#------------------------------------------------------------------------------ #$Date: 2009-06-07 09:06:07 +0300 (Sun, 07 Jun 2009) $ #$Revision: 754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221817.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221817_Fobs loop_ _publ_author_name 'Tang, Si-Ping' _publ_section_title ; [1-Phenyl-2-(4-pyridyl)ethylidene]hydrazine ; _journal_coeditor_code SJ2620 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1090 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.7428 _cell_length_b 10.8751 _cell_length_c 17.6358 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file sj2620Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' im in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 131.82 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 55.21 51.24 2.11 o 4 0 0 440.43 456.32 6.68 o 6 0 0 155.23 169.19 7.75 o 1 1 0 412.15 416.59 4.86 o 2 1 0 603.25 581.85 6.96 o 3 1 0 0.50 0.69 0.28 o 4 1 0 20.69 18.77 1.36 o 5 1 0 395.36 435.04 7.24 o 6 1 0 4.33 4.02 1.20 o 7 1 0 0.11 -0.78 0.89 o 0 2 0 4024.28 3921.48 92.70 o 1 2 0 2329.53 2330.81 72.25 o 2 2 0 689.57 720.29 7.32 o 3 2 0 58.15 53.68 1.38 o 4 2 0 43.68 43.41 1.25 o 5 2 0 168.98 178.99 4.15 o 6 2 0 14.99 13.49 1.41 o 7 2 0 0.00 -1.04 1.46 o 1 3 0 467.54 423.69 4.56 o 2 3 0 356.57 373.38 3.83 o 3 3 0 276.99 302.89 3.56 o 4 3 0 62.88 62.64 1.88 o 5 3 0 12.26 11.79 1.21 o 6 3 0 3.46 5.27 1.28 o 0 4 0 111.38 115.70 1.94 o 1 4 0 479.74 489.31 5.33 o 2 4 0 123.74 147.07 1.91 o 3 4 0 105.60 109.74 2.17 o 4 4 0 8.11 8.49 0.97 o 5 4 0 2.20 1.65 2.05 o 6 4 0 2.35 1.64 0.95 o 1 5 0 16.13 11.38 0.59 o 2 5 0 154.56 170.89 3.35 o 3 5 0 216.45 240.76 4.52 o 4 5 0 88.86 87.07 2.97 o 5 5 0 0.10 0.30 0.70 o 6 5 0 10.11 7.01 1.84 o 0 6 0 16.96 15.06 1.27 o 1 6 0 2.45 1.25 0.32 o 2 6 0 25.07 27.64 1.35 o 3 6 0 0.00 0.48 0.47 o 4 6 0 6.43 5.64 0.86 o 5 6 0 9.66 8.88 1.48 o 6 6 0 0.15 0.47 0.85 o 1 7 0 61.23 60.34 1.49 o 2 7 0 88.89 97.44 2.61 o 3 7 0 29.86 32.23 1.68 o 4 7 0 0.38 0.32 0.51 o 5 7 0 0.55 0.13 0.70 o 6 7 0 4.06 4.68 1.36 o 0 8 0 149.26 142.69 5.11 o 1 8 0 12.79 12.70 1.30 o 2 8 0 0.60 0.15 0.48 o 3 8 0 27.90 22.80 1.77 o 4 8 0 5.74 3.74 0.84 o 5 8 0 0.02 -1.09 0.73 o 1 9 0 26.33 26.32 2.93 o 2 9 0 202.26 208.77 4.43 o 3 9 0 5.29 4.49 1.18 o 4 9 0 19.76 18.60 1.63 o 5 9 0 0.17 0.50 0.83 o 0 10 0 0.18 0.43 0.75 o 1 10 0 0.28 -0.46 0.71 o 2 10 0 49.78 55.45 2.90 o 3 10 0 12.20 9.39 1.51 o 4 10 0 7.90 6.43 1.08 o 1 11 0 0.40 -0.39 1.00 o 2 11 0 3.54 0.96 1.18 o 3 11 0 10.63 14.04 1.89 o 4 11 0 22.20 21.58 4.45 o 1 12 0 4.88 6.86 1.79 o 2 12 0 0.00 1.50 1.21 o 3 12 0 3.51 5.11 2.11 o 1 0 1 1944.78 2076.04 38.42 o 2 0 1 1142.29 1166.96 11.31 o 3 0 1 1.74 1.48 0.30 o 4 0 1 13.87 14.06 0.71 o 5 0 1 19.61 19.46 1.19 o 6 0 1 93.78 95.51 4.05 o 7 0 1 5.56 5.61 1.39 o 0 1 1 117.10 126.87 2.79 o 1 1 1 3588.87 3712.33 34.14 o 2 1 1 101.91 98.88 1.24 o 3 1 1 33.35 30.46 0.70 o 4 1 1 136.62 133.75 1.62 o 5 1 1 145.08 149.86 2.62 o 6 1 1 20.92 22.24 1.91 o 7 1 1 1.02 2.33 0.90 o 0 2 1 99.98 91.40 2.13 o 1 2 1 2061.42 2050.07 14.38 o 2 2 1 547.36 551.49 4.14 o 3 2 1 91.15 99.02 1.32 o 4 2 1 46.54 44.44 0.96 o 5 2 1 122.88 138.22 3.05 o 6 2 1 60.36 71.32 1.92 o 0 3 1 3.35 5.40 0.32 o 1 3 1 55.31 47.94 0.87 o 2 3 1 155.54 165.29 1.61 o 3 3 1 505.14 555.93 4.45 o 4 3 1 16.90 16.56 0.71 o 5 3 1 17.76 17.59 1.00 o 6 3 1 3.86 1.85 0.64 o 0 4 1 210.11 199.93 2.53 o 1 4 1 1213.22 1232.07 9.07 o 2 4 1 108.05 126.54 1.53 o 3 4 1 29.46 25.53 0.66 o 4 4 1 56.52 56.75 1.45 o 5 4 1 12.22 11.14 1.09 o 6 4 1 1.35 0.72 0.59 o 0 5 1 60.86 66.00 1.11 o 1 5 1 35.68 39.04 0.77 o 2 5 1 20.79 22.50 0.68 o 3 5 1 5.10 4.73 0.51 o 4 5 1 7.75 5.33 0.61 o 5 5 1 9.41 7.62 0.95 o 6 5 1 5.79 6.69 1.13 o 0 6 1 209.89 219.05 2.59 o 1 6 1 110.99 117.14 1.47 o 2 6 1 96.75 92.07 1.48 o 3 6 1 5.74 5.49 0.57 o 4 6 1 48.73 45.73 1.40 o 5 6 1 8.65 7.14 1.26 o 6 6 1 9.65 11.62 2.03 o 0 7 1 309.55 310.76 4.01 o 1 7 1 150.75 155.81 1.85 o 2 7 1 2.39 2.50 0.39 o 3 7 1 44.16 38.78 1.25 o 4 7 1 53.84 48.69 1.51 o 5 7 1 0.88 0.75 0.52 o 6 7 1 0.48 -0.34 0.86 o 0 8 1 0.58 0.88 0.36 o 1 8 1 147.57 143.04 2.13 o 2 8 1 10.87 9.77 0.73 o 3 8 1 9.01 7.06 0.68 o 4 8 1 8.59 7.05 0.74 o 5 8 1 0.99 -0.11 0.60 o 0 9 1 38.92 38.40 1.83 o 1 9 1 19.02 19.16 1.36 o 2 9 1 79.22 78.16 1.79 o 3 9 1 13.24 10.67 0.86 o 4 9 1 3.60 3.40 0.64 o 5 9 1 2.73 2.79 0.75 o 0 10 1 4.96 4.90 0.93 o 1 10 1 82.40 92.24 6.41 o 2 10 1 39.87 41.03 2.21 o 3 10 1 12.38 11.04 1.15 o 4 10 1 26.62 28.59 1.58 o 1 11 1 41.50 46.27 2.50 o 2 11 1 9.83 12.41 1.40 o 3 11 1 31.06 37.77 2.42 o 4 11 1 6.45 7.62 1.59 o 1 12 1 34.47 42.92 3.50 o 2 12 1 4.39 3.23 1.12 o 3 12 1 1.00 1.11 1.25 o 0 0 2 619.20 657.90 10.23 o 1 0 2 41.71 43.60 1.68 o 2 0 2 69.25 63.53 1.15 o 3 0 2 180.97 189.48 2.90 o 4 0 2 197.04 195.18 3.26 o 5 0 2 168.40 186.73 3.60 o 6 0 2 68.26 78.65 4.36 o 7 0 2 6.23 9.86 1.74 o 0 1 2 188.60 171.25 2.73 o 1 1 2 4513.59 4258.75 44.43 o 2 1 2 304.35 325.95 2.66 o 3 1 2 441.24 463.37 3.83 o 4 1 2 47.01 45.95 1.43 o 5 1 2 33.21 35.22 1.02 o 6 1 2 3.35 4.04 0.73 o 7 1 2 5.42 5.84 1.16 o 0 2 2 846.90 784.61 7.55 o 1 2 2 873.50 886.74 6.54 o 2 2 2 1257.09 1330.91 9.11 o 3 2 2 10.47 11.00 0.45 o 4 2 2 83.84 83.61 2.09 o 5 2 2 16.86 16.81 0.95 o 6 2 2 31.09 29.62 1.53 o 0 3 2 487.87 515.32 7.08 o 1 3 2 942.16 934.95 6.96 o 2 3 2 344.28 367.12 3.28 o 3 3 2 23.43 21.16 0.57 o 4 3 2 2.73 3.19 0.50 o 5 3 2 95.30 96.96 1.91 o 6 3 2 25.98 24.84 1.63 o 0 4 2 0.32 0.49 0.19 o 1 4 2 98.83 79.70 1.08 o 2 4 2 126.17 116.53 1.46 o 3 4 2 166.10 157.67 2.00 o 4 4 2 86.66 85.48 2.27 o 5 4 2 4.92 3.84 0.74 o 6 4 2 4.49 4.56 1.07 o 0 5 2 225.00 233.42 5.07 o 1 5 2 163.88 157.89 1.94 o 2 5 2 252.29 272.19 3.54 o 3 5 2 15.25 13.45 1.00 o 4 5 2 15.28 14.30 0.98 o 5 5 2 36.64 33.49 1.76 o 6 5 2 1.03 0.54 0.63 o 0 6 2 0.53 0.40 0.22 o 1 6 2 345.45 351.19 3.58 o 2 6 2 7.34 6.34 0.52 o 3 6 2 11.53 10.24 0.80 o 4 6 2 10.40 10.16 0.89 o 5 6 2 26.35 24.33 1.62 o 6 6 2 1.65 1.13 0.68 o 0 7 2 16.94 18.00 0.91 o 1 7 2 67.26 69.88 1.38 o 2 7 2 47.18 45.05 1.24 o 3 7 2 25.51 23.17 1.06 o 4 7 2 2.55 2.35 0.55 o 5 7 2 7.12 8.12 1.88 o 6 7 2 1.84 2.56 0.79 o 0 8 2 4.12 3.55 0.60 o 1 8 2 26.80 24.66 0.87 o 2 8 2 69.49 66.96 1.75 o 3 8 2 31.07 29.41 1.23 o 4 8 2 1.85 0.79 0.97 o 5 8 2 8.17 5.58 0.92 o 0 9 2 7.68 11.73 1.14 o 1 9 2 27.89 26.78 1.83 o 2 9 2 67.10 65.11 2.01 o 3 9 2 65.41 66.39 1.78 o 4 9 2 0.26 0.62 0.51 o 5 9 2 15.37 18.23 2.13 o 0 10 2 82.68 94.41 4.57 o 1 10 2 10.41 11.52 1.19 o 2 10 2 36.87 36.16 2.03 o 3 10 2 12.22 12.19 1.43 o 4 10 2 0.32 0.59 0.59 o 1 11 2 62.66 57.13 3.96 o 2 11 2 12.05 11.38 1.34 o 3 11 2 4.86 4.84 1.07 o 4 11 2 6.71 5.47 1.28 o 1 12 2 17.51 18.35 2.64 o 2 12 2 1.04 3.00 1.20 o 3 12 2 5.16 5.95 1.20 o 1 0 3 2673.69 2660.39 28.10 o 2 0 3 314.64 329.17 4.81 o 3 0 3 21.06 22.44 0.73 o 4 0 3 13.44 13.27 1.09 o 5 0 3 297.46 331.54 6.02 o 6 0 3 0.01 -0.10 0.90 o 7 0 3 4.64 7.62 1.54 o 0 1 3 21.93 18.89 0.78 o 1 1 3 1289.72 1187.61 17.46 o 2 1 3 186.65 183.74 1.86 o 3 1 3 50.25 55.16 0.93 o 4 1 3 51.00 49.55 1.38 o 5 1 3 49.56 49.90 1.58 o 6 1 3 10.14 10.01 1.00 o 0 2 3 17377.05 16760.17 352.42 o 1 2 3 6197.08 6443.22 41.29 o 2 2 3 253.04 293.57 2.75 o 3 2 3 549.46 590.31 4.65 o 4 2 3 120.56 109.67 1.95 o 5 2 3 7.20 5.97 0.85 o 6 2 3 12.35 12.04 1.27 o 0 3 3 233.21 243.47 3.79 o 1 3 3 114.02 121.78 1.30 o 2 3 3 231.79 221.58 2.28 o 3 3 3 208.45 211.84 2.40 o 4 3 3 23.92 20.59 1.18 o 5 3 3 12.16 11.88 1.09 o 6 3 3 20.63 25.57 2.31 o 0 4 3 26.10 24.60 0.73 o 1 4 3 362.27 377.39 3.31 o 2 4 3 420.22 461.03 4.04 o 3 4 3 29.83 32.16 0.83 o 4 4 3 45.50 40.85 1.55 o 5 4 3 18.33 15.43 1.12 o 6 4 3 4.68 3.97 0.82 o 0 5 3 587.31 649.85 6.99 o 1 5 3 288.35 291.55 2.82 o 2 5 3 150.27 156.18 2.32 o 3 5 3 63.52 55.27 1.45 o 4 5 3 44.74 45.43 1.70 o 5 5 3 0.16 0.40 0.44 o 6 5 3 13.67 15.37 1.43 o 0 6 3 44.84 38.83 1.05 o 1 6 3 16.40 18.49 1.25 o 2 6 3 18.96 20.42 0.86 o 3 6 3 6.18 5.06 0.62 o 4 6 3 37.35 33.13 1.66 o 5 6 3 20.47 19.99 1.30 o 6 6 3 0.30 -0.51 0.55 o 0 7 3 40.20 44.35 1.19 o 1 7 3 0.21 0.17 0.21 o 2 7 3 54.22 50.77 1.58 o 3 7 3 4.12 4.05 0.58 o 4 7 3 16.99 17.83 1.20 o 5 7 3 9.68 8.00 0.93 o 0 8 3 7.10 7.01 0.80 o 1 8 3 10.83 10.24 0.63 o 2 8 3 64.48 69.34 1.79 o 3 8 3 25.54 24.28 1.26 o 4 8 3 7.70 6.60 0.82 o 5 8 3 8.05 7.17 0.89 o 0 9 3 38.68 36.92 1.65 o 1 9 3 120.32 126.91 2.71 o 2 9 3 13.47 12.83 1.07 o 3 9 3 21.68 22.29 1.28 o 4 9 3 19.37 20.89 1.41 o 5 9 3 5.40 5.51 1.05 o 0 10 3 129.12 141.59 5.71 o 1 10 3 3.81 3.22 0.93 o 2 10 3 10.73 8.32 1.14 o 3 10 3 5.47 5.49 1.15 o 4 10 3 14.44 17.40 1.32 o 0 11 3 44.22 42.71 3.25 o 1 11 3 49.91 55.16 2.35 o 2 11 3 28.29 35.51 2.22 o 3 11 3 13.82 15.73 1.65 o 1 12 3 0.74 0.46 1.07 o 2 12 3 7.73 6.37 1.12 o 3 12 3 0.52 0.82 0.81 o 0 0 4 321.00 369.61 6.59 o 1 0 4 55.78 50.14 1.60 o 2 0 4 190.92 191.41 3.03 o 3 0 4 12.43 11.23 0.89 o 4 0 4 30.33 33.34 1.29 o 5 0 4 7.14 5.17 1.05 o 6 0 4 0.77 0.35 0.91 o 0 1 4 800.50 862.99 8.36 o 1 1 4 417.12 428.41 3.20 o 2 1 4 435.78 432.57 3.71 o 3 1 4 549.78 637.57 4.96 o 4 1 4 133.83 125.61 2.20 o 5 1 4 55.46 56.56 1.42 o 6 1 4 29.12 31.26 1.56 o 0 2 4 3715.62 3917.95 35.70 o 1 2 4 2750.78 2770.06 18.07 o 2 2 4 39.63 32.63 0.66 o 3 2 4 65.64 57.51 0.94 o 4 2 4 36.33 32.96 1.06 o 5 2 4 21.68 24.01 1.21 o 6 2 4 26.83 23.90 1.63 o 0 3 4 2998.85 3166.65 38.57 o 1 3 4 295.50 283.15 2.38 o 2 3 4 63.59 59.73 1.12 o 3 3 4 162.58 170.58 2.10 o 4 3 4 62.51 61.92 2.26 o 5 3 4 20.36 20.14 1.32 o 6 3 4 1.84 2.99 0.95 o 0 4 4 510.36 496.68 5.44 o 1 4 4 312.88 318.70 2.95 o 2 4 4 748.18 787.71 6.90 o 3 4 4 71.53 65.29 1.29 o 4 4 4 139.95 138.93 3.02 o 5 4 4 74.88 77.05 2.38 o 6 4 4 20.17 23.89 1.68 o 0 5 4 1419.28 1620.24 15.70 o 1 5 4 3.57 2.93 0.30 o 2 5 4 233.92 231.19 2.97 o 3 5 4 57.95 59.75 1.35 o 4 5 4 18.15 15.68 1.16 o 5 5 4 2.57 2.61 0.62 o 6 5 4 1.37 2.55 0.76 o 0 6 4 16.79 14.42 0.70 o 1 6 4 373.14 388.15 3.68 o 2 6 4 17.41 17.82 0.84 o 3 6 4 15.70 13.75 1.00 o 4 6 4 28.52 23.59 1.42 o 5 6 4 10.90 7.83 0.89 o 6 6 4 0.98 1.86 1.36 o 0 7 4 54.57 50.16 1.30 o 1 7 4 61.37 64.24 1.51 o 2 7 4 53.04 48.76 1.37 o 3 7 4 107.83 105.29 2.83 o 4 7 4 0.47 -0.23 0.57 o 5 7 4 18.99 19.13 1.56 o 0 8 4 8.57 9.09 0.89 o 1 8 4 30.95 27.39 1.09 o 2 8 4 33.08 31.71 1.58 o 3 8 4 40.14 38.81 1.72 o 4 8 4 117.27 134.66 3.43 o 5 8 4 9.35 11.48 1.24 o 0 9 4 103.81 110.17 3.70 o 1 9 4 92.56 91.03 2.29 o 2 9 4 49.85 49.32 1.91 o 3 9 4 17.59 15.84 1.14 o 4 9 4 8.00 8.26 1.09 o 5 9 4 0.61 2.21 0.72 o 0 10 4 0.80 1.27 0.69 o 1 10 4 35.12 32.32 1.81 o 2 10 4 4.31 4.19 0.84 o 3 10 4 0.82 -0.79 0.53 o 4 10 4 23.88 24.25 1.54 o 0 11 4 2.34 1.89 1.18 o 1 11 4 22.57 19.17 3.30 o 2 11 4 3.00 0.74 1.29 o 3 11 4 5.46 6.01 1.08 o 1 12 4 19.65 18.67 2.07 o 2 12 4 4.42 3.31 0.92 o 1 13 4 6.12 6.46 1.89 o 1 0 5 223.54 206.96 2.80 o 2 0 5 2174.94 2287.77 24.87 o 3 0 5 1.08 -0.05 0.40 o 4 0 5 1.12 1.06 0.43 o 5 0 5 3.04 1.55 0.65 o 6 0 5 10.51 8.61 2.14 o 0 1 5 54.83 77.28 1.52 o 1 1 5 220.95 233.24 2.02 o 2 1 5 332.06 356.85 3.24 o 3 1 5 154.60 156.49 2.44 o 4 1 5 25.51 28.05 1.02 o 5 1 5 67.64 68.97 2.52 o 6 1 5 18.15 17.84 1.69 o 0 2 5 182.30 168.74 3.70 o 1 2 5 98.05 102.44 1.27 o 2 2 5 61.69 67.14 1.03 o 3 2 5 48.95 49.41 0.99 o 4 2 5 78.12 73.85 1.62 o 5 2 5 27.15 25.72 1.45 o 6 2 5 20.98 21.54 2.23 o 0 3 5 356.72 343.46 4.00 o 1 3 5 1936.15 2065.17 13.78 o 2 3 5 588.14 623.70 5.69 o 3 3 5 45.41 44.86 1.58 o 4 3 5 77.34 75.59 2.23 o 5 3 5 40.65 40.50 2.16 o 6 3 5 16.55 18.57 2.15 o 0 4 5 40.76 44.90 1.10 o 1 4 5 349.75 382.14 3.45 o 2 4 5 12.64 12.39 0.58 o 3 4 5 20.27 16.36 0.74 o 4 4 5 36.30 37.67 1.60 o 5 4 5 34.34 33.23 1.74 o 6 4 5 12.75 15.78 1.74 o 0 5 5 82.31 92.40 2.14 o 1 5 5 248.71 256.23 2.65 o 2 5 5 51.04 42.48 1.17 o 3 5 5 32.08 30.96 1.16 o 4 5 5 149.94 153.97 3.74 o 5 5 5 22.14 20.77 1.62 o 6 5 5 13.07 18.52 1.67 o 0 6 5 19.95 17.90 0.85 o 1 6 5 317.18 329.72 3.29 o 2 6 5 16.43 14.10 0.95 o 3 6 5 52.70 49.98 1.77 o 4 6 5 2.52 2.66 0.64 o 5 6 5 20.74 17.58 1.46 o 6 6 5 3.34 0.94 0.81 o 0 7 5 265.28 292.60 4.64 o 1 7 5 97.39 99.58 1.93 o 2 7 5 107.38 103.79 2.28 o 3 7 5 0.59 0.58 0.59 o 4 7 5 37.44 40.68 1.89 o 5 7 5 20.05 19.14 1.41 o 0 8 5 0.94 0.48 0.45 o 1 8 5 68.05 63.32 1.45 o 2 8 5 99.76 102.77 3.26 o 3 8 5 29.20 29.51 1.59 o 4 8 5 6.94 5.35 0.88 o 5 8 5 21.03 23.22 1.83 o 0 9 5 8.63 7.50 1.55 o 1 9 5 51.11 46.98 1.64 o 2 9 5 33.82 31.32 1.49 o 3 9 5 28.04 29.94 2.49 o 4 9 5 34.89 33.47 1.71 o 0 10 5 49.65 55.88 2.79 o 1 10 5 33.46 34.26 2.81 o 2 10 5 8.89 6.28 1.02 o 3 10 5 23.80 22.76 1.53 o 4 10 5 1.49 1.03 0.60 o 0 11 5 12.23 13.53 1.72 o 1 11 5 1.55 2.72 0.96 o 2 11 5 15.92 17.56 2.16 o 3 11 5 1.86 3.70 0.92 o 1 12 5 0.14 -1.21 1.29 o 2 12 5 0.48 0.59 0.75 o 0 0 6 1132.52 973.97 13.51 o 1 0 6 1919.92 1978.08 18.54 o 2 0 6 112.28 142.39 2.59 o 3 0 6 605.20 694.72 7.90 o 4 0 6 35.01 33.03 1.30 o 5 0 6 0.36 -0.10 0.49 o 6 0 6 0.82 1.80 0.77 o 0 1 6 20.26 14.99 1.02 o 1 1 6 27.38 25.91 0.54 o 2 1 6 517.32 529.37 4.51 o 3 1 6 3.44 2.82 0.34 o 4 1 6 18.31 15.38 0.83 o 5 1 6 17.08 18.75 1.07 o 6 1 6 6.36 6.80 0.98 o 0 2 6 1799.66 1873.48 17.75 o 1 2 6 108.75 113.72 1.29 o 2 2 6 738.81 782.83 6.26 o 3 2 6 4.63 5.30 0.50 o 4 2 6 243.51 254.70 3.45 o 5 2 6 15.64 15.35 0.94 o 6 2 6 11.69 14.09 1.56 o 0 3 6 420.87 422.24 4.85 o 1 3 6 87.68 73.19 1.03 o 2 3 6 168.55 158.82 2.11 o 3 3 6 6.63 6.34 0.53 o 4 3 6 32.60 32.87 1.15 o 5 3 6 25.32 26.71 1.58 o 6 3 6 19.13 19.65 3.64 o 0 4 6 65.78 72.18 1.50 o 1 4 6 1473.91 1527.83 11.35 o 2 4 6 343.70 343.17 3.68 o 3 4 6 89.49 83.17 1.61 o 4 4 6 19.70 16.94 1.02 o 5 4 6 7.28 5.45 0.86 o 6 4 6 4.10 4.74 1.01 o 0 5 6 68.83 77.93 1.93 o 1 5 6 3.23 2.76 0.31 o 2 5 6 126.25 118.21 1.87 o 3 5 6 16.10 15.45 0.91 o 4 5 6 29.12 26.72 2.43 o 5 5 6 2.46 2.17 0.66 o 6 5 6 8.59 7.82 1.37 o 0 6 6 2.00 2.61 0.59 o 1 6 6 28.91 31.54 0.85 o 2 6 6 12.35 12.57 0.80 o 3 6 6 54.16 54.89 1.59 o 4 6 6 11.41 9.03 1.18 o 5 6 6 1.84 2.06 0.70 o 6 6 6 2.71 1.70 0.82 o 0 7 6 0.69 0.53 0.36 o 1 7 6 93.61 95.01 2.48 o 2 7 6 397.59 405.67 5.06 o 3 7 6 64.14 70.93 2.22 o 4 7 6 82.16 82.81 2.60 o 5 7 6 2.34 1.38 0.76 o 0 8 6 58.79 55.08 1.96 o 1 8 6 9.90 9.04 0.67 o 2 8 6 28.54 30.36 1.23 o 3 8 6 64.33 68.80 3.06 o 4 8 6 23.24 24.34 1.67 o 5 8 6 3.43 4.90 0.85 o 0 9 6 21.01 20.83 1.80 o 1 9 6 17.31 16.94 1.02 o 2 9 6 13.57 14.14 1.14 o 3 9 6 13.40 14.54 1.27 o 4 9 6 5.98 5.77 0.90 o 0 10 6 0.14 1.05 0.66 o 1 10 6 4.26 4.44 0.70 o 2 10 6 12.60 11.65 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2 5 8 72.29 61.69 1.42 o 3 5 8 139.85 136.33 2.65 o 4 5 8 125.19 141.76 3.36 o 5 5 8 2.66 1.62 0.65 o 6 5 8 11.67 12.55 1.36 o 0 6 8 2.13 1.02 0.38 o 1 6 8 1.19 1.25 0.32 o 2 6 8 39.30 36.07 1.19 o 3 6 8 49.81 52.74 1.85 o 4 6 8 49.35 50.63 2.06 o 5 6 8 7.79 7.22 1.00 o 0 7 8 2.46 1.87 0.42 o 1 7 8 21.75 20.65 0.92 o 2 7 8 2.35 2.45 0.53 o 3 7 8 9.48 8.70 0.99 o 4 7 8 7.09 7.65 1.01 o 5 7 8 0.46 -0.49 0.87 o 0 8 8 52.99 49.89 2.48 o 1 8 8 39.49 41.46 1.26 o 2 8 8 60.45 62.80 1.78 o 3 8 8 15.79 15.60 1.29 o 4 8 8 1.62 1.76 0.84 o 5 8 8 8.21 9.27 1.22 o 0 9 8 63.91 64.38 2.96 o 1 9 8 35.32 35.63 1.46 o 2 9 8 11.51 9.37 0.99 o 3 9 8 13.39 12.18 1.23 o 4 9 8 2.83 1.97 0.71 o 0 10 8 31.49 33.29 2.39 o 1 10 8 8.15 7.92 0.95 o 2 10 8 7.08 8.66 1.64 o 3 10 8 7.87 8.03 1.05 o 0 11 8 6.46 4.42 1.17 o 1 11 8 1.36 1.07 0.82 o 2 11 8 20.35 21.94 1.91 o 3 11 8 3.13 5.57 1.19 o 0 12 8 0.01 0.32 0.82 o 1 12 8 3.82 2.42 1.08 o 1 0 9 131.14 137.03 2.05 o 2 0 9 159.56 187.84 3.05 o 3 0 9 6.16 6.65 0.69 o 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5.77 0.69 o 5 2 13 6.65 4.56 0.75 o 0 3 13 8.15 7.75 1.06 o 1 3 13 114.49 114.67 2.27 o 2 3 13 38.82 36.48 1.22 o 3 3 13 175.83 188.97 3.04 o 4 3 13 13.20 13.02 0.97 o 5 3 13 5.06 5.08 0.92 o 0 4 13 3.83 3.49 0.59 o 1 4 13 61.31 61.27 1.39 o 2 4 13 70.35 73.22 1.95 o 3 4 13 4.21 3.10 0.54 o 4 4 13 6.94 6.70 0.87 o 5 4 13 6.71 7.68 1.13 o 0 5 13 55.85 52.31 1.80 o 1 5 13 28.77 26.82 1.11 o 2 5 13 88.89 91.76 2.62 o 3 5 13 1.06 0.72 0.48 o 4 5 13 15.51 14.80 1.22 o 5 5 13 0.37 0.67 0.77 o 0 6 13 21.72 20.07 1.19 o 1 6 13 7.83 8.29 0.72 o 2 6 13 25.52 23.72 1.30 o 3 6 13 40.95 40.56 1.71 o 4 6 13 3.54 2.74 0.64 o 0 7 13 12.03 11.77 1.13 o 1 7 13 37.87 33.31 1.29 o 2 7 13 5.10 5.45 0.74 o 3 7 13 20.59 19.83 1.35 o 4 7 13 2.22 2.65 0.79 o 0 8 13 15.08 14.50 1.87 o 1 8 13 23.43 27.55 1.36 o 2 8 13 24.17 22.68 1.36 o 3 8 13 13.27 13.04 1.16 o 0 9 13 7.90 7.43 1.89 o 1 9 13 0.10 0.68 0.50 o 2 9 13 5.48 5.83 0.82 o 3 9 13 1.14 1.43 0.76 o 0 10 13 7.45 10.56 3.12 o 1 10 13 2.61 1.40 0.65 o 2 10 13 12.28 14.78 1.74 o 0 0 14 14.10 10.77 1.31 o 1 0 14 13.45 11.91 0.94 o 2 0 14 30.16 27.71 1.38 o 3 0 14 62.93 60.14 2.38 o 4 0 14 60.33 65.27 2.73 o 5 0 14 6.56 4.28 1.34 o 0 1 14 3.04 2.80 0.57 o 1 1 14 148.20 149.18 2.62 o 2 1 14 165.40 169.35 2.38 o 3 1 14 33.86 30.00 1.18 o 4 1 14 15.25 13.10 1.04 o 5 1 14 3.57 4.00 0.70 o 0 2 14 33.82 33.13 1.63 o 1 2 14 11.56 9.85 0.73 o 2 2 14 69.47 69.36 1.68 o 3 2 14 91.57 95.50 2.10 o 4 2 14 59.83 64.02 1.91 o 5 2 14 3.89 4.49 0.76 o 0 3 14 122.81 124.15 3.21 o 1 3 14 158.97 169.76 2.73 o 2 3 14 19.71 15.69 0.92 o 3 3 14 23.86 23.98 1.21 o 4 3 14 1.39 0.53 0.46 o 5 3 14 7.40 12.65 1.30 o 0 4 14 44.51 37.49 1.76 o 1 4 14 0.23 -0.10 0.33 o 2 4 14 33.74 33.53 1.45 o 3 4 14 2.49 2.07 0.48 o 4 4 14 10.60 8.05 1.06 o 0 5 14 1.59 0.27 0.53 o 1 5 14 16.20 15.56 1.60 o 2 5 14 10.69 8.96 0.88 o 3 5 14 5.73 6.22 0.81 o 4 5 14 1.86 1.03 0.60 o 0 6 14 18.64 15.09 3.55 o 1 6 14 22.04 22.17 1.23 o 2 6 14 0.48 0.62 0.50 o 3 6 14 16.69 16.72 1.26 o 4 6 14 3.38 4.36 0.80 o 0 7 14 1.23 0.81 0.71 o 1 7 14 3.92 3.72 0.63 o 2 7 14 7.48 5.61 0.77 o 3 7 14 7.93 8.45 0.97 o 0 8 14 1.06 1.64 0.84 o 1 8 14 5.81 7.27 0.90 o 2 8 14 15.07 15.22 1.18 o 3 8 14 16.12 18.74 1.36 o 0 9 14 6.81 10.04 2.93 o 1 9 14 7.41 9.44 1.33 o 2 9 14 19.88 24.43 1.50 o 0 10 14 0.54 1.48 1.23 o 1 10 14 6.02 7.26 1.53 o 1 0 15 7.47 6.72 0.81 o 2 0 15 11.85 11.82 1.04 o 3 0 15 9.73 8.53 1.15 o 4 0 15 5.02 5.96 1.09 o 5 0 15 1.20 0.91 0.83 o 0 1 15 134.57 137.37 2.95 o 1 1 15 88.80 90.01 1.80 o 2 1 15 92.15 96.62 1.79 o 3 1 15 3.94 4.20 0.58 o 4 1 15 5.71 6.89 0.81 o 5 1 15 1.48 0.99 0.60 o 0 2 15 0.01 0.45 0.52 o 1 2 15 52.43 53.74 1.49 o 2 2 15 40.95 38.98 1.35 o 3 2 15 19.69 19.26 1.09 o 4 2 15 7.78 5.48 0.76 o 5 2 15 23.68 29.21 1.56 o 0 3 15 6.29 3.46 0.79 o 1 3 15 28.31 27.00 1.16 o 2 3 15 24.55 25.57 1.47 o 3 3 15 18.90 18.60 1.09 o 4 3 15 6.65 7.85 1.09 o 0 4 15 112.21 99.26 2.98 o 1 4 15 5.62 5.66 0.76 o 2 4 15 6.80 5.88 0.77 o 3 4 15 7.85 7.39 0.78 o 4 4 15 3.42 3.12 0.69 o 0 5 15 9.31 8.05 1.10 o 1 5 15 45.31 42.27 2.44 o 2 5 15 7.48 6.92 0.82 o 3 5 15 2.19 2.28 0.61 o 4 5 15 0.17 0.35 0.56 o 0 6 15 38.55 33.21 2.38 o 1 6 15 7.51 9.38 0.92 o 2 6 15 18.69 20.03 1.50 o 3 6 15 1.62 1.73 0.61 o 4 6 15 5.42 6.34 0.97 o 0 7 15 8.61 5.68 2.12 o 1 7 15 3.58 5.45 0.74 o 2 7 15 6.90 7.00 0.88 o 3 7 15 6.26 5.95 0.85 o 0 8 15 9.50 8.34 1.50 o 1 8 15 2.23 1.51 0.56 o 2 8 15 8.59 11.39 1.08 o 0 9 15 1.39 1.88 0.96 o 1 9 15 4.45 6.92 1.16 o 0 0 16 49.48 52.38 2.70 o 1 0 16 120.39 142.25 4.62 o 2 0 16 1.19 0.93 0.52 o 3 0 16 13.69 12.92 1.42 o 4 0 16 0.30 -0.47 0.64 o 0 1 16 181.71 191.84 5.55 o 1 1 16 94.14 102.73 2.00 o 2 1 16 32.76 31.10 1.12 o 3 1 16 4.13 4.32 0.61 o 4 1 16 48.89 51.32 1.85 o 0 2 16 15.60 16.43 1.39 o 1 2 16 103.07 111.43 2.29 o 2 2 16 1.18 0.88 0.41 o 3 2 16 13.51 14.93 0.96 o 4 2 16 6.59 8.16 0.91 o 0 3 16 3.06 2.49 0.70 o 1 3 16 33.53 33.54 1.30 o 2 3 16 13.51 13.01 1.07 o 3 3 16 2.81 2.36 0.55 o 4 3 16 1.77 1.21 0.74 o 0 4 16 0.03 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4.38 2.93 1.61 o 1 6 18 1.24 1.49 0.58 o 2 6 18 1.04 0.95 0.61 o 0 7 18 0.02 1.50 1.54 o 1 7 18 2.51 2.59 0.74 o 1 0 19 18.30 17.01 1.67 o 2 0 19 5.09 3.89 1.19 o 3 0 19 4.58 3.70 1.34 o 0 1 19 39.38 46.10 4.45 o 1 1 19 10.93 10.39 0.94 o 2 1 19 1.46 1.54 0.54 o 3 1 19 7.12 9.21 0.96 o 0 2 19 1.03 2.84 1.06 o 1 2 19 0.73 1.26 0.61 o 2 2 19 3.44 3.27 0.69 o 3 2 19 4.12 2.68 0.72 o 0 3 19 46.80 48.54 2.98 o 1 3 19 7.38 9.24 1.02 o 2 3 19 9.40 9.63 1.06 o 3 3 19 4.01 3.21 0.75 o 0 4 19 2.15 -0.57 1.25 o 1 4 19 8.13 9.76 1.19 o 2 4 19 7.16 8.78 1.02 o 0 5 19 4.31 3.86 1.89 o 1 5 19 2.39 1.47 0.71 o 2 5 19 1.50 1.47 0.61 o 0 6 19 5.51 3.57 1.86 o 1 6 19 2.20 2.51 0.93 o 0 0 20 11.68 13.68 2.71 o 1 0 20 57.93 55.08 2.62 o 2 0 20 7.01 9.28 4.70 o 0 1 20 45.39 46.51 3.03 o 1 1 20 16.29 17.38 1.20 o 2 1 20 4.34 4.56 0.84 o 0 2 20 13.78 16.58 2.04 o 1 2 20 17.89 18.65 1.36 o 2 2 20 3.90 4.04 0.78 o 0 3 20 37.23 45.23 3.02 o 1 3 20 4.10 4.28 0.82 o 2 3 20 0.39 0.95 0.60 o 0 4 20 11.50 11.93 2.68 o 1 4 20 6.70 5.92 1.01 o 0 5 20 15.10 18.00 3.21 o 1 0 21 2.59 1.53 1.03 o 0 1 21 15.95 16.20 2.13 o 1 1 21 6.13 7.75 1.13 o 0 2 21 2.04 4.06 1.29 o 1 2 21 11.55 13.51 1.65 o 0 3 21 0.06 1.25 1.61 o