#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:05:47 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181140 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/19/2221997.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2221997_Fobs loop_ _publ_author_name 'Gaye, Papa Aly' 'Barry, Aliou Hamady' 'Gaye, Mohamed' 'Sarr, Aminata Diasse' 'Sall, Abdou Salam' _publ_section_title ; 4,6-Dimethyl-2-thioxo-1,2-dihydropyrimidin-3-ium chloride--thiourea (1/1) ; _journal_coeditor_code ER2066 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1252 _journal_volume 65 _journal_year 2009 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6460 _cell_length_b 21.6140 _cell_length_c 8.3880 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.8316 _cod_data_source_file er2066Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CrystalBuilderInfo $orthorhombic $Cmcm $? $? $' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, -z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z-1/2' '-x, y, z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 18338.76 19070.68 390.84 o 6 0 0 3116.09 3305.54 108.55 o 1 1 0 3377.47 3203.21 37.37 o 3 1 0 659.32 803.47 18.69 o 5 1 0 29.54 13.12 10.90 o 7 1 0 0.01 13.12 17.80 o 2 2 0 5232.02 4774.12 58.73 o 4 2 0 2477.65 2681.80 48.94 o 6 2 0 696.80 971.86 32.25 o 1 3 0 7996.25 6812.39 85.64 o 3 3 0 779.44 672.90 12.23 o 5 3 0 25.69 -2.22 8.90 o 7 3 0 3.64 -4.45 15.57 o 0 4 0 0.90 4.45 4.45 o 2 4 0 13.26 15.79 4.45 o 4 4 0 15.75 8.90 4.45 o 6 4 0 8.08 4.45 17.80 o 1 5 0 4024.75 4347.47 56.06 o 3 5 0 527.04 639.09 14.24 o 5 5 0 116.01 104.77 8.68 o 7 5 0 25.40 20.02 17.80 o 0 6 0 1165.33 911.14 22.69 o 2 6 0 513.38 634.41 11.79 o 4 6 0 123.61 180.63 8.90 o 6 6 0 31.90 51.38 8.90 o 1 7 0 3115.60 3034.60 41.60 o 3 7 0 1552.41 1391.84 21.13 o 5 7 0 396.46 438.44 13.79 o 7 7 0 67.45 93.43 26.47 o 0 8 0 699.94 819.49 24.25 o 2 8 0 250.24 206.87 9.57 o 4 8 0 28.82 0.00 22.24 o 6 8 0 8.62 -2.22 8.90 o 1 9 0 1338.52 1281.51 23.58 o 3 9 0 421.09 510.29 14.90 o 5 9 0 89.81 104.77 8.68 o 7 9 0 12.51 37.59 18.02 o 0 10 0 97.09 75.41 11.57 o 2 10 0 7.22 8.90 4.45 o 4 10 0 4.94 8.90 6.67 o 6 10 0 5.65 0.00 22.24 o 1 11 0 1538.85 1961.30 37.59 o 3 11 0 735.47 558.34 15.57 o 5 11 0 156.66 108.55 10.90 o 7 11 0 23.14 28.92 19.80 o 0 12 0 10.76 -6.67 9.12 o 2 12 0 5.73 4.45 6.90 o 4 12 0 5.08 17.57 8.68 o 6 12 0 2.53 -6.67 9.12 o 1 13 0 395.97 462.46 16.24 o 3 13 0 256.59 178.18 11.34 o 5 13 0 79.35 62.06 11.12 o 0 14 0 150.87 62.06 13.35 o 2 14 0 55.08 48.72 8.45 o 4 14 0 4.22 24.47 8.90 o 6 14 0 0.01 -4.45 13.35 o 1 15 0 2332.39 2537.21 52.27 o 3 15 0 1046.20 1195.20 32.70 o 5 15 0 280.68 317.87 20.24 o 0 16 0 344.54 224.89 19.80 o 2 16 0 124.00 111.67 12.90 o 4 16 0 11.03 4.45 11.12 o 6 16 0 2.27 17.57 19.80 o 1 17 0 326.92 350.57 17.57 o 3 17 0 368.75 354.13 17.80 o 5 17 0 210.90 170.62 19.80 o 0 18 0 1.83 15.79 15.79 o 2 18 0 10.19 8.90 11.12 o 4 18 0 39.04 17.57 13.57 o 1 19 0 2016.07 2237.80 49.16 o 3 19 0 815.61 995.67 32.70 o 5 19 0 211.82 218.00 29.14 o 0 20 0 1056.56 1370.71 52.50 o 2 20 0 592.27 712.71 27.81 o 4 20 0 134.40 122.79 17.80 o 1 21 0 5.96 -2.22 15.79 o 3 21 0 40.04 40.04 17.80 o 0 22 0 2.82 42.26 24.47 o 2 22 0 17.87 2.22 15.79 o 4 22 0 29.57 2.22 24.69 o 1 23 0 20.18 4.45 22.47 o 3 23 0 48.79 30.92 24.25 o 0 24 0 164.72 189.75 42.93 o 2 24 0 80.43 106.77 29.14 o 1 25 0 304.29 364.81 37.82 o 1 1 1 1887.90 1728.53 16.67 o 3 1 1 563.94 670.62 9.40 o 5 1 1 127.23 129.23 4.48 o 7 1 1 31.65 44.46 17.68 o 0 2 1 2139.06 2032.93 25.58 o 2 2 1 1355.28 1423.69 15.10 o 4 2 1 320.97 365.26 8.17 o 6 2 1 55.76 57.31 10.04 o 1 3 1 261.47 215.90 4.88 o 3 3 1 36.35 32.01 3.06 o 5 3 1 1.49 -6.74 11.01 o 7 3 1 0.02 32.37 21.13 o 0 4 1 3.22 20.02 4.67 o 2 4 1 49.48 20.43 1.83 o 4 4 1 38.27 16.01 2.11 o 6 4 1 2.24 -0.58 5.75 o 1 5 1 3367.22 3189.37 31.89 o 3 5 1 1800.28 1905.33 20.37 o 5 5 1 583.88 669.83 13.46 o 7 5 1 111.55 97.44 13.48 o 0 6 1 3.74 2.22 4.45 o 2 6 1 67.24 29.67 4.34 o 4 6 1 102.63 74.56 4.64 o 6 6 1 38.22 44.27 6.89 o 1 7 1 9044.58 9054.25 82.50 o 3 7 1 2344.75 2471.14 26.50 o 5 7 1 414.62 425.34 13.68 o 7 7 1 57.68 55.01 12.66 o 0 8 1 13985.67 14159.76 190.86 o 2 8 1 7254.64 7173.80 64.85 o 4 8 1 1600.33 1511.93 31.25 o 6 8 1 277.61 242.87 11.14 o 1 9 1 445.69 429.67 8.90 o 3 9 1 0.92 13.52 8.79 o 5 9 1 14.43 14.81 5.34 o 7 9 1 2.37 2.22 11.27 o 0 10 1 1305.73 1241.24 23.36 o 2 10 1 1454.35 1493.92 18.01 o 4 10 1 1030.26 1177.44 24.25 o 6 10 1 348.09 414.11 12.85 o 1 11 1 1175.60 1169.09 18.24 o 3 11 1 178.06 178.21 8.02 o 5 11 1 6.28 3.18 5.34 o 7 11 1 0.03 16.34 18.80 o 0 12 1 9165.17 9540.68 129.02 o 2 12 1 5169.54 5599.19 57.20 o 4 12 1 1439.91 1566.51 27.92 o 6 12 1 325.96 314.09 14.00 o 1 13 1 1437.69 1525.08 20.84 o 3 13 1 415.58 341.38 10.85 o 5 13 1 68.18 41.08 7.71 o 0 14 1 17.15 26.92 11.34 o 2 14 1 92.05 120.98 7.70 o 4 14 1 141.39 175.21 9.19 o 6 14 1 54.11 37.74 10.09 o 1 15 1 43.69 46.66 6.05 o 3 15 1 110.59 141.56 8.66 o 5 15 1 68.82 78.53 15.68 o 0 16 1 87.86 84.53 11.34 o 2 16 1 21.80 25.70 6.29 o 4 16 1 0.01 -7.78 7.78 o 6 16 1 0.07 -14.31 15.45 o 1 17 1 511.46 501.84 14.74 o 3 17 1 174.62 114.49 9.59 o 5 17 1 40.97 21.06 11.72 o 0 18 1 395.54 434.66 19.58 o 2 18 1 222.82 195.52 11.25 o 4 18 1 52.30 51.03 22.13 o 1 19 1 4.11 -5.93 9.95 o 3 19 1 1.93 17.98 11.12 o 5 19 1 6.57 13.92 13.37 o 0 20 1 15.06 15.79 13.35 o 2 20 1 6.60 4.34 9.44 o 4 20 1 0.67 -10.00 10.93 o 1 21 1 65.32 55.73 19.02 o 3 21 1 39.58 23.36 11.17 o 0 22 1 117.43 99.88 22.69 o 2 22 1 87.72 119.81 17.31 o 4 22 1 38.83 84.49 25.58 o 1 23 1 134.28 141.64 25.36 o 3 23 1 70.92 90.09 19.85 o 0 24 1 31.80 46.71 24.47 o 2 24 1 34.77 26.52 18.54 o 1 25 1 10.87 29.85 20.30 o 0 0 2 22052.12 21157.00 411.52 o 2 0 2 11220.92 10815.29 166.83 o 4 0 2 2668.14 2676.91 43.82 o 6 0 2 547.49 536.32 15.35 o 1 1 2 8407.08 8314.37 102.86 o 3 1 2 1273.51 1497.53 20.13 o 5 1 2 155.28 174.34 20.02 o 7 1 2 22.43 20.99 11.88 o 0 2 2 1145.70 1162.72 19.35 o 2 2 2 1262.33 1281.88 20.20 o 4 2 2 860.69 990.29 31.03 o 6 2 2 295.26 339.03 10.45 o 1 3 2 1171.50 1065.92 11.80 o 3 3 2 972.80 1017.76 18.13 o 5 3 2 387.65 464.09 12.19 o 7 3 2 77.44 77.92 13.46 o 0 4 2 11568.67 11432.13 131.02 o 2 4 2 4618.60 4751.25 43.44 o 4 4 2 762.32 818.16 13.37 o 6 4 2 151.88 142.37 8.70 o 1 5 2 7617.83 7651.82 72.71 o 3 5 2 2562.40 2255.89 40.37 o 5 5 2 507.60 435.70 16.68 o 7 5 2 85.12 62.01 12.23 o 0 6 2 540.93 516.74 10.68 o 2 6 2 58.36 69.16 3.87 o 4 6 2 13.49 7.56 4.45 o 6 6 2 17.03 14.59 6.89 o 1 7 2 139.91 117.15 4.69 o 3 7 2 162.64 229.90 6.13 o 5 7 2 97.40 108.02 7.44 o 7 7 2 25.51 42.16 14.51 o 0 8 2 2.27 4.45 4.45 o 2 8 2 10.66 7.79 3.15 o 4 8 2 8.54 19.19 4.72 o 6 8 2 0.06 4.51 7.94 o 1 9 2 157.41 146.14 10.23 o 3 9 2 16.89 3.40 6.59 o 5 9 2 1.02 -1.20 5.56 o 7 9 2 0.20 -13.28 13.28 o 0 10 2 394.82 289.85 11.34 o 2 10 2 209.56 224.36 8.02 o 4 10 2 69.92 113.83 9.01 o 6 10 2 22.49 11.21 11.12 o 1 11 2 209.06 209.54 7.71 o 3 11 2 115.04 141.62 6.99 o 5 11 2 29.50 34.03 6.29 o 7 11 2 5.92 -1.00 26.69 o 0 12 2 296.40 396.18 15.13 o 2 12 2 279.17 242.37 9.28 o 4 12 2 145.99 94.38 14.13 o 6 12 2 39.16 14.32 9.52 o 1 13 2 10.10 10.93 5.67 o 3 13 2 34.80 27.45 6.56 o 5 13 2 31.64 21.00 7.40 o 0 14 2 1252.87 1301.75 30.70 o 2 14 2 778.55 873.54 18.65 o 4 14 2 246.62 277.58 11.59 o 6 14 2 59.44 45.15 12.83 o 1 15 2 1221.28 1206.68 20.84 o 3 15 2 446.81 511.78 29.81 o 5 15 2 107.88 134.61 12.46 o 0 16 2 4.93 2.22 8.90 o 2 16 2 1.26 -1.59 8.26 o 4 16 2 18.29 12.12 9.59 o 6 16 2 11.48 12.62 18.78 o 1 17 2 316.69 341.08 16.57 o 3 17 2 321.79 316.74 15.79 o 5 17 2 132.57 132.55 13.23 o 0 18 2 3.08 8.90 13.12 o 2 18 2 27.16 21.84 18.91 o 4 18 2 52.19 35.71 25.47 o 1 19 2 649.54 682.26 19.91 o 3 19 2 209.50 227.97 17.02 o 5 19 2 39.41 27.47 14.15 o 0 20 2 1038.45 1055.95 36.70 o 2 20 2 597.74 586.00 21.75 o 4 20 2 162.55 148.48 22.13 o 1 21 2 44.24 56.54 12.50 o 3 21 2 0.51 2.17 12.66 o 0 22 2 33.34 11.12 22.47 o 2 22 2 65.00 40.59 25.47 o 1 23 2 9.91 -19.13 19.13 o 3 23 2 1.07 29.30 23.91 o 0 24 2 320.73 312.76 41.82 o 2 24 2 176.35 179.88 29.92 o 1 25 2 248.57 239.97 29.25 o 1 1 3 6.81 5.19 2.22 o 3 1 3 34.48 46.71 3.15 o 5 1 3 33.91 43.26 4.80 o 7 1 3 14.36 6.69 10.93 o 0 2 3 2002.33 1785.79 27.81 o 2 2 3 1366.53 1320.15 18.02 o 4 2 3 389.81 401.76 7.65 o 6 2 3 68.10 66.80 7.86 o 1 3 3 9723.51 9828.53 131.02 o 3 3 3 2458.03 2524.71 31.72 o 5 3 3 428.28 406.09 28.58 o 7 3 3 63.15 69.85 17.80 o 0 4 3 768.32 779.67 15.79 o 2 4 3 543.94 655.39 26.47 o 4 4 3 282.48 339.22 9.83 o 6 4 3 93.97 91.05 9.20 o 1 5 3 644.54 609.61 9.91 o 3 5 3 585.00 451.07 10.55 o 5 5 3 212.48 205.87 14.90 o 7 5 3 31.43 53.48 16.79 o 0 6 3 1835.50 1870.54 28.47 o 2 6 3 625.31 587.26 10.41 o 4 6 3 39.44 16.02 5.22 o 6 6 3 0.84 6.86 9.52 o 1 7 3 309.58 203.57 6.68 o 3 7 3 102.39 79.99 10.01 o 5 7 3 14.20 -4.73 8.44 o 7 7 3 0.87 -2.80 19.78 o 0 8 3 3532.19 3097.33 42.04 o 2 8 3 1611.83 1721.58 27.36 o 4 8 3 368.15 439.82 11.81 o 6 8 3 98.83 84.67 12.23 o 1 9 3 44.66 36.92 4.56 o 3 9 3 120.72 165.75 6.73 o 5 9 3 81.43 81.33 8.10 o 7 9 3 15.60 6.31 15.29 o 0 10 3 1580.14 1785.79 31.81 o 2 10 3 1621.29 1678.14 23.09 o 4 10 3 971.61 1008.93 20.02 o 6 10 3 264.47 273.79 21.02 o 1 11 3 698.99 699.80 15.02 o 3 11 3 92.33 90.14 7.11 o 5 11 3 2.11 8.68 7.05 o 0 12 3 2949.75 3240.58 53.61 o 2 12 3 1676.21 1812.43 26.88 o 4 12 3 413.96 374.59 26.36 o 6 12 3 71.07 44.64 11.62 o 1 13 3 4871.47 5045.12 56.86 o 3 13 3 1785.80 1955.46 39.60 o 5 13 3 446.34 448.36 16.18 o 0 14 3 501.34 569.46 20.24 o 2 14 3 193.23 184.48 24.91 o 4 14 3 6.64 0.00 10.01 o 6 14 3 1.09 13.19 14.57 o 1 15 3 627.16 626.12 15.76 o 3 15 3 655.01 694.03 18.42 o 5 15 3 335.59 361.86 30.48 o 0 16 3 1844.64 1932.16 45.60 o 2 16 3 1122.63 1229.51 24.51 o 4 16 3 352.66 285.76 14.54 o 1 17 3 1011.34 1161.91 27.36 o 3 17 3 430.37 399.39 16.62 o 5 17 3 118.81 96.70 14.31 o 0 18 3 109.46 90.76 15.35 o 2 18 3 136.66 152.78 11.78 o 4 18 3 114.50 115.69 14.23 o 1 19 3 55.01 39.73 12.23 o 3 19 3 16.38 6.67 11.72 o 0 20 3 0.84 4.45 15.57 o 2 20 3 1.49 5.49 17.80 o 4 20 3 0.50 1.66 17.58 o 1 21 3 63.89 55.61 20.13 o 3 21 3 33.85 7.61 17.15 o 0 22 3 88.67 73.63 29.14 o 2 22 3 62.21 108.51 20.94 o 1 23 3 154.95 155.17 23.60 o 0 24 3 74.33 51.38 31.14 o 0 0 4 4905.70 4372.38 87.42 o 2 0 4 2481.77 2652.66 58.28 o 4 0 4 590.67 668.00 14.68 o 6 0 4 122.10 127.02 8.45 o 1 1 4 1685.94 1516.77 19.29 o 3 1 4 377.03 308.45 14.01 o 5 1 4 61.57 36.78 9.90 o 7 1 4 13.66 26.60 17.22 o 0 2 4 10.50 6.67 4.45 o 2 2 4 134.51 103.18 6.78 o 4 2 4 243.42 285.68 9.14 o 6 2 4 93.79 89.33 10.84 o 1 3 4 864.77 857.15 12.64 o 3 3 4 917.91 871.42 16.68 o 5 3 4 442.79 462.58 12.98 o 7 3 4 110.36 138.79 35.92 o 0 4 4 4499.21 4806.82 65.40 o 2 4 4 2252.28 2260.48 49.38 o 4 4 4 481.34 425.66 11.65 o 6 4 4 99.13 62.26 8.01 o 1 5 4 12043.04 12652.55 116.13 o 3 5 4 4332.22 4790.46 60.01 o 5 5 4 971.26 973.31 20.76 o 7 5 4 172.79 148.38 21.45 o 0 6 4 126.93 101.88 6.67 o 2 6 4 15.38 6.52 10.12 o 4 6 4 15.53 21.93 5.34 o 6 6 4 24.31 6.39 5.45 o 1 7 4 53.52 30.50 3.78 o 3 7 4 122.92 157.80 6.87 o 5 7 4 79.42 82.97 8.64 o 7 7 4 20.95 0.95 23.67 o 0 8 4 412.14 394.17 13.12 o 2 8 4 201.99 205.34 7.09 o 4 8 4 43.83 23.91 7.56 o 6 8 4 13.07 -1.14 9.52 o 1 9 4 31.70 27.55 3.78 o 3 9 4 19.00 30.92 4.88 o 5 9 4 3.64 -0.44 7.40 o 0 10 4 306.02 336.56 10.45 o 2 10 4 220.86 287.33 8.42 o 4 10 4 86.26 122.13 24.36 o 6 10 4 21.66 14.52 13.33 o 1 11 4 855.11 966.20 33.70 o 3 11 4 407.25 498.25 10.49 o 5 11 4 125.30 125.52 16.91 o 0 12 4 14.51 30.92 8.90 o 2 12 4 26.65 17.57 4.72 o 4 12 4 33.87 18.66 6.79 o 6 12 4 18.51 21.80 12.93 o 1 13 4 124.86 148.02 8.10 o 3 13 4 133.03 107.06 7.90 o 5 13 4 75.66 41.91 13.35 o 0 14 4 2383.36 2392.18 50.72 o 2 14 4 1575.50 1687.71 28.63 o 4 14 4 572.50 623.14 19.75 o 1 15 4 390.96 399.34 27.25 o 3 15 4 136.06 184.54 10.84 o 5 15 4 28.66 28.47 14.57 o 0 16 4 265.75 302.97 18.02 o 2 16 4 285.55 279.73 12.27 o 4 16 4 197.31 149.19 17.57 o 1 17 4 10.32 32.82 24.47 o 3 17 4 32.79 25.71 9.43 o 5 17 4 14.90 31.97 16.37 o 0 18 4 128.43 137.92 17.80 o 2 18 4 163.02 159.22 15.97 o 4 18 4 124.63 87.75 15.89 o 1 19 4 125.69 102.10 13.46 o 3 19 4 18.52 20.62 13.95 o 0 20 4 1111.46 1162.72 51.38 o 2 20 4 681.50 679.34 30.06 o 4 20 4 211.22 158.87 20.01 o 1 21 4 27.58 24.87 17.74 o 3 21 4 0.04 20.44 18.26 o 0 22 4 1.26 15.79 24.69 o 2 22 4 13.88 22.07 19.73 o 1 23 4 36.36 2.81 38.82 o 1 1 5 85.77 101.43 19.13 o 3 1 5 46.17 61.59 7.79 o 5 1 5 20.62 16.57 5.29 o 0 2 5 1467.43 1427.21 24.91 o 2 2 5 736.75 871.97 16.59 o 4 2 5 163.63 213.06 32.03 o 6 2 5 28.08 26.73 6.37 o 1 3 5 511.87 541.36 8.89 o 3 3 5 220.50 225.33 9.42 o 5 3 5 49.40 26.92 4.14 o 0 4 5 0.07 -4.45 4.45 o 2 4 5 24.01 12.61 5.56 o 4 4 5 51.97 50.93 6.89 o 6 4 5 16.70 12.15 7.90 o 1 5 5 138.99 154.54 8.79 o 3 5 5 204.25 189.89 16.91 o 5 5 5 108.39 94.03 7.45 o 0 6 5 0.52 -2.22 4.45 o 2 6 5 18.66 16.02 5.22 o 4 6 5 42.50 43.12 8.49 o 6 6 5 15.69 6.23 15.65 o 1 7 5 1866.35 1735.61 23.47 o 3 7 5 543.43 582.38 16.91 o 5 7 5 95.71 92.29 20.24 o 0 8 5 1466.36 1427.21 32.03 o 2 8 5 845.53 853.87 17.91 o 4 8 5 223.19 215.63 8.96 o 6 8 5 47.89 47.46 13.39 o 1 9 5 0.36 -4.72 4.72 o 3 9 5 64.16 58.54 8.90 o 5 9 5 44.70 53.07 7.87 o 0 10 5 110.73 115.67 11.12 o 2 10 5 219.92 204.41 12.12 o 4 10 5 253.43 235.56 12.13 o 6 10 5 96.51 92.75 17.42 o 1 11 5 65.90 74.53 6.29 o 3 11 5 0.13 -3.47 7.00 o 5 11 5 8.36 14.89 9.43 o 0 12 5 3152.29 3299.98 54.28 o 2 12 5 1815.14 1963.43 29.57 o 4 12 5 489.84 475.11 15.77 o 1 13 5 2121.89 2424.44 32.87 o 3 13 5 835.01 884.92 21.02 o 5 13 5 199.91 137.91 16.24 o 0 14 5 14.31 6.67 9.12 o 2 14 5 1.90 -0.27 7.00 o 4 14 5 30.45 14.21 8.97 o 1 15 5 8.74 1.48 6.95 o 3 15 5 58.73 73.53 9.09 o 5 15 5 57.82 23.33 16.97 o 0 16 5 442.95 460.46 20.24 o 2 16 5 247.68 226.45 13.50 o 4 16 5 68.16 40.15 13.24 o 1 17 5 456.36 439.17 15.99 o 3 17 5 181.84 156.83 12.58 o 0 18 5 8.01 22.24 13.35 o 2 18 5 0.37 -4.34 13.24 o 4 18 5 4.00 9.98 14.15 o 1 19 5 9.25 -0.39 13.30 o 3 19 5 14.90 19.38 11.44 o 0 20 5 18.66 17.57 22.24 o 2 20 5 11.49 0.00 12.74 o 1 21 5 3.15 1.27 16.62 o 0 22 5 123.18 68.96 22.02 o 0 0 6 11983.31 12169.76 228.90 o 2 0 6 7361.11 11502.87 273.16 o 4 0 6 2355.87 2471.14 51.61 o 6 0 6 573.61 732.96 51.16 o 1 1 6 796.93 792.71 21.24 o 3 1 6 168.13 168.27 12.23 o 5 1 6 11.22 -0.12 14.46 o 0 2 6 205.42 230.68 12.90 o 2 2 6 370.15 354.73 40.93 o 4 2 6 394.72 445.16 33.81 o 6 2 6 157.60 282.20 25.64 o 1 3 6 176.40 166.11 6.01 o 3 3 6 5.32 13.30 15.57 o 5 3 6 1.87 14.97 8.39 o 0 4 6 598.58 497.61 12.68 o 2 4 6 295.12 323.15 11.34 o 4 4 6 57.27 55.51 9.43 o 6 4 6 12.83 -0.32 21.52 o 1 5 6 1359.26 1432.66 22.65 o 3 5 6 453.11 458.43 13.52 o 5 5 6 99.19 72.33 8.77 o 0 6 6 13.09 24.47 8.90 o 2 6 6 0.03 1.59 8.26 o 4 6 6 11.60 13.16 9.43 o 6 6 6 9.01 26.92 24.47 o 1 7 6 243.12 185.44 8.52 o 3 7 6 240.87 215.53 13.12 o 5 7 6 108.84 107.51 18.24 o 0 8 6 98.62 142.37 11.34 o 2 8 6 47.31 41.20 7.94 o 4 8 6 11.24 2.22 8.70 o 1 9 6 5.87 -1.71 6.39 o 3 9 6 7.27 21.02 7.86 o 5 9 6 3.04 11.87 12.23 o 0 10 6 13.00 11.12 8.90 o 2 10 6 19.18 22.02 11.01 o 4 10 6 18.64 31.11 11.09 o 1 11 6 13.85 6.78 9.01 o 3 11 6 9.12 8.72 8.64 o 5 11 6 2.47 11.12 13.90 o 0 12 6 2.08 -8.90 8.90 o 2 12 6 3.65 -1.47 10.11 o 4 12 6 4.29 4.99 11.81 o 1 13 6 56.45 68.83 7.70 o 3 13 6 54.45 40.47 5.83 o 5 13 6 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