#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/14/2221478.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221478_Fobs loop_ _publ_author_name 'Li, Ming' 'Wen, Wen' 'Ha, Wuzu' 'Chang, Liang' _publ_section_title ; Hydroxonium 1-ammonioethane-1,1-diyldiphosphonate ; _journal_coeditor_code RN2053 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o787 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.705 _cell_angle_gamma 90.000 _cell_length_a 7.3372 _cell_length_b 10.6553 _cell_length_c 10.6128 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file rn2053Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 160.60 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10066.75 10914.57 250.38 o 3 0 0 796.91 661.86 4.84 o 4 0 0 5991.19 5971.25 42.89 o 5 0 0 13327.18 12865.81 156.37 o 6 0 0 9.68 12.25 0.97 o 7 0 0 3795.86 3754.90 34.38 o 8 0 0 10.08 8.16 1.67 o 9 0 0 1806.59 1898.21 31.23 o 1 1 0 41.63 41.37 0.64 o 2 1 0 525.55 498.16 3.27 o 3 1 0 269.23 214.38 1.85 o 4 1 0 51.73 28.90 0.54 o 5 1 0 132.67 102.41 1.29 o 6 1 0 109.58 95.01 1.73 o 7 1 0 0.53 0.95 0.40 o 8 1 0 1.82 1.54 0.71 o 9 1 0 11.52 10.35 1.42 o 0 2 0 17263.59 15760.98 204.42 o 1 2 0 779.02 696.78 4.68 o 2 2 0 13004.91 12436.65 127.94 o 3 2 0 620.94 695.12 5.55 o 4 2 0 875.77 883.81 5.27 o 5 2 0 4080.34 3972.83 22.40 o 6 2 0 0.02 0.95 0.33 o 7 2 0 3013.05 2939.43 23.04 o 8 2 0 0.15 0.09 0.60 o 9 2 0 664.00 655.61 14.32 o 1 3 0 115.21 78.56 1.17 o 2 3 0 36.39 23.75 0.51 o 3 3 0 202.03 172.22 1.67 o 4 3 0 14.21 7.81 0.38 o 5 3 0 188.10 168.37 1.94 o 6 3 0 8.97 8.69 0.62 o 7 3 0 10.18 9.93 0.86 o 8 3 0 0.52 0.46 0.64 o 9 3 0 10.81 10.32 1.43 o 0 4 0 916.21 1238.68 17.32 o 1 4 0 350.88 341.41 3.44 o 2 4 0 149.30 123.25 1.75 o 3 4 0 1301.37 1325.45 10.70 o 4 4 0 0.95 4.17 0.31 o 5 4 0 110.20 82.61 1.48 o 6 4 0 39.28 48.66 1.45 o 7 4 0 321.03 331.07 4.55 o 8 4 0 150.60 162.24 4.37 o 9 4 0 208.74 206.88 7.37 o 1 5 0 37.86 50.51 1.21 o 2 5 0 87.52 88.21 1.62 o 3 5 0 0.92 1.70 0.33 o 4 5 0 202.56 203.81 2.63 o 5 5 0 143.94 139.72 8.80 o 6 5 0 35.82 34.04 2.39 o 7 5 0 67.09 65.98 2.05 o 8 5 0 32.31 31.07 1.62 o 0 6 0 131.41 178.09 3.12 o 1 6 0 475.28 504.44 5.11 o 2 6 0 24.44 27.74 0.95 o 3 6 0 484.56 466.10 4.93 o 4 6 0 654.65 614.39 11.15 o 5 6 0 60.41 52.03 2.00 o 6 6 0 53.72 51.93 2.42 o 7 6 0 0.27 2.90 1.04 o 8 6 0 94.12 108.55 3.72 o 1 7 0 156.77 159.39 2.51 o 2 7 0 0.02 3.73 3.26 o 3 7 0 37.94 36.27 1.55 o 4 7 0 5.37 4.14 0.74 o 5 7 0 48.26 47.72 1.98 o 6 7 0 92.23 93.31 2.98 o 7 7 0 34.81 40.00 2.13 o 8 7 0 0.16 1.38 1.38 o 0 8 0 214.26 190.21 3.64 o 1 8 0 207.64 211.91 2.77 o 2 8 0 530.02 496.79 6.73 o 3 8 0 369.36 351.86 6.88 o 4 8 0 322.38 295.37 7.76 o 5 8 0 13.90 18.64 2.41 o 6 8 0 180.05 169.04 4.21 o 7 8 0 23.41 26.07 2.14 o 1 9 0 0.06 0.83 0.35 o 2 9 0 26.16 28.21 1.50 o 3 9 0 77.42 73.17 4.90 o 4 9 0 87.63 85.16 2.76 o 5 9 0 14.41 11.33 1.23 o 6 9 0 5.52 2.01 0.86 o 7 9 0 172.19 182.38 7.07 o 0 10 0 160.37 165.11 3.77 o 1 10 0 179.90 180.61 2.81 o 2 10 0 7.84 12.27 1.17 o 3 10 0 16.67 15.23 1.32 o 4 10 0 55.57 61.77 3.94 o 5 10 0 195.93 209.77 4.90 o 6 10 0 44.36 45.46 3.50 o 1 11 0 21.15 19.80 1.04 o 2 11 0 59.28 66.85 2.07 o 3 11 0 0.18 1.15 0.63 o 4 11 0 0.24 2.64 1.19 o 5 11 0 7.17 13.36 2.14 o 0 12 0 313.69 324.29 6.13 o 1 12 0 32.90 26.12 1.43 o 2 12 0 310.39 297.91 5.24 o 3 12 0 403.66 414.75 13.37 o 4 12 0 287.42 271.81 6.05 o 5 12 0 134.60 130.46 9.25 o 1 13 0 48.13 45.11 2.33 o 2 13 0 19.85 24.08 1.84 o 3 13 0 34.62 29.70 2.86 o 1 14 0 78.02 90.46 4.91 o -9 1 1 2.61 1.05 0.64 o -8 1 1 30.61 27.32 1.18 o -7 1 1 100.22 108.77 2.02 o -6 1 1 40.46 38.16 0.87 o -5 1 1 184.09 189.80 2.39 o -4 1 1 10.09 13.81 0.56 o -3 1 1 520.80 521.92 4.88 o -2 1 1 1327.23 1498.17 14.14 o -1 1 1 489.91 520.30 4.58 o 0 1 1 1389.38 1503.07 10.15 o 1 1 1 14.13 6.79 0.31 o 2 1 1 1974.55 1910.65 11.40 o 3 1 1 13.83 28.08 0.84 o 4 1 1 398.89 431.69 3.00 o 5 1 1 498.10 484.68 5.24 o 6 1 1 26.00 28.10 1.98 o 7 1 1 168.38 166.93 5.21 o 8 1 1 54.74 56.13 3.72 o 9 1 1 100.97 95.89 7.92 o -9 2 1 13.10 15.32 1.25 o -8 2 1 101.55 112.69 2.25 o -7 2 1 64.53 73.35 1.70 o -6 2 1 185.70 203.88 2.57 o -5 2 1 349.79 405.52 3.94 o -4 2 1 1483.66 1426.39 12.32 o -3 2 1 10364.41 10470.74 124.33 o -2 2 1 4467.58 4976.17 80.49 o -1 2 1 8.63 47.53 0.79 o 0 2 1 288.02 377.97 9.07 o 1 2 1 172.77 178.19 1.92 o 2 2 1 25793.78 24736.76 1120.31 o 3 2 1 5056.43 5604.20 55.10 o 4 2 1 2596.05 2818.98 18.82 o 5 2 1 191.07 189.16 4.15 o 6 2 1 1926.11 1911.86 20.24 o 7 2 1 1148.25 1166.48 14.12 o 8 2 1 203.81 220.31 9.95 o 9 2 1 321.95 329.97 6.81 o -9 3 1 57.80 72.52 3.02 o -8 3 1 83.22 92.03 2.04 o -7 3 1 220.33 219.12 3.01 o -6 3 1 95.00 95.32 1.55 o -5 3 1 255.06 263.16 2.98 o -4 3 1 91.92 101.07 1.56 o -3 3 1 1082.88 1076.04 7.73 o -2 3 1 631.56 807.05 5.84 o -1 3 1 123.45 70.47 3.34 o 0 3 1 2415.55 2452.43 25.11 o 1 3 1 700.53 581.31 5.10 o 2 3 1 31.27 52.53 1.07 o 3 3 1 406.14 372.99 3.91 o 4 3 1 18.13 15.06 0.60 o 5 3 1 69.65 65.51 2.06 o 6 3 1 8.81 9.07 1.02 o 7 3 1 3.59 4.58 1.60 o 8 3 1 25.98 29.01 1.92 o 9 3 1 5.16 9.05 1.42 o -9 4 1 33.42 36.06 2.96 o -8 4 1 441.13 471.57 7.95 o -7 4 1 151.45 166.99 2.59 o -6 4 1 264.85 262.97 2.81 o -5 4 1 1358.31 1389.16 15.29 o -4 4 1 435.64 502.16 3.98 o -3 4 1 3721.69 4189.99 23.78 o -2 4 1 1449.93 1399.74 8.46 o -1 4 1 3144.99 3068.19 23.68 o 0 4 1 716.98 606.61 5.45 o 1 4 1 1102.11 1182.83 9.69 o 2 4 1 4529.43 5031.68 53.14 o 3 4 1 2859.57 2743.73 21.28 o 4 4 1 5138.42 5249.38 39.60 o 5 4 1 193.11 258.31 8.42 o 6 4 1 232.80 247.06 7.32 o 7 4 1 733.38 787.69 10.79 o 8 4 1 61.66 60.19 2.65 o 9 4 1 693.90 691.55 10.98 o -9 5 1 12.05 6.23 1.01 o -8 5 1 48.00 57.09 2.05 o -7 5 1 0.17 -0.18 0.38 o -6 5 1 50.77 51.82 1.37 o -5 5 1 13.81 18.10 1.64 o -4 5 1 126.47 135.98 1.96 o -3 5 1 308.13 294.53 2.55 o -2 5 1 2.68 10.56 0.44 o -1 5 1 669.51 618.53 4.99 o 0 5 1 362.95 248.15 4.90 o 1 5 1 669.54 612.31 6.46 o 2 5 1 0.29 6.42 0.63 o 3 5 1 45.43 37.45 1.08 o 4 5 1 19.32 17.75 0.84 o 5 5 1 9.41 7.82 0.91 o 6 5 1 0.17 0.67 0.51 o 7 5 1 13.26 17.54 1.48 o 8 5 1 8.78 5.71 1.04 o -8 6 1 516.64 511.16 16.09 o -7 6 1 953.63 962.44 12.49 o -6 6 1 3.85 5.98 0.90 o -5 6 1 595.03 650.90 6.73 o -4 6 1 226.80 226.00 3.28 o -3 6 1 2875.65 2825.80 21.10 o -2 6 1 116.62 133.79 2.08 o -1 6 1 309.72 362.49 3.70 o 0 6 1 279.40 233.59 3.02 o 1 6 1 38.65 37.23 1.10 o 2 6 1 1194.45 1195.97 10.36 o 3 6 1 73.04 92.82 1.84 o 4 6 1 581.11 666.35 18.36 o 5 6 1 659.38 734.09 9.61 o 6 6 1 125.24 123.27 3.38 o 7 6 1 354.68 333.11 20.90 o 8 6 1 79.23 73.06 2.98 o -8 7 1 1.28 2.50 1.45 o -7 7 1 298.77 307.16 6.03 o -6 7 1 10.30 9.92 1.13 o -5 7 1 222.53 223.24 8.13 o -4 7 1 114.01 107.30 2.79 o -3 7 1 216.24 215.80 3.94 o -2 7 1 878.81 870.26 13.84 o -1 7 1 219.67 170.57 2.27 o 0 7 1 313.82 356.32 5.14 o 1 7 1 64.35 42.31 1.28 o 2 7 1 333.25 326.77 4.03 o 3 7 1 0.28 0.11 0.34 o 4 7 1 20.04 19.23 2.19 o 5 7 1 24.64 26.40 1.57 o 6 7 1 24.57 27.71 1.76 o 7 7 1 0.20 1.15 0.70 o 8 7 1 0.10 -0.32 0.78 o -7 8 1 1358.40 1338.55 23.92 o -6 8 1 26.41 25.83 1.72 o -5 8 1 1624.49 1700.35 18.80 o -4 8 1 7.16 9.04 1.00 o -3 8 1 1119.08 1121.36 12.89 o -2 8 1 2262.03 2173.34 15.60 o -1 8 1 384.72 370.92 3.93 o 0 8 1 2324.84 2286.57 16.25 o 1 8 1 406.50 407.58 4.87 o 2 8 1 2210.18 2147.75 19.06 o 3 8 1 331.76 339.24 5.57 o 4 8 1 398.81 426.44 6.72 o 5 8 1 457.79 477.18 15.65 o 6 8 1 228.41 211.94 4.86 o 7 8 1 1241.69 1298.52 36.62 o -7 9 1 0.40 -1.03 1.03 o -6 9 1 18.39 18.41 2.36 o -5 9 1 135.28 127.83 5.23 o -4 9 1 254.13 248.89 4.90 o -3 9 1 19.99 21.39 1.44 o -2 9 1 1.46 5.16 3.36 o -1 9 1 46.36 56.57 1.43 o 0 9 1 225.07 231.55 3.08 o 1 9 1 35.63 44.11 1.49 o 2 9 1 42.34 44.15 1.89 o 3 9 1 19.82 18.27 2.30 o 4 9 1 0.65 1.21 0.62 o 5 9 1 27.43 28.18 1.80 o 6 9 1 6.62 5.07 1.08 o 7 9 1 0.04 -0.18 0.77 o -6 10 1 118.88 115.57 5.42 o -5 10 1 1731.10 1674.94 27.74 o -4 10 1 306.21 283.31 5.74 o -3 10 1 299.22 309.75 4.67 o -2 10 1 1660.88 1606.61 14.65 o -1 10 1 433.61 414.62 4.61 o 0 10 1 4446.14 4335.43 36.87 o 1 10 1 62.02 62.15 3.35 o 2 10 1 1517.19 1484.97 13.57 o 3 10 1 52.91 55.01 2.25 o 4 10 1 621.56 619.16 12.05 o 5 10 1 1318.74 1357.37 16.52 o 6 10 1 127.40 128.39 4.01 o -6 11 1 3.13 2.73 1.48 o -5 11 1 224.73 214.11 5.29 o -4 11 1 54.54 50.41 3.48 o -3 11 1 25.16 28.16 1.83 o -2 11 1 3.94 5.71 1.90 o -1 11 1 72.81 71.05 2.10 o 0 11 1 101.93 98.92 2.12 o 1 11 1 0.01 -0.17 0.44 o 2 11 1 37.44 37.15 1.59 o 3 11 1 33.17 34.25 1.96 o 4 11 1 2.06 1.04 1.23 o 5 11 1 21.30 20.38 1.77 o -5 12 1 634.25 598.33 12.40 o -4 12 1 202.12 200.40 5.12 o -3 12 1 62.74 64.32 2.77 o -2 12 1 421.35 393.70 8.62 o -1 12 1 94.04 90.31 3.14 o 0 12 1 1507.09 1514.98 12.51 o 1 12 1 8.68 9.43 0.85 o 2 12 1 335.93 323.92 5.13 o 3 12 1 24.06 24.19 1.50 o 4 12 1 185.17 170.60 4.58 o -3 13 1 0.00 -0.07 1.79 o -2 13 1 4.90 6.70 1.22 o -1 13 1 16.51 11.75 2.50 o 0 13 1 82.76 96.56 3.36 o 1 13 1 0.28 1.29 0.75 o 2 13 1 3.07 4.74 1.09 o 3 13 1 4.18 1.32 1.52 o 0 14 1 168.75 177.62 6.82 o -9 0 2 120.32 109.07 8.63 o -8 0 2 198.77 191.08 4.20 o -7 0 2 1768.87 1742.82 17.74 o -6 0 2 1072.98 1060.90 12.16 o -5 0 2 557.91 568.98 8.34 o -4 0 2 21.71 16.53 1.32 o -3 0 2 14.01 4.86 0.49 o -2 0 2 8499.37 8131.21 61.82 o -1 0 2 11794.46 12258.07 116.07 o 0 0 2 17756.38 18420.74 356.69 o 1 0 2 418.18 712.88 7.22 o 2 0 2 4962.92 4425.08 52.44 o 3 0 2 1159.50 1200.87 12.34 o 4 0 2 5035.42 5266.11 125.44 o 5 0 2 5665.56 5458.94 114.10 o 6 0 2 1042.25 1074.94 12.44 o 7 0 2 1687.31 1738.36 27.51 o 8 0 2 1650.56 1656.52 27.29 o 9 0 2 1524.75 1426.34 25.39 o -9 1 2 53.47 54.13 1.92 o -8 1 2 19.43 16.94 0.96 o -7 1 2 21.33 22.71 1.15 o -6 1 2 48.89 41.24 1.17 o -5 1 2 4.21 10.58 0.59 o -4 1 2 505.35 437.67 3.97 o -3 1 2 202.60 148.99 3.22 o -2 1 2 503.01 339.56 2.78 o -1 1 2 96.94 78.98 1.62 o 0 1 2 464.05 440.55 4.38 o 1 1 2 2.87 1.11 0.36 o 2 1 2 72.80 92.58 1.27 o 3 1 2 600.12 567.10 4.71 o 4 1 2 373.89 323.50 2.44 o 5 1 2 73.60 59.67 1.71 o 6 1 2 7.11 11.12 1.06 o 7 1 2 158.65 156.67 6.53 o 8 1 2 0.45 1.03 0.73 o 9 1 2 12.63 9.03 1.45 o -9 2 2 525.77 531.81 5.84 o -8 2 2 293.67 298.66 3.84 o -7 2 2 728.66 734.04 9.70 o -6 2 2 518.74 520.68 5.07 o -5 2 2 1952.90 1860.50 15.51 o -4 2 2 1.30 2.75 0.41 o -3 2 2 482.94 398.57 4.05 o -2 2 2 1051.08 1073.97 7.57 o -1 2 2 1125.04 1358.32 11.59 o 0 2 2 13153.06 12351.05 119.11 o 1 2 2 4745.12 4538.34 29.28 o 2 2 2 581.30 631.16 4.43 o 3 2 2 88.67 63.47 1.16 o 4 2 2 1876.50 1803.99 12.87 o 5 2 2 1773.13 1746.36 18.53 o 6 2 2 917.20 925.80 11.49 o 7 2 2 1102.21 1098.45 13.65 o 8 2 2 164.57 160.94 4.32 o 9 2 2 654.93 680.32 19.57 o -9 3 2 1.30 0.56 0.51 o -8 3 2 15.32 15.71 0.95 o -7 3 2 0.13 -0.26 0.35 o -6 3 2 35.91 34.82 1.20 o -5 3 2 29.84 41.38 1.27 o -4 3 2 120.43 110.16 1.94 o -3 3 2 555.24 523.34 6.99 o -2 3 2 156.88 175.06 1.88 o -1 3 2 495.24 534.14 4.15 o 0 3 2 1621.60 1662.76 35.06 o 1 3 2 175.44 186.64 3.16 o 2 3 2 1442.87 1507.95 12.13 o 3 3 2 5.13 8.73 0.50 o 4 3 2 715.41 779.68 17.89 o 5 3 2 231.41 219.27 3.24 o 6 3 2 272.00 269.66 6.12 o 7 3 2 166.96 162.22 4.08 o 8 3 2 3.59 2.85 0.88 o 9 3 2 151.85 149.38 4.70 o -9 4 2 318.09 309.50 9.61 o -8 4 2 220.43 222.62 3.98 o -7 4 2 612.95 589.27 6.77 o -6 4 2 253.76 239.81 3.09 o -5 4 2 2601.34 2485.42 16.96 o -4 4 2 150.76 130.41 2.22 o -3 4 2 2044.80 2014.66 16.18 o -2 4 2 127.91 90.11 1.10 o -1 4 2 1595.04 1605.73 11.16 o 0 4 2 174.41 194.04 6.65 o 1 4 2 0.16 -0.38 0.25 o 2 4 2 1744.06 1638.54 13.23 o 3 4 2 147.05 161.54 2.41 o 4 4 2 135.74 99.49 1.95 o 5 4 2 5.94 1.82 0.46 o 6 4 2 211.97 232.22 6.05 o 7 4 2 410.84 414.60 10.93 o 8 4 2 45.24 44.99 2.94 o -9 5 2 108.73 117.69 5.76 o -8 5 2 23.01 22.50 1.72 o -7 5 2 172.01 166.99 2.74 o -6 5 2 49.08 52.02 1.23 o -5 5 2 1438.28 1449.56 13.31 o -4 5 2 160.26 162.59 2.18 o -3 5 2 1384.28 1407.44 11.96 o -2 5 2 501.16 480.16 3.71 o -1 5 2 1454.35 1537.51 12.55 o 0 5 2 2292.40 2506.60 19.50 o 1 5 2 25.16 26.65 0.87 o 2 5 2 2039.67 2159.29 17.20 o 3 5 2 0.41 1.83 1.40 o 4 5 2 1178.48 1231.69 10.99 o 5 5 2 154.17 154.27 3.55 o 6 5 2 62.26 63.02 4.56 o 7 5 2 173.54 170.70 15.95 o 8 5 2 0.03 0.28 0.66 o -8 6 2 382.55 393.32 10.80 o -7 6 2 356.70 375.65 7.39 o -6 6 2 56.10 62.83 1.57 o -5 6 2 1192.21 1092.86 8.67 o -4 6 2 102.98 84.14 1.57 o -3 6 2 3913.63 3896.42 22.69 o -2 6 2 142.08 137.44 1.55 o -1 6 2 791.99 801.09 5.94 o 0 6 2 128.59 134.33 2.17 o 1 6 2 262.67 271.38 3.37 o 2 6 2 2570.87 2502.38 19.92 o 3 6 2 64.52 69.22 2.62 o 4 6 2 1340.07 1245.00 19.96 o 5 6 2 0.05 1.29 0.55 o 6 6 2 44.33 42.07 2.72 o 7 6 2 45.02 50.78 2.38 o 8 6 2 11.31 10.95 1.46 o -8 7 2 85.29 85.69 4.85 o -7 7 2 258.79 241.91 7.75 o -6 7 2 6.47 6.69 1.26 o -5 7 2 207.80 220.65 3.36 o -4 7 2 143.40 134.49 2.35 o -3 7 2 692.38 735.85 6.08 o -2 7 2 658.33 671.77 4.87 o -1 7 2 21.16 17.61 0.89 o 0 7 2 28.73 28.79 2.09 o 1 7 2 367.48 382.62 4.47 o 2 7 2 782.58 848.82 8.12 o 3 7 2 108.57 105.42 2.42 o 4 7 2 42.75 46.24 3.13 o 5 7 2 4.95 3.69 1.04 o 6 7 2 35.81 37.14 2.00 o 7 7 2 152.82 168.69 4.52 o 8 7 2 0.04 0.83 0.84 o -7 8 2 13.08 8.98 1.93 o -6 8 2 323.61 318.81 8.87 o -5 8 2 52.39 45.36 3.18 o -4 8 2 15.21 15.61 3.46 o -3 8 2 1380.67 1291.31 11.86 o -2 8 2 103.98 104.82 2.65 o -1 8 2 19.06 12.02 0.68 o 0 8 2 100.63 93.31 2.03 o 1 8 2 2.41 6.13 0.65 o 2 8 2 1019.95 1001.02 16.91 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