#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/19/2221986.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221986_Fobs loop_ _publ_author_name 'Zhao, Qing-Lan' 'Li, Guo-Peng' _publ_section_title ; Dibromido(2,2':6',2''-terpyridine-\k^3^N,N',N'')zinc(II) ; _journal_coeditor_code CV2561 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m693 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 126.051 _cell_angle_gamma 90.000 _cell_length_a 17.0972 _cell_length_b 9.3528 _cell_length_c 11.5334 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file cv2561Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 361.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 35292.81 35411.33 454.05 o 4 0 0 23692.46 24617.42 314.17 o 6 0 0 3264.38 3181.29 48.38 o 8 0 0 34583.45 33329.00 429.02 o 10 0 0 11356.42 11385.91 263.33 o 12 0 0 1120.45 1158.69 34.41 o 14 0 0 36.46 35.92 16.33 o 16 0 0 2568.15 2495.90 93.95 o 1 1 0 479.50 485.14 7.29 o 3 1 0 6834.45 6989.02 66.15 o 5 1 0 17904.24 18305.75 182.36 o 7 1 0 5303.19 5337.34 60.47 o 9 1 0 6600.30 6635.19 62.19 o 11 1 0 1089.63 1120.94 22.25 o 13 1 0 2018.61 2011.38 44.66 o 15 1 0 116.16 136.98 24.66 o 0 2 0 11669.94 12190.63 157.93 o 2 2 0 10281.43 10372.76 105.37 o 4 2 0 9805.72 9683.71 89.31 o 6 2 0 5926.70 5994.72 54.65 o 8 2 0 2376.99 2424.61 25.97 o 10 2 0 2190.61 2190.30 32.23 o 12 2 0 1115.53 1128.15 23.95 o 14 2 0 1284.85 1259.58 32.27 o 16 2 0 832.87 832.66 42.08 o 1 3 0 13793.91 14171.96 97.94 o 3 3 0 10088.27 10393.13 77.07 o 5 3 0 4954.40 4928.13 40.31 o 7 3 0 8509.04 8693.96 64.08 o 9 3 0 3576.53 3496.86 41.94 o 11 3 0 1192.12 1201.14 23.87 o 13 3 0 703.28 640.05 24.56 o 15 3 0 103.66 109.52 23.44 o 0 4 0 165.95 155.11 12.05 o 2 4 0 9211.09 9507.57 68.17 o 4 4 0 52683.24 51549.74 344.88 o 6 4 0 14961.20 15570.32 104.12 o 8 4 0 1822.65 1775.05 26.69 o 10 4 0 199.50 187.03 12.07 o 12 4 0 9800.56 9784.15 129.23 o 14 4 0 2159.16 2143.79 45.15 o 1 5 0 24159.32 25535.16 166.30 o 3 5 0 3143.46 3088.61 31.36 o 5 5 0 10002.33 10227.35 79.83 o 7 5 0 1923.53 1840.80 29.29 o 9 5 0 3974.25 3920.53 48.36 o 11 5 0 2.97 0.00 13.89 o 13 5 0 960.77 1001.91 32.21 o 15 5 0 17.23 2.34 29.66 o 0 6 0 10782.90 10905.25 94.43 o 2 6 0 2873.24 2902.05 28.01 o 4 6 0 1994.32 2025.17 25.75 o 6 6 0 1961.29 1982.18 38.20 o 8 6 0 3011.11 3043.32 40.92 o 10 6 0 3568.17 3641.23 58.49 o 12 6 0 9.75 0.00 15.94 o 14 6 0 41.36 54.44 25.82 o 1 7 0 3370.98 3373.32 38.62 o 3 7 0 532.00 531.06 16.60 o 5 7 0 507.58 503.80 16.58 o 7 7 0 55.63 31.63 13.71 o 9 7 0 511.02 473.19 35.47 o 11 7 0 296.92 265.59 21.15 o 13 7 0 806.10 785.14 30.53 o 0 8 0 16475.67 17074.57 230.34 o 2 8 0 1242.87 1299.51 41.10 o 4 8 0 1466.68 1526.74 34.85 o 6 8 0 3302.34 3270.41 55.10 o 8 8 0 11620.63 11430.22 144.22 o 10 8 0 1615.14 1600.43 40.15 o 12 8 0 55.30 61.95 20.44 o 1 9 0 3631.02 3331.68 58.38 o 3 9 0 2072.47 2148.61 44.29 o 5 9 0 6775.63 6767.84 94.98 o 7 9 0 183.50 163.33 19.66 o 9 9 0 1768.52 1732.05 42.13 o 0 10 0 18.24 9.88 26.06 o 2 10 0 900.41 818.70 27.31 o 4 10 0 2690.44 2776.78 65.08 o 6 10 0 1353.08 1422.18 43.62 o 8 10 0 139.55 132.01 22.53 o 1 11 0 74.60 83.51 21.99 o 3 11 0 808.79 767.41 28.05 o 5 11 0 252.54 203.01 23.27 o -17 1 1 179.16 194.03 26.61 o -15 1 1 1.55 0.00 14.50 o -13 1 1 82.15 69.83 10.75 o -11 1 1 11819.92 11750.37 114.78 o -9 1 1 29954.36 30273.09 214.80 o -7 1 1 6.76 8.73 3.47 o -5 1 1 680.86 732.66 14.36 o -3 1 1 10852.33 11101.96 75.22 o -1 1 1 35592.65 34558.12 249.63 o 1 1 1 11669.60 11702.78 80.14 o 3 1 1 16453.97 17183.97 123.45 o 5 1 1 7131.27 6787.81 56.07 o 7 1 1 20957.13 21034.28 136.82 o 9 1 1 1611.31 1627.92 25.35 o 11 1 1 191.39 215.09 12.79 o 13 1 1 1090.68 1137.94 30.51 o 15 1 1 2243.10 2349.90 64.91 o -16 2 1 9.89 16.03 18.61 o -14 2 1 3672.27 3593.30 56.47 o -12 2 1 23.55 9.71 9.30 o -10 2 1 3399.48 3187.27 35.13 o -8 2 1 1855.34 2003.80 21.92 o -6 2 1 24639.06 24655.95 166.56 o -4 2 1 1576.71 1567.77 17.21 o -2 2 1 68674.36 67356.34 480.32 o 0 2 1 1057.91 1083.27 13.06 o 2 2 1 45560.17 45256.19 372.35 o 4 2 1 3429.91 3403.36 31.78 o 6 2 1 17059.59 16679.51 133.16 o 8 2 1 4658.54 4685.34 50.55 o 10 2 1 11214.21 11296.17 104.46 o 12 2 1 4062.97 3887.83 53.91 o 14 2 1 809.26 839.16 33.11 o -17 3 1 27.73 16.88 25.17 o -15 3 1 4125.58 4094.31 73.63 o -13 3 1 3328.48 3370.24 57.83 o -11 3 1 484.80 484.54 15.28 o -9 3 1 794.86 955.94 15.52 o -7 3 1 23828.26 23599.28 170.62 o -5 3 1 39785.92 39671.33 297.22 o -3 3 1 2190.25 2353.35 22.67 o -1 3 1 3404.69 3518.58 31.12 o 1 3 1 30850.56 30266.15 230.76 o 3 3 1 40528.92 39669.88 319.98 o 5 3 1 138.21 146.14 6.93 o 7 3 1 719.25 675.54 13.56 o 9 3 1 2228.75 2215.52 31.72 o 11 3 1 5494.37 5438.47 68.34 o 13 3 1 547.13 551.86 35.25 o 15 3 1 68.85 51.78 21.59 o -16 4 1 75.51 70.06 20.76 o -14 4 1 49.82 64.64 16.54 o -12 4 1 838.87 798.28 23.57 o -10 4 1 817.28 810.61 20.99 o -8 4 1 496.01 537.88 12.14 o -6 4 1 392.54 450.91 22.00 o -4 4 1 17.83 12.05 4.26 o -2 4 1 3373.37 3434.14 26.96 o 0 4 1 296.96 309.98 8.03 o 2 4 1 62.39 60.93 5.47 o 4 4 1 7.02 13.80 5.27 o 6 4 1 207.38 191.91 9.31 o 8 4 1 351.23 349.50 13.35 o 10 4 1 86.01 92.05 12.71 o 12 4 1 6.89 2.74 13.50 o 14 4 1 43.38 25.81 20.19 o -15 5 1 1935.94 1955.42 50.30 o -13 5 1 2549.23 2527.89 47.49 o -11 5 1 174.09 198.58 14.79 o -9 5 1 937.37 973.87 21.70 o -7 5 1 11798.57 11989.24 87.24 o -5 5 1 21420.14 21744.80 150.65 o -3 5 1 65.63 42.62 6.70 o -1 5 1 655.34 751.49 11.35 o 1 5 1 18003.88 18106.79 154.49 o 3 5 1 11432.17 11063.00 97.48 o 5 5 1 417.57 398.90 11.79 o 7 5 1 33.68 54.37 9.69 o 9 5 1 4896.87 4906.73 62.96 o 11 5 1 6267.96 6181.40 156.33 o 13 5 1 98.96 62.16 19.92 o -14 6 1 1763.99 1774.55 47.58 o -12 6 1 570.67 553.79 23.56 o -10 6 1 17043.97 17078.95 201.38 o -8 6 1 1577.02 1614.81 40.42 o -6 6 1 10376.52 10334.00 94.46 o -4 6 1 36.44 79.42 16.53 o -2 6 1 19496.72 18758.12 120.26 o 0 6 1 2164.47 2298.67 25.47 o 2 6 1 12331.11 12283.19 122.47 o 4 6 1 1190.72 1321.31 21.73 o 6 6 1 8940.96 8751.32 99.09 o 8 6 1 2061.21 2060.31 44.67 o 10 6 1 318.76 317.13 20.81 o 12 6 1 112.54 88.22 21.01 o -13 7 1 51.61 66.50 21.17 o -11 7 1 2334.73 2392.96 90.30 o -9 7 1 2117.79 2122.84 60.77 o -7 7 1 1071.52 1079.33 25.84 o -5 7 1 58.05 56.66 11.40 o -3 7 1 14333.76 14462.30 129.49 o -1 7 1 16880.98 17087.03 130.24 o 1 7 1 95.87 105.70 10.76 o 3 7 1 2449.79 2459.02 47.89 o 5 7 1 6317.44 6319.24 76.93 o 7 7 1 13455.76 13534.02 148.08 o 9 7 1 71.11 90.80 19.62 o 11 7 1 1603.39 1639.39 46.79 o -12 8 1 112.77 91.81 22.17 o -10 8 1 48.21 71.24 17.29 o -8 8 1 122.49 154.90 17.41 o -6 8 1 1100.66 1070.98 30.41 o -4 8 1 1013.69 962.05 22.84 o -2 8 1 662.23 613.90 18.70 o 0 8 1 24.24 24.76 10.55 o 2 8 1 717.09 746.00 23.72 o 4 8 1 930.34 951.04 26.11 o 6 8 1 195.45 195.48 33.08 o 8 8 1 484.17 501.75 28.24 o 10 8 1 33.30 36.49 21.63 o -11 9 1 777.22 841.83 36.48 o -9 9 1 2441.75 2386.63 48.79 o -7 9 1 659.79 708.57 24.61 o -5 9 1 131.11 159.80 24.81 o -3 9 1 3916.14 3667.01 59.75 o -1 9 1 6120.36 5829.50 74.42 o 1 9 1 483.65 469.29 20.50 o 3 9 1 521.81 497.08 23.74 o 5 9 1 3262.67 3254.50 57.66 o 7 9 1 2459.06 2555.89 50.97 o 9 9 1 88.86 88.83 23.93 o -8 10 1 82.17 124.03 22.49 o -6 10 1 4009.64 4105.21 68.00 o -4 10 1 1227.24 1175.85 35.51 o -2 10 1 1118.58 1121.12 40.61 o 0 10 1 21.79 14.18 15.26 o 2 10 1 4517.05 4440.10 64.33 o 4 10 1 1721.21 1565.49 57.74 o 6 10 1 552.41 561.57 28.03 o -5 11 1 3484.67 3644.70 79.24 o -3 11 1 26.55 87.74 26.52 o -1 11 1 267.43 285.50 25.42 o 1 11 1 2533.32 2684.62 49.59 o 3 11 1 4019.10 4223.84 65.01 o -18 0 2 1681.72 1784.57 80.21 o -16 0 2 592.76 626.26 35.46 o -14 0 2 1895.35 1743.56 61.99 o -12 0 2 21403.77 20974.93 277.50 o -10 0 2 8138.04 8242.88 77.74 o -8 0 2 2949.26 2908.50 30.88 o -6 0 2 5.57 20.61 5.36 o -4 0 2 130757.06 115679.24 965.35 o -2 0 2 18686.84 18698.69 283.89 o 0 0 2 2343.49 2545.16 28.40 o 2 0 2 76254.61 76956.66 605.74 o 4 0 2 45374.13 45759.43 358.47 o 6 0 2 24502.17 24849.12 199.19 o 8 0 2 723.85 735.65 20.20 o 10 0 2 577.63 579.43 31.38 o 12 0 2 4983.34 4988.78 102.41 o 14 0 2 2185.47 2273.69 66.33 o -17 1 2 1600.87 1566.78 46.29 o -15 1 2 411.84 472.46 24.41 o -13 1 2 1990.29 1959.25 27.16 o -11 1 2 3300.64 3341.56 26.89 o -9 1 2 6208.74 6330.50 41.07 o -7 1 2 9231.86 8874.84 54.24 o -5 1 2 7526.86 7474.71 43.30 o -3 1 2 24211.07 24438.91 138.75 o -1 1 2 1747.72 1828.10 13.60 o 1 1 2 104412.30 101090.48 587.57 o 3 1 2 1639.98 1994.11 14.89 o 5 1 2 14964.01 15289.13 95.90 o 7 1 2 53.89 51.09 4.66 o 9 1 2 3225.66 3198.51 45.66 o 11 1 2 91.93 92.30 14.52 o 13 1 2 852.76 882.68 45.51 o 15 1 2 52.15 40.82 21.97 o -18 2 2 45.73 29.80 21.26 o -16 2 2 404.83 426.11 21.97 o -14 2 2 2314.07 2369.94 42.70 o -12 2 2 1303.55 1288.04 23.26 o -10 2 2 3591.90 3546.32 28.86 o -8 2 2 9702.40 9760.89 66.09 o -6 2 2 4953.06 4842.47 31.34 o -4 2 2 4550.38 4649.74 30.56 o -2 2 2 6875.54 6858.33 46.10 o 0 2 2 14395.23 14302.04 91.74 o 2 2 2 12628.06 12506.56 78.09 o 4 2 2 4522.97 4574.49 32.05 o 6 2 2 2238.50 2227.36 20.37 o 8 2 2 1905.35 1916.50 28.09 o 10 2 2 1942.01 1967.39 33.93 o 12 2 2 915.32 898.77 26.22 o 14 2 2 101.39 83.87 21.72 o -17 3 2 25.82 10.60 20.00 o -15 3 2 609.74 652.57 25.36 o -13 3 2 749.45 731.66 21.73 o -11 3 2 3535.93 3625.96 43.11 o -9 3 2 3247.29 3338.56 33.32 o -7 3 2 3971.74 3689.98 27.18 o -5 3 2 11121.82 11834.71 74.72 o -3 3 2 14428.63 14780.90 92.44 o -1 3 2 3256.17 3328.90 23.66 o 1 3 2 8355.98 8257.79 55.82 o 3 3 2 894.48 880.66 11.76 o 5 3 2 5180.31 5101.89 38.34 o 7 3 2 4.68 21.59 6.48 o 9 3 2 949.21 934.84 23.59 o 11 3 2 0.24 0.00 14.00 o 13 3 2 625.70 643.96 29.14 o -16 4 2 4832.41 4714.21 82.31 o -14 4 2 1605.99 1707.05 37.65 o -12 4 2 1006.77 1012.49 24.19 o -10 4 2 2032.85 2157.42 25.95 o -8 4 2 34019.55 33902.70 199.26 o -6 4 2 20617.07 21012.39 130.79 o -4 4 2 2532.44 2446.75 18.38 o -2 4 2 56.42 109.00 7.17 o 0 4 2 77059.66 75740.70 501.03 o 2 4 2 52723.98 54265.20 343.89 o 4 4 2 1826.19 1778.87 19.04 o 6 4 2 315.18 329.44 12.16 o 8 4 2 15691.40 15669.27 170.37 o 10 4 2 6760.37 6722.47 107.99 o 12 4 2 22.61 6.15 16.77 o 14 4 2 23.78 21.06 22.58 o -15 5 2 479.15 509.70 36.98 o -13 5 2 1006.68 1001.15 26.41 o -11 5 2 5377.52 5306.51 73.56 o -9 5 2 1506.67 1522.95 24.84 o -7 5 2 9566.25 9595.17 75.31 o -5 5 2 3494.76 3539.17 29.02 o -3 5 2 12665.02 12150.92 75.83 o -1 5 2 79.50 69.38 5.08 o 1 5 2 5283.35 4663.06 40.06 o 3 5 2 3005.18 3197.51 28.99 o 5 5 2 10302.10 10324.42 92.74 o 7 5 2 20.16 29.19 11.05 o 9 5 2 3402.96 3454.15 50.31 o 11 5 2 170.99 170.94 18.59 o 13 5 2 1640.84 1665.96 48.73 o -16 6 2 74.97 60.22 22.58 o -14 6 2 2884.68 2849.54 59.53 o -12 6 2 1489.75 1466.83 34.72 o -10 6 2 171.35 195.96 14.32 o -8 6 2 1169.03 1197.12 24.92 o -6 6 2 2457.84 2574.03 41.08 o -4 6 2 13056.50 13339.93 87.87 o -2 6 2 6210.89 6202.42 46.66 o 0 6 2 618.54 616.76 12.67 o 2 6 2 1231.61 1245.15 31.39 o 4 6 2 2514.23 2447.01 31.00 o 6 6 2 6649.19 6740.54 80.72 o 8 6 2 1048.08 1021.95 27.39 o 10 6 2 76.97 74.11 19.02 o 12 6 2 322.27 389.88 28.98 o -15 7 2 221.19 188.74 23.50 o -13 7 2 22.92 28.85 19.09 o -11 7 2 239.84 244.98 18.46 o -9 7 2 0.66 0.00 11.47 o -7 7 2 3339.15 3191.47 49.51 o -5 7 2 85.54 91.72 8.85 o -3 7 2 5031.97 5000.40 45.09 o -1 7 2 37.04 29.28 9.57 o 1 7 2 984.60 953.89 19.60 o 3 7 2 987.67 987.32 24.65 o 5 7 2 3097.61 3067.50 46.12 o 7 7 2 159.06 154.79 16.17 o 9 7 2 2030.36 2034.30 62.11 o 11 7 2 138.56 107.96 23.57 o -12 8 2 6818.70 6752.26 108.26 o -10 8 2 2729.78 2665.51 68.13 o -8 8 2 847.05 842.62 23.38 o -6 8 2 1700.64 1787.35 30.80 o -4 8 2 25213.01 25400.24 262.52 o -2 8 2 6415.10 6280.68 77.63 o 0 8 2 2388.07 2251.54 35.14 o 2 8 2 187.97 154.58 14.35 o 4 8 2 7374.62 7481.13 90.55 o 6 8 2 6038.53 6161.95 87.87 o 8 8 2 94.82 96.66 21.10 o 10 8 2 3.68 15.25 22.40 o -11 9 2 379.96 368.17 26.62 o -9 9 2 1846.15 1893.02 41.94 o -7 9 2 2311.15 2385.97 41.64 o -5 9 2 166.22 207.04 34.87 o -3 9 2 1452.44 1506.11 62.18 o -1 9 2 413.19 477.88 18.74 o 1 9 2 3947.14 4124.28 66.91 o 3 9 2 178.50 147.03 18.65 o 5 9 2 2152.91 2184.50 135.46 o 7 9 2 302.30 294.18 38.62 o -8 10 2 2598.87 2615.46 57.41 o -6 10 2 913.17 859.79 79.12 o -4 10 2 8.57 0.00 19.38 o -2 10 2 608.09 571.99 23.87 o 0 10 2 2759.78 2680.93 47.24 o 2 10 2 2066.89 2062.26 56.33 o 4 10 2 383.95 355.07 32.58 o 6 10 2 1.06 13.35 22.12 o -5 11 2 3.06 0.00 40.68 o -3 11 2 29.09 24.60 22.83 o -1 11 2 370.02 405.94 25.90 o 1 11 2 261.68 288.31 24.11 o -19 1 3 121.38 129.52 20.24 o -17 1 3 139.79 119.51 19.56 o -15 1 3 1019.26 970.56 26.63 o -13 1 3 11849.52 11627.27 124.17 o -11 1 3 491.30 478.26 8.54 o -9 1 3 22.48 47.56 5.62 o -7 1 3 32731.03 33789.46 186.67 o -5 1 3 49883.80 47973.38 258.38 o -3 1 3 4703.69 4753.31 37.08 o -1 1 3 24738.61 25478.37 158.73 o 1 1 3 7520.89 7547.78 43.66 o 3 1 3 45950.26 46295.48 247.81 o 5 1 3 481.42 442.45 7.83 o 7 1 3 1134.60 1132.98 16.21 o 9 1 3 325.65 333.49 17.15 o 11 1 3 5091.64 4860.85 71.18 o 13 1 3 1666.09 1584.16 40.02 o -18 2 3 1677.74 1694.38 46.83 o -16 2 3 15.24 13.21 16.01 o -14 2 3 6450.12 6227.93 90.49 o -12 2 3 735.44 769.88 15.23 o -10 2 3 19180.02 19578.21 116.89 o -8 2 3 25820.04 27432.59 160.37 o -6 2 3 17985.21 17844.18 97.56 o -4 2 3 19164.71 19458.56 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489.80 15.27 o -7 3 12 150.45 155.26 8.66 o -5 3 12 793.56 837.04 16.69 o -3 3 12 141.21 149.89 11.29 o -16 4 12 3280.71 3451.49 40.88 o -14 4 12 6.11 0.00 8.61 o -12 4 12 12.48 13.12 7.66 o -10 4 12 3605.88 3660.24 53.62 o -8 4 12 6314.56 6321.41 68.84 o -6 4 12 91.31 86.45 9.52 o -4 4 12 238.18 248.63 12.43 o -15 5 12 1.16 8.73 10.18 o -13 5 12 2167.03 2179.47 30.13 o -11 5 12 652.43 581.80 18.09 o -9 5 12 575.47 590.78 18.37 o -7 5 12 317.77 325.70 15.46 o -12 6 12 1152.38 1162.63 22.92 o -10 6 12 179.80 183.19 13.96 o -17 1 13 113.83 106.53 11.75 o -15 1 13 2732.38 2789.13 45.75 o -13 1 13 1731.27 1751.13 63.51 o -11 1 13 16.99 15.45 11.20 o -9 1 13 78.39 64.21 8.11 o -7 1 13 1244.00 1338.75 22.68 o -5 1 13 1497.26 1505.53 24.39 o -16 2 13 187.43 206.99 9.08 o -14 2 13 1540.85 1525.77 24.68 o -12 2 13 185.16 235.36 20.78 o -10 2 13 2977.36 3064.34 87.98 o -8 2 13 264.11 287.39 14.25 o -6 2 13 2127.71 2194.46 23.84 o -15 3 13 140.70 123.73 9.26 o -13 3 13 306.74 310.54 13.17 o -11 3 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