#------------------------------------------------------------------------------ #$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $ #$Revision: 717 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221561.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221561_Fobs loop_ _publ_author_name 'H\"okelek, Tuncer' 'Dal, Hakan' 'Tercan, Bar\?i\,s' '\"Ozbek, F. Elif' 'Necefo\(glu, Hacali' _publ_section_title ; Diaquabis(2-chlorobenzoato-\kO)bis(nicotinamide-\kN^1^)nickel(II) ; _journal_coeditor_code XU2501 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m466 _journal_page_last m467 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.600 _cell_angle_gamma 90.000 _cell_length_a 7.8602 _cell_length_b 17.9529 _cell_length_c 9.8446 _exptl_crystal_F_000 668.00 _reflns_d_resolution_high 0.7495 _[local]_cod_data_source_file xu2501Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' el13 in P 21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 167.42 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6474.74 7210.05 204.54 o 4 0 0 1147.59 1666.42 70.86 o 6 0 0 321.45 356.35 29.67 o 8 0 0 2105.11 2072.95 71.55 o 10 0 0 49.29 68.70 29.47 o 1 1 0 11300.35 11645.74 222.52 o 2 1 0 499.74 627.62 13.09 o 3 1 0 1409.54 1367.54 22.94 o 4 1 0 2531.21 3001.14 84.01 o 5 1 0 751.73 780.06 34.35 o 6 1 0 5.13 32.94 7.62 o 7 1 0 2514.03 2550.75 50.68 o 8 1 0 197.55 210.91 25.61 o 9 1 0 738.42 685.19 34.86 o 10 1 0 133.13 136.82 33.73 o 0 2 0 3921.66 3773.16 271.84 o 1 2 0 3.08 3.37 1.62 o 2 2 0 586.78 663.11 26.23 o 3 2 0 2285.32 2582.88 64.74 o 4 2 0 5244.22 5792.98 148.98 o 5 2 0 19.33 17.10 4.86 o 6 2 0 4578.93 4486.39 222.88 o 7 2 0 54.29 101.59 22.89 o 8 2 0 617.47 651.78 31.48 o 9 2 0 41.99 52.40 17.58 o 10 2 0 81.94 43.68 27.01 o 1 3 0 1474.71 1277.56 26.20 o 2 3 0 7163.15 7266.86 126.06 o 3 3 0 1907.15 1895.24 48.94 o 4 3 0 914.76 1078.54 31.57 o 5 3 0 822.62 822.42 41.21 o 6 3 0 345.39 361.81 14.16 o 7 3 0 585.15 612.53 26.20 o 8 3 0 239.76 278.12 24.07 o 9 3 0 419.09 443.51 44.30 o 0 4 0 3957.95 3612.44 173.08 o 1 4 0 9481.39 9504.85 219.03 o 2 4 0 2286.32 2202.07 32.33 o 3 4 0 751.83 777.06 21.36 o 4 4 0 3798.44 3920.41 125.73 o 5 4 0 2.54 3.98 6.14 o 6 4 0 18.63 22.20 7.99 o 7 4 0 465.98 456.62 26.19 o 8 4 0 101.55 83.12 17.14 o 9 4 0 0.07 -2.93 20.96 o 1 5 0 6524.23 7287.77 135.50 o 2 5 0 275.49 262.84 7.59 o 3 5 0 1266.88 1138.80 23.19 o 4 5 0 313.05 324.22 12.16 o 5 5 0 4197.01 4160.50 186.33 o 6 5 0 96.37 124.26 10.39 o 7 5 0 1351.83 1430.90 31.10 o 8 5 0 7.40 -12.69 17.84 o 9 5 0 7.91 24.24 23.54 o 0 6 0 165.21 236.67 16.43 o 1 6 0 2610.99 2616.17 60.04 o 2 6 0 3028.70 3008.88 59.30 o 3 6 0 2586.63 2718.63 59.42 o 4 6 0 5018.10 5032.91 161.72 o 5 6 0 56.39 69.58 8.19 o 6 6 0 785.73 707.92 32.22 o 7 6 0 105.82 127.20 21.18 o 8 6 0 54.86 37.63 23.15 o 9 6 0 552.56 528.18 49.03 o 1 7 0 6127.18 5638.95 139.41 o 2 7 0 1208.31 1296.19 34.19 o 3 7 0 906.25 882.90 17.03 o 4 7 0 1.32 -0.94 4.77 o 5 7 0 5.39 3.52 6.57 o 6 7 0 909.82 831.86 39.65 o 7 7 0 3.38 -2.13 11.89 o 8 7 0 33.28 98.47 18.46 o 9 7 0 774.24 803.26 57.69 o 0 8 0 597.54 520.14 14.60 o 1 8 0 2371.11 2389.67 47.67 o 2 8 0 5897.30 5903.63 123.53 o 3 8 0 2394.12 2445.57 52.07 o 4 8 0 350.93 338.17 19.30 o 5 8 0 7.63 11.97 8.84 o 6 8 0 9.56 3.60 8.90 o 7 8 0 720.12 728.24 42.59 o 8 8 0 613.51 630.40 78.56 o 9 8 0 30.78 18.46 25.10 o 1 9 0 536.30 488.22 32.07 o 2 9 0 485.36 526.31 14.62 o 3 9 0 221.31 171.16 8.65 o 4 9 0 1006.56 1015.42 36.31 o 5 9 0 783.83 731.12 20.97 o 6 9 0 1116.10 1042.00 33.81 o 7 9 0 1227.71 1253.42 83.07 o 8 9 0 17.55 32.28 16.30 o 9 9 0 208.42 227.07 39.78 o 0 10 0 2452.47 2305.89 30.52 o 1 10 0 217.28 248.29 15.16 o 2 10 0 3736.18 3671.72 87.40 o 3 10 0 312.87 327.11 12.42 o 4 10 0 401.56 747.44 31.97 o 5 10 0 1.05 1.55 9.31 o 6 10 0 3.05 -2.47 9.10 o 7 10 0 29.80 23.05 17.21 o 8 10 0 51.60 43.63 17.77 o 9 10 0 216.70 256.30 41.30 o 1 11 0 164.38 127.81 5.54 o 2 11 0 211.27 186.83 7.10 o 3 11 0 4.10 1.31 4.26 o 4 11 0 660.23 644.98 44.94 o 5 11 0 362.09 341.74 24.32 o 6 11 0 4.90 5.64 12.56 o 7 11 0 92.45 111.82 19.80 o 8 11 0 24.52 14.28 16.16 o 0 12 0 88.50 117.88 10.37 o 1 12 0 782.03 836.29 40.79 o 2 12 0 397.26 349.32 15.44 o 3 12 0 0.06 0.16 7.73 o 4 12 0 26.03 24.96 11.87 o 5 12 0 520.00 485.86 27.10 o 6 12 0 1492.79 1383.54 43.65 o 7 12 0 39.31 32.57 15.73 o 8 12 0 157.30 169.54 24.46 o 1 13 0 110.44 100.17 6.92 o 2 13 0 2513.05 2680.02 57.99 o 3 13 0 817.69 824.50 61.93 o 4 13 0 461.46 459.90 25.52 o 5 13 0 278.02 280.97 23.64 o 6 13 0 660.00 636.60 32.64 o 7 13 0 4.94 -11.46 15.79 o 8 13 0 224.95 228.14 26.80 o 0 14 0 1332.16 1272.89 27.99 o 1 14 0 120.94 155.34 11.82 o 2 14 0 1185.21 1212.10 32.35 o 3 14 0 193.26 196.44 24.44 o 4 14 0 157.35 167.42 18.52 o 5 14 0 487.76 474.03 29.76 o 6 14 0 44.19 36.95 15.90 o 7 14 0 64.55 83.46 20.16 o 8 14 0 3.32 -15.57 15.57 o 1 15 0 3.63 -4.88 7.24 o 2 15 0 440.11 469.39 24.09 o 3 15 0 58.99 120.42 22.02 o 4 15 0 2.32 -10.37 10.45 o 5 15 0 770.43 789.81 34.99 o 6 15 0 219.50 224.18 24.15 o 7 15 0 269.25 286.79 28.37 o 0 16 0 73.82 63.94 19.13 o 1 16 0 62.13 45.32 19.40 o 2 16 0 593.34 613.78 27.04 o 3 16 0 60.68 58.97 14.58 o 4 16 0 491.35 527.98 29.06 o 5 16 0 430.87 440.87 29.31 o 6 16 0 730.54 739.63 37.69 o 7 16 0 9.59 13.66 17.67 o 1 17 0 1221.81 1316.85 37.15 o 2 17 0 243.31 246.05 22.60 o 3 17 0 288.29 311.00 23.45 o 4 17 0 93.28 96.83 26.80 o 5 17 0 41.39 56.21 17.40 o 6 17 0 8.06 5.16 15.58 o 7 17 0 4.09 -14.31 16.57 o 0 18 0 345.76 342.45 33.73 o 1 18 0 26.55 15.45 12.71 o 2 18 0 162.69 174.41 28.61 o 3 18 0 1289.03 1333.30 127.45 o 4 18 0 564.05 609.08 62.09 o 5 18 0 5.59 -9.22 14.27 o 6 18 0 173.81 161.75 24.72 o 1 19 0 58.12 48.76 14.99 o 2 19 0 66.26 80.57 24.71 o 3 19 0 1346.25 1287.84 63.82 o 4 19 0 86.14 65.62 18.24 o 5 19 0 866.51 948.44 42.10 o 6 19 0 80.21 84.72 21.77 o 0 20 0 1452.58 1538.01 63.31 o 1 20 0 136.29 151.57 28.65 o 2 20 0 836.18 812.04 51.84 o 3 20 0 381.15 364.55 40.87 o 4 20 0 372.51 351.04 42.86 o 5 20 0 100.03 86.88 20.97 o 1 21 0 1690.55 1774.21 72.14 o 2 21 0 9.53 6.44 20.06 o 3 21 0 118.51 128.74 31.58 o 4 21 0 8.97 -1.25 22.95 o 0 22 0 243.44 245.26 35.09 o 1 22 0 3.30 2.38 21.78 o 2 22 0 91.05 118.47 30.21 o 3 22 0 301.12 298.93 40.83 o 1 23 0 31.13 8.63 24.05 o 2 23 0 298.54 285.42 40.48 o -9 0 1 186.48 168.05 32.28 o -7 0 1 281.88 281.17 23.29 o -5 0 1 713.96 817.53 44.05 o -3 0 1 2050.31 2063.17 57.51 o -1 0 1 420.55 351.74 16.32 o 1 0 1 11225.63 12775.23 218.97 o 3 0 1 1688.78 1935.51 58.85 o 5 0 1 611.41 608.32 37.05 o 7 0 1 6801.79 6504.00 112.54 o 9 0 1 608.04 557.50 46.30 o -10 1 1 858.02 978.36 43.11 o -9 1 1 69.98 77.53 21.53 o -8 1 1 916.70 914.78 36.23 o -7 1 1 149.15 152.16 13.81 o -6 1 1 17.77 23.94 6.19 o -5 1 1 1671.76 1794.92 63.97 o -4 1 1 4559.95 4970.56 105.30 o -3 1 1 344.70 331.35 7.96 o -2 1 1 1608.85 1501.30 10.43 o -1 1 1 1831.84 1870.07 50.83 o 0 1 1 1411.99 1359.06 123.11 o 1 1 1 185.30 232.99 3.58 o 2 1 1 508.96 416.48 6.37 o 3 1 1 3693.92 4434.62 93.65 o 4 1 1 1496.82 1523.18 59.34 o 5 1 1 681.98 715.80 32.53 o 6 1 1 51.32 53.89 8.27 o 7 1 1 697.46 676.68 29.68 o 8 1 1 497.93 456.41 28.14 o 9 1 1 218.32 214.40 23.98 o -10 2 1 5.08 7.46 25.22 o -9 2 1 973.73 1016.21 40.49 o -8 2 1 16.76 7.68 14.00 o -7 2 1 474.72 522.64 28.77 o -6 2 1 289.48 306.18 13.89 o -5 2 1 238.97 246.88 9.13 o -4 2 1 54.96 56.69 7.50 o -3 2 1 84.73 131.12 5.13 o -2 2 1 471.92 450.00 10.63 o -1 2 1 12495.97 12097.94 581.26 o 0 2 1 0.39 5.39 1.13 o 1 2 1 6022.41 6260.60 89.54 o 2 2 1 331.70 299.12 5.27 o 3 2 1 5435.77 5819.64 100.07 o 4 2 1 87.74 120.67 6.80 o 5 2 1 397.92 416.23 20.42 o 6 2 1 419.95 449.53 24.17 o 7 2 1 643.50 650.12 29.98 o 8 2 1 10.48 4.49 12.79 o 9 2 1 9.75 18.97 22.68 o -10 3 1 2.44 7.14 25.57 o -9 3 1 5.75 -1.37 14.82 o -8 3 1 415.54 461.81 40.75 o -7 3 1 23.53 19.51 10.04 o -6 3 1 1985.84 1915.98 67.35 o -5 3 1 165.25 191.38 18.80 o -4 3 1 9850.67 10038.72 249.63 o -3 3 1 4381.36 4678.93 119.38 o -2 3 1 1194.11 1043.36 18.83 o -1 3 1 166.64 153.75 6.87 o 0 3 1 26.21 11.79 1.52 o 1 3 1 7108.57 6691.61 531.70 o 2 3 1 747.18 697.47 17.11 o 3 3 1 80.92 118.23 5.12 o 4 3 1 745.03 771.53 22.80 o 5 3 1 320.46 335.50 16.48 o 6 3 1 230.51 247.93 14.17 o 7 3 1 454.74 557.70 54.79 o 8 3 1 1305.91 1306.37 41.22 o 9 3 1 375.04 334.02 40.83 o -10 4 1 287.05 317.90 44.38 o -9 4 1 23.91 21.20 24.01 o -8 4 1 236.03 267.65 24.45 o -7 4 1 1240.38 1217.26 63.27 o -6 4 1 3254.89 3124.42 139.19 o -5 4 1 3200.94 3098.26 129.47 o -4 4 1 541.31 632.26 13.75 o -3 4 1 1874.76 1594.85 35.87 o -2 4 1 108.89 95.90 5.25 o -1 4 1 213.36 155.55 5.27 o 0 4 1 5006.26 5111.84 105.39 o 1 4 1 8642.06 8785.92 203.59 o 2 4 1 529.92 555.55 13.53 o 3 4 1 6169.50 6804.86 139.23 o 4 4 1 104.42 88.71 7.07 o 5 4 1 1347.83 1277.53 65.84 o 6 4 1 2833.17 2760.36 159.90 o 7 4 1 574.23 607.88 35.11 o 8 4 1 188.71 185.57 31.58 o 9 4 1 353.20 359.82 42.24 o -10 5 1 412.83 475.37 50.39 o -9 5 1 28.56 8.86 23.15 o -8 5 1 2112.19 1876.33 73.31 o -7 5 1 1.12 -1.47 8.61 o -6 5 1 3941.99 3945.39 154.40 o -5 5 1 1458.30 1422.98 58.14 o -4 5 1 1211.71 1217.42 37.05 o -3 5 1 254.08 236.07 8.42 o -2 5 1 225.30 301.76 11.84 o -1 5 1 1441.54 1600.80 40.10 o 0 5 1 14322.47 13366.49 418.09 o 1 5 1 989.20 1037.66 16.96 o 2 5 1 5762.88 5487.56 134.16 o 3 5 1 381.37 393.00 13.26 o 4 5 1 847.98 776.11 33.08 o 5 5 1 141.01 169.36 14.41 o 6 5 1 31.13 28.27 8.17 o 7 5 1 189.54 182.68 20.08 o 8 5 1 4.78 4.14 19.75 o 9 5 1 12.19 7.65 21.94 o -9 6 1 8.27 -2.19 22.80 o -8 6 1 68.37 57.96 16.18 o -7 6 1 6.09 2.06 8.90 o -6 6 1 215.47 234.55 13.94 o -5 6 1 1291.90 1169.46 41.95 o -4 6 1 5.96 -0.29 5.10 o -3 6 1 3915.57 3642.94 99.18 o -2 6 1 3224.81 3174.87 69.46 o -1 6 1 739.63 740.93 13.28 o 0 6 1 11448.36 11645.62 246.16 o 1 6 1 3380.43 3142.61 62.13 o 2 6 1 44.60 49.84 5.93 o 3 6 1 3622.92 3556.44 73.13 o 4 6 1 3810.35 3691.11 130.66 o 5 6 1 1798.74 1641.62 68.24 o 6 6 1 136.95 129.59 12.84 o 7 6 1 948.41 940.84 109.26 o 8 6 1 7.90 -8.43 19.52 o 9 6 1 404.20 437.70 46.69 o -9 7 1 245.43 263.49 39.74 o -8 7 1 22.95 -0.54 13.80 o -7 7 1 50.17 61.19 13.08 o -6 7 1 1165.41 1036.76 36.51 o -5 7 1 463.80 551.95 26.53 o -4 7 1 1797.12 1589.75 60.52 o -3 7 1 42.18 48.34 5.40 o -2 7 1 8766.51 8572.19 223.67 o -1 7 1 812.82 827.91 31.48 o 0 7 1 892.65 728.39 22.07 o 1 7 1 60.27 71.71 3.70 o 2 7 1 831.73 1028.01 16.24 o 3 7 1 155.62 159.09 8.51 o 4 7 1 3.09 6.37 10.20 o 5 7 1 111.85 100.94 11.25 o 6 7 1 4576.60 4283.19 205.22 o 7 7 1 302.54 293.06 24.09 o 8 7 1 915.48 854.83 55.08 o 9 7 1 4.25 -16.36 20.73 o -9 8 1 359.14 388.36 45.63 o -8 8 1 24.76 14.73 15.54 o -7 8 1 367.75 312.04 23.33 o -6 8 1 1352.95 1340.73 82.67 o -5 8 1 64.88 74.70 9.75 o -4 8 1 538.57 536.49 18.18 o -3 8 1 333.68 255.17 8.73 o -2 8 1 33.18 59.12 4.32 o -1 8 1 2157.56 2133.87 70.82 o 0 8 1 2957.13 2979.37 95.18 o 1 8 1 1369.90 1135.95 29.65 o 2 8 1 444.99 497.26 12.05 o 3 8 1 3373.83 3234.80 80.86 o 4 8 1 951.22 928.71 52.07 o 5 8 1 2232.58 2070.74 75.44 o 6 8 1 631.25 565.92 44.08 o 7 8 1 143.98 136.85 19.36 o 8 8 1 224.43 227.49 24.21 o 9 8 1 70.66 46.84 28.69 o -9 9 1 9.51 -15.07 22.48 o -8 9 1 667.74 628.26 48.01 o -7 9 1 491.59 467.87 33.59 o -6 9 1 1058.36 1041.26 67.21 o -5 9 1 40.64 50.57 11.70 o -4 9 1 135.11 129.52 9.81 o -3 9 1 43.11 41.97 4.86 o -2 9 1 217.35 184.59 8.43 o -1 9 1 538.99 523.83 10.74 o 0 9 1 2112.04 1947.58 68.29 o 1 9 1 2192.56 2286.35 66.51 o 2 9 1 1930.22 1581.50 34.58 o 3 9 1 478.09 473.33 13.37 o 4 9 1 219.67 184.19 12.28 o 5 9 1 147.43 127.46 18.83 o 6 9 1 14.07 2.31 9.25 o 7 9 1 26.35 26.95 14.55 o 8 9 1 3.21 -8.35 14.04 o 9 9 1 5.63 -1.80 24.20 o -9 10 1 42.72 33.10 27.60 o -8 10 1 60.93 64.33 18.23 o -7 10 1 87.25 83.89 18.11 o -6 10 1 120.37 120.73 14.82 o -5 10 1 8.28 -8.97 9.41 o -4 10 1 9.82 12.27 6.89 o -3 10 1 2096.33 2005.48 59.10 o -2 10 1 343.42 335.61 9.79 o -1 10 1 1508.91 1407.30 58.27 o 0 10 1 1295.01 1319.38 40.43 o 1 10 1 37.61 17.21 3.63 o 2 10 1 3.82 5.50 3.78 o 3 10 1 161.04 182.57 7.56 o 4 10 1 145.01 128.31 11.29 o 5 10 1 1960.98 1826.50 65.03 o 6 10 1 8.12 -5.06 9.53 o 7 10 1 849.78 913.68 89.19 o 8 10 1 49.21 61.70 18.54 o -9 11 1 86.96 56.31 20.51 o -8 11 1 102.62 104.84 20.49 o -7 11 1 433.68 415.71 28.83 o -6 11 1 1376.19 1324.38 41.87 o -5 11 1 0.09 -9.19 9.19 o -4 11 1 1027.16 877.38 64.50 o -3 11 1 77.24 61.81 8.41 o -2 11 1 1622.45 1565.66 49.56 o -1 11 1 262.66 236.29 11.12 o 0 11 1 7.04 9.13 3.44 o 1 11 1 766.88 759.27 26.11 o 2 11 1 93.26 57.97 5.94 o 3 11 1 1249.40 1218.47 24.03 o 4 11 1 67.47 53.64 14.50 o 5 11 1 923.31 908.00 46.23 o 6 11 1 654.23 608.43 31.31 o 7 11 1 27.21 15.02 15.18 o 8 11 1 43.55 49.62 18.82 o -8 12 1 18.77 22.69 17.29 o -7 12 1 902.08 980.57 40.17 o -6 12 1 13.39 9.46 13.59 o -5 12 1 10.64 11.60 12.31 o -4 12 1 0.92 -10.29 10.29 o -3 12 1 177.41 190.89 10.80 o -2 12 1 11.13 4.29 4.84 o -1 12 1 698.03 612.05 27.95 o 0 12 1 76.06 107.85 6.21 o 1 12 1 4763.76 4583.90 127.15 o 2 12 1 608.65 662.02 15.51 o 3 12 1 2601.67 2517.05 67.07 o 4 12 1 59.12 42.59 10.96 o 5 12 1 125.87 134.09 14.95 o 6 12 1 164.01 163.20 20.62 o 7 12 1 344.90 337.78 28.59 o 8 12 1 0.53 -14.94 14.94 o -8 13 1 405.44 418.34 32.38 o -7 13 1 73.59 77.70 19.34 o -6 13 1 352.13 368.52 27.61 o -5 13 1 940.93 948.67 64.88 o -4 13 1 92.60 97.46 15.76 o -3 13 1 1.09 -3.70 10.07 o -2 13 1 2275.91 2186.44 102.12 o -1 13 1 420.47 423.18 14.40 o 0 13 1 377.09 349.73 18.58 o 1 13 1 570.44 573.11 17.27 o 2 13 1 528.88 503.61 25.83 o 3 13 1 632.24 636.59 27.43 o 4 13 1 715.73 732.10 30.81 o 5 13 1 492.85 472.37 28.18 o 6 13 1 331.63 355.92 38.33 o 7 13 1 161.06 153.57 24.08 o 8 13 1 56.43 37.46 19.12 o -8 14 1 10.56 10.20 17.34 o -7 14 1 3.33 6.82 15.44 o -6 14 1 18.79 19.66 15.97 o -5 14 1 60.57 79.88 16.63 o -4 14 1 8.05 17.45 12.40 o -3 14 1 5152.57 5411.79 286.79 o -2 14 1 20.03 23.26 8.30 o -1 14 1 2170.63 2470.59 33.56 o 0 14 1 90.10 101.03 10.34 o 1 14 1 3.80 0.64 7.38 o 2 14 1 14.20 11.01 8.08 o 3 14 1 18.15 24.86 11.77 o 4 14 1 49.25 48.50 21.41 o 5 14 1 2484.15 2396.00 56.15 o 6 14 1 160.21 147.53 21.49 o 7 14 1 1431.01 1480.55 51.62 o -8 15 1 58.95 84.74 31.66 o -7 15 1 771.89 803.39 39.82 o -6 15 1 110.69 134.32 21.14 o -5 15 1 76.02 74.88 17.21 o -4 15 1 1056.20 1039.36 59.31 o -3 15 1 1185.55 1305.16 98.11 o -2 15 1 1575.32 1697.38 55.99 o -1 15 1 1445.30 1507.59 37.00 o 0 15 1 164.96 176.26 12.92 o 1 15 1 180.17 202.88 14.02 o 2 15 1 847.58 876.88 48.72 o 3 15 1 1.21 -9.32 10.46 o 4 15 1 517.21 529.03 32.22 o 5 15 1 104.61 118.95 19.20 o 6 15 1 257.58 287.14 26.92 o 7 15 1 3.77 3.37 16.52 o -7 16 1 49.64 59.81 20.11 o -6 16 1 147.01 171.91 23.33 o -5 16 1 219.29 224.80 23.49 o -4 16 1 7.52 -5.03 12.24 o -3 16 1 21.97 30.57 12.81 o -2 16 1 49.75 47.90 10.16 o -1 16 1 182.52 187.58 17.76 o 0 16 1 0.14 -0.77 10.57 o 1 16 1 1597.68 1621.99 31.02 o 2 16 1 340.12 355.01 22.79 o 3 16 1 1900.04 1995.56 112.42 o 4 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