#------------------------------------------------------------------------------ #$Date: 2009-06-07 09:06:07 +0300 (Sun, 07 Jun 2009) $ #$Revision: 754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221812.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221812_Fobs loop_ _publ_author_name 'Wang, Guo-Ming' 'Li, Zeng-Xin' 'Xue, Shu-Yun' 'Liu, Hui-Luan' _publ_section_title ; Poly[tetraaqua-\m~3~-benzene-1,2-dicarboxylato-\m~3~-bromido-penta-\m~2~-bromido-octa-\m~3~-isonicotinato-heptacopper(I)trilanthanum(III)] ; _journal_coeditor_code SJ2614 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m550 _journal_page_last m551 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.480 _cell_angle_gamma 90.000 _cell_length_a 10.1071 _cell_length_b 19.6311 _cell_length_c 34.4015 _exptl_crystal_F_000 4848.00 _reflns_d_resolution_high 0.8106 _[local]_cod_data_source_file sj2614Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1543.21 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 677.85 322.73 159.61 o 2 0 0 138516.47 166435.38 4328.84 o 3 0 0 180118.56 205551.09 5385.11 o 4 0 0 53.33 499.25 326.74 o 5 0 0 5732.22 3681.23 386.44 o 6 0 0 80907.59 70625.05 2195.12 o 7 0 0 0.53 1205.39 442.35 o 8 0 0 79547.88 80496.77 2616.63 o 9 0 0 20176.67 20403.53 1172.89 o 10 0 0 564.25 958.10 662.96 o 11 0 0 43110.28 41684.04 3267.61 o 12 0 0 3739.34 5304.10 1417.78 o 1 1 0 4892.56 2499.97 99.77 o 3 1 0 108514.80 90199.01 1755.02 o 4 1 0 13094.12 13663.05 429.42 o 5 1 0 34779.50 32905.32 904.42 o 6 1 0 23272.49 23367.28 793.51 o 7 1 0 35215.17 33309.96 1206.20 o 8 1 0 3522.44 3426.58 428.66 o 9 1 0 18062.46 20079.86 1195.45 o 10 1 0 112.17 616.86 429.73 o 11 1 0 39157.93 37184.83 1784.61 o 12 1 0 1243.91 3449.34 914.03 o 0 2 0 76.76 731.79 89.02 o 2 2 0 89.11 328.38 93.15 o 3 2 0 7843.65 8810.23 300.17 o 4 2 0 343.76 1224.00 195.25 o 5 2 0 19847.78 21788.84 625.55 o 6 2 0 25148.12 24205.28 718.49 o 7 2 0 12069.94 12265.92 554.03 o 8 2 0 1691.99 1857.24 326.24 o 9 2 0 10891.45 10343.00 1303.59 o 10 2 0 708.44 1483.67 471.48 o 11 2 0 8334.97 7717.61 1183.23 o 12 2 0 1260.47 -956.08 1282.51 o 1 3 0 24118.65 28426.57 614.33 o 2 3 0 2184.63 1155.99 103.43 o 3 3 0 2428.01 2878.68 303.60 o 4 3 0 1026.65 824.38 166.33 o 5 3 0 216.30 618.76 189.46 o 6 3 0 18309.32 18372.70 613.97 o 7 3 0 8987.10 8708.54 486.66 o 8 3 0 92.98 281.44 292.55 o 9 3 0 1701.51 2233.01 557.71 o 10 3 0 46.90 -318.34 450.02 o 11 3 0 871.82 837.34 808.62 o 12 3 0 1815.66 1666.49 881.51 o 0 4 0 3366.23 4220.74 291.44 o 1 4 0 74174.23 80706.66 1575.51 o 2 4 0 42739.05 39513.95 948.30 o 3 4 0 28826.05 36420.33 811.06 o 4 4 0 283.32 261.56 126.93 o 5 4 0 77582.70 79663.15 1862.16 o 6 4 0 16846.69 19152.13 757.92 o 7 4 0 75289.53 75169.10 1890.52 o 8 4 0 9024.08 9612.80 624.44 o 9 4 0 40705.61 39651.20 1496.36 o 10 4 0 6767.73 7026.10 771.00 o 11 4 0 12494.50 11301.50 1009.57 o 12 4 0 811.71 463.99 836.70 o 1 5 0 206.93 485.47 141.47 o 2 5 0 36882.83 35094.58 890.10 o 3 5 0 2651.66 3737.62 269.41 o 4 5 0 149103.39 146006.14 2827.37 o 5 5 0 13293.46 13640.58 482.75 o 6 5 0 31146.71 31599.57 859.98 o 7 5 0 44314.43 42328.90 1246.10 o 8 5 0 1102.04 701.50 350.35 o 9 5 0 17205.88 18470.89 1058.91 o 10 5 0 19147.57 20127.21 1179.62 o 11 5 0 40126.05 37283.05 2607.88 o 12 5 0 41.04 1552.68 827.99 o 0 6 0 442624.09 465646.28 12022.00 o 2 6 0 327066.03 345497.69 6356.00 o 3 6 0 27978.99 26617.48 1062.86 o 4 6 0 144200.44 143760.86 3102.81 o 5 6 0 8860.70 7976.40 372.57 o 6 6 0 61178.36 59235.43 1537.69 o 7 6 0 1424.04 904.10 379.60 o 8 6 0 3540.88 4373.27 565.22 o 9 6 0 8039.54 8586.20 771.40 o 10 6 0 1139.55 1541.79 554.70 o 11 6 0 11590.92 14700.68 1104.09 o 12 6 0 4613.75 4968.44 917.93 o 1 7 0 10959.67 9212.75 376.03 o 3 7 0 481.00 1895.80 344.36 o 4 7 0 16163.87 15877.44 637.45 o 5 7 0 17828.87 17266.41 681.18 o 6 7 0 8739.88 9054.38 540.82 o 7 7 0 1399.97 1565.27 333.45 o 8 7 0 1215.21 1507.67 445.52 o 9 7 0 2079.61 1852.18 516.89 o 10 7 0 22.09 606.24 501.39 o 11 7 0 8633.01 7604.96 1045.88 o 0 8 0 27109.54 22717.53 1306.42 o 1 8 0 99198.87 111735.60 2266.85 o 2 8 0 44122.82 46010.76 1075.75 o 3 8 0 24411.05 25463.12 1302.67 o 4 8 0 206143.80 203511.56 4325.62 o 5 8 0 16495.73 18041.68 1533.07 o 6 8 0 24.75 174.24 243.35 o 7 8 0 48395.14 45836.14 1593.51 o 8 8 0 4310.81 5384.25 795.55 o 9 8 0 4613.29 4922.20 674.48 o 10 8 0 7873.41 8290.97 865.50 o 11 8 0 57.77 871.38 670.30 o 1 9 0 224693.25 225724.39 4333.14 o 2 9 0 545.75 1488.02 206.74 o 3 9 0 9721.49 12403.91 602.61 o 4 9 0 12.55 282.68 225.54 o 5 9 0 9547.87 9530.65 549.08 o 6 9 0 12630.65 14331.00 869.21 o 7 9 0 451.46 164.39 378.39 o 8 9 0 201.30 1041.05 479.38 o 9 9 0 576.92 722.58 494.52 o 10 9 0 423.87 1199.82 551.84 o 11 9 0 10876.70 12806.49 1323.80 o 0 10 0 12287.76 15133.06 822.82 o 1 10 0 853.81 1052.02 224.77 o 2 10 0 238.98 484.57 234.02 o 3 10 0 1813.25 1979.40 325.65 o 4 10 0 790.47 913.04 327.25 o 5 10 0 63836.54 64749.42 1704.92 o 6 10 0 1248.02 1439.16 428.79 o 7 10 0 25796.84 23498.06 1189.21 o 8 10 0 11773.78 12947.05 955.77 o 9 10 0 4167.78 5144.55 728.23 o 10 10 0 8915.84 9986.15 1145.24 o 11 10 0 1100.03 592.68 708.73 o 1 11 0 28438.93 28809.52 861.66 o 2 11 0 11209.57 10448.58 502.70 o 3 11 0 22862.17 23695.08 909.30 o 4 11 0 19779.46 19175.21 1336.36 o 5 11 0 30819.07 28435.10 1200.55 o 6 11 0 1819.78 2142.55 486.50 o 7 11 0 9079.79 9827.31 865.48 o 8 11 0 9322.50 8409.61 825.32 o 9 11 0 6905.01 6409.38 792.61 o 10 11 0 8938.46 10239.03 1204.68 o 11 11 0 4109.30 3600.88 951.53 o 0 12 0 70899.55 72199.62 2392.65 o 1 12 0 1889.70 2768.57 335.46 o 2 12 0 40167.31 38527.49 1148.83 o 3 12 0 688.71 1360.11 340.08 o 4 12 0 40463.21 40230.47 1487.43 o 5 12 0 33252.36 33945.05 1366.42 o 6 12 0 82336.34 77909.06 2402.67 o 7 12 0 5752.78 4841.58 685.42 o 8 12 0 6864.30 7097.74 1161.84 o 9 12 0 2533.23 2860.97 654.30 o 10 12 0 8022.17 7984.71 2098.54 o 1 13 0 53404.21 52608.18 1359.63 o 2 13 0 18058.01 17972.53 949.94 o 3 13 0 10102.55 9152.53 671.92 o 4 13 0 4950.80 5115.47 620.80 o 5 13 0 7185.98 9302.03 812.40 o 6 13 0 17006.24 17363.40 1099.76 o 7 13 0 1158.93 1089.57 512.22 o 8 13 0 17189.36 17100.57 1187.05 o 9 13 0 861.00 1063.68 686.79 o 10 13 0 2786.23 1691.67 856.00 o 0 14 0 101978.09 99684.74 4275.46 o 1 14 0 311.23 225.51 280.29 o 2 14 0 29629.72 29651.83 1130.89 o 3 14 0 1126.57 834.05 370.06 o 4 14 0 1003.39 512.71 444.53 o 5 14 0 11178.37 10481.97 1051.65 o 6 14 0 484.28 676.81 497.11 o 7 14 0 1289.56 954.39 542.70 o 8 14 0 5168.79 4258.98 728.51 o 9 14 0 455.12 374.62 667.56 o 10 14 0 4852.27 6840.08 1127.69 o 1 15 0 40407.83 42225.26 1915.67 o 2 15 0 2625.63 2576.13 482.56 o 3 15 0 66210.34 69972.45 2237.74 o 4 15 0 12.57 -68.13 452.44 o 5 15 0 11082.66 12705.01 993.53 o 6 15 0 635.41 -13.33 546.41 o 7 15 0 12.73 182.45 525.94 o 8 15 0 1486.98 1103.95 797.97 o 9 15 0 5916.68 7960.00 1129.13 o 0 16 0 221.48 -626.62 444.01 o 1 16 0 1610.30 1667.94 449.55 o 2 16 0 12085.13 14466.53 899.14 o 3 16 0 25388.44 23355.96 1261.43 o 4 16 0 2080.84 2527.10 596.69 o 5 16 0 8808.28 11416.82 980.32 o 6 16 0 760.21 494.53 557.35 o 7 16 0 2227.85 2231.81 651.44 o 8 16 0 2443.10 2437.85 845.66 o 9 16 0 1700.74 1053.99 807.07 o 1 17 0 19089.45 18719.33 1013.27 o 2 17 0 16700.07 16685.65 1111.54 o 3 17 0 31729.47 29753.29 1430.67 o 4 17 0 65.50 300.56 510.29 o 5 17 0 39818.08 38660.88 1685.02 o 6 17 0 2788.57 2799.46 794.04 o 7 17 0 1302.71 1793.67 675.40 o 8 17 0 3293.13 2947.71 837.54 o 0 18 0 1908.00 1958.33 1792.15 o 1 18 0 4256.62 5375.69 733.25 o 2 18 0 5767.55 5253.63 754.45 o 3 18 0 10452.21 11406.12 1002.31 o 4 18 0 5512.09 5901.38 806.83 o 5 18 0 19666.86 20942.76 1370.40 o 6 18 0 23847.02 21824.25 1545.99 o 7 18 0 9593.82 8464.33 1164.23 o 8 18 0 14104.83 12866.68 1438.36 o 1 19 0 337.27 1227.05 733.24 o 2 19 0 14627.21 16136.40 1186.54 o 3 19 0 48.71 -447.42 714.42 o 4 19 0 28015.99 26736.90 1529.05 o 5 19 0 1761.01 1308.49 665.03 o 6 19 0 27429.47 23018.27 1676.47 o 7 19 0 497.36 1191.90 774.15 o 0 20 0 338.29 446.73 1333.89 o 1 20 0 1229.32 3718.19 926.77 o 2 20 0 1783.92 1195.01 642.99 o 3 20 0 768.79 532.31 617.69 o 4 20 0 1657.75 720.10 652.43 o 5 20 0 11207.07 10668.36 2047.71 o 6 20 0 3483.27 4171.42 834.71 o 7 20 0 2498.76 2441.24 1048.01 o 1 21 0 11080.27 10914.75 1258.39 o 2 21 0 184.46 96.31 744.93 o 3 21 0 3668.99 3157.34 758.32 o 4 21 0 59.53 -945.40 630.26 o 5 21 0 4197.31 4589.74 848.98 o 6 21 0 1652.10 1304.12 830.65 o 0 22 0 262.14 -98.57 1155.62 o 1 22 0 3102.18 4322.92 1185.31 o 2 22 0 220.31 326.58 811.94 o 3 22 0 432.09 493.23 815.11 o 4 22 0 4206.03 4490.14 842.88 o 5 22 0 999.41 1146.20 721.92 o 1 23 0 39385.78 40235.12 2849.54 o 2 23 0 242.69 -287.47 772.07 o 3 23 0 24588.15 20783.50 2924.23 o 0 24 0 644.95 337.67 1503.77 o 1 24 0 393.74 800.37 1237.41 o -12 1 1 115.05 1560.89 907.09 o -11 1 1 8536.39 8225.03 957.73 o -10 1 1 1250.67 672.47 653.57 o -9 1 1 4417.84 3547.50 475.07 o -8 1 1 1454.68 1692.00 314.56 o -7 1 1 58280.11 57288.28 1502.01 o -6 1 1 4523.23 5366.09 395.19 o -5 1 1 121159.70 125145.02 2476.48 o -4 1 1 16238.90 14932.34 530.88 o -3 1 1 61719.64 65763.57 1319.34 o -2 1 1 11639.42 10241.21 278.41 o -1 1 1 64.09 501.44 83.24 o 0 1 1 2349.05 2171.13 172.68 o 1 1 1 11084.11 10845.85 245.30 o 2 1 1 4331.35 5146.27 236.05 o 3 1 1 8280.38 8654.49 297.76 o 4 1 1 13154.42 11638.88 399.27 o 5 1 1 20213.77 20727.65 655.94 o 6 1 1 13146.21 12692.98 515.29 o 7 1 1 3394.66 3602.64 390.89 o 8 1 1 3675.27 3988.61 405.52 o 9 1 1 10688.68 11889.56 723.56 o 10 1 1 3424.86 4655.66 716.43 o 11 1 1 2084.85 1845.86 865.14 o 12 1 1 59.86 -1.88 651.39 o -12 2 1 1126.29 2076.34 1226.93 o -11 2 1 30884.59 33014.48 4394.91 o -10 2 1 10.99 109.06 368.79 o -9 2 1 24426.47 25359.87 1131.36 o -8 2 1 188.28 481.93 266.94 o -7 2 1 58765.04 56669.17 1360.59 o -6 2 1 31348.71 28178.09 793.08 o -5 2 1 402.91 965.60 208.41 o -4 2 1 20289.09 20470.64 555.58 o -3 2 1 111054.60 117445.80 2246.29 o -2 2 1 10212.66 12609.47 356.37 o -1 2 1 5756.85 5591.59 171.99 o 0 2 1 88108.80 101021.27 1872.99 o 1 2 1 1771.55 1369.23 94.70 o 2 2 1 2207.66 1803.41 112.30 o 3 2 1 123.86 378.76 105.16 o 4 2 1 19400.41 19411.13 695.64 o 5 2 1 76610.84 77340.15 1629.93 o 6 2 1 1644.15 2841.79 280.26 o 7 2 1 14212.61 14519.64 603.81 o 8 2 1 89054.65 87111.85 2174.54 o 9 2 1 20445.07 17383.55 859.85 o 10 2 1 3744.14 4457.57 619.60 o 11 2 1 21068.17 20753.82 3061.02 o 12 2 1 3394.05 4114.27 965.78 o -12 3 1 241.21 1687.29 845.81 o -11 3 1 25012.82 22321.14 1464.00 o -10 3 1 1232.41 691.84 508.93 o -9 3 1 5013.13 3794.36 744.09 o -8 3 1 1.45 -321.88 274.66 o -7 3 1 4462.50 4388.06 414.42 o -6 3 1 39244.12 40333.85 1018.95 o -5 3 1 70963.41 66958.67 1449.11 o -3 3 1 4237.11 5712.45 334.22 o -2 3 1 9669.64 11314.62 319.51 o -1 3 1 33112.90 35063.24 730.51 o 0 3 1 447205.09 489336.66 8822.19 o 1 3 1 39421.41 40932.61 922.56 o 2 3 1 535558.50 577593.31 11353.59 o 3 3 1 14109.49 14714.27 407.81 o 4 3 1 385919.44 377826.56 6938.58 o 5 3 1 89806.05 84282.61 1759.40 o 6 3 1 35485.96 38770.99 988.62 o 7 3 1 7888.30 7349.48 446.80 o 8 3 1 35977.89 34147.19 1119.62 o 9 3 1 5509.42 7113.56 991.27 o 10 3 1 528.11 1359.76 563.12 o 11 3 1 7581.63 4155.91 816.05 o 12 3 1 85.01 353.77 720.64 o -12 4 1 351.07 1285.30 845.22 o -11 4 1 8473.07 8287.88 880.16 o -10 4 1 2536.79 4108.75 665.38 o -9 4 1 9901.36 11552.28 738.01 o -8 4 1 1351.34 2087.45 382.28 o -7 4 1 43302.83 41437.67 1220.53 o -6 4 1 25903.79 23936.97 721.31 o -5 4 1 490.93 577.56 175.50 o -4 4 1 126.17 72.83 118.92 o -3 4 1 551.64 1618.57 148.26 o -2 4 1 36680.07 49380.51 1030.12 o -1 4 1 19977.05 22173.79 528.57 o 0 4 1 7287.18 7135.42 252.73 o 1 4 1 28421.40 28447.02 634.87 o 3 4 1 4382.81 3373.62 256.20 o 4 4 1 18351.17 20660.01 598.63 o 5 4 1 7862.50 7882.44 376.18 o 6 4 1 5865.05 5337.48 361.21 o 7 4 1 341.60 359.49 253.44 o 8 4 1 37.67 543.41 317.31 o 9 4 1 24655.13 24675.20 1432.78 o 10 4 1 883.40 2448.70 634.20 o 11 4 1 24303.38 25116.65 1380.35 o 12 4 1 259.85 1652.06 721.36 o -12 5 1 17093.87 15174.35 1676.47 o -11 5 1 4693.21 5762.21 893.81 o -10 5 1 5674.36 6008.46 728.04 o -9 5 1 40633.88 45765.70 2236.20 o -8 5 1 23906.90 24572.02 1294.66 o -7 5 1 77.13 1.91 250.66 o -6 5 1 197.59 815.17 212.29 o -5 5 1 1816.90 2274.69 229.06 o -4 5 1 448.88 1271.50 171.58 o -3 5 1 196652.78 204122.73 3831.06 o -2 5 1 15161.81 14606.19 413.84 o -1 5 1 62931.45 70043.48 1422.04 o 0 5 1 7878.46 8444.29 414.81 o 1 5 1 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