#------------------------------------------------------------------------------ #$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $ #$Revision: 717 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221482.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221482_Fobs loop_ _publ_author_name 'Marimuthu, Thashree' 'Bala, Muhammad D.' 'Friedrich, Holger B.' _publ_section_title ; 2,8-Dimethyl-10-p-tolyl-10H-phenoxaphosphine ; _journal_coeditor_code RZ2300 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o828 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.532 _cell_angle_gamma 90.000 _cell_length_a 10.9363 _cell_length_b 11.6323 _cell_length_c 14.0458 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file rz2300Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 8m_kznd17_0s in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 221.49 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 830.77 856.94 20.51 o 2 0 0 6.18 5.36 0.26 o 3 0 0 379.25 447.61 6.96 o 4 0 0 83.66 105.30 2.05 o 5 0 0 728.41 730.15 19.19 o 6 0 0 202.91 252.26 5.38 o 7 0 0 513.53 577.04 15.01 o 8 0 0 583.26 611.89 15.27 o 9 0 0 88.91 80.88 2.08 o 10 0 0 623.92 660.77 25.52 o 11 0 0 12.63 12.42 2.20 o 12 0 0 85.89 78.70 5.36 o 13 0 0 58.23 64.64 6.37 o 1 1 0 616.73 659.84 6.84 o 2 1 0 555.09 612.66 4.95 o 3 1 0 496.98 550.68 6.87 o 4 1 0 113.28 120.01 1.84 o 5 1 0 433.53 484.48 7.02 o 6 1 0 139.64 156.14 1.86 o 7 1 0 320.16 346.56 5.33 o 8 1 0 46.50 46.51 1.19 o 9 1 0 19.31 20.01 0.91 o 10 1 0 5.38 4.92 0.99 o 11 1 0 1.15 -0.72 1.19 o 12 1 0 15.78 15.78 2.05 o 13 1 0 0.01 -1.94 1.94 o 0 2 0 21518.85 17471.63 337.04 o 1 2 0 9275.68 8844.38 56.08 o 2 2 0 6630.26 6616.74 64.62 o 3 2 0 240.14 262.62 3.67 o 4 2 0 6.30 5.00 0.34 o 5 2 0 480.53 479.40 6.40 o 6 2 0 7.93 10.62 0.45 o 7 2 0 322.15 333.43 4.02 o 8 2 0 405.26 405.74 5.81 o 9 2 0 15.17 12.88 0.95 o 10 2 0 291.58 285.61 6.17 o 11 2 0 2.99 2.99 1.17 o 12 2 0 48.07 53.62 3.21 o 13 2 0 124.87 125.03 6.52 o 1 3 0 1803.28 1824.23 16.98 o 2 3 0 2.63 2.28 0.20 o 3 3 0 297.36 307.63 2.99 o 4 3 0 1038.86 1016.71 15.16 o 5 3 0 141.47 162.48 3.12 o 6 3 0 21.79 19.99 1.14 o 7 3 0 68.39 72.50 1.49 o 8 3 0 14.16 15.43 0.87 o 9 3 0 82.03 79.33 2.07 o 10 3 0 3.65 3.01 1.00 o 11 3 0 38.16 40.48 1.86 o 12 3 0 23.45 21.76 2.16 o 13 3 0 4.63 2.41 2.20 o 0 4 0 153.22 160.45 3.22 o 1 4 0 1351.46 1426.23 15.98 o 2 4 0 1387.10 1403.05 16.23 o 3 4 0 840.20 1007.99 10.94 o 4 4 0 0.09 0.58 0.66 o 5 4 0 297.30 302.75 3.07 o 6 4 0 257.14 261.26 4.16 o 7 4 0 6.44 2.90 0.79 o 8 4 0 58.31 67.28 1.91 o 9 4 0 27.95 26.52 1.45 o 10 4 0 40.55 32.43 3.35 o 11 4 0 0.85 -0.15 1.09 o 12 4 0 7.41 5.83 1.55 o 1 5 0 4517.85 4573.62 58.67 o 2 5 0 0.04 2.77 0.42 o 3 5 0 1844.39 2026.47 25.05 o 4 5 0 454.61 426.42 5.91 o 5 5 0 44.51 44.46 1.24 o 6 5 0 385.25 363.67 6.12 o 7 5 0 196.92 182.44 3.51 o 8 5 0 235.49 236.71 4.68 o 9 5 0 547.28 562.11 7.99 o 10 5 0 66.57 66.60 2.22 o 11 5 0 34.31 45.57 2.52 o 12 5 0 0.26 -0.98 1.40 o 0 6 0 760.87 734.33 11.76 o 1 6 0 42.65 47.44 0.82 o 2 6 0 1222.04 1393.11 20.85 o 3 6 0 3.46 5.67 0.41 o 4 6 0 50.88 59.05 0.81 o 5 6 0 14.40 17.94 1.00 o 6 6 0 14.70 17.32 1.08 o 7 6 0 258.20 246.82 4.37 o 8 6 0 129.61 127.32 3.37 o 9 6 0 29.06 29.66 1.59 o 10 6 0 328.19 317.37 6.40 o 11 6 0 44.46 43.75 2.66 o 12 6 0 37.88 41.08 2.74 o 1 7 0 796.28 797.07 16.69 o 2 7 0 859.71 930.16 13.15 o 3 7 0 1699.70 1753.56 30.49 o 4 7 0 561.44 543.06 8.29 o 5 7 0 729.44 656.08 11.31 o 6 7 0 104.53 95.05 2.05 o 7 7 0 294.77 294.26 3.57 o 8 7 0 12.53 12.70 1.52 o 9 7 0 281.45 285.87 4.62 o 10 7 0 26.46 25.93 2.49 o 11 7 0 155.46 171.23 6.72 o 0 8 0 22.04 20.93 1.07 o 1 8 0 143.45 136.68 2.16 o 2 8 0 442.30 364.66 5.80 o 3 8 0 512.88 497.83 9.22 o 4 8 0 121.98 123.18 3.27 o 5 8 0 25.54 20.85 1.05 o 6 8 0 5.95 6.35 1.10 o 7 8 0 0.97 -1.03 1.03 o 8 8 0 74.19 71.61 2.63 o 9 8 0 3.38 0.36 1.38 o 10 8 0 117.94 129.08 6.16 o 11 8 0 7.45 5.26 2.10 o 1 9 0 725.83 724.16 8.55 o 2 9 0 14.07 15.08 0.92 o 3 9 0 302.99 311.88 6.30 o 4 9 0 152.45 159.30 3.19 o 5 9 0 55.68 50.13 1.97 o 6 9 0 8.05 6.01 1.18 o 7 9 0 20.04 18.67 1.55 o 8 9 0 2.00 -0.20 1.37 o 9 9 0 5.14 1.44 1.61 o 10 9 0 0.34 -1.78 1.87 o 0 10 0 86.20 97.18 3.30 o 1 10 0 1146.90 1108.06 17.41 o 2 10 0 121.88 118.07 3.13 o 3 10 0 2.76 2.12 0.77 o 4 10 0 461.59 460.96 9.13 o 5 10 0 295.14 287.94 6.02 o 6 10 0 55.21 56.20 2.25 o 7 10 0 166.74 163.52 3.78 o 8 10 0 205.22 211.17 4.35 o 9 10 0 0.15 -1.73 1.73 o 10 10 0 84.30 90.06 4.26 o 1 11 0 1.55 1.58 1.08 o 2 11 0 108.94 101.84 2.93 o 3 11 0 308.76 294.63 6.43 o 4 11 0 103.40 102.86 2.72 o 5 11 0 15.53 11.30 1.49 o 6 11 0 0.07 -0.93 1.17 o 7 11 0 43.45 40.88 2.30 o 8 11 0 48.91 56.03 2.74 o 9 11 0 0.02 -1.37 1.93 o 0 12 0 40.41 41.57 2.57 o 1 12 0 122.70 115.37 2.89 o 2 12 0 149.58 153.47 4.40 o 3 12 0 347.05 350.45 8.34 o 4 12 0 1.44 2.62 1.46 o 5 12 0 61.94 62.37 2.70 o 6 12 0 122.14 130.58 3.63 o 7 12 0 15.57 14.72 1.89 o 8 12 0 100.80 112.81 3.71 o 1 13 0 101.65 109.51 2.64 o 2 13 0 35.36 33.74 1.98 o 3 13 0 252.48 252.11 9.29 o 4 13 0 21.78 22.49 2.15 o 5 13 0 55.10 55.88 3.08 o 6 13 0 40.96 37.88 2.65 o 7 13 0 3.31 -0.21 1.55 o 0 14 0 123.84 142.75 9.55 o 1 14 0 0.38 0.33 1.24 o 2 14 0 8.09 8.10 1.91 o 3 14 0 8.36 8.17 2.06 o 4 14 0 29.23 26.03 2.77 o 5 14 0 42.27 34.76 2.67 o 1 15 0 121.72 123.15 4.58 o 2 15 0 27.50 30.36 2.74 o -13 1 1 33.51 40.96 2.71 o -12 1 1 16.81 19.30 1.89 o -11 1 1 42.52 42.48 2.10 o -10 1 1 16.27 17.52 1.21 o -9 1 1 225.90 243.20 4.48 o -8 1 1 1465.39 1419.44 23.81 o -7 1 1 288.95 329.20 5.75 o -6 1 1 2124.56 2175.80 29.59 o -5 1 1 33.79 22.59 0.63 o -4 1 1 169.51 187.20 2.12 o -3 1 1 182.88 173.04 1.47 o -2 1 1 3055.90 3106.87 30.01 o -1 1 1 6835.85 6551.90 51.82 o 0 1 1 7343.56 6675.71 91.57 o 1 1 1 292.82 306.15 2.33 o 2 1 1 14413.68 13528.81 160.06 o 3 1 1 6.23 10.87 0.53 o 4 1 1 466.36 481.07 7.44 o 5 1 1 252.42 273.35 3.57 o 6 1 1 368.54 323.49 4.59 o 7 1 1 998.11 939.02 17.45 o 8 1 1 0.07 1.02 0.54 o 9 1 1 296.42 290.72 6.07 o 10 1 1 299.18 292.32 7.66 o 11 1 1 146.55 137.01 5.24 o 12 1 1 230.50 232.09 5.95 o 13 1 1 42.38 53.66 4.85 o -13 2 1 1.88 1.81 1.80 o -12 2 1 72.00 68.66 3.08 o -11 2 1 47.24 42.92 2.03 o -10 2 1 11.39 11.56 1.14 o -9 2 1 514.60 489.03 11.04 o -8 2 1 756.32 774.90 12.81 o -7 2 1 3.21 10.30 0.46 o -6 2 1 0.03 2.07 0.31 o -5 2 1 1015.41 1106.83 11.92 o -4 2 1 2184.15 2254.68 31.94 o -3 2 1 924.88 959.79 12.10 o -2 2 1 32.02 34.38 0.43 o -1 2 1 193.43 219.36 1.97 o 0 2 1 2578.70 2595.51 36.01 o 1 2 1 8295.54 8186.17 72.33 o 2 2 1 17208.71 16126.72 204.60 o 3 2 1 609.04 654.43 7.97 o 4 2 1 55.83 51.82 0.98 o 5 2 1 116.32 114.34 2.18 o 6 2 1 387.40 387.89 5.86 o 7 2 1 389.16 448.18 6.86 o 8 2 1 77.20 68.58 1.48 o 9 2 1 179.36 186.23 4.47 o 10 2 1 1.78 1.32 0.97 o 11 2 1 53.32 52.63 2.43 o 12 2 1 11.83 7.28 2.14 o 13 2 1 1.38 1.70 2.11 o -13 3 1 25.88 23.76 2.77 o -12 3 1 40.94 36.50 2.20 o -11 3 1 114.70 116.51 2.67 o -10 3 1 21.04 17.88 1.32 o -9 3 1 177.70 181.46 4.20 o -8 3 1 161.34 136.07 2.69 o -7 3 1 11.24 10.47 0.86 o -6 3 1 2746.30 2851.24 48.79 o -5 3 1 282.03 271.90 4.47 o -4 3 1 615.03 687.72 11.00 o -3 3 1 4.85 0.96 0.32 o -2 3 1 741.86 701.17 8.26 o -1 3 1 840.01 849.74 12.97 o 0 3 1 361.02 368.35 4.17 o 1 3 1 2757.68 2978.37 35.83 o 2 3 1 647.74 704.15 8.08 o 3 3 1 280.88 304.27 3.11 o 4 3 1 169.72 159.85 2.12 o 5 3 1 31.93 55.91 1.15 o 6 3 1 153.66 162.68 2.95 o 7 3 1 595.42 589.63 8.00 o 8 3 1 0.02 -0.46 0.51 o 9 3 1 46.37 40.20 1.65 o 10 3 1 0.02 -0.90 0.90 o 11 3 1 46.27 48.60 2.42 o 12 3 1 46.17 45.41 3.26 o -13 4 1 3.86 2.94 2.01 o -12 4 1 47.39 44.09 4.54 o -11 4 1 14.36 9.12 1.58 o -10 4 1 9.96 7.31 1.13 o -9 4 1 178.61 179.21 3.25 o -8 4 1 384.91 377.55 7.83 o -7 4 1 207.14 176.89 4.16 o -6 4 1 11.99 14.25 0.86 o -5 4 1 302.73 262.74 3.86 o -4 4 1 1260.72 1189.81 13.58 o -3 4 1 708.25 691.54 8.87 o -2 4 1 2957.26 2832.21 36.09 o -1 4 1 2113.19 2199.04 21.21 o 0 4 1 81.76 60.89 0.87 o 1 4 1 2538.32 2552.29 28.12 o 2 4 1 95.79 108.73 0.96 o 3 4 1 482.32 476.43 7.62 o 4 4 1 231.78 185.71 2.10 o 5 4 1 2.05 1.03 0.25 o 6 4 1 412.25 381.50 6.99 o 7 4 1 3.09 2.70 0.84 o 8 4 1 786.90 730.19 29.78 o 9 4 1 5.87 3.36 0.87 o 10 4 1 25.91 33.00 1.83 o 11 4 1 79.21 86.87 2.92 o 12 4 1 50.23 50.99 2.77 o -12 5 1 34.53 33.70 2.23 o -11 5 1 22.73 23.00 1.58 o -10 5 1 125.32 133.17 3.83 o -9 5 1 83.31 89.13 2.35 o -8 5 1 109.35 109.46 2.33 o -7 5 1 69.97 62.90 1.77 o -6 5 1 6.12 6.12 1.02 o -5 5 1 137.68 174.81 2.39 o -4 5 1 46.56 55.70 0.86 o -3 5 1 330.54 408.33 7.14 o -2 5 1 289.09 288.70 3.95 o -1 5 1 922.49 936.77 19.80 o 0 5 1 734.04 826.81 11.47 o 1 5 1 0.50 11.12 0.46 o 2 5 1 0.03 0.56 0.30 o 3 5 1 539.16 517.53 5.81 o 4 5 1 235.31 220.41 2.97 o 5 5 1 131.88 131.98 2.67 o 6 5 1 7.86 8.42 0.84 o 7 5 1 154.77 142.64 2.94 o 8 5 1 84.24 76.67 2.07 o 9 5 1 113.55 109.87 2.85 o 10 5 1 187.17 187.20 4.99 o 11 5 1 22.33 18.65 1.87 o 12 5 1 0.61 0.78 1.53 o -12 6 1 94.98 99.00 3.76 o -11 6 1 22.45 22.75 1.92 o -10 6 1 301.90 309.67 8.99 o -9 6 1 310.00 315.21 7.16 o -8 6 1 118.52 111.70 3.07 o -7 6 1 1678.52 1564.24 21.71 o -6 6 1 123.77 113.54 2.32 o -5 6 1 367.52 341.04 6.27 o -4 6 1 214.61 176.25 2.82 o -3 6 1 152.95 182.72 2.95 o -2 6 1 298.69 265.34 3.40 o -1 6 1 149.55 185.59 3.63 o 0 6 1 270.01 227.61 3.30 o 1 6 1 566.10 563.82 7.69 o 2 6 1 211.46 261.86 3.48 o 3 6 1 1615.48 1719.17 23.88 o 4 6 1 9.39 15.06 0.56 o 5 6 1 433.08 451.19 6.65 o 6 6 1 896.98 822.47 12.75 o 7 6 1 3.09 0.27 0.94 o 8 6 1 199.12 185.81 5.51 o 9 6 1 285.05 294.02 4.95 o 10 6 1 88.92 95.79 2.88 o 11 6 1 122.85 120.31 4.22 o 12 6 1 4.92 4.74 1.85 o -12 7 1 3.61 3.76 2.06 o -11 7 1 128.92 132.08 4.59 o -10 7 1 151.44 147.43 4.35 o -9 7 1 83.46 84.05 2.83 o -8 7 1 20.43 18.74 1.62 o -7 7 1 141.56 127.17 2.39 o -6 7 1 233.41 241.55 3.90 o -5 7 1 41.41 34.67 0.83 o -4 7 1 366.19 381.58 7.77 o -3 7 1 2.04 -0.50 0.50 o -2 7 1 449.84 498.47 6.50 o -1 7 1 653.65 655.90 20.71 o 0 7 1 207.77 174.28 2.88 o 1 7 1 31.93 26.19 0.85 o 2 7 1 396.31 347.09 7.06 o 3 7 1 69.29 68.36 1.20 o 4 7 1 98.95 114.74 2.00 o 5 7 1 88.91 93.33 1.27 o 6 7 1 97.30 103.16 2.40 o 7 7 1 60.04 60.14 1.91 o 8 7 1 6.67 5.86 1.15 o 9 7 1 20.14 18.88 1.95 o 10 7 1 32.70 37.13 3.42 o 11 7 1 59.40 68.02 4.18 o -11 8 1 30.80 30.84 2.94 o -10 8 1 89.82 91.94 3.53 o -9 8 1 0.76 -1.36 1.36 o -8 8 1 124.83 114.40 3.20 o -7 8 1 1040.38 952.56 16.94 o -6 8 1 32.98 26.36 1.51 o -5 8 1 1122.44 1153.35 22.21 o -4 8 1 54.20 56.45 1.64 o -3 8 1 20.59 12.19 0.85 o -2 8 1 540.72 487.26 8.39 o -1 8 1 66.80 60.37 1.58 o 0 8 1 192.98 190.63 2.93 o 1 8 1 69.70 72.56 1.85 o 2 8 1 13.67 16.61 1.21 o 3 8 1 427.60 430.39 8.48 o 4 8 1 45.70 33.67 1.00 o 5 8 1 13.37 10.26 0.85 o 6 8 1 8.75 11.14 1.23 o 7 8 1 9.46 7.90 1.29 o 8 8 1 2.30 -0.25 1.21 o 9 8 1 47.88 42.80 3.11 o 10 8 1 67.06 77.74 3.94 o 11 8 1 52.96 51.23 3.45 o -11 9 1 184.12 194.87 5.88 o -10 9 1 72.71 70.96 3.27 o -9 9 1 216.37 232.44 4.97 o -8 9 1 67.55 63.40 2.87 o -7 9 1 0.22 -0.44 1.05 o -6 9 1 132.10 129.35 2.96 o -5 9 1 75.57 64.88 2.15 o -4 9 1 100.39 91.27 2.05 o -3 9 1 0.61 -0.65 0.65 o -2 9 1 583.80 552.80 9.28 o -1 9 1 691.36 634.35 10.57 o 0 9 1 411.25 406.98 6.44 o 1 9 1 195.95 209.61 3.51 o 2 9 1 569.10 559.59 11.27 o 3 9 1 171.39 179.66 4.08 o 4 9 1 0.05 -0.54 0.54 o 5 9 1 68.76 67.52 2.17 o 6 9 1 293.90 288.30 5.48 o 7 9 1 250.91 229.39 4.13 o 8 9 1 7.71 6.20 1.46 o 9 9 1 183.08 196.30 6.88 o 10 9 1 94.58 105.39 4.51 o -10 10 1 22.47 26.67 2.90 o -9 10 1 0.08 -1.50 1.50 o -8 10 1 91.76 86.20 3.04 o -7 10 1 12.14 5.46 1.42 o -6 10 1 1.43 -0.46 1.02 o -5 10 1 8.03 5.24 1.18 o -4 10 1 433.21 431.19 8.08 o -3 10 1 42.70 43.65 1.48 o -2 10 1 31.63 35.74 1.35 o -1 10 1 4.10 3.77 0.77 o 0 10 1 0.30 1.06 0.83 o 1 10 1 47.60 34.16 1.39 o 2 10 1 3.93 1.88 0.72 o 3 10 1 16.86 14.63 0.92 o 4 10 1 9.54 10.45 1.14 o 5 10 1 0.69 -0.06 0.99 o 6 10 1 1.26 1.06 1.20 o 7 10 1 0.60 -1.15 1.15 o 8 10 1 5.16 7.59 1.82 o 9 10 1 10.29 7.79 2.25 o -9 11 1 128.41 139.40 4.36 o -8 11 1 132.88 129.15 3.76 o -7 11 1 0.46 1.16 1.34 o -6 11 1 100.71 98.37 3.05 o -5 11 1 91.27 94.80 2.91 o -4 11 1 147.79 143.20 3.48 o -3 11 1 586.42 578.13 10.55 o -2 11 1 0.52 -0.28 0.81 o -1 11 1 128.97 114.50 2.65 o 0 11 1 90.51 93.49 2.25 o 1 11 1 152.32 159.90 3.48 o 2 11 1 98.87 101.31 2.31 o 3 11 1 6.00 4.80 0.96 o 4 11 1 320.14 318.04 5.01 o 5 11 1 143.01 139.92 3.43 o 6 11 1 7.39 5.60 1.41 o 7 11 1 139.02 138.36 3.66 o 8 11 1 34.63 38.14 2.66 o 9 11 1 54.90 56.61 3.63 o -8 12 1 2.70 2.75 1.57 o -7 12 1 18.28 14.75 1.85 o -6 12 1 7.58 4.74 1.54 o -5 12 1 19.13 21.28 1.80 o -4 12 1 14.70 10.60 1.55 o -3 12 1 10.75 8.69 1.44 o -2 12 1 265.62 273.70 5.29 o -1 12 1 223.55 194.60 8.03 o 0 12 1 2.82 3.43 1.04 o 1 12 1 68.98 67.76 2.18 o 2 12 1 12.26 8.53 1.17 o 3 12 1 223.62 220.50 4.67 o 4 12 1 3.94 3.82 1.45 o 5 12 1 114.72 119.25 4.37 o 6 12 1 10.16 6.50 1.53 o 7 12 1 0.07 -1.37 1.37 o 8 12 1 13.87 13.79 2.24 o -7 13 1 95.28 106.56 3.92 o -6 13 1 172.62 185.70 4.87 o -5 13 1 206.91 208.55 5.50 o -4 13 1 102.26 105.40 3.67 o -3 13 1 111.43 105.68 4.02 o -2 13 1 0.24 0.26 1.16 o -1 13 1 95.07 102.19 3.88 o 0 13 1 27.63 30.57 1.66 o 1 13 1 28.30 27.67 1.66 o 2 13 1 59.26 63.29 2.54 o 3 13 1 7.12 5.60 1.62 o 4 13 1 20.57 20.98 2.15 o 5 13 1 18.12 17.21 2.13 o 6 13 1 0.06 -1.24 1.51 o -5 14 1 2.83 4.00 1.75 o -4 14 1 3.03 2.15 1.66 o -3 14 1 11.78 11.28 2.10 o -2 14 1 58.63 58.62 3.31 o -1 14 1 74.04 75.93 3.90 o 0 14 1 11.81 10.49 1.59 o 1 14 1 25.62 26.27 1.95 o 2 14 1 48.65 48.21 3.10 o 3 14 1 387.05 413.55 16.07 o 4 14 1 15.67 16.98 2.17 o 5 14 1 184.55 215.08 5.36 o -3 15 1 6.52 9.84 2.29 o -2 15 1 2.29 -0.26 1.82 o -1 15 1 7.52 8.94 1.85 o 0 15 1 9.72 11.68 1.73 o 1 15 1 0.46 0.49 1.76 o 2 15 1 2.38 0.67 1.85 o -13 0 2 43.10 38.37 3.38 o -12 0 2 381.81 375.08 16.52 o -11 0 2 17.22 16.47 2.39 o 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