#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222009.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222009_Fobs loop_ _publ_author_name 'Chang, Chin-Pei' 'Hong, Fung-E' _publ_section_title ; Bis[1,3(\h^3^)-allyl][\m-2(\h^4^)-1,3-bis(diphenylphosphino)-2,4-diphenylcyclobuta-1,3-diene-1:3\k^2^P:P']dichlorido-1\kCl,3\kCl-[2(\h^5^)-isopropylcyclopentadienyl]-2-cobalt(I)-1,3-dipalladium(II) dichloromethane solvate ; _journal_coeditor_code GK2195 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m669 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.617 _cell_angle_beta 102.136 _cell_angle_gamma 115.166 _cell_length_a 10.8890 _cell_length_b 12.4990 _cell_length_c 21.7460 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.8087 _[local]_cod_data_source_file gk2195Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in space group P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 389.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 53524.77 57715.54 511.06 o 2 0 0 4569.00 4366.06 62.64 o 3 0 0 1788.80 1566.39 54.17 o 4 0 0 14391.53 15868.86 506.88 o 5 0 0 17002.74 17347.33 197.92 o 6 0 0 2.56 -0.83 31.55 o 7 0 0 160.35 126.67 42.57 o 8 0 0 10.78 -16.55 38.32 o 9 0 0 85.54 45.17 66.08 o 10 0 0 220.11 175.65 81.13 o 11 0 0 468.83 392.29 107.90 o -12 1 0 20.26 82.81 78.62 o -11 1 0 185.24 173.98 90.33 o -10 1 0 1942.71 1866.08 158.92 o -9 1 0 1685.06 1548.29 88.69 o -8 1 0 250.73 220.88 54.37 o -7 1 0 297.42 329.13 52.60 o -6 1 0 1757.19 1745.04 75.92 o -5 1 0 6278.77 6756.56 121.56 o -4 1 0 631.17 739.78 76.95 o -3 1 0 3234.13 3795.73 108.74 o -2 1 0 2660.81 2587.92 69.42 o -1 1 0 31455.71 34778.88 300.28 o 1 1 0 562.63 507.71 22.58 o 2 1 0 2128.61 2373.06 110.83 o 3 1 0 6130.30 6626.83 203.67 o 4 1 0 216.83 250.47 35.56 o 5 1 0 3062.33 3231.80 248.00 o 6 1 0 944.24 888.30 62.30 o 7 1 0 71.64 46.00 36.67 o 8 1 0 428.77 304.46 81.97 o 9 1 0 821.29 890.80 127.97 o 10 1 0 439.72 374.72 104.55 o 11 1 0 53.80 39.31 81.13 o -12 2 0 223.34 72.77 83.64 o -11 2 0 1815.77 1577.51 145.54 o -10 2 0 598.80 596.61 74.44 o -9 2 0 487.78 583.16 69.18 o -8 2 0 84.53 86.10 40.76 o -7 2 0 981.53 918.02 66.83 o -6 2 0 723.20 803.79 59.33 o -5 2 0 15752.93 15651.33 258.46 o -4 2 0 29430.88 29396.43 345.45 o -3 2 0 670.58 545.35 57.71 o -2 2 0 17469.75 19613.51 221.65 o -1 2 0 16994.78 19314.91 194.05 o 1 2 0 51912.46 55122.59 448.33 o 2 2 0 12.98 25.08 17.47 o 3 2 0 1707.07 2005.70 54.93 o 4 2 0 6815.55 7086.99 148.47 o 5 2 0 3071.52 3146.61 87.20 o 6 2 0 518.07 534.48 94.52 o 7 2 0 1178.77 1175.19 120.45 o 8 2 0 38.29 61.06 73.61 o 9 2 0 405.01 536.99 115.43 o 10 2 0 147.75 66.91 99.54 o -12 3 0 31.22 -34.29 53.53 o -11 3 0 29.19 -18.17 42.04 o -10 3 0 2340.50 2228.64 107.93 o -9 3 0 1434.53 1479.66 92.26 o -8 3 0 44.58 18.25 36.04 o -7 3 0 2212.38 2204.00 132.16 o -6 3 0 62.41 110.41 56.04 o -5 3 0 4538.62 5083.84 152.23 o -4 3 0 1392.73 1455.39 88.66 o -3 3 0 1592.14 1283.92 76.95 o -2 3 0 54.54 65.43 32.62 o -1 3 0 207.16 270.75 55.62 o 0 3 0 894.13 891.54 72.35 o 1 3 0 1936.44 1665.34 81.13 o 2 3 0 460.58 475.22 43.08 o 3 3 0 3169.68 3483.40 64.01 o 4 3 0 1610.94 1714.63 59.70 o 5 3 0 85.45 186.52 71.93 o 6 3 0 1151.97 1125.84 120.45 o 7 3 0 46.23 119.61 75.28 o 8 3 0 1.78 -0.84 72.77 o 9 3 0 274.81 323.70 110.41 o 10 3 0 125.70 138.01 97.03 o -12 4 0 435.54 418.82 71.97 o -11 4 0 1733.75 1653.76 99.95 o -10 4 0 999.50 1108.10 87.91 o -9 4 0 2233.97 2002.85 98.41 o -8 4 0 687.32 700.93 97.86 o -7 4 0 423.04 299.44 71.10 o -6 4 0 131.18 159.76 58.55 o -5 4 0 3678.16 3100.66 126.30 o -4 4 0 21484.30 22333.59 301.12 o -3 4 0 9807.37 8777.93 261.39 o -2 4 0 575.16 721.73 36.47 o -1 4 0 340.97 393.12 28.95 o 0 4 0 8714.71 8881.10 100.19 o 1 4 0 19270.55 19068.16 270.17 o 2 4 0 646.55 519.42 64.41 o 3 4 0 914.15 922.59 85.32 o 4 4 0 61.73 23.42 49.35 o 5 4 0 82.62 153.07 66.08 o 6 4 0 12.28 45.17 66.08 o 7 4 0 1094.97 1117.47 124.63 o 8 4 0 2503.71 2180.58 179.00 o 9 4 0 365.34 418.22 122.12 o -13 5 0 102.50 87.22 54.02 o -12 5 0 0.47 -7.79 47.74 o -11 5 0 201.84 227.65 57.83 o -10 5 0 560.88 564.89 69.18 o -9 5 0 428.36 418.22 92.01 o -8 5 0 1018.14 1053.07 112.08 o -7 5 0 1365.81 1053.91 104.55 o -6 5 0 601.43 659.11 83.64 o -5 5 0 6.40 -8.36 42.66 o -4 5 0 123.37 310.89 46.13 o -3 5 0 1677.85 1642.07 48.74 o -2 5 0 136.60 120.90 24.21 o -1 5 0 0.09 41.65 30.12 o 0 5 0 14.35 5.26 21.55 o 1 5 0 487.05 511.06 65.24 o 2 5 0 1100.87 1153.44 96.19 o 3 5 0 4.01 30.95 45.17 o 4 5 0 694.23 706.79 100.37 o 5 5 0 70.29 110.41 66.08 o 6 5 0 1503.44 1451.21 131.32 o 7 5 0 265.77 300.28 96.19 o 8 5 0 94.74 30.95 73.61 o 9 5 0 28.99 -74.44 76.95 o -13 6 0 0.29 -43.56 43.56 o -12 6 0 69.80 -37.91 49.64 o -11 6 0 95.09 134.16 53.19 o -10 6 0 35.73 16.73 61.90 o -9 6 0 274.82 179.83 73.61 o -8 6 0 944.54 891.64 107.06 o -7 6 0 635.03 476.77 83.64 o -6 6 0 317.29 312.83 68.59 o -5 6 0 3839.07 3756.42 147.21 o -4 6 0 8972.83 8554.60 108.37 o -3 6 0 12761.37 12545.34 163.95 o -2 6 0 838.19 883.62 40.49 o -1 6 0 113.53 120.69 23.31 o 0 6 0 112.79 97.55 19.49 o 1 6 0 4353.29 4007.35 150.56 o 2 6 0 584.12 746.93 92.01 o 3 6 0 3720.54 3421.01 163.10 o 4 6 0 2306.82 2265.06 145.54 o 5 6 0 428.51 479.28 101.21 o 6 6 0 3.70 -15.06 64.41 o 7 6 0 1442.96 1467.10 157.25 o 8 6 0 1376.55 1290.62 155.58 o -13 7 0 198.31 142.52 64.39 o -12 7 0 0.06 4.82 43.34 o -11 7 0 451.52 461.15 71.55 o -10 7 0 56.54 55.20 74.44 o -9 7 0 203.19 121.28 72.77 o -8 7 0 1.33 -20.91 61.06 o -7 7 0 2604.04 2377.98 140.52 o -6 7 0 5454.04 5180.03 184.85 o -5 7 0 1019.88 964.65 69.55 o -4 7 0 0.35 -8.96 23.02 o -3 7 0 2463.44 2513.40 66.26 o -2 7 0 5039.45 5461.04 89.31 o -1 7 0 2069.98 2143.68 71.79 o 0 7 0 296.50 295.79 60.99 o 1 7 0 1257.71 1201.40 83.23 o 2 7 0 2098.53 2124.54 136.34 o 3 7 0 72.33 66.08 59.39 o 4 7 0 231.54 163.10 77.79 o 5 7 0 39.01 -17.57 60.22 o 6 7 0 538.72 714.31 125.46 o 7 7 0 184.04 196.56 102.04 o -13 8 0 35.60 72.35 54.41 o -12 8 0 188.73 222.78 60.57 o -11 8 0 79.59 82.81 74.44 o -10 8 0 81.14 47.68 75.28 o -9 8 0 48.07 44.33 61.06 o -8 8 0 5095.93 4725.85 207.44 o -7 8 0 5945.35 5144.06 199.07 o -6 8 0 558.67 515.24 86.99 o -5 8 0 158.68 157.88 39.38 o -4 8 0 8409.06 8352.30 120.40 o -3 8 0 12281.64 12371.02 278.02 o -2 8 0 759.73 833.32 46.62 o -1 8 0 2693.80 2848.82 67.14 o 0 8 0 151.07 112.60 43.21 o 1 8 0 4311.63 3888.48 249.26 o 2 8 0 181.64 148.89 72.77 o 3 8 0 1596.59 1460.41 127.97 o 4 8 0 1466.48 1317.38 132.16 o 5 8 0 5.84 45.17 73.61 o 6 8 0 54.32 -0.84 83.64 o -12 9 0 162.17 123.79 93.68 o -11 9 0 434.37 409.02 98.70 o -10 9 0 1635.25 1539.04 145.54 o -9 9 0 199.08 180.67 76.95 o -8 9 0 472.14 431.60 90.33 o -7 9 0 1170.54 1134.20 119.61 o -6 9 0 1940.79 1921.85 97.84 o -5 9 0 20.16 -32.77 32.77 o -4 9 0 321.93 463.56 47.23 o -3 9 0 1525.28 1468.55 70.53 o -2 9 0 2643.10 2658.66 175.94 o -1 9 0 380.56 533.22 67.69 o 0 9 0 127.85 92.36 70.26 o 1 9 0 1.53 -34.15 38.74 o 2 9 0 537.74 689.57 104.55 o 3 9 0 46.36 14.22 60.22 o 4 9 0 360.55 260.13 92.01 o 5 9 0 54.82 97.03 81.97 o -12 10 0 139.09 159.76 80.30 o -11 10 0 27.29 73.61 67.75 o -10 10 0 151.32 1.67 61.90 o -9 10 0 66.22 102.04 73.61 o -8 10 0 2958.26 2990.25 177.32 o -7 10 0 1318.21 1510.60 133.83 o -6 10 0 378.28 379.66 65.03 o -5 10 0 1472.36 1485.62 66.95 o -4 10 0 2299.77 2460.40 78.99 o -3 10 0 4233.51 4514.94 100.37 o -2 10 0 406.99 576.13 104.14 o -1 10 0 346.14 437.78 65.05 o 0 10 0 865.20 1095.99 92.62 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116.26 o -10 13 0 745.82 801.30 142.19 o -9 13 0 368.15 379.74 109.57 o -8 13 0 339.61 318.68 97.03 o -7 13 0 928.62 974.11 89.82 o -6 13 0 1563.55 1616.82 148.89 o -5 13 0 521.88 548.70 120.45 o -4 13 0 110.10 66.08 81.97 o -3 13 0 10.63 87.83 84.48 o -2 13 0 384.49 141.36 84.48 o -1 13 0 201.93 35.97 79.46 o 0 13 0 22.64 -69.42 69.42 o 1 13 0 164.91 135.50 110.41 o -10 14 0 34.49 62.73 87.83 o -9 14 0 4.44 -61.90 61.90 o -8 14 0 25.22 -52.70 52.70 o -7 14 0 324.61 276.86 109.57 o -6 14 0 198.82 79.46 92.84 o -5 14 0 0.13 -63.57 63.57 o -4 14 0 387.08 480.95 120.45 o -3 14 0 53.99 31.78 81.97 o -2 14 0 187.62 235.87 102.04 o -1 14 0 174.30 122.12 93.68 o -8 15 0 202.35 164.78 118.77 o -7 15 0 269.27 167.29 111.25 o -6 15 0 673.24 888.29 148.89 o -5 15 0 1016.97 1025.47 155.58 o -4 15 0 36.51 -48.51 85.32 o 4 -15 1 530.45 554.55 125.46 o 5 -15 1 117.88 156.41 103.72 o 6 -15 1 146.51 200.74 107.06 o 7 -15 1 47.73 97.03 114.59 o 8 -15 1 345.58 385.60 132.99 o 1 -14 1 23.49 -63.57 74.44 o 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689.56 928.44 132.99 o 10 -12 1 1013.87 1036.34 143.03 o 11 -12 1 93.99 20.91 66.91 o -4 -11 1 63.40 41.90 55.24 o -3 -11 1 5.50 -3.07 56.30 o -2 -11 1 51.81 63.60 58.12 o -1 -11 1 255.97 312.19 68.86 o 0 -11 1 808.70 862.98 104.55 o 1 -11 1 71.77 64.56 52.01 o 2 -11 1 429.01 520.28 71.45 o 3 -11 1 120.66 175.69 53.78 o 4 -11 1 536.78 621.18 55.86 o 5 -11 1 193.82 172.88 42.74 o 6 -11 1 609.18 671.42 59.99 o 7 -11 1 2029.28 2138.76 148.89 o 8 -11 1 261.49 398.98 96.19 o 9 -11 1 81.24 68.59 71.93 o 10 -11 1 55.25 -15.89 70.26 o 11 -11 1 275.74 198.23 86.15 o 12 -11 1 14.33 -24.26 58.55 o -5 -10 1 179.81 203.25 91.17 o -4 -10 1 42.47 56.96 60.22 o -3 -10 1 96.74 93.45 54.37 o -2 -10 1 447.09 366.19 73.15 o -1 -10 1 466.61 364.67 68.49 o 0 -10 1 114.88 74.29 49.97 o 1 -10 1 422.12 531.68 72.63 o 2 -10 1 22.76 -26.24 76.12 o 3 -10 1 8.93 21.99 43.91 o 4 -10 1 174.61 174.45 39.22 o 5 -10 1 1596.91 1493.78 75.09 o 6 -10 1 2818.59 2757.43 114.28 o 7 -10 1 936.41 867.38 107.90 o 8 -10 1 577.28 490.99 102.04 o 9 -10 1 3263.80 3431.05 194.89 o 10 -10 1 4875.18 3811.62 206.60 o 11 -10 1 135.95 193.22 92.01 o 12 -10 1 20.18 -2.51 67.75 o -6 -9 1 248.23 190.71 102.88 o -5 -9 1 345.58 214.13 100.37 o -4 -9 1 1052.66 1237.08 139.68 o -3 -9 1 316.31 350.47 86.15 o -2 -9 1 277.81 269.41 60.91 o -1 -9 1 331.83 357.30 64.11 o 0 -9 1 1339.66 1296.18 90.40 o 1 -9 1 1508.32 1594.45 90.94 o 2 -9 1 841.80 796.70 48.91 o 3 -9 1 2263.43 2373.75 73.70 o 4 -9 1 265.96 256.92 40.83 o 5 -9 1 245.34 373.88 48.69 o 6 -9 1 1546.06 1612.52 89.10 o 7 -9 1 2919.81 2714.22 155.58 o 8 -9 1 217.49 154.74 70.26 o 9 -9 1 842.99 751.12 112.08 o 10 -9 1 168.78 10.04 57.71 o 11 -9 1 573.52 669.98 123.79 o 12 -9 1 205.72 151.39 97.03 o -7 -8 1 0.03 -75.28 88.66 o -6 -8 1 159.80 65.24 82.81 o -5 -8 1 1454.94 1554.93 148.05 o -4 -8 1 9.51 -33.46 53.53 o -3 -8 1 933.22 1013.76 125.46 o -2 -8 1 204.98 324.54 81.97 o -1 -8 1 1714.20 1800.64 112.92 o 0 -8 1 9.06 -0.99 53.11 o 1 -8 1 3650.10 3596.89 74.77 o 2 -8 1 5044.96 5240.71 122.12 o 3 -8 1 85.20 108.01 32.50 o 4 -8 1 1949.65 1908.69 67.68 o 5 -8 1 15957.07 16215.08 190.64 o 6 -8 1 8580.61 7995.46 234.20 o 7 -8 1 2256.71 2244.15 143.03 o 8 -8 1 591.87 670.82 104.55 o 9 -8 1 3362.04 3232.81 176.49 o 11 -8 1 983.60 849.82 127.14 o 12 -8 1 0.23 25.84 48.57 o -7 -7 1 291.65 317.01 110.41 o -6 -7 1 191.26 176.49 93.68 o -5 -7 1 2055.06 1768.22 143.03 o -4 -7 1 5438.88 5673.52 229.18 o -3 -7 1 2543.23 2276.77 142.19 o -2 -7 1 146.56 187.36 68.59 o -1 -7 1 2194.40 2235.76 94.28 o 0 -7 1 14096.31 13858.18 123.52 o 1 -7 1 3643.26 3414.35 76.68 o 2 -7 1 2670.71 2585.67 65.99 o 3 -7 1 7935.18 8499.82 141.56 o 4 -7 1 2660.56 2823.83 72.80 o 5 -7 1 3240.99 3407.49 107.05 o 6 -7 1 675.33 770.35 100.37 o 7 -7 1 3167.55 2925.84 153.90 o 8 -7 1 509.77 256.78 78.62 o 9 -7 1 55.88 102.04 79.46 o 10 -7 1 24.72 33.46 61.90 o 11 -7 1 303.05 143.87 79.46 o 12 -7 1 43.86 -7.88 44.86 o 13 -7 1 4.37 -19.87 47.90 o -8 -6 1 46.19 -24.26 74.44 o -7 -6 1 23.19 -45.17 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