#------------------------------------------------------------------------------ #$Date: 2009-06-07 09:06:07 +0300 (Sun, 07 Jun 2009) $ #$Revision: 754 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2221873.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221873_Fobs loop_ _publ_author_name 'H\"okelek, Tuncer' 'Dal, Hakan' 'Tercan, Bar\?i\,s' '\"Ozbek, F. Elif' 'Necefo\(glu, Hacali' _publ_section_title ; Diaquabis(2-bromobenzoato-\kO)bis(nicotinamide-\kN^1^)zinc(II) ; _journal_coeditor_code XU2517 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m607 _journal_page_last m608 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.346 _cell_angle_gamma 90.000 _cell_length_a 7.9111 _cell_length_b 18.1604 _cell_length_c 9.8345 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.7455 _[local]_cod_data_source_file xu2517Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' el30 in P 21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 210.78 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10298.72 11630.24 55.05 o 4 0 0 5598.81 6377.79 62.53 o 6 0 0 198.86 278.67 28.57 o 8 0 0 4428.11 4358.14 70.64 o 10 0 0 1141.72 1026.81 57.52 o 1 1 0 9423.17 10309.65 235.02 o 2 1 0 7162.06 7723.57 101.65 o 3 1 0 2077.71 2028.60 35.57 o 4 1 0 6222.49 6716.50 137.79 o 5 1 0 1934.38 1948.36 41.86 o 6 1 0 839.92 872.76 21.42 o 7 1 0 2416.76 2443.77 33.84 o 8 1 0 1930.09 2048.40 145.72 o 9 1 0 586.38 541.06 30.66 o 10 1 0 42.53 91.31 24.53 o 0 2 0 188.07 184.97 17.84 o 1 2 0 453.62 472.60 16.68 o 2 2 0 301.75 366.27 13.18 o 3 2 0 5600.54 5893.45 124.34 o 4 2 0 13772.33 14164.90 243.12 o 5 2 0 142.10 144.40 7.64 o 6 2 0 9967.98 10082.65 80.19 o 7 2 0 812.84 955.11 44.59 o 8 2 0 187.08 265.09 22.06 o 9 2 0 160.98 192.22 22.75 o 10 2 0 621.81 628.49 35.71 o 1 3 0 6489.96 6577.08 184.15 o 2 3 0 16446.36 17468.60 156.84 o 3 3 0 1121.56 1216.58 17.35 o 4 3 0 2448.21 2636.55 117.88 o 5 3 0 9.97 21.19 6.73 o 6 3 0 2079.74 2185.78 120.44 o 7 3 0 841.06 821.52 20.77 o 8 3 0 1588.70 1614.82 41.50 o 9 3 0 1769.53 1775.75 41.27 o 10 3 0 73.47 86.08 33.58 o 0 4 0 9941.69 9495.30 636.87 o 1 4 0 18404.18 19097.56 598.15 o 2 4 0 2970.55 2994.21 146.34 o 3 4 0 5361.17 5658.60 37.31 o 4 4 0 2061.71 2309.36 27.52 o 5 4 0 4.28 18.84 10.72 o 6 4 0 1.42 12.83 12.64 o 7 4 0 85.58 111.55 12.38 o 8 4 0 763.51 750.05 27.45 o 9 4 0 81.43 108.24 21.54 o 1 5 0 15970.33 17178.66 672.62 o 2 5 0 12.24 21.01 3.15 o 3 5 0 3411.90 3508.18 31.74 o 4 5 0 469.75 464.22 17.06 o 5 5 0 14010.34 14495.16 237.21 o 6 5 0 17.58 27.85 14.16 o 7 5 0 2227.33 2306.46 43.94 o 8 5 0 160.34 179.22 19.05 o 9 5 0 334.09 371.21 64.66 o 0 6 0 430.78 492.71 43.06 o 1 6 0 248.87 291.54 14.25 o 2 6 0 3724.41 4028.88 111.21 o 3 6 0 10763.56 11739.87 59.52 o 4 6 0 6771.73 7235.11 51.27 o 5 6 0 0.45 14.75 15.25 o 6 6 0 1199.91 1195.59 35.71 o 7 6 0 2433.49 2430.71 31.04 o 8 6 0 81.55 68.10 17.50 o 9 6 0 1400.00 1400.81 39.40 o 1 7 0 15043.20 14624.10 751.90 o 2 7 0 1567.85 1713.13 64.30 o 3 7 0 259.43 287.46 9.08 o 4 7 0 35.77 47.09 4.87 o 5 7 0 1885.22 1933.09 63.67 o 6 7 0 989.82 1007.62 20.36 o 7 7 0 6.76 7.78 11.83 o 8 7 0 6.90 8.23 14.26 o 9 7 0 2890.10 2886.94 51.26 o 0 8 0 67.46 63.51 5.26 o 1 8 0 6181.31 6431.45 291.56 o 2 8 0 5445.66 5852.39 217.40 o 3 8 0 8536.30 8999.78 384.46 o 4 8 0 1440.08 1510.25 25.00 o 5 8 0 81.32 92.71 9.85 o 6 8 0 168.96 191.79 14.81 o 7 8 0 3370.57 3369.73 57.00 o 8 8 0 497.31 462.65 24.55 o 9 8 0 173.63 175.34 24.05 o 1 9 0 10.63 20.49 4.59 o 2 9 0 81.29 76.56 5.72 o 3 9 0 1441.55 1376.14 52.88 o 4 9 0 1853.09 1920.24 60.62 o 5 9 0 3472.29 3471.59 55.74 o 6 9 0 372.64 366.67 18.34 o 7 9 0 1536.15 1572.77 30.20 o 8 9 0 337.41 338.88 22.78 o 9 9 0 6.01 10.55 20.27 o 0 10 0 8020.42 7986.65 430.27 o 1 10 0 32.73 24.56 6.54 o 2 10 0 6357.24 6613.85 388.65 o 3 10 0 1924.87 1894.95 104.33 o 4 10 0 40.18 39.85 8.77 o 5 10 0 154.22 168.87 13.17 o 6 10 0 304.10 306.96 18.42 o 7 10 0 643.09 668.20 24.93 o 8 10 0 505.51 516.52 26.42 o 9 10 0 303.52 313.38 27.49 o 1 11 0 1006.14 972.76 84.42 o 2 11 0 3572.80 3505.72 229.73 o 3 11 0 48.83 65.92 6.87 o 4 11 0 1527.90 1552.33 56.56 o 5 11 0 58.83 59.25 12.45 o 6 11 0 706.79 698.81 23.79 o 7 11 0 343.87 334.37 21.92 o 8 11 0 716.86 694.26 29.15 o 9 11 0 1158.52 1204.38 52.88 o 0 12 0 2205.95 2127.16 263.63 o 1 12 0 352.61 394.40 36.95 o 2 12 0 139.52 140.97 8.48 o 3 12 0 125.45 140.22 16.83 o 4 12 0 1907.22 1835.82 85.09 o 5 12 0 123.26 130.43 15.37 o 6 12 0 4555.93 4499.55 49.39 o 7 12 0 2.17 14.23 15.44 o 8 12 0 18.61 20.79 17.72 o 1 13 0 277.88 273.40 26.91 o 2 13 0 7927.31 7856.56 674.69 o 3 13 0 1124.14 1038.51 120.80 o 4 13 0 1021.41 1000.13 58.60 o 5 13 0 356.15 356.59 31.46 o 6 13 0 2073.43 2105.97 38.51 o 7 13 0 1.25 15.72 16.11 o 8 13 0 1201.31 1188.88 36.65 o 0 14 0 5313.61 5018.81 769.91 o 1 14 0 60.94 64.04 11.48 o 2 14 0 1918.57 1916.06 139.60 o 3 14 0 381.68 347.63 42.08 o 4 14 0 218.11 213.14 18.09 o 5 14 0 876.76 832.27 58.32 o 6 14 0 385.00 369.19 24.04 o 7 14 0 8.23 15.31 17.59 o 8 14 0 293.53 303.83 26.00 o 1 15 0 180.68 148.13 17.35 o 2 15 0 2050.93 1967.15 213.06 o 3 15 0 473.46 493.90 50.63 o 4 15 0 25.53 24.97 14.08 o 5 15 0 2043.26 2049.61 127.14 o 6 15 0 965.11 962.66 32.39 o 7 15 0 340.75 344.70 26.54 o 8 15 0 756.49 751.58 74.89 o 0 16 0 50.61 58.51 16.48 o 1 16 0 584.75 537.27 63.49 o 2 16 0 705.23 769.20 64.99 o 3 16 0 719.65 611.23 83.77 o 4 16 0 1927.42 2065.31 132.72 o 5 16 0 392.81 409.50 25.22 o 6 16 0 1379.96 1387.06 45.02 o 7 16 0 229.33 230.89 24.35 o 1 17 0 3965.74 4107.99 310.40 o 2 17 0 745.63 695.45 83.77 o 3 17 0 38.21 43.03 18.44 o 4 17 0 135.76 122.23 21.57 o 5 17 0 209.26 185.59 28.76 o 6 17 0 132.15 128.80 22.27 o 7 17 0 15.11 6.02 21.14 o 0 18 0 895.43 878.28 171.97 o 1 18 0 502.29 564.16 41.68 o 2 18 0 155.82 150.85 22.86 o 3 18 0 2995.33 2805.69 378.88 o 4 18 0 387.69 345.18 30.69 o 5 18 0 13.99 17.92 20.85 o 6 18 0 222.38 206.81 28.63 o 1 19 0 604.81 598.85 45.13 o 2 19 0 7.93 -4.19 20.00 o 3 19 0 2438.56 2415.93 166.57 o 4 19 0 132.54 148.08 24.97 o 5 19 0 3054.30 3112.67 125.26 o 6 19 0 189.13 185.30 29.35 o 0 20 0 1629.84 1853.42 286.81 o 1 20 0 556.97 609.48 82.61 o 2 20 0 1091.68 1122.44 157.11 o 3 20 0 1154.93 1235.72 193.39 o 4 20 0 214.94 221.51 28.88 o 5 20 0 139.86 133.50 27.13 o 1 21 0 2752.96 3076.08 258.25 o 2 21 0 293.22 301.30 62.53 o 3 21 0 33.61 39.97 25.23 o 4 21 0 70.38 72.20 26.30 o 5 21 0 270.14 271.02 33.48 o 0 22 0 38.49 27.61 25.25 o 1 22 0 74.27 83.50 27.38 o 2 22 0 31.12 33.89 26.05 o 3 22 0 590.62 674.91 43.65 o 4 22 0 1364.60 1403.76 74.89 o 1 23 0 27.69 19.82 27.53 o 2 23 0 1047.52 1125.23 94.19 o 3 23 0 899.41 1012.75 50.55 o 1 24 0 1.75 -10.62 28.39 o -9 0 1 1433.32 1490.03 55.59 o -7 0 1 2458.75 2631.10 54.04 o -5 0 1 2838.97 3089.95 120.04 o -3 0 1 13048.83 13535.57 367.09 o -1 0 1 1133.17 1179.34 69.43 o 3 0 1 44.22 95.14 8.57 o 5 0 1 3569.60 3671.15 44.39 o 7 0 1 16540.68 15934.82 100.36 o 9 0 1 895.69 873.56 46.71 o -10 1 1 1283.14 1386.39 43.92 o -9 1 1 594.81 671.71 33.01 o -8 1 1 1740.99 1703.55 60.22 o -7 1 1 1204.48 1312.84 29.42 o -6 1 1 9.45 20.97 7.73 o -5 1 1 8090.58 8073.97 153.21 o -4 1 1 4284.73 4576.10 129.10 o -3 1 1 533.96 508.97 24.07 o -2 1 1 945.63 1025.60 38.72 o -1 1 1 11240.79 10949.20 487.54 o 0 1 1 2455.77 2458.33 122.28 o 1 1 1 1263.17 1331.23 28.95 o 2 1 1 1695.41 1720.87 21.42 o 3 1 1 11610.87 12921.56 74.52 o 4 1 1 1632.63 1699.73 17.63 o 5 1 1 3903.14 3924.70 32.30 o 6 1 1 33.45 51.04 11.22 o 7 1 1 170.63 169.85 20.84 o 8 1 1 619.03 596.77 24.57 o 9 1 1 1531.05 1480.71 37.32 o -10 2 1 212.52 279.28 28.79 o -9 2 1 3153.93 3191.46 52.50 o -8 2 1 10.52 28.72 21.04 o -7 2 1 3008.01 3140.10 42.36 o -6 2 1 1357.72 1417.37 22.86 o -5 2 1 20.88 49.12 9.23 o -4 2 1 372.76 363.23 19.73 o -3 2 1 3582.35 3694.73 129.43 o -2 2 1 1699.99 1698.77 65.77 o -1 2 1 11275.00 11353.86 575.24 o 0 2 1 544.45 444.73 37.03 o 1 2 1 18520.12 18442.24 493.95 o 2 2 1 658.84 598.04 18.24 o 3 2 1 11966.55 12087.35 313.18 o 4 2 1 298.62 263.49 7.29 o 5 2 1 2.72 16.23 5.11 o 6 2 1 273.82 317.05 17.20 o 7 2 1 70.93 101.52 21.23 o 8 2 1 322.20 354.31 31.27 o 9 2 1 82.63 139.52 21.54 o -10 3 1 1.88 27.69 23.90 o -9 3 1 202.42 280.56 47.87 o -8 3 1 7.18 15.73 16.65 o -7 3 1 413.20 476.93 31.62 o -6 3 1 1587.40 1623.88 34.92 o -5 3 1 408.23 396.34 15.49 o -4 3 1 16938.03 17493.19 450.90 o -3 3 1 4145.37 4523.84 157.66 o -2 3 1 5505.92 5509.46 184.20 o -1 3 1 3077.38 3025.15 179.22 o 0 3 1 78.52 90.45 6.86 o 1 3 1 10356.44 10382.24 364.48 o 2 3 1 124.50 125.09 5.55 o 3 3 1 2007.27 2140.38 62.75 o 4 3 1 1211.99 1320.72 22.83 o 5 3 1 1992.53 2030.33 27.18 o 6 3 1 2274.17 2383.45 32.46 o 7 3 1 1242.86 1330.99 43.23 o 8 3 1 2713.82 2664.61 37.14 o 9 3 1 1649.85 1568.53 44.59 o -10 4 1 1107.22 1092.07 61.18 o -9 4 1 111.69 108.64 21.16 o -8 4 1 196.58 226.98 27.02 o -7 4 1 409.17 385.29 26.28 o -6 4 1 8245.85 8464.80 74.20 o -5 4 1 4196.08 4227.41 63.48 o -4 4 1 19.97 14.19 3.88 o -3 4 1 6656.12 6521.46 153.04 o -2 4 1 576.05 579.84 26.72 o -1 4 1 943.28 922.85 46.75 o 0 4 1 693.91 742.45 69.73 o 1 4 1 4090.57 4459.61 133.97 o 2 4 1 1229.43 1319.82 15.65 o 3 4 1 4252.82 4817.48 105.09 o 4 4 1 2811.78 2631.37 95.57 o 5 4 1 3756.53 3769.22 37.64 o 6 4 1 4182.33 4280.99 44.20 o 7 4 1 1893.69 1952.15 52.31 o 8 4 1 1402.64 1428.98 53.46 o 9 4 1 359.54 355.50 41.88 o -10 5 1 971.12 998.02 44.20 o -9 5 1 4.58 -3.18 18.82 o -8 5 1 7339.36 7217.31 208.84 o -7 5 1 6.80 19.68 11.94 o -6 5 1 5724.73 6112.65 128.91 o -5 5 1 2975.79 2922.86 23.60 o -4 5 1 26.18 34.21 5.41 o -3 5 1 283.16 265.24 8.98 o -2 5 1 2948.85 2994.34 168.42 o -1 5 1 369.08 448.56 24.81 o 0 5 1 21865.67 19860.87 1630.83 o 1 5 1 414.24 461.91 19.14 o 2 5 1 19091.26 20064.13 604.46 o 3 5 1 1250.79 1327.96 16.41 o 4 5 1 1319.55 1338.16 20.81 o 5 5 1 10.32 5.71 10.04 o 6 5 1 1663.86 1710.69 31.58 o 7 5 1 1.34 3.14 17.95 o 8 5 1 203.48 214.65 17.47 o 9 5 1 175.50 220.72 22.48 o -9 6 1 51.80 58.59 21.89 o -8 6 1 56.71 60.22 29.34 o -7 6 1 56.50 90.69 13.75 o -6 6 1 3062.81 3171.77 34.96 o -5 6 1 1849.15 1812.75 25.07 o -4 6 1 1002.18 996.32 12.91 o -3 6 1 3446.75 3530.35 118.85 o -2 6 1 9942.72 9784.61 586.49 o -1 6 1 869.80 975.28 57.94 o 0 6 1 26665.07 25747.66 1787.18 o 1 6 1 4205.96 4169.03 243.46 o 2 6 1 96.94 94.15 4.89 o 3 6 1 4583.50 4785.54 42.34 o 4 6 1 11735.39 11773.63 96.50 o 5 6 1 1820.71 1830.26 31.13 o 6 6 1 553.78 559.52 23.17 o 7 6 1 867.27 840.94 33.90 o 8 6 1 540.86 529.21 23.56 o 9 6 1 637.11 630.83 30.82 o -9 7 1 261.68 286.65 26.25 o -8 7 1 972.21 894.52 28.70 o -7 7 1 282.36 276.68 18.54 o -6 7 1 911.43 852.32 22.47 o -5 7 1 762.48 800.82 19.88 o -4 7 1 7540.71 7669.64 178.36 o -3 7 1 86.40 103.91 4.79 o -2 7 1 19121.65 19507.09 970.59 o -1 7 1 392.26 385.44 34.73 o 0 7 1 84.33 90.25 6.33 o 1 7 1 24.55 38.91 3.37 o 2 7 1 5599.04 6040.85 140.07 o 3 7 1 269.50 284.54 12.72 o 4 7 1 11.55 11.55 8.35 o 5 7 1 5.97 9.89 10.99 o 6 7 1 10742.85 10817.69 87.15 o 7 7 1 325.90 329.27 26.84 o 8 7 1 2149.91 2169.51 95.93 o 9 7 1 27.11 5.85 19.56 o -9 8 1 830.31 819.33 37.08 o -8 8 1 53.14 51.04 16.57 o -7 8 1 1043.57 1033.31 27.37 o -6 8 1 5461.39 5535.86 87.16 o -5 8 1 71.19 85.96 11.05 o -4 8 1 1952.78 2021.09 56.89 o -3 8 1 45.11 41.92 4.84 o -2 8 1 692.58 604.16 42.55 o -1 8 1 1863.13 1826.26 139.10 o 0 8 1 8947.69 8809.40 583.42 o 1 8 1 4104.92 3779.16 254.68 o 2 8 1 1119.34 1200.43 46.97 o 3 8 1 5926.02 6170.89 67.08 o 4 8 1 4653.72 4826.90 41.27 o 5 8 1 1674.23 1694.92 32.79 o 6 8 1 1141.13 1134.17 31.05 o 7 8 1 521.10 504.81 32.17 o 8 8 1 1544.42 1504.12 30.12 o 9 8 1 164.04 139.84 22.21 o -9 9 1 104.05 66.60 22.56 o -8 9 1 2599.30 2538.44 42.02 o -7 9 1 1204.76 1175.54 29.74 o -6 9 1 2494.11 2539.70 36.92 o -5 9 1 825.43 812.26 21.90 o -4 9 1 1324.20 1203.99 63.51 o -3 9 1 69.40 72.10 5.77 o -2 9 1 85.37 105.55 7.60 o -1 9 1 3207.84 2850.91 236.56 o 0 9 1 4983.48 4630.49 332.06 o 1 9 1 1102.07 1206.50 73.63 o 2 9 1 6956.53 6449.61 228.29 o 3 9 1 1919.97 1983.93 49.80 o 4 9 1 389.11 382.45 17.05 o 5 9 1 165.66 151.78 16.22 o 6 9 1 631.68 616.63 27.22 o 7 9 1 106.27 93.28 23.33 o 8 9 1 15.00 15.94 14.63 o 9 9 1 228.75 227.77 24.02 o -9 10 1 26.92 32.52 22.49 o -8 10 1 31.78 32.84 17.02 o -7 10 1 13.79 7.46 14.32 o -6 10 1 700.10 690.69 24.15 o -5 10 1 415.50 416.89 19.61 o -4 10 1 50.36 58.70 10.67 o -3 10 1 7945.72 7900.41 427.01 o -2 10 1 1345.60 1304.69 96.68 o -1 10 1 2913.07 2756.92 205.00 o 0 10 1 3312.15 3236.33 217.08 o 1 10 1 1126.78 1154.40 67.44 o 2 10 1 150.36 156.83 9.29 o 3 10 1 1149.75 1130.28 37.37 o 4 10 1 807.81 787.26 15.93 o 5 10 1 4700.57 4914.56 53.04 o 6 10 1 5.28 20.11 9.63 o 7 10 1 3180.51 3262.74 47.07 o 8 10 1 454.65 425.77 23.40 o -9 11 1 26.05 2.81 19.76 o -8 11 1 34.22 33.45 17.90 o -7 11 1 1437.06 1442.04 33.82 o -6 11 1 1352.67 1227.40 29.58 o -5 11 1 1276.51 1274.67 36.40 o -4 11 1 2225.11 2146.98 102.46 o -3 11 1 256.62 254.16 13.18 o -2 11 1 3484.12 3394.36 219.50 o -1 11 1 4506.41 4157.31 283.40 o 0 11 1 9.72 18.11 5.05 o 1 11 1 2688.28 2648.48 159.14 o 2 11 1 5.43 13.89 5.71 o 3 11 1 3820.12 3703.60 161.93 o 4 11 1 21.14 19.46 8.54 o 5 11 1 4096.25 4127.84 64.46 o 6 11 1 1846.20 1868.59 48.89 o 7 11 1 0.43 7.23 13.69 o 8 11 1 101.46 116.02 18.08 o -9 12 1 3639.06 3728.55 120.05 o -8 12 1 11.45 10.59 18.55 o -7 12 1 3321.78 3340.02 75.65 o -6 12 1 47.38 55.21 15.55 o -5 12 1 56.78 57.05 13.81 o -4 12 1 7.70 11.61 11.51 o -3 12 1 2543.91 2488.33 168.30 o -2 12 1 48.82 37.13 5.50 o -1 12 1 392.17 329.92 23.74 o 0 12 1 204.65 231.13 13.61 o 1 12 1 13208.37 12666.03 805.44 o 2 12 1 836.97 887.07 45.90 o 3 12 1 6225.06 6151.25 289.61 o 4 12 1 59.12 56.38 10.63 o 5 12 1 36.36 39.60 11.04 o 6 12 1 236.50 242.02 18.43 o 7 12 1 1536.74 1571.72 33.20 o 8 12 1 10.32 5.16 17.06 o -8 13 1 454.67 458.93 29.83 o -7 13 1 866.61 869.28 32.07 o -6 13 1 753.44 774.73 28.23 o -5 13 1 4824.30 4569.48 295.84 o -4 13 1 400.26 415.71 28.94 o -3 13 1 102.49 96.18 9.85 o -2 13 1 2312.46 2425.49 126.00 o -1 13 1 4177.41 4194.77 256.06 o 0 13 1 431.74 446.30 29.62 o 1 13 1 1605.49 1574.53 118.23 o 2 13 1 524.50 509.69 24.60 o 3 13 1 2378.27 2400.12 82.89 o 4 13 1 668.50 705.86 28.74 o 5 13 1 2717.46 2738.89 82.83 o 6 13 1 359.57 365.40 22.38 o 7 13 1 32.44 43.67 16.45 o 8 13 1 217.91 217.87 22.41 o -8 14 1 36.80 43.44 21.07 o -7 14 1 126.23 137.58 20.65 o -6 14 1 8.63 7.53 15.65 o -5 14 1 617.27 643.34 27.26 o -4 14 1 175.88 168.65 25.28 o -3 14 1 11754.38 11341.52 1293.83 o -2 14 1 32.91 31.83 8.85 o -1 14 1 2903.83 2936.39 220.19 o 0 14 1 16.92 14.49 8.52 o 1 14 1 886.32 852.57 45.62 o 2 14 1 58.52 72.56 8.93 o 3 14 1 422.83 422.36 24.63 o 4 14 1 529.22 525.86 32.28 o 5 14 1 4188.47 4107.51 184.70 o 6 14 1 99.76 116.52 17.75 o 7 14 1 2989.95 3168.17 69.48 o 8 14 1 52.12 51.73 44.01 o -8 15 1 623.12 697.74 36.59 o -7 15 1 1519.78 1561.00 46.03 o -6 15 1 154.85 171.70 20.29 o -5 15 1 1078.01 1058.37 61.53 o -4 15 1 175.43 184.72 24.89 o -3 15 1 1601.45 1400.44 290.86 o -2 15 1 1101.41 1111.90 120.40 o -1 15 1 4626.21 4580.91 368.06 o 0 15 1 691.36 686.56 52.44 o 1 15 1 470.33 455.40 39.61 o 2 15 1 2701.72 2862.22 98.30 o 3 15 1 375.33 372.64 36.72 o 4 15 1 833.28 877.74 42.92 o 5 15 1 708.47 749.92 32.45 o 6 15 1 33.43 43.94 17.84 o 7 15 1 47.78 48.77 19.52 o -7 16 1 433.58 467.38 30.82 o -6 16 1 836.53 920.29 48.14 o -5 16 1 74.69 55.01 20.94 o -4 16 1 132.03 126.55 20.83 o -3 16 1 140.54 103.45 19.69 o -2 16 1 216.20 235.34 24.13 o -1 16 1 312.68 324.92 32.98 o 0 16 1 798.95 797.15 52.26 o 1 16 1 3986.56 3604.00 322.94 o 2 16 1 374.39 314.51 63.50 o 3 16 1 3206.80 3226.11 247.72 o 4 16 1 1263.98 1280.22 104.50 o 5 16 1 122.50 116.62 18.49 o 6 16 1 569.28 542.77 30.03 o 7 16 1 11.74 16.41 19.48 o -7 17 1 258.80 226.65 30.12 o -6 17 1 233.87 198.54 26.56 o -5 17 1 959.46 906.02 40.14 o -4 17 1 4173.15 3716.54 498.54 o -3 17 1 173.73 176.97 49.80 o -2 17 1 2144.86 1886.65 218.77 o -1 17 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