#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:04:59 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181139 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/18/2221814.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221814_Fobs loop_ _publ_author_name 'Zhang, Xiao-Qin' 'Luo, Mei-Ming' _publ_section_title ; [3,3'-Dimesityl-1,1'-(4,5:16,17-dibenzo-3,6,9,12,15,18-hexaoxaeicosane-1,20-diyl)diimidazolin-2-ylidene]dithiocyanatopalladium(II) ; _journal_coeditor_code SJ2617 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m568 _journal_page_last m569 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.133 _cell_angle_gamma 90.000 _cell_length_a 14.1433 _cell_length_b 19.8035 _cell_length_c 17.1007 _exptl_crystal_F_000 2040.00 _reflns_d_resolution_high 0.8248 _cod_data_source_file sj2617Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZXQ1 IN P21/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 477.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12447.22 15236.56 33.56 o 4 0 0 2382.92 2130.65 39.24 o 6 0 0 4124.43 3893.50 63.68 o 8 0 0 2346.81 2174.21 58.54 o 10 0 0 315.69 299.96 36.27 o 12 0 0 3895.80 3781.64 108.04 o 14 0 0 1264.57 1238.59 87.23 o 16 0 0 138.99 118.51 121.19 o 1 1 0 253.94 558.88 8.88 o 2 1 0 22562.00 22310.46 58.49 o 3 1 0 41878.13 41329.32 543.31 o 4 1 0 16001.24 18698.31 107.00 o 5 1 0 6154.55 7281.33 75.67 o 6 1 0 2492.07 2574.15 53.79 o 7 1 0 911.56 1201.13 42.47 o 8 1 0 1822.79 1757.94 53.45 o 9 1 0 1370.64 1316.49 51.12 o 10 1 0 2835.84 2364.86 75.51 o 11 1 0 324.13 293.22 43.45 o 12 1 0 2058.38 1954.87 79.01 o 13 1 0 231.05 286.70 80.62 o 14 1 0 390.80 307.51 61.56 o 15 1 0 77.18 46.79 108.54 o 16 1 0 1374.31 1165.29 159.39 o 0 2 0 49929.75 45097.50 269.50 o 1 2 0 31582.27 29113.03 240.68 o 2 2 0 18018.69 21430.10 61.19 o 3 2 0 2814.61 3000.49 39.37 o 4 2 0 810.85 698.78 25.64 o 5 2 0 12538.61 13487.56 106.37 o 6 2 0 18861.14 18487.64 136.35 o 7 2 0 931.14 853.93 38.31 o 8 2 0 3566.51 3081.99 69.73 o 9 2 0 1706.99 1905.93 61.03 o 10 2 0 192.66 178.90 38.47 o 11 2 0 547.54 543.00 57.96 o 12 2 0 747.14 740.70 91.89 o 13 2 0 631.62 580.88 93.30 o 14 2 0 714.67 737.57 67.90 o 15 2 0 131.54 2.47 107.69 o 16 2 0 19.64 0.05 115.75 o 1 3 0 1915.80 1667.80 20.26 o 2 3 0 67.69 68.37 12.62 o 3 3 0 25542.54 26229.30 120.92 o 4 3 0 2194.16 2117.74 40.83 o 5 3 0 1351.74 1058.58 36.45 o 6 3 0 987.11 1047.84 40.43 o 7 3 0 14087.88 15719.83 140.30 o 8 3 0 1772.42 1522.81 53.29 o 9 3 0 260.45 208.39 37.51 o 10 3 0 4945.37 4827.94 101.99 o 11 3 0 1370.51 1379.93 66.44 o 12 3 0 357.02 316.40 48.97 o 13 3 0 832.53 1080.56 67.87 o 14 3 0 87.01 0.03 88.76 o 15 3 0 201.08 177.10 96.03 o 16 3 0 281.13 264.54 108.99 o 0 4 0 404.14 441.83 13.20 o 1 4 0 219.00 201.20 14.40 o 2 4 0 10769.10 12089.62 55.94 o 3 4 0 2844.03 2390.15 41.97 o 4 4 0 7841.10 7012.23 72.72 o 5 4 0 20223.50 20436.02 135.08 o 6 4 0 5749.36 5648.97 81.18 o 7 4 0 851.28 868.83 39.24 o 8 4 0 3505.33 3306.25 75.11 o 9 4 0 10417.25 11541.51 148.76 o 10 4 0 69.41 17.02 69.04 o 11 4 0 225.96 273.95 73.86 o 12 4 0 13.65 15.27 60.29 o 13 4 0 4.40 58.96 71.05 o 14 4 0 191.16 209.45 90.94 o 15 4 0 140.09 126.04 93.35 o 16 4 0 9.28 60.58 84.94 o 1 5 0 412.90 245.50 17.23 o 2 5 0 16.29 53.02 15.80 o 3 5 0 146.03 116.34 19.49 o 4 5 0 173.83 141.65 20.04 o 5 5 0 10098.93 9403.57 97.86 o 6 5 0 147.47 180.10 28.50 o 7 5 0 10642.52 11600.50 127.44 o 8 5 0 3.82 35.39 51.33 o 9 5 0 3641.92 4190.19 96.32 o 10 5 0 792.74 839.75 56.74 o 11 5 0 498.84 466.77 49.60 o 12 5 0 11.24 48.65 64.64 o 13 5 0 1303.90 1451.78 109.84 o 14 5 0 104.90 0.05 92.58 o 15 5 0 85.80 66.44 86.14 o 16 5 0 21.58 0.05 95.76 o 0 6 0 63.43 184.15 14.26 o 1 6 0 3386.71 3567.71 38.02 o 2 6 0 17951.44 17154.40 82.64 o 3 6 0 42059.39 37744.30 176.78 o 4 6 0 4070.23 4360.38 66.97 o 5 6 0 8062.14 7995.59 94.54 o 6 6 0 275.99 247.68 28.85 o 7 6 0 25.89 0.03 49.52 o 8 6 0 990.16 1200.82 52.33 o 9 6 0 8247.96 9102.63 135.93 o 10 6 0 317.08 204.06 73.78 o 11 6 0 730.14 919.89 56.47 o 12 6 0 6.52 63.63 69.81 o 13 6 0 260.91 323.71 56.10 o 14 6 0 13.04 7.13 80.38 o 15 6 0 238.02 150.62 99.47 o 16 6 0 34.70 0.05 105.49 o 1 7 0 6908.20 7092.45 55.97 o 2 7 0 14094.09 16137.26 86.56 o 3 7 0 1543.64 1511.09 43.45 o 4 7 0 1087.32 1273.01 42.87 o 5 7 0 13606.97 14937.43 131.69 o 6 7 0 2237.91 2281.66 59.84 o 7 7 0 4848.56 4931.39 86.56 o 8 7 0 8.24 28.90 54.19 o 9 7 0 506.55 547.42 53.50 o 10 7 0 511.09 569.43 53.98 o 11 7 0 370.54 496.52 52.60 o 12 7 0 184.43 40.83 94.62 o 13 7 0 1877.55 2088.39 132.96 o 14 7 0 49.64 0.05 95.23 o 15 7 0 281.93 343.07 59.31 o 16 7 0 39.60 0.05 106.21 o 0 8 0 1531.64 1633.23 29.03 o 1 8 0 71.26 70.95 19.59 o 2 8 0 5.73 0.03 27.71 o 3 8 0 9478.04 10183.64 116.84 o 4 8 0 3363.67 3558.44 67.16 o 5 8 0 15206.30 16026.39 142.85 o 6 8 0 2422.02 2432.07 61.80 o 7 8 0 89.87 82.21 51.09 o 8 8 0 917.20 1035.19 53.74 o 9 8 0 1300.13 1388.07 62.52 o 10 8 0 320.10 366.13 46.87 o 11 8 0 2379.31 2658.51 94.54 o 12 8 0 323.44 256.24 99.66 o 13 8 0 58.54 175.51 96.37 o 14 8 0 357.52 399.91 106.61 o 15 8 0 457.04 445.78 119.78 o 1 9 0 5251.07 4976.94 56.63 o 2 9 0 382.22 286.99 25.80 o 3 9 0 0.29 0.03 46.29 o 4 9 0 4594.05 5233.05 84.79 o 5 9 0 76.23 96.05 33.41 o 6 9 0 373.45 479.90 37.30 o 7 9 0 388.78 465.66 40.59 o 8 9 0 318.43 368.55 42.90 o 9 9 0 2.35 0.03 70.07 o 10 9 0 30.46 61.83 66.15 o 11 9 0 696.34 899.66 66.39 o 12 9 0 422.66 228.22 110.95 o 13 9 0 1137.52 1188.70 130.25 o 14 9 0 147.80 386.87 65.06 o 15 9 0 302.66 323.55 121.08 o 0 10 0 30748.68 31521.76 136.62 o 1 10 0 2647.85 2726.54 48.54 o 2 10 0 1833.65 1840.58 41.94 o 3 10 0 3311.42 3191.93 86.19 o 4 10 0 570.84 514.97 41.23 o 5 10 0 26.66 14.93 48.89 o 6 10 0 479.62 525.76 39.42 o 7 10 0 20.87 0.03 57.88 o 8 10 0 2121.56 2330.68 75.69 o 9 10 0 315.82 296.91 44.46 o 10 10 0 19.94 47.62 41.07 o 11 10 0 1196.11 1165.32 69.94 o 12 10 0 1740.16 1910.25 131.13 o 13 10 0 67.80 84.60 94.70 o 14 10 0 1020.84 1171.02 134.55 o 15 10 0 112.67 150.30 112.86 o 1 11 0 10.48 7.77 35.61 o 2 11 0 3935.41 4159.33 60.79 o 3 11 0 1868.29 1882.26 78.93 o 4 11 0 9071.44 9637.46 142.11 o 5 11 0 728.57 689.08 47.32 o 6 11 0 85.08 101.01 57.21 o 7 11 0 41.50 56.18 62.33 o 8 11 0 465.15 472.42 49.18 o 9 11 0 1588.18 1719.29 72.91 o 10 11 0 1014.18 1102.83 67.82 o 11 11 0 1.54 91.57 79.48 o 12 11 0 234.74 149.95 102.02 o 13 11 0 58.83 0.05 97.49 o 14 11 0 87.66 16.20 104.70 o 15 11 0 24.19 46.63 102.87 o 0 12 0 10394.89 9542.34 85.42 o 1 12 0 3179.69 3464.40 58.78 o 2 12 0 2514.28 2516.22 54.16 o 3 12 0 403.54 399.51 63.47 o 4 12 0 981.86 968.25 77.15 o 5 12 0 241.48 184.21 35.13 o 6 12 0 4286.39 4405.26 97.78 o 7 12 0 80.73 0.03 71.79 o 8 12 0 2915.52 3068.99 92.26 o 9 12 0 74.56 0.03 85.24 o 10 12 0 50.40 10.37 81.92 o 11 12 0 330.82 299.56 96.85 o 12 12 0 1182.68 1214.26 117.24 o 13 12 0 43.88 62.01 95.79 o 14 12 0 651.31 690.48 121.32 o 1 13 0 1020.99 1076.08 41.33 o 2 13 0 3931.70 3916.67 108.81 o 3 13 0 875.68 856.77 66.89 o 4 13 0 4397.07 4573.88 118.85 o 5 13 0 7.46 18.24 32.32 o 6 13 0 321.20 136.96 81.71 o 7 13 0 157.96 110.98 84.71 o 8 13 0 649.76 721.53 63.13 o 9 13 0 385.72 534.91 54.85 o 10 13 0 2737.04 3078.78 149.02 o 11 13 0 83.48 92.61 89.96 o 12 13 0 90.92 0.05 101.97 o 13 13 0 1.58 0.05 91.60 o 14 13 0 26.32 2.89 93.22 o 0 14 0 106.53 133.33 22.56 o 1 14 0 63.96 98.07 41.44 o 2 14 0 1169.98 1155.64 74.31 o 3 14 0 854.03 880.97 74.34 o 4 14 0 433.02 607.98 79.27 o 5 14 0 232.24 216.87 82.40 o 6 14 0 6560.87 6473.45 132.27 o 7 14 0 3.57 104.83 76.62 o 8 14 0 2197.22 2124.74 91.55 o 9 14 0 1271.51 1441.81 86.43 o 10 14 0 4.21 0.03 94.41 o 11 14 0 68.93 19.35 89.11 o 12 14 0 411.95 518.37 89.43 o 13 14 0 12.70 0.05 97.91 o 1 15 0 382.23 323.95 36.06 o 2 15 0 1319.74 1451.96 89.58 o 3 15 0 193.22 133.46 66.73 o 4 15 0 3145.52 3334.91 116.76 o 5 15 0 2988.87 3016.24 91.44 o 6 15 0 877.84 738.55 62.36 o 7 15 0 849.08 955.37 72.06 o 8 15 0 536.34 599.39 62.99 o 9 15 0 817.48 721.77 116.57 o 10 15 0 683.12 755.54 108.28 o 11 15 0 7.08 0.05 93.59 o 12 15 0 13.68 35.08 81.63 o 13 15 0 154.60 152.52 60.45 o 0 16 0 724.41 571.79 40.01 o 1 16 0 658.15 669.22 38.97 o 2 16 0 567.74 674.92 85.82 o 3 16 0 2454.80 2469.16 115.59 o 4 16 0 355.31 235.43 87.97 o 5 16 0 460.17 336.73 93.06 o 6 16 0 2268.54 2274.13 92.45 o 7 16 0 300.99 377.53 54.19 o 8 16 0 592.86 537.00 66.86 o 9 16 0 922.02 1139.52 124.40 o 10 16 0 267.85 188.93 109.36 o 11 16 0 361.23 388.77 102.31 o 12 16 0 112.40 163.34 98.68 o 1 17 0 2500.12 2607.10 78.48 o 2 17 0 41.22 27.97 82.59 o 3 17 0 0.95 0.03 89.96 o 4 17 0 769.39 885.21 97.75 o 5 17 0 254.02 245.32 96.95 o 6 17 0 836.96 741.70 63.89 o 7 17 0 992.36 1023.79 74.05 o 8 17 0 71.55 0.05 90.01 o 9 17 0 161.85 0.03 109.97 o 10 17 0 62.74 73.12 94.81 o 11 17 0 26.26 0.05 104.94 o 0 18 0 10.35 0.03 73.97 o 1 18 0 1934.13 1963.54 75.21 o 2 18 0 400.66 324.27 98.31 o 3 18 0 2828.22 3123.58 151.62 o 4 18 0 7.86 0.03 94.91 o 5 18 0 768.57 789.13 63.79 o 6 18 0 7.22 0.05 79.27 o 7 18 0 97.06 25.85 83.73 o 8 18 0 17.77 0.05 91.41 o 9 18 0 565.50 485.70 112.23 o 10 18 0 37.67 0.05 99.29 o 11 18 0 485.17 298.50 127.39 o 1 19 0 4750.61 5056.96 108.59 o 2 19 0 1.96 0.03 89.19 o 3 19 0 78.38 19.51 85.77 o 4 19 0 16.83 146.72 74.26 o 5 19 0 239.26 211.89 55.73 o 6 19 0 4.25 0.05 84.76 o 7 19 0 53.51 59.73 87.09 o 8 19 0 12.46 26.09 87.25 o 9 19 0 48.31 140.67 48.97 o 10 19 0 1.68 0.05 110.48 o 0 20 0 827.15 690.77 79.19 o 1 20 0 659.38 529.98 72.99 o 2 20 0 287.69 296.72 61.00 o 3 20 0 1027.63 969.74 82.16 o 4 20 0 3.60 0.05 88.60 o 5 20 0 190.70 68.37 100.93 o 6 20 0 159.97 22.80 100.30 o 7 20 0 96.62 0.05 104.80 o 8 20 0 49.25 0.05 101.25 o 9 20 0 275.32 402.53 65.41 o 1 21 0 633.01 584.75 71.42 o 2 21 0 15.78 9.70 94.09 o 3 21 0 33.79 0.05 99.21 o 4 21 0 450.30 441.83 115.57 o 5 21 0 581.71 731.44 69.62 o 6 21 0 108.25 85.95 100.91 o 7 21 0 350.20 306.75 67.77 o 8 21 0 182.41 98.73 109.20 o 0 22 0 682.24 629.66 72.83 o 1 22 0 286.85 244.65 59.04 o 2 22 0 286.38 199.11 101.67 o 3 22 0 239.91 233.44 61.59 o 4 22 0 0.19 150.30 84.31 o 5 22 0 32.44 0.05 105.94 o 6 22 0 649.72 706.68 83.73 o 1 23 0 20.10 0.05 95.58 o 2 23 0 176.06 160.72 55.65 o 3 23 0 24.92 64.27 91.52 o 4 23 0 621.05 686.45 86.22 o 0 24 0 57.25 5.78 98.97 o -15 0 1 1715.70 2082.13 151.68 o -13 0 1 99.94 178.29 82.80 o -11 0 1 5063.89 5005.12 113.68 o -9 0 1 1634.44 1831.78 59.47 o -7 0 1 314.83 251.12 26.91 o -5 0 1 15675.12 15085.13 109.10 o -3 0 1 8704.93 11901.23 74.23 o -1 0 1 6563.61 6818.61 37.09 o 1 0 1 29508.46 25779.36 200.99 o 3 0 1 82720.53 76559.38 769.65 o 5 0 1 5.35 0.00 30.70 o 7 0 1 391.64 358.95 29.69 o 9 0 1 102.53 70.52 44.20 o 11 0 1 11088.86 11262.66 165.04 o 13 0 1 4.34 6.20 69.06 o 15 0 1 1291.07 1490.75 153.00 o -16 1 1 67.57 2.73 108.81 o -15 1 1 1180.19 1091.32 142.87 o -14 1 1 23.64 0.03 89.53 o -13 1 1 2613.53 2707.61 95.58 o -12 1 1 29.23 0.03 78.24 o -11 1 1 489.71 811.64 55.65 o -10 1 1 72.19 101.99 54.35 o -9 1 1 27.84 46.48 47.03 o -8 1 1 3259.31 3444.17 72.86 o -7 1 1 3736.32 3981.97 69.33 o -6 1 1 3326.96 4118.74 64.29 o -5 1 1 4394.93 4602.46 60.34 o -4 1 1 1253.27 1577.18 34.17 o -3 1 1 3.80 37.86 26.49 o -2 1 1 5636.45 5835.11 45.15 o -1 1 1 78394.55 42661.14 371.86 o 1 1 1 44657.98 39499.01 262.21 o 2 1 1 916.02 1241.06 18.69 o 3 1 1 652.93 1118.26 27.71 o 4 1 1 2528.64 2739.16 44.81 o 5 1 1 3836.56 4324.24 70.31 o 6 1 1 3659.12 3902.27 63.07 o 7 1 1 10839.77 12765.60 125.22 o 8 1 1 163.95 148.44 25.05 o 9 1 1 640.23 848.18 42.84 o 10 1 1 187.67 178.56 36.32 o 11 1 1 968.35 832.43 100.45 o 12 1 1 16.32 108.70 69.54 o 13 1 1 691.06 632.66 102.36 o 14 1 1 4.08 29.53 82.90 o 15 1 1 1077.48 1206.44 137.97 o 16 1 1 78.71 43.61 111.30 o -16 2 1 36.93 0.05 106.10 o -15 2 1 794.41 670.86 134.28 o -14 2 1 57.07 0.03 97.14 o -13 2 1 23.50 0.03 82.13 o -12 2 1 1006.35 1101.21 65.75 o -11 2 1 4955.03 5214.33 114.43 o -10 2 1 587.69 537.85 47.88 o -9 2 1 2402.61 2526.10 67.61 o -8 2 1 712.73 657.18 39.16 o -7 2 1 4180.29 5025.30 78.50 o -6 2 1 3685.29 3308.58 60.63 o -5 2 1 2412.97 2352.74 45.55 o -4 2 1 22588.41 23704.04 125.06 o -3 2 1 15985.07 14622.20 85.05 o -2 2 1 8917.24 9030.31 58.99 o -1 2 1 16960.34 16176.66 66.65 o 0 2 1 14431.32 12921.65 38.97 o 1 2 1 2516.25 2396.01 19.65 o 2 2 1 187.81 402.35 14.69 o 3 2 1 18.48 98.31 27.25 o 4 2 1 406.88 365.05 24.10 o 5 2 1 563.66 576.56 30.52 o 6 2 1 1313.26 1407.82 43.64 o 7 2 1 187.66 122.35 25.24 o 8 2 1 3.72 61.61 44.35 o 9 2 1 1232.84 1254.79 56.15 o 10 2 1 531.52 465.61 48.01 o 11 2 1 3553.66 3922.24 100.03 o 12 2 1 1146.44 1297.85 92.37 o 13 2 1 195.27 110.56 95.42 o 14 2 1 374.65 393.60 62.28 o 15 2 1 820.06 691.09 124.34 o 16 2 1 246.92 246.46 117.13 o -16 3 1 221.46 102.07 110.26 o -15 3 1 130.14 20.20 107.29 o -14 3 1 147.06 0.03 90.83 o -13 3 1 252.58 302.82 47.48 o -12 3 1 400.84 412.58 47.51 o -11 3 1 169.04 139.29 42.02 o -10 3 1 1399.33 1495.92 63.05 o -9 3 1 5513.44 4995.37 95.74 o -8 3 1 3151.79 3118.73 72.54 o -7 3 1 4443.59 5337.08 82.27 o -6 3 1 382.14 400.68 26.88 o -5 3 1 22860.60 28511.52 155.39 o -4 3 1 13199.93 13829.35 98.65 o -3 3 1 2605.10 3738.35 46.29 o -2 3 1 4505.18 4740.19 45.57 o -1 3 1 23535.81 19766.46 83.88 o 0 3 1 553.71 733.11 13.15 o 1 3 1 1851.15 1732.20 19.46 o 2 3 1 32657.73 31928.70 84.23 o 3 3 1 9492.67 12108.29 83.17 o 4 3 1 9827.14 10606.40 87.89 o 5 3 1 15361.32 16174.14 119.89 o 6 3 1 7374.28 8586.71 95.55 o 7 3 1 8733.97 9895.74 113.05 o 8 3 1 3772.52 4328.00 83.43 o 9 3 1 2968.38 3500.14 81.87 o 10 3 1 2230.10 2560.94 80.57 o 11 3 1 93.87 143.46 39.85 o 12 3 1 0.78 1.91 61.75 o 13 3 1 626.23 591.70 98.78 o 14 3 1 0.74 87.46 71.61 o 15 3 1 39.42 47.93 94.38 o 16 3 1 188.74 159.89 101.22 o -16 4 1 16.32 0.05 88.79 o -15 4 1 62.02 2.55 87.28 o -14 4 1 474.76 451.71 93.24 o -13 4 1 124.41 63.97 75.88 o -12 4 1 395.39 404.89 48.07 o -11 4 1 472.29 506.73 51.46 o -10 4 1 315.61 354.31 44.28 o -9 4 1 7857.76 8870.97 127.92 o -8 4 1 3834.50 3841.88 80.04 o -7 4 1 322.35 347.71 30.73 o -6 4 1 21049.41 22842.77 157.11 o -5 4 1 11.22 89.74 20.47 o -4 4 1 577.61 856.02 30.20 o -3 4 1 3978.10 4365.57 54.93 o -2 4 1 12729.87 13274.40 83.91 o -1 4 1 1054.14 975.36 23.68 o 0 4 1 2179.81 2406.69 24.29 o 1 4 1 164.57 151.70 11.59 o 2 4 1 1790.18 1993.90 24.95 o 3 4 1 4149.93 5121.94 57.61 o 4 4 1 537.80 497.61 27.36 o 5 4 1 1069.91 1195.86 39.29 o 6 4 1 19924.30 21339.61 156.24 o 7 4 1 870.68 846.14 42.31 o 8 4 1 4884.56 5174.72 90.11 o 9 4 1 1976.04 2176.57 71.00 o 10 4 1 7.04 6.28 65.62 o 11 4 1 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