5 506.80 538.07 5.05 o 2 2 -5 149.97 139.78 2.34 o 3 2 -5 112.68 125.12 3.40 o 4 2 -5 392.10 390.98 6.54 o 5 2 -5 77.34 70.08 1.70 o 6 2 -5 76.57 80.32 1.86 o 7 2 -5 98.54 112.19 2.22 o 8 2 -5 23.83 25.23 1.35 o 9 2 -5 233.95 244.64 3.34 o 10 2 -5 60.77 60.11 1.98 o 11 2 -5 224.05 220.31 6.03 o 12 2 -5 0.96 1.59 2.16 o 13 2 -5 17.61 16.04 1.58 o 14 2 -5 7.53 5.50 1.52 o 15 2 -5 42.01 44.28 2.45 o 16 2 -5 9.26 10.50 2.57 o 17 2 -5 79.22 84.55 2.87 o 0 3 -5 276.87 301.42 3.24 o 1 3 -5 44.01 45.07 1.47 o 2 3 -5 199.07 192.54 3.37 o 3 3 -5 218.51 204.77 2.76 o 4 3 -5 109.46 107.86 4.07 o 5 3 -5 150.45 145.28 2.48 o 6 3 -5 49.61 51.93 1.74 o 7 3 -5 35.43 34.31 1.52 o 8 3 -5 261.53 248.75 3.47 o 9 3 -5 103.55 100.12 2.46 o 10 3 -5 74.84 75.81 3.07 o 11 3 -5 59.86 58.32 2.14 o 12 3 -5 9.68 8.68 1.56 o 13 3 -5 46.67 44.69 2.12 o 14 3 -5 18.31 16.40 2.55 o 15 3 -5 27.64 28.71 2.08 o 16 3 -5 31.04 33.70 4.07 o 1 4 -5 10.21 12.59 2.58 o 2 4 -5 81.36 80.21 1.96 o 3 4 -5 3.53 1.99 1.08 o 4 4 -5 123.69 120.84 2.47 o 5 4 -5 43.57 43.25 1.74 o 6 4 -5 150.86 150.80 2.83 o 7 4 -5 14.45 13.76 1.50 o 8 4 -5 206.35 210.43 3.42 o 9 4 -5 91.81 99.01 3.09 o 10 4 -5 137.10 138.60 3.10 o 11 4 -5 4.90 4.56 1.46 o 12 4 -5 11.40 11.96 2.26 o 13 4 -5 29.41 29.31 1.89 o 14 4 -5 10.02 10.38 1.67 o 15 4 -5 1.98 2.11 2.37 o 0 5 -5 20.37 18.93 1.45 o 1 5 -5 33.01 35.20 1.65 o 2 5 -5 3.93 4.27 1.24 o 3 5 -5 21.58 21.86 1.51 o 4 5 -5 17.49 16.95 1.49 o 5 5 -5 56.73 53.87 2.09 o 6 5 -5 86.34 83.05 2.49 o 7 5 -5 218.31 229.20 3.75 o 8 5 -5 12.17 12.51 1.62 o 9 5 -5 28.31 26.30 1.93 o 10 5 -5 3.03 2.51 2.40 o 11 5 -5 5.77 9.93 1.59 o 12 5 -5 0.28 0.75 1.76 o 13 5 -5 14.41 13.22 1.85 o 14 5 -5 1.32 3.74 1.91 o 1 6 -5 64.63 69.00 2.31 o 2 6 -5 1.36 1.47 2.10 o 3 6 -5 18.13 15.26 1.63 o 4 6 -5 8.25 6.74 1.56 o 5 6 -5 10.08 8.95 1.55 o 6 6 -5 23.56 25.21 1.85 o 7 6 -5 9.00 10.56 1.64 o 8 6 -5 5.46 6.79 1.62 o 9 6 -5 7.75 10.37 1.70 o 10 6 -5 27.77 25.39 2.59 o 11 6 -5 30.67 29.79 2.25 o 12 6 -5 13.21 13.03 3.18 o 0 7 -5 13.57 14.17 1.98 o 1 7 -5 6.49 4.19 1.65 o 2 7 -5 20.12 17.70 1.88 o 3 7 -5 1.61 0.58 2.19 o 4 7 -5 11.07 10.29 1.85 o 5 7 -5 2.13 1.66 1.78 o 6 7 -5 6.47 8.27 1.79 o 7 7 -5 25.47 22.20 5.53 o 8 7 -5 63.52 59.58 2.76 o 9 7 -5 0.56 2.50 1.87 o 1 8 -5 4.10 1.59 3.74 o 2 8 -5 2.39 1.85 3.17 o 3 8 -5 5.67 -1.06 3.70 o 4 8 -5 2.06 3.01 3.34 o 0 0 -4 708.15 743.94 6.53 o 2 0 -4 1315.65 1350.33 10.48 o 4 0 -4 305.15 321.65 3.84 o 6 0 -4 863.22 908.25 8.47 o 8 0 -4 108.44 97.84 2.68 o 10 0 -4 306.64 303.15 4.88 o 12 0 -4 149.54 140.42 3.89 o 14 0 -4 342.44 327.92 6.08 o 16 0 -4 259.04 261.26 5.87 o 18 0 -4 33.28 36.62 3.20 o 1 1 -4 90.96 98.61 2.13 o 2 1 -4 480.80 506.52 7.11 o 3 1 -4 696.05 734.67 4.92 o 4 1 -4 428.71 420.64 3.17 o 5 1 -4 225.41 244.83 4.15 o 6 1 -4 88.78 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1.37 o 18 1 -1 15.79 18.19 1.76 o 19 1 -1 26.70 30.00 2.17 o 1 2 -1 11140.28 14203.93 335.47 o 2 2 -1 377.23 417.10 3.01 o 3 2 -1 800.22 774.60 15.18 o 4 2 -1 1254.15 1314.31 46.25 o 5 2 -1 1566.76 1573.00 40.25 o 6 2 -1 549.07 556.02 15.99 o 7 2 -1 1024.30 983.76 15.61 o 8 2 -1 672.35 668.86 4.68 o 9 2 -1 274.27 290.52 5.19 o 10 2 -1 168.88 165.39 5.97 o 11 2 -1 151.48 142.50 2.68 o 12 2 -1 101.87 99.06 2.24 o 13 2 -1 602.30 567.98 12.77 o 14 2 -1 50.98 46.84 2.43 o 15 2 -1 69.69 67.59 2.26 o 16 2 -1 0.37 -1.80 2.02 o 17 2 -1 5.58 7.57 1.53 o 18 2 -1 0.04 3.19 1.39 o 19 2 -1 82.01 79.76 3.12 o 0 3 -1 2412.13 2646.98 15.02 o 1 3 -1 32.26 31.07 1.01 o 2 3 -1 351.20 385.60 3.86 o 3 3 -1 277.87 280.90 2.49 o 4 3 -1 413.76 414.22 3.48 o 5 3 -1 231.69 224.05 2.94 o 6 3 -1 236.54 251.69 9.06 o 7 3 -1 374.45 372.26 6.66 o 8 3 -1 143.04 153.77 2.35 o 9 3 -1 142.54 149.48 4.53 o 10 3 -1 337.87 336.33 10.98 o 11 3 -1 0.86 2.97 2.44 o 12 3 -1 93.13 95.02 5.11 o 13 3 -1 28.79 28.60 2.98 o 14 3 -1 64.53 61.82 2.18 o 15 3 -1 20.67 17.84 1.71 o 16 3 -1 4.92 4.59 1.52 o 17 3 -1 19.09 17.55 2.88 o 18 3 -1 26.83 27.30 2.14 o 1 4 -1 106.40 101.17 1.83 o 2 4 -1 449.20 498.86 13.52 o 3 4 -1 161.47 172.00 2.33 o 4 4 -1 74.40 76.10 1.70 o 5 4 -1 750.99 801.76 10.93 o 6 4 -1 27.65 32.30 2.18 o 7 4 -1 78.83 80.68 3.89 o 8 4 -1 106.07 104.80 2.16 o 9 4 -1 61.09 58.92 1.93 o 10 4 -1 80.04 84.32 3.07 o 11 4 -1 17.73 19.87 1.81 o 12 4 -1 250.16 253.81 9.13 o 13 4 -1 1.84 -0.68 1.89 o 14 4 -1 16.42 17.84 1.63 o 15 4 -1 41.54 44.02 2.32 o 16 4 -1 2.06 3.11 1.78 o 17 4 -1 23.03 22.56 1.99 o 18 4 -1 13.26 11.82 2.97 o 0 5 -1 71.12 66.35 3.17 o 1 5 -1 234.67 248.68 9.28 o 2 5 -1 79.07 82.91 1.93 o 3 5 -1 100.29 98.37 5.25 o 4 5 -1 20.07 21.51 1.28 o 5 5 -1 0.78 1.49 1.04 o 6 5 -1 4.11 1.16 1.55 o 7 5 -1 38.08 38.21 1.64 o 8 5 -1 92.73 90.62 2.35 o 9 5 -1 17.03 18.07 1.65 o 10 5 -1 27.58 27.27 3.24 o 11 5 -1 2.62 2.23 1.57 o 12 5 -1 14.14 14.45 1.59 o 13 5 -1 7.79 8.17 2.37 o 14 5 -1 0.24 -0.50 1.71 o 15 5 -1 30.61 28.04 4.51 o 16 5 -1 7.55 10.19 1.71 o 1 6 -1 76.95 81.43 2.24 o 2 6 -1 32.28 44.25 7.17 o 3 6 -1 32.34 28.22 2.49 o 4 6 -1 97.94 102.15 3.71 o 5 6 -1 0.76 -0.59 1.56 o 6 6 -1 4.87 3.67 2.06 o 7 6 -1 14.87 13.41 1.82 o 8 6 -1 65.40 62.23 2.22 o 9 6 -1 0.23 -2.03 2.03 o 10 6 -1 47.43 46.77 3.89 o 11 6 -1 46.18 46.67 3.47 o 12 6 -1 46.47 43.41 2.83 o 13 6 -1 51.53 52.46 2.47 o 14 6 -1 1.00 3.26 1.83 o 15 6 -1 3.90 5.29 3.89 o 0 7 -1 89.95 89.91 2.61 o 1 7 -1 16.10 15.33 2.19 o 2 7 -1 18.89 19.85 1.75 o 3 7 -1 29.99 28.81 3.46 o 4 7 -1 1.94 2.38 2.18 o 5 7 -1 5.07 3.76 2.28 o 6 7 -1 13.69 15.54 2.35 o 7 7 -1 5.30 2.12 1.79 o 8 7 -1 6.28 6.28 1.54 o 9 7 -1 8.61 13.86 3.03 o 10 7 -1 2.74 -3.12 3.22 o 11 7 -1 0.68 1.72 2.46 o 12 7 -1 0.50 2.10 1.92 o 1 8 -1 9.06 13.27 2.40 o 2 8 -1 42.72 41.82 3.39 o 3 8 -1 0.93 1.51 2.12 o 4 8 -1 6.53 13.12 2.32 o 5 8 -1 12.15 9.87 2.58 o 6 8 -1 10.73 10.25 2.58 o 7 8 -1 13.58 18.97 2.84 o 8 8 -1 19.92 15.48 2.98 o 9 8 -1 1.15 4.83 2.41 o 0 9 -1 5.41 7.82 2.55 o 1 9 -1 6.97 5.83 2.76 o 2 9 -1 10.03 12.69 2.64 o 2 0 0 1508.17 1263.61 5.45 o 4 0 0 3527.58 2728.09 11.47 o 6 0 0 2532.59 2064.87 11.91 o 8 0 0 253.04 231.54 3.29 o 10 0 0 88.63 80.49 2.31 o 12 0 0 197.67 181.53 3.81 o 14 0 0 613.13 595.97 7.42 o 16 0 0 6.05 7.31 1.90 o 18 0 0 0.26 0.70 1.92 o 20 0 0 8.20 7.37 2.59 o 1 1 0 118.36 136.66 2.69 o 2 1 0 113.30 98.81 2.23 o 3 1 0 13.42 18.51 0.56 o 4 1 0 4.86 6.15 0.46 o 5 1 0 864.54 831.44 13.26 o 6 1 0 141.80 144.04 1.63 o 7 1 0 3662.01 3444.92 33.91 o 8 1 0 727.97 729.55 9.85 o 9 1 0 0.71 -0.59 1.94 o 10 1 0 0.51 0.65 1.29 o 11 1 0 211.66 196.09 3.40 o 12 1 0 37.72 33.37 2.75 o 13 1 0 352.86 339.25 9.90 o 14 1 0 19.62 17.52 1.42 o 15 1 0 19.61 23.45 1.58 o 16 1 0 2.71 -0.91 1.83 o 17 1 0 6.35 8.05 1.75 o 18 1 0 0.41 0.51 2.08 o 19 1 0 36.78 44.64 2.26 o 20 1 0 1.71 3.38 1.96 o 0 2 0 4198.69 4542.06 42.50 o 1 2 0 22198.94 24429.42 101.21 o 2 2 0 60.33 70.35 6.50 o 3 2 0 5.17 6.02 0.59 o 4 2 0 92.09 122.05 4.76 o 5 2 0 283.74 286.97 8.52 o 6 2 0 367.76 399.97 13.51 o 7 2 0 0.01 1.64 0.62 o 8 2 0 1.37 3.60 0.73 o 9 2 0 4.53 4.65 0.83 o 10 2 0 2.19 2.17 1.39 o 11 2 0 82.21 74.86 1.83 o 12 2 0 1.82 4.27 1.07 o 13 2 0 15.85 13.24 1.75 o 14 2 0 0.06 1.71 1.41 o 15 2 0 138.91 142.42 2.94 o 16 2 0 13.08 11.22 1.54 o 17 2 0 4.09 6.13 1.30 o 18 2 0 62.83 60.30 2.58 o 19 2 0 0.47 -0.78 3.68 o 1 3 0 1142.76 1153.35 6.69 o 2 3 0 19.36 20.41 0.85 o 3 3 0 39.59 37.85 1.02 o 4 3 0 290.74 331.32 4.09 o 5 3 0 59.58 62.54 1.37 o 6 3 0 167.21 183.58 4.16 o 7 3 0 79.85 82.65 1.67 o 8 3 0 655.01 691.16 18.90 o 9 3 0 0.91 1.53 0.95 o 10 3 0 84.99 77.25 3.38 o 11 3 0 16.82 17.25 1.32 o 12 3 0 5.21 6.70 1.19 o 13 3 0 15.51 14.73 1.43 o 14 3 0 37.82 38.30 1.90 o 15 3 0 3.67 3.00 1.58 o 16 3 0 9.80 9.22 1.53 o 17 3 0 4.08 3.89 1.62 o 18 3 0 62.14 64.86 2.71 o 19 3 0 4.97 2.38 2.01 o 0 4 0 5746.86 6289.99 63.41 o 1 4 0 1462.47 1539.07 16.88 o 2 4 0 281.61 286.54 5.56 o 3 4 0 248.40 275.77 4.07 o 4 4 0 26.06 40.75 11.80 o 5 4 0 378.12 407.67 5.89 o 6 4 0 372.33 380.69 7.03 o 7 4 0 44.69 44.00 1.52 o 8 4 0 80.28 79.18 1.95 o 9 4 0 173.47 177.04 3.62 o 10 4 0 9.58 11.65 1.27 o 11 4 0 203.33 200.28 5.87 o 12 4 0 27.49 28.25 1.65 o 13 4 0 53.99 54.46 2.13 o 14 4 0 78.86 82.01 2.58 o 15 4 0 0.39 2.70 1.69 o 16 4 0 0.54 0.54 2.16 o 17 4 0 3.74 5.33 1.60 o 18 4 0 16.96 16.69 2.06 o 1 5 0 259.64 264.48 3.18 o 2 5 0 204.21 201.28 3.28 o 3 5 0 1.81 -0.81 1.29 o 4 5 0 59.72 61.87 2.93 o 5 5 0 30.79 32.19 1.46 o 6 5 0 7.56 8.64 1.11 o 7 5 0 136.41 145.52 5.06 o 8 5 0 3.33 2.49 1.64 o 9 5 0 119.56 127.31 4.42 o 10 5 0 25.95 27.08 1.67 o 11 5 0 2.56 2.21 1.36 o 12 5 0 8.17 7.32 1.50 o 13 5 0 2.54 4.51 1.41 o 14 5 0 0.04 0.38 2.06 o 15 5 0 0.40 -1.10 2.09 o 16 5 0 15.81 16.80 1.88 o 0 6 0 283.45 268.42 6.64 o 1 6 0 289.35 294.80 3.80 o 2 6 0 158.91 147.55 2.85 o 3 6 0 0.39 0.67 1.58 o 4 6 0 4.42 2.04 1.43 o 5 6 0 3.14 2.32 1.50 o 6 6 0 1.00 -1.67 2.95 o 7 6 0 63.12 60.88 2.28 o 8 6 0 42.59 45.49 2.04 o 9 6 0 91.40 90.35 2.76 o 10 6 0 26.88 29.97 2.38 o 11 6 0 44.29 46.87 4.19 o 12 6 0 1.16 3.40 1.55 o 13 6 0 7.25 9.20 1.66 o 14 6 0 0.05 -2.30 2.30 o 15 6 0 0.55 3.37 1.62 o 1 7 0 8.47 5.06 2.31 o 2 7 0 42.52 45.92 1.97 o 3 7 0 9.62 7.97 1.49 o 4 7 0 9.96 12.21 1.57 o 5 7 0 7.24 2.49 1.47 o 6 7 0 9.63 9.17 2.02 o 7 7 0 0.02 -2.05 2.05 o 8 7 0 13.86 14.30 1.76 o 9 7 0 16.61 18.17 4.42 o 10 7 0 10.62 13.39 3.32 o 11 7 0 12.95 15.48 2.11 o 12 7 0 0.35 2.02 2.47 o 0 8 0 55.10 53.32 3.55 o 1 8 0 77.44 57.86 3.80 o 2 8 0 0.54 3.08 2.12 o 3 8 0 0.77 0.23 3.06 o 4 8 0 5.70 6.81 2.26 o 5 8 0 0.03 -1.92 2.85 o 6 8 0 3.43 5.77 2.23 o 7 8 0 0.14 -1.01 3.30 o 8 8 0 0.00 -3.65 3.65 o 9 8 0 7.14 2.47 2.71 o 1 9 0 2.21 2.43 3.94 o 2 9 0 2.24 -2.44 3.61 o 3 9 0 16.00 15.19 2.89 o