#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:04:59 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181139 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/18/2221845.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221845_Fobs loop_ _publ_author_name 'El Ashry, El Sayed H.' 'Amer, Mohammed R.' 'Shah, M. Raza' 'Ng, Seik Weng' _publ_section_title ; 2,3,4,6-Tetra-O-acetyl-\b-D-galactopyranosyl 2-(2,4-dichloroanilino)-4,4-dimethyl-6-oxocyclohex-1-enecarbodithioate ; _journal_coeditor_code TK2430 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1106 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.486 _cell_angle_gamma 90.000 _cell_length_a 13.8257 _cell_length_b 8.7697 _cell_length_c 14.0690 _exptl_crystal_F_000 720.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file tk2430Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 199.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 -11 0 15.66 22.41 36.36 o 0 -10 0 67.35 103.68 36.65 o 1 -10 0 6.07 12.32 20.38 o 2 -10 0 60.22 34.43 22.22 o 3 -10 0 126.72 188.40 42.64 o 4 -10 0 26.95 49.32 32.79 o 5 -10 0 104.37 160.92 43.13 o 6 -10 0 50.50 92.20 37.28 o 7 -10 0 106.13 96.59 40.16 o 8 -10 0 61.12 19.60 37.12 o 1 -9 0 78.42 35.18 20.87 o 2 -9 0 69.61 163.57 60.50 o 3 -9 0 28.99 92.23 23.02 o 4 -9 0 5.59 -13.28 23.88 o 5 -9 0 5.59 45.60 32.32 o 6 -9 0 12.89 4.64 27.16 o 7 -9 0 178.79 172.80 45.56 o 8 -9 0 80.28 52.12 35.44 o 9 -9 0 111.01 119.58 53.96 o 10 -9 0 66.27 66.49 24.90 o 0 -8 0 618.80 596.77 57.12 o 1 -8 0 129.09 107.04 21.24 o 2 -8 0 129.73 192.68 24.94 o 3 -8 0 247.64 257.92 28.41 o 4 -8 0 234.76 204.65 38.88 o 5 -8 0 19.32 70.96 30.44 o 6 -8 0 63.84 93.26 20.58 o 7 -8 0 113.93 111.83 22.14 o 8 -8 0 218.52 219.82 29.57 o 9 -8 0 46.16 43.07 34.12 o 10 -8 0 188.88 225.38 37.58 o 11 -8 0 57.03 74.13 25.70 o 12 -8 0 299.55 273.33 37.71 o 1 -7 0 408.22 346.56 29.37 o 2 -7 0 94.07 213.21 101.00 o 3 -7 0 122.11 115.20 28.92 o 4 -7 0 612.86 590.25 38.72 o 5 -7 0 79.83 113.77 30.88 o 6 -7 0 362.59 358.62 32.22 o 7 -7 0 107.64 116.66 21.91 o 8 -7 0 214.72 210.51 27.83 o 9 -7 0 159.42 165.73 62.14 o 10 -7 0 66.29 108.34 34.28 o 11 -7 0 133.50 157.80 28.89 o 12 -7 0 23.64 48.89 25.20 o 13 -7 0 118.24 109.58 61.06 o 0 -6 0 56.88 83.96 22.24 o 1 -6 0 458.46 414.31 29.16 o 2 -6 0 413.81 431.57 56.37 o 3 -6 0 288.52 295.04 17.80 o 4 -6 0 212.44 263.00 19.68 o 5 -6 0 360.75 402.53 24.94 o 6 -6 0 106.03 122.26 19.78 o 7 -6 0 284.25 241.31 20.20 o 8 -6 0 10.62 29.39 16.32 o 9 -6 0 536.08 630.45 77.58 o 10 -6 0 151.91 181.02 27.55 o 11 -6 0 116.50 137.71 26.60 o 12 -6 0 138.42 173.55 29.39 o 13 -6 0 46.92 80.74 25.07 o 14 -6 0 65.81 64.03 32.66 o 1 -5 0 747.82 650.36 29.60 o 2 -5 0 846.37 1125.86 42.65 o 3 -5 0 98.39 78.19 9.65 o 4 -5 0 930.69 848.89 36.65 o 5 -5 0 74.31 638.90 98.50 o 6 -5 0 260.38 226.30 17.55 o 7 -5 0 153.55 155.95 15.54 o 8 -5 0 434.45 366.48 32.32 o 9 -5 0 189.36 232.87 42.72 o 10 -5 0 25.63 37.31 17.98 o 11 -5 0 179.14 221.68 29.50 o 12 -5 0 182.63 235.92 62.12 o 13 -5 0 24.28 61.99 23.15 o 14 -5 0 132.43 97.33 26.57 o 15 -5 0 14.95 36.61 23.73 o 0 -4 0 5136.41 5067.08 216.75 o 1 -4 0 141.04 159.54 10.96 o 2 -4 0 2590.34 3424.39 105.24 o 3 -4 0 193.24 229.87 17.58 o 4 -4 0 345.92 401.37 20.63 o 5 -4 0 48.61 648.85 53.08 o 6 -4 0 35.15 27.89 8.53 o 7 -4 0 368.49 400.66 22.00 o 8 -4 0 458.72 454.04 25.34 o 9 -4 0 31.23 33.91 15.58 o 10 -4 0 15.18 64.96 18.18 o 11 -4 0 264.53 287.23 31.03 o 12 -4 0 329.65 347.29 35.37 o 13 -4 0 78.51 122.41 26.00 o 14 -4 0 115.89 142.94 28.06 o 15 -4 0 100.84 134.99 38.54 o 16 -4 0 22.02 34.49 41.22 o 1 -3 0 376.55 236.99 11.43 o 2 -3 0 1813.17 1752.88 55.28 o 3 -3 0 108.16 130.58 13.36 o 4 -3 0 2066.80 1764.04 64.78 o 5 -3 0 1137.12 1616.41 139.54 o 6 -3 0 460.49 445.25 21.52 o 7 -3 0 2431.53 2197.18 81.06 o 8 -3 0 282.24 226.17 13.36 o 9 -3 0 529.48 490.31 27.46 o 10 -3 0 478.88 471.23 28.29 o 11 -3 0 87.15 128.77 17.17 o 12 -3 0 223.32 259.06 23.10 o 13 -3 0 22.52 26.31 19.78 o 14 -3 0 125.10 159.96 47.36 o 15 -3 0 47.53 32.15 21.57 o 16 -3 0 105.46 90.07 26.72 o 0 -2 0 39649.44 37822.00 1570.73 o 1 -2 0 4258.38 3601.66 108.24 o 2 -2 0 602.26 665.14 26.03 o 3 -2 0 1369.70 1226.02 45.17 o 4 -2 0 323.16 309.33 12.96 o 5 -2 0 787.30 973.44 50.21 o 6 -2 0 436.45 357.77 16.02 o 7 -2 0 591.06 519.60 20.45 o 8 -2 0 73.03 55.28 11.20 o 9 -2 0 284.33 239.11 19.64 o 10 -2 0 357.96 352.58 24.24 o 11 -2 0 382.55 407.48 26.98 o 12 -2 0 103.18 83.14 16.12 o 13 -2 0 466.24 490.47 36.83 o 14 -2 0 11.30 1.05 14.42 o 15 -2 0 228.08 174.31 23.47 o 16 -2 0 2.06 -1.02 19.16 o 1 -1 0 2593.48 2263.73 78.10 o 2 -1 0 214.83 219.84 16.60 o 3 -1 0 3772.44 3066.90 92.39 o 4 -1 0 1100.19 952.01 36.60 o 5 -1 0 3609.86 3476.69 121.28 o 6 -1 0 223.32 218.37 12.83 o 7 -1 0 650.76 784.02 31.79 o 8 -1 0 61.82 87.62 9.93 o 9 -1 0 8.17 90.08 21.24 o 10 -1 0 417.25 409.38 30.63 o 11 -1 0 801.68 735.28 36.80 o 12 -1 0 186.53 162.25 18.97 o 13 -1 0 25.55 26.04 14.06 o 14 -1 0 122.88 116.20 18.86 o 15 -1 0 41.67 42.05 16.72 o 16 -1 0 33.74 32.91 20.30 o 17 -1 0 41.93 86.95 26.04 o 2 0 0 503.02 215.73 16.68 o 3 0 0 5358.43 3851.60 468.55 o 4 0 0 1034.13 828.40 39.51 o 5 0 0 1053.18 975.51 46.60 o 6 0 0 247.60 210.00 18.34 o 7 0 0 384.44 406.00 26.10 o 8 0 0 1445.66 1300.86 63.77 o 9 0 0 7.95 14.91 13.16 o 10 0 0 253.89 316.20 27.16 o 11 0 0 217.72 228.18 32.44 o 12 0 0 224.97 273.99 27.93 o 13 0 0 306.63 270.92 29.63 o 14 0 0 125.32 85.90 26.08 o 15 0 0 49.09 71.21 18.21 o 16 0 0 16.31 71.45 22.15 o 17 0 0 87.52 148.59 28.20 o 1 1 0 2575.59 2405.59 145.20 o 2 1 0 228.26 187.57 9.44 o 3 1 0 3751.41 3173.54 110.37 o 4 1 0 1124.24 998.27 46.65 o 5 1 0 3627.44 3547.68 161.63 o 6 1 0 229.73 197.69 17.59 o 7 1 0 651.93 830.68 43.23 o 8 1 0 56.89 66.50 13.74 o 9 1 0 7.33 43.28 17.96 o 10 1 0 414.37 399.81 30.18 o 11 1 0 802.39 804.79 47.49 o 12 1 0 183.28 167.08 23.90 o 13 1 0 21.91 -15.61 15.25 o 14 1 0 125.63 128.58 25.11 o 15 1 0 44.62 42.47 20.41 o 16 1 0 34.64 57.16 23.44 o 17 1 0 42.35 45.60 34.61 o 0 2 0 39714.68 39992.35 2365.74 o 1 2 0 4292.69 3896.01 235.69 o 2 2 0 582.80 526.61 38.44 o 3 2 0 1347.24 1188.73 38.00 o 4 2 0 308.91 314.78 30.97 o 5 2 0 818.09 1058.52 40.33 o 6 2 0 428.92 389.58 24.97 o 7 2 0 601.57 478.02 29.08 o 8 2 0 74.22 60.89 15.24 o 9 2 0 270.13 215.26 21.84 o 10 2 0 355.11 396.87 31.69 o 11 2 0 368.39 347.72 30.60 o 12 2 0 102.05 121.45 21.43 o 13 2 0 463.66 448.77 37.61 o 14 2 0 11.83 20.58 18.01 o 15 2 0 225.37 229.97 45.20 o 16 2 0 1.89 1.71 28.39 o 1 3 0 373.28 279.05 18.60 o 2 3 0 1842.07 1795.74 114.72 o 3 3 0 105.71 135.69 11.06 o 4 3 0 2058.92 1844.83 58.41 o 5 3 0 1158.02 1947.39 61.86 o 6 3 0 454.85 466.64 21.47 o 7 3 0 2435.55 2318.16 84.55 o 8 3 0 281.26 277.09 23.34 o 9 3 0 515.61 482.19 32.15 o 10 3 0 473.69 451.79 32.62 o 11 3 0 94.72 147.69 59.88 o 12 3 0 227.82 274.35 28.94 o 13 3 0 24.66 19.31 26.04 o 14 3 0 120.14 96.59 34.56 o 15 3 0 48.19 41.72 30.69 o 16 3 0 103.80 160.60 44.60 o 0 4 0 5144.08 5353.18 326.21 o 1 4 0 144.46 173.35 16.53 o 2 4 0 2594.24 2942.48 184.69 o 3 4 0 195.22 241.26 16.35 o 4 4 0 338.42 358.27 21.44 o 5 4 0 48.94 616.51 34.28 o 6 4 0 35.17 38.89 7.20 o 7 4 0 371.71 396.33 20.19 o 8 4 0 457.13 436.72 22.34 o 9 4 0 31.35 11.09 12.65 o 10 4 0 14.77 117.49 23.08 o 11 4 0 255.66 303.16 46.68 o 12 4 0 337.74 285.76 48.09 o 13 4 0 73.23 90.64 35.44 o 14 4 0 116.59 218.24 45.20 o 15 4 0 103.81 85.20 36.84 o 16 4 0 21.69 6.52 31.28 o 1 5 0 730.20 715.64 39.40 o 2 5 0 876.82 1179.46 96.68 o 3 5 0 97.17 106.39 12.33 o 4 5 0 908.75 917.09 52.45 o 5 5 0 77.80 711.43 38.14 o 6 5 0 276.49 246.80 21.18 o 7 5 0 160.21 152.71 17.03 o 8 5 0 429.32 372.05 47.80 o 9 5 0 186.82 293.28 43.96 o 10 5 0 28.60 53.04 29.48 o 11 5 0 183.95 176.61 38.96 o 12 5 0 178.22 248.60 47.56 o 13 5 0 23.08 9.84 28.08 o 14 5 0 133.84 107.32 40.52 o 15 5 0 15.28 65.92 34.92 o 0 6 0 55.77 53.84 18.76 o 1 6 0 458.34 415.33 28.92 o 2 6 0 412.90 437.38 29.94 o 3 6 0 295.63 330.59 18.97 o 4 6 0 209.71 328.65 43.56 o 5 6 0 362.90 415.67 33.34 o 6 6 0 104.08 108.30 14.72 o 7 6 0 289.25 350.99 24.12 o 8 6 0 11.40 9.88 23.64 o 9 6 0 529.92 676.85 67.49 o 10 6 0 151.13 178.60 40.20 o 11 6 0 110.97 95.64 36.44 o 12 6 0 139.18 73.97 36.65 o 13 6 0 45.29 36.84 34.85 o 14 6 0 65.72 90.04 39.88 o 1 7 0 413.47 340.90 28.76 o 2 7 0 93.31 267.56 31.64 o 3 7 0 124.47 147.98 20.26 o 4 7 0 616.03 620.27 38.44 o 5 7 0 84.00 148.02 21.11 o 6 7 0 370.81 422.83 35.25 o 7 7 0 107.13 162.33 25.50 o 8 7 0 213.27 207.56 42.43 o 9 7 0 162.06 189.25 41.68 o 10 7 0 67.95 112.84 37.12 o 11 7 0 129.65 162.64 44.00 o 12 7 0 24.32 44.28 35.28 o 13 7 0 121.54 179.80 48.20 o 0 8 0 619.21 713.73 63.92 o 1 8 0 128.06 126.90 17.15 o 2 8 0 127.78 183.41 16.92 o 3 8 0 246.17 284.58 20.30 o 4 8 0 234.76 365.17 41.31 o 5 8 0 19.13 45.65 12.49 o 6 8 0 65.15 100.72 14.84 o 7 8 0 114.02 131.61 25.44 o 8 8 0 215.54 232.88 31.13 o 9 8 0 46.47 46.00 32.55 o 10 8 0 192.64 284.16 51.64 o 11 8 0 57.80 96.88 39.56 o 12 8 0 298.58 404.36 65.20 o 1 9 0 77.98 65.26 17.23 o 2 9 0 69.42 173.28 34.83 o 3 9 0 27.35 54.27 15.13 o 4 9 0 5.53 9.37 11.31 o 5 9 0 6.05 43.23 13.36 o 6 9 0 12.52 16.45 15.97 o 7 9 0 178.31 210.17 24.64 o 8 9 0 80.56 90.44 20.77 o 9 9 0 111.27 121.92 40.60 o 10 9 0 66.22 59.32 38.12 o 0 10 0 66.01 94.13 25.20 o 1 10 0 5.49 -19.25 12.83 o 2 10 0 63.79 89.60 19.16 o 3 10 0 131.65 179.97 23.29 o 4 10 0 26.54 44.23 16.52 o 5 10 0 99.03 182.89 43.68 o 6 10 0 49.73 78.76 25.63 o 7 10 0 104.81 77.91 26.27 o 8 10 0 62.29 54.96 26.25 o 1 11 0 187.17 240.61 36.07 o 2 11 0 24.68 69.96 35.68 o 3 11 0 37.61 24.24 28.19 o 4 11 0 15.48 32.52 34.48 o -4 -11 1 74.33 116.80 43.80 o -3 -11 1 9.42 -3.12 33.12 o -2 -11 1 107.02 148.28 44.04 o -1 -11 1 39.00 71.44 37.20 o 0 -11 1 3.27 -20.04 32.40 o 1 -11 1 71.34 97.88 43.17 o 2 -11 1 36.83 14.95 37.44 o -8 -10 1 120.44 122.44 46.00 o -7 -10 1 419.36 278.12 53.72 o -6 -10 1 33.11 -25.44 30.69 o -5 -10 1 217.20 262.32 51.56 o -4 -10 1 13.16 6.08 30.52 o -3 -10 1 43.57 59.88 33.40 o -2 -10 1 14.68 52.72 33.72 o -1 -10 1 14.22 8.12 27.92 o 0 -10 1 232.75 204.16 43.96 o 1 -10 1 198.79 158.08 32.26 o 2 -10 1 42.97 68.55 23.98 o 3 -10 1 51.48 113.44 35.72 o 4 -10 1 19.34 20.11 30.12 o 5 -10 1 45.13 85.28 37.76 o 6 -10 1 5.25 -0.56 31.88 o 7 -10 1 63.53 48.16 36.04 o -10 -9 1 93.50 72.12 39.92 o -9 -9 1 63.71 45.96 36.16 o -8 -9 1 256.24 166.96 45.16 o -7 -9 1 72.26 31.28 33.72 o -6 -9 1 80.12 36.88 31.96 o -5 -9 1 122.86 142.64 39.12 o -4 -9 1 201.20 163.52 39.07 o -3 -9 1 147.15 162.41 26.21 o -2 -9 1 307.27 333.76 33.65 o -1 -9 1 156.95 79.83 22.07 o 0 -9 1 207.90 189.80 27.40 o 1 -9 1 240.47 211.16 28.28 o 2 -9 1 44.33 49.27 21.18 o 3 -9 1 163.42 153.32 28.90 o 4 -9 1 82.89 62.76 31.69 o 5 -9 1 136.25 182.40 40.76 o 6 -9 1 490.82 417.08 58.44 o 7 -9 1 101.74 51.96 21.17 o 8 -9 1 176.85 181.33 29.50 o 9 -9 1 105.35 202.82 45.10 o 10 -9 1 6.58 17.72 21.60 o -12 -8 1 156.64 166.45 57.02 o -11 -8 1 38.89 45.06 23.24 o -10 -8 1 2.11 12.62 18.90 o -9 -8 1 124.02 143.20 26.98 o -8 -8 1 165.95 109.90 26.70 o -7 -8 1 145.22 114.19 35.36 o -6 -8 1 21.94 24.67 18.19 o -5 -8 1 20.88 5.28 24.72 o -4 -8 1 285.97 305.65 45.60 o -3 -8 1 109.96 87.10 20.28 o -2 -8 1 146.53 205.12 51.28 o -1 -8 1 7.08 1.41 15.11 o 0 -8 1 1385.96 1331.68 70.55 o 1 -8 1 3.59 -6.55 15.69 o 2 -8 1 87.35 216.85 91.12 o 3 -8 1 36.47 12.20 17.64 o 4 -8 1 253.15 274.41 42.57 o 5 -8 1 60.84 86.46 26.12 o 6 -8 1 15.19 13.92 16.75 o 7 -8 1 70.08 80.10 21.52 o 8 -8 1 61.86 59.40 21.39 o 9 -8 1 101.63 126.40 26.66 o 10 -8 1 129.00 164.63 45.12 o 11 -8 1 125.83 105.72 27.92 o -13 -7 1 32.20 57.50 26.25 o -12 -7 1 55.71 69.99 25.31 o -11 -7 1 278.34 261.76 33.19 o -10 -7 1 40.84 100.65 23.90 o -9 -7 1 93.85 204.33 40.22 o -8 -7 1 109.65 113.76 23.07 o -7 -7 1 385.98 392.92 27.30 o -6 -7 1 86.18 87.22 15.00 o -5 -7 1 153.59 209.42 24.93 o -4 -7 1 342.36 333.64 30.23 o -3 -7 1 895.51 941.85 85.05 o -2 -7 1 585.49 495.27 27.81 o -1 -7 1 323.34 323.53 31.34 o 0 -7 1 330.23 298.37 30.38 o 1 -7 1 308.48 306.92 28.33 o 2 -7 1 308.78 269.16 26.57 o 3 -7 1 308.39 266.91 21.20 o 4 -7 1 124.43 130.12 20.15 o 5 -7 1 167.11 282.27 27.93 o 6 -7 1 54.01 57.27 33.29 o 7 -7 1 207.63 210.23 26.65 o 8 -7 1 151.96 127.63 23.20 o 9 -7 1 32.35 2.54 20.32 o 10 -7 1 10.82 21.31 18.78 o 11 -7 1 91.93 105.64 26.76 o 12 -7 1 68.36 77.58 26.37 o 13 -7 1 19.42 2.78 22.39 o -14 -6 1 21.95 -17.95 20.74 o -13 -6 1 12.20 17.05 24.44 o -12 -6 1 75.25 104.82 39.90 o -11 -6 1 41.00 62.51 26.18 o -10 -6 1 78.36 72.04 30.70 o -9 -6 1 182.47 212.94 76.98 o -8 -6 1 176.95 141.27 17.03 o -7 -6 1 404.13 378.89 35.56 o -6 -6 1 14.07 16.32 10.51 o -5 -6 1 104.78 211.26 49.52 o -4 -6 1 317.83 335.30 22.30 o -3 -6 1 179.47 210.55 28.10 o -2 -6 1 288.35 332.31 21.15 o -1 -6 1 12.07 1.16 9.21 o 0 -6 1 240.73 235.64 18.68 o 1 -6 1 318.39 335.98 26.55 o 2 -6 1 6.30 25.70 13.75 o 3 -6 1 546.18 471.66 32.99 o 4 -6 1 137.61 139.88 18.92 o 5 -6 1 930.31 793.69 46.22 o 6 -6 1 246.48 254.29 26.23 o 7 -6 1 211.43 199.74 24.89 o 8 -6 1 117.16 129.18 23.42 o 9 -6 1 1.36 16.35 16.63 o 10 -6 1 68.38 71.88 21.57 o 11 -6 1 25.41 36.31 20.29 o 12 -6 1 58.87 47.58 22.27 o 13 -6 1 158.08 205.18 33.12 o 14 -6 1 29.55 63.34 42.57 o -15 -5 1 139.04 165.11 31.87 o -14 -5 1 32.04 39.97 21.94 o -13 -5 1 73.25 97.86 25.18 o -12 -5 1 17.32 5.99 17.35 o -11 -5 1 249.82 208.88 28.39 o -10 -5 1 63.87 103.52 20.96 o -9 -5 1 132.39 278.43 83.60 o -8 -5 1 268.85 264.80 20.23 o -7 -5 1 292.30 279.08 20.21 o -6 -5 1 251.73 240.45 18.75 o -5 -5 1 771.44 833.29 36.74 o -4 -5 1 118.41 122.08 13.19 o -3 -5 1 1421.65 1433.91 87.72 o -2 -5 1 872.90 1133.28 63.73 o -1 -5 1 54.11 37.75 9.49 o 0 -5 1 2305.96 2242.30 83.34 o 1 -5 1 906.93 825.16 30.45 o 2 -5 1 354.69 402.94 21.14 o 3 -5 1 162.98 140.29 13.90 o 4 -5 1 107.21 104.55 15.80 o 5 -5 1 147.95 259.38 68.64 o 6 -5 1 62.39 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