#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/17/2221797.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221797_Fobs loop_ _publ_author_name 'Hao, Xin-Qi' 'Li, Hong-Mei' 'Jiang, Hui' 'Ma, Yong-Tao' 'Song, Mao-Ping' _publ_section_title ; Bromido{dicyclohexyl[2'-(dimethylamino)biphenyl-2-yl]phosphine-\kP}[2-(4,6-dimethylpyrimidin-2-yl)ferrocenyl-\k^2^C^1^,N]palladium(II) dichloromethane solvate ; _journal_coeditor_code SI2165 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m529 _journal_page_last m530 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.195 _cell_angle_beta 76.590 _cell_angle_gamma 72.647 _cell_length_a 10.2059 _cell_length_b 10.3637 _cell_length_c 21.9003 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file si2165Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 277.47 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10289.80 9654.17 81.90 o 3 0 0 19814.96 21156.54 160.35 o 4 0 0 1544.31 1512.90 22.99 o 5 0 0 455.21 465.41 11.19 o 6 0 0 1427.95 1415.67 21.71 o 7 0 0 435.24 425.01 17.44 o 8 0 0 13.79 16.09 10.84 o 9 0 0 148.56 147.04 18.57 o 10 0 0 647.96 637.30 38.41 o 11 0 0 40.57 77.44 21.14 o -11 1 0 410.34 487.07 38.96 o -10 1 0 242.28 251.89 26.81 o -9 1 0 57.28 82.81 18.69 o -8 1 0 2851.70 2896.17 49.26 o -7 1 0 1394.88 1368.87 29.69 o -6 1 0 197.27 169.13 16.67 o -5 1 0 410.35 459.50 12.02 o -4 1 0 2911.35 3136.64 33.63 o -3 1 0 761.41 973.02 14.37 o -2 1 0 1447.27 1732.72 18.64 o -1 1 0 1516.81 1508.64 18.43 o 1 1 0 14158.39 14276.31 179.97 o 2 1 0 7207.87 7081.17 69.75 o 3 1 0 6479.66 6492.88 72.83 o 4 1 0 7037.79 7400.03 96.19 o 5 1 0 6280.48 6709.27 59.27 o 6 1 0 3868.72 3625.34 38.23 o 7 1 0 1921.72 2101.92 73.50 o 8 1 0 1093.68 1133.04 40.06 o 9 1 0 76.03 96.66 11.40 o 10 1 0 77.77 73.26 19.32 o 11 1 0 427.29 418.06 34.78 o -10 2 0 17.76 40.06 17.98 o -9 2 0 8.24 -1.74 13.01 o -8 2 0 353.68 350.16 18.77 o -7 2 0 49.96 68.63 7.70 o -6 2 0 1903.27 1947.04 28.61 o -5 2 0 395.89 484.59 12.87 o -4 2 0 8.37 23.08 4.25 o -3 2 0 5435.91 5209.20 48.21 o -2 2 0 168.89 155.06 6.07 o -1 2 0 6024.90 5404.98 50.97 o 0 2 0 38260.84 41508.55 382.05 o 1 2 0 1801.29 1872.27 22.64 o 2 2 0 7439.34 7357.94 73.05 o 3 2 0 1203.59 1337.47 21.18 o 4 2 0 12334.14 12112.70 120.48 o 5 2 0 8182.31 7871.70 162.18 o 6 2 0 1357.99 1312.04 29.14 o 7 2 0 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19.68 10.08 o 10 7 0 163.98 162.50 16.24 o 11 7 0 211.56 228.80 37.58 o -6 8 0 349.74 340.89 22.01 o -5 8 0 37.48 59.15 13.49 o -4 8 0 869.39 868.82 30.00 o -3 8 0 1022.06 977.19 30.87 o -2 8 0 430.40 431.83 20.88 o -1 8 0 1213.36 1241.75 32.42 o 0 8 0 1337.18 1182.69 62.85 o 1 8 0 917.27 824.92 25.84 o 2 8 0 673.28 587.42 43.45 o 3 8 0 634.19 658.14 22.06 o 4 8 0 1337.01 1337.97 30.72 o 5 8 0 29.93 25.16 11.51 o 6 8 0 110.55 82.65 14.75 o 7 8 0 137.22 150.79 19.48 o 8 8 0 442.65 423.02 21.68 o 9 8 0 10.57 10.19 15.10 o 10 8 0 207.70 185.18 17.14 o -5 9 0 134.45 162.48 17.46 o -4 9 0 26.82 43.52 11.88 o -3 9 0 486.18 515.52 25.07 o -2 9 0 264.03 296.84 19.42 o -1 9 0 0.15 -4.97 9.64 o 0 9 0 488.74 502.92 22.80 o 1 9 0 46.65 56.98 16.88 o 2 9 0 585.00 461.81 30.95 o 3 9 0 718.19 785.19 25.51 o 4 9 0 75.87 106.74 12.02 o 5 9 0 186.84 178.00 20.27 o 6 9 0 1.00 0.08 10.09 o 7 9 0 387.62 409.07 29.50 o 8 9 0 412.60 357.02 29.26 o 9 9 0 12.09 5.84 13.17 o 10 9 0 5.27 1.26 14.35 o -4 10 0 356.99 346.08 23.54 o -3 10 0 26.34 38.93 12.40 o -2 10 0 957.21 943.24 33.19 o -1 10 0 1109.67 1049.17 53.79 o 0 10 0 30.07 11.98 10.40 o 1 10 0 258.95 251.15 18.48 o 2 10 0 0.51 -12.86 8.57 o 3 10 0 138.59 152.87 14.60 o 4 10 0 179.06 110.02 18.77 o 5 10 0 411.64 376.02 29.34 o 6 10 0 27.61 20.27 14.04 o 7 10 0 15.92 33.52 15.69 o 8 10 0 600.48 601.81 37.54 o 9 10 0 24.97 28.31 17.11 o -2 11 0 352.96 364.61 24.14 o -1 11 0 472.12 502.44 26.88 o 0 11 0 61.31 26.68 12.97 o 1 11 0 897.76 893.58 33.19 o 2 11 0 499.65 523.37 25.67 o 3 11 0 8.51 4.95 10.67 o 4 11 0 1033.10 1059.93 48.42 o 5 11 0 268.63 327.60 28.86 o 6 11 0 1.94 -3.31 12.22 o 7 11 0 197.18 216.25 25.71 o 8 11 0 0.15 3.47 15.69 o 1 12 0 92.18 109.56 17.45 o 2 12 0 266.77 263.36 21.25 o 3 12 0 0.20 -18.34 12.22 o 4 12 0 747.48 821.77 44.79 o 5 12 0 826.60 861.35 46.92 o 6 12 0 53.88 46.14 19.32 o -5 -12 1 0.05 5.60 16.01 o -4 -12 1 842.75 907.49 48.34 o -3 -12 1 301.65 339.67 32.49 o -2 -12 1 34.65 30.78 13.13 o -1 -12 1 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