#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/20/2222012.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222012_Fobs loop_ _publ_author_name 'Becker, Eva' 'Kirchner, Karl' 'Mereiter, Kurt' _publ_section_title ; (\h^5^-Cyclopentadienyl)(\h^6^-mesitylamine)ruthenium(II) hexafluoridophosphate ; _journal_coeditor_code GK2208 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m631 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.5119 _cell_length_b 10.2047 _cell_length_c 21.1818 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.7104 _[local]_cod_data_source_file gk2208Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Ru(Cp)(eta6-C6H2(CH3)3NH2)]PF6 at 173K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 357.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3711.13 4046.88 49.19 o 4 0 0 15571.92 16434.48 194.20 o 6 0 0 840.95 792.28 15.49 o 8 0 0 1067.11 1161.66 32.15 o 10 0 0 10.61 8.21 7.23 o 1 1 0 17833.96 19407.96 169.09 o 2 1 0 473.88 490.83 5.88 o 3 1 0 6796.02 6583.00 56.16 o 4 1 0 2675.17 2829.13 26.42 o 5 1 0 768.31 756.53 9.91 o 7 1 0 1262.96 1388.98 21.18 o 8 1 0 14.80 17.34 4.74 o 9 1 0 441.48 434.82 13.70 o 10 1 0 6.11 23.32 5.70 o 0 2 0 111889.81 107111.43 6783.59 o 1 2 0 7122.37 7476.53 62.37 o 2 2 0 0.23 -0.70 1.28 o 4 2 0 24153.81 25193.89 220.70 o 5 2 0 526.72 592.29 8.87 o 6 2 0 488.84 456.28 11.12 o 7 2 0 109.26 111.71 8.00 o 8 2 0 1936.98 2031.51 33.28 o 9 2 0 3.45 23.31 5.79 o 10 2 0 4.14 5.47 4.72 o 1 3 0 13960.36 14052.06 116.25 o 2 3 0 396.75 329.48 4.72 o 3 3 0 6849.36 6735.33 57.96 o 4 3 0 2401.42 2516.80 24.22 o 5 3 0 59.64 46.12 2.83 o 6 3 0 81.07 96.08 4.26 o 7 3 0 1037.61 1087.35 18.07 o 8 3 0 179.56 196.88 12.54 o 9 3 0 596.94 593.72 18.80 o 10 3 0 125.75 169.60 9.79 o 0 4 0 4689.58 4251.26 52.10 o 1 4 0 1369.83 1230.77 12.19 o 2 4 0 132.82 127.69 3.17 o 3 4 0 784.94 867.35 10.13 o 4 4 0 10203.09 10160.96 87.04 o 5 4 0 821.45 888.46 11.48 o 6 4 0 0.71 5.69 2.59 o 7 4 0 8.18 16.07 3.70 o 8 4 0 1975.17 1936.45 32.08 o 9 4 0 157.50 182.99 14.97 o 10 4 0 13.59 30.86 7.15 o 1 5 0 1644.31 1526.97 15.20 o 2 5 0 2076.42 1954.46 19.12 o 3 5 0 5183.09 4991.02 44.53 o 4 5 0 107.54 103.45 3.99 o 5 5 0 361.72 327.77 7.27 o 6 5 0 1098.39 1053.43 16.29 o 7 5 0 2547.23 2490.37 31.27 o 8 5 0 438.00 425.11 14.48 o 9 5 0 53.30 45.11 11.88 o 0 6 0 5743.23 5734.44 71.16 o 1 6 0 1753.25 1675.63 16.92 o 2 6 0 92.82 88.38 3.23 o 3 6 0 8.59 19.22 2.54 o 4 6 0 1325.14 1350.72 15.55 o 5 6 0 863.87 857.84 12.30 o 6 6 0 0.73 3.35 3.51 o 7 6 0 40.94 63.40 5.79 o 8 6 0 540.32 529.21 18.74 o 9 6 0 193.40 208.81 14.79 o 1 7 0 711.69 739.27 9.96 o 2 7 0 9247.74 9385.34 81.13 o 3 7 0 5506.44 5615.84 50.78 o 4 7 0 545.90 541.54 9.52 o 5 7 0 4.21 21.77 4.17 o 6 7 0 1002.06 918.51 19.66 o 7 7 0 398.11 371.33 12.55 o 8 7 0 1.83 2.05 4.73 o 9 7 0 48.17 43.19 8.63 o 0 8 0 276.52 256.06 7.40 o 1 8 0 2425.23 2580.09 25.63 o 2 8 0 0.29 4.87 2.56 o 4 8 0 507.76 489.90 10.63 o 5 8 0 1107.38 1100.05 18.63 o 6 8 0 26.18 34.67 5.49 o 7 8 0 155.59 160.57 9.08 o 8 8 0 200.97 207.50 11.30 o 1 9 0 233.93 270.02 7.51 o 2 9 0 9432.08 9754.41 100.66 o 3 9 0 555.83 541.37 11.28 o 4 9 0 769.39 723.40 26.33 o 5 9 0 66.96 74.01 10.44 o 6 9 0 599.64 568.53 15.33 o 7 9 0 26.23 42.56 7.14 o 8 9 0 9.81 11.96 5.36 o 0 10 0 66.34 61.25 9.46 o 1 10 0 1353.30 1427.51 28.03 o 2 10 0 581.53 558.99 13.51 o 3 10 0 340.46 376.27 12.42 o 4 10 0 16.78 28.50 4.35 o 5 10 0 710.47 691.16 18.27 o 6 10 0 0.16 3.71 4.44 o 7 10 0 200.34 170.74 9.60 o 1 11 0 2.24 8.70 5.43 o 2 11 0 3377.72 3491.19 55.22 o 3 11 0 60.51 65.00 7.43 o 4 11 0 261.55 217.18 11.76 o 5 11 0 161.50 154.35 10.89 o 6 11 0 1252.54 1167.21 29.31 o 0 12 0 0.01 5.43 7.18 o 1 12 0 1363.02 1365.04 29.01 o 2 12 0 0.87 -0.35 4.59 o 3 12 0 288.28 319.15 18.37 o 4 12 0 1.41 0.85 7.04 o 5 12 0 491.95 455.80 22.92 o 1 13 0 0.74 2.75 5.37 o 2 13 0 1520.11 1596.21 48.15 o 3 13 0 9.19 7.29 5.46 o 4 13 0 30.57 28.65 14.41 o 0 14 0 106.02 128.81 14.68 o 1 14 0 792.94 856.02 23.19 o 2 14 0 38.09 51.29 7.99 o 1 0 1 260.32 251.28 3.36 o 2 0 1 542.27 454.75 5.17 o 3 0 1 2637.68 2531.56 23.02 o 4 0 1 1808.31 1786.17 17.78 o 5 0 1 2374.63 2315.66 23.04 o 6 0 1 829.44 814.86 11.76 o 7 0 1 1403.35 1373.88 21.12 o 8 0 1 7.45 9.24 5.24 o 9 0 1 874.03 971.81 21.12 o 10 0 1 443.15 445.08 14.38 o -10 1 1 582.09 612.62 16.93 o -9 1 1 237.76 240.95 10.52 o -8 1 1 52.36 82.98 7.05 o -7 1 1 268.09 299.21 8.83 o -6 1 1 5494.81 5526.35 53.14 o -5 1 1 3004.93 2986.23 28.52 o -4 1 1 35.72 35.79 2.29 o -3 1 1 3422.58 3266.25 29.09 o -2 1 1 9609.12 10234.53 85.20 o -1 1 1 33900.31 35370.79 1059.30 o 0 1 1 1986.86 2095.67 36.98 o 1 1 1 33832.50 37377.23 815.06 o 2 1 1 10062.32 10941.67 91.16 o 3 1 1 3445.48 3317.40 29.60 o 4 1 1 32.63 39.77 2.44 o 5 1 1 3015.81 3038.90 28.96 o 6 1 1 5553.79 5686.63 51.55 o 7 1 1 259.55 297.47 8.79 o 8 1 1 50.91 82.82 6.89 o 9 1 1 243.55 266.55 13.75 o 10 1 1 578.22 606.31 16.88 o -10 2 1 501.35 520.10 15.54 o -9 2 1 694.14 722.57 18.30 o -8 2 1 265.55 292.19 10.91 o -7 2 1 1270.82 1309.01 20.54 o -6 2 1 349.53 350.15 9.03 o -5 2 1 2682.13 2702.26 27.84 o -4 2 1 2010.15 1952.10 20.54 o -3 2 1 4846.57 4941.96 49.58 o -2 2 1 8383.29 8616.49 72.34 o -1 2 1 540.15 564.19 5.55 o 0 2 1 249.84 253.20 3.82 o 1 2 1 469.34 477.48 6.52 o 2 2 1 8001.07 8202.50 68.81 o 3 2 1 4792.21 4904.69 38.28 o 4 2 1 2025.24 1964.62 18.57 o 5 2 1 2678.47 2703.51 26.37 o 6 2 1 323.76 326.94 7.00 o 7 2 1 1289.56 1299.47 22.48 o 8 2 1 269.70 288.61 10.91 o 9 2 1 694.77 693.50 17.39 o 10 2 1 493.63 522.20 16.37 o -10 3 1 660.06 679.47 17.91 o -9 3 1 472.40 470.80 18.31 o -8 3 1 206.34 259.44 13.28 o -7 3 1 568.89 590.57 11.94 o -6 3 1 2105.28 2162.42 29.17 o -5 3 1 2013.21 1986.32 22.58 o -4 3 1 579.94 653.72 8.85 o -3 3 1 4947.67 4961.96 43.61 o -2 3 1 6320.49 6471.51 55.22 o -1 3 1 5698.59 5626.36 47.77 o 0 3 1 420.74 367.23 4.37 o 1 3 1 5642.68 5519.78 55.78 o 2 3 1 6410.04 6564.31 55.80 o 3 3 1 4934.50 4921.97 43.14 o 4 3 1 570.83 651.27 8.68 o 5 3 1 2011.00 1940.72 21.27 o 6 3 1 2219.55 2284.01 27.76 o 7 3 1 581.10 617.77 12.75 o 8 3 1 208.87 262.72 10.53 o 9 3 1 490.29 479.87 14.35 o 10 3 1 671.26 682.41 17.82 o -10 4 1 483.03 461.54 17.80 o -9 4 1 522.54 503.07 21.74 o -8 4 1 559.67 587.32 13.35 o -7 4 1 808.14 795.31 14.35 o -6 4 1 680.01 621.62 10.33 o -5 4 1 581.77 595.89 9.00 o -4 4 1 2754.19 2739.78 26.50 o -3 4 1 2761.71 2804.38 26.31 o -2 4 1 3977.48 3838.76 34.04 o -1 4 1 5183.31 5399.39 46.42 o 0 4 1 3614.91 3774.93 32.99 o 1 4 1 5234.34 5437.04 46.65 o 2 4 1 3950.23 3761.44 33.44 o 3 4 1 2793.49 2801.32 26.13 o 4 4 1 2772.08 2701.26 25.98 o 5 4 1 606.05 615.97 10.16 o 6 4 1 632.90 582.99 13.85 o 7 4 1 802.77 786.46 22.74 o 8 4 1 554.82 564.85 15.02 o 9 4 1 501.14 494.08 14.40 o 10 4 1 459.26 469.16 16.98 o -9 5 1 187.72 189.93 14.49 o -8 5 1 426.24 422.02 12.72 o -7 5 1 495.88 518.74 16.66 o -6 5 1 2402.65 2447.00 27.16 o -5 5 1 2302.49 2354.72 24.30 o -4 5 1 569.55 594.10 8.60 o -3 5 1 2867.54 2959.11 27.88 o -2 5 1 4634.23 4637.38 41.00 o -1 5 1 2954.80 2968.31 27.10 o 0 5 1 1267.71 1161.48 12.03 o 1 5 1 2925.00 2908.11 27.03 o 2 5 1 4593.93 4517.11 40.07 o 3 5 1 2867.77 2900.40 27.41 o 4 5 1 532.07 551.22 8.19 o 5 5 1 2353.25 2336.64 42.30 o 6 5 1 2451.87 2368.59 60.64 o 7 5 1 508.13 528.68 14.79 o 8 5 1 443.48 454.55 18.81 o 9 5 1 196.78 182.42 11.23 o -9 6 1 218.23 236.94 15.12 o -8 6 1 549.33 542.95 16.82 o -7 6 1 797.59 768.74 15.95 o -6 6 1 939.11 891.57 16.63 o -5 6 1 459.78 452.42 9.45 o -4 6 1 2595.83 2572.81 25.77 o -3 6 1 2552.57 2539.85 24.89 o -2 6 1 2754.68 2784.48 26.35 o -1 6 1 3102.34 3089.78 28.69 o 0 6 1 4048.89 4351.71 38.91 o 1 6 1 3102.83 3104.84 28.73 o 2 6 1 2762.13 2800.29 28.94 o 3 6 1 2569.24 2557.61 25.08 o 4 6 1 2534.86 2524.17 25.35 o 5 6 1 425.35 430.52 8.19 o 6 6 1 923.78 849.47 14.42 o 7 6 1 799.22 763.08 15.83 o 8 6 1 546.48 574.47 17.56 o 9 6 1 217.67 238.59 14.98 o -9 7 1 83.89 86.66 20.51 o -8 7 1 245.17 240.85 11.73 o -7 7 1 770.46 744.04 18.76 o -6 7 1 1344.43 1330.18 24.96 o -5 7 1 3016.23 2982.89 40.44 o -4 7 1 358.36 388.51 8.93 o -3 7 1 397.87 417.48 7.93 o -2 7 1 3584.43 3548.44 31.08 o -1 7 1 2710.01 2728.53 26.33 o 0 7 1 2816.50 2941.87 28.01 o 1 7 1 2699.64 2709.10 26.13 o 2 7 1 3650.31 3635.84 37.04 o 3 7 1 420.07 430.45 7.41 o 4 7 1 369.37 406.03 7.45 o 5 7 1 3063.98 2999.48 34.67 o 6 7 1 1359.81 1360.51 21.97 o 7 7 1 766.67 717.03 17.49 o 8 7 1 247.35 257.66 11.91 o 9 7 1 81.99 79.71 10.27 o -8 8 1 635.75 583.43 17.71 o -7 8 1 338.48 310.82 13.57 o -6 8 1 229.12 191.57 9.42 o -5 8 1 279.60 284.23 8.96 o -4 8 1 1911.73 1822.69 34.22 o -3 8 1 4080.43 4108.43 59.42 o -2 8 1 1518.17 1579.60 19.06 o -1 8 1 2824.94 2840.54 27.85 o 0 8 1 175.78 204.98 4.73 o 1 8 1 2737.55 2763.69 27.12 o 2 8 1 1528.18 1553.12 26.67 o 3 8 1 4084.38 4081.84 46.03 o 4 8 1 1873.50 1877.82 25.06 o 5 8 1 283.37 273.37 10.87 o 6 8 1 234.34 209.89 9.62 o 7 8 1 332.63 303.59 11.57 o 8 8 1 640.80 609.77 33.49 o -8 9 1 224.71 215.71 10.88 o -7 9 1 560.08 549.41 15.65 o -6 9 1 287.05 274.76 10.85 o -5 9 1 981.67 936.82 21.30 o -4 9 1 1049.32 1039.94 22.65 o -3 9 1 446.39 465.01 10.97 o -2 9 1 1306.54 1363.99 19.81 o -1 9 1 1656.41 1653.41 25.39 o 0 9 1 1003.35 1034.49 15.88 o 1 9 1 1669.96 1668.35 22.55 o 2 9 1 1308.76 1323.39 19.59 o 3 9 1 439.39 457.27 11.10 o 4 9 1 1047.08 1052.36 18.17 o 5 9 1 983.38 913.85 20.45 o 6 9 1 291.44 282.37 11.01 o 7 9 1 558.91 519.57 15.24 o 8 9 1 229.17 214.87 11.14 o -7 10 1 177.14 183.97 9.92 o -6 10 1 81.37 90.30 7.48 o -5 10 1 220.06 210.95 12.31 o -4 10 1 940.14 894.75 18.17 o -3 10 1 1838.40 1796.65 28.37 o -2 10 1 419.59 470.53 14.82 o -1 10 1 1471.24 1533.39 29.59 o 0 10 1 158.60 197.19 9.93 o 1 10 1 1464.51 1514.87 29.24 o 2 10 1 429.94 448.52 12.14 o 3 10 1 1858.67 1859.15 25.72 o 4 10 1 960.34 942.45 17.28 o 5 10 1 228.57 216.80 11.35 o 6 10 1 85.46 94.41 10.81 o 7 10 1 177.38 165.96 9.56 o -6 11 1 64.96 69.25 8.91 o -5 11 1 445.85 367.52 20.02 o -4 11 1 422.87 401.49 15.34 o -3 11 1 526.47 524.46 18.76 o -2 11 1 112.00 126.75 9.12 o -1 11 1 746.82 758.07 19.74 o 0 11 1 1818.08 1810.57 44.01 o 1 11 1 743.40 725.09 19.20 o 2 11 1 111.89 127.73 9.18 o 3 11 1 519.74 532.28 31.37 o 4 11 1 403.31 391.70 18.88 o 5 11 1 444.69 419.11 19.34 o 6 11 1 62.07 59.77 8.59 o -5 12 1 379.80 374.27 21.14 o -4 12 1 362.52 367.81 15.30 o -3 12 1 421.91 438.05 15.44 o -2 12 1 21.43 39.67 6.70 o -1 12 1 562.94 588.60 23.52 o 0 12 1 756.30 796.77 35.29 o 1 12 1 569.34 621.03 18.43 o 2 12 1 21.91 29.43 6.56 o 3 12 1 426.41 468.13 23.20 o 4 12 1 367.13 343.03 35.47 o 5 12 1 386.90 388.20 59.65 o -4 13 1 345.36 310.96 55.61 o -3 13 1 214.83 238.36 14.74 o -2 13 1 15.39 40.62 7.20 o -1 13 1 205.35 213.07 11.90 o 0 13 1 894.31 889.73 23.10 o 1 13 1 207.55 221.63 12.10 o 2 13 1 15.22 40.52 12.63 o 3 13 1 214.12 237.07 14.04 o 4 13 1 347.24 314.26 20.16 o -2 14 1 14.11 33.51 7.05 o -1 14 1 290.46 336.90 19.16 o 0 14 1 228.90 274.04 13.46 o 1 14 1 293.65 358.13 15.15 o 2 14 1 13.17 23.28 6.49 o 1 0 2 2307.40 2284.08 22.63 o 2 0 2 0.15 -0.93 0.93 o 3 0 2 5641.70 5738.55 49.21 o 4 0 2 406.98 328.39 5.51 o 5 0 2 11554.51 11822.70 100.68 o 6 0 2 199.59 207.65 5.72 o 7 0 2 4887.35 5116.34 59.61 o 8 0 2 3.23 1.66 4.02 o 9 0 2 226.09 252.69 10.79 o 10 0 2 1.46 14.27 5.44 o -10 1 2 249.24 320.85 12.39 o -9 1 2 16.45 19.41 5.09 o -8 1 2 3340.14 3434.08 49.62 o -7 1 2 98.93 120.58 6.13 o -6 1 2 104.97 111.63 4.70 o -5 1 2 29.49 48.92 2.70 o -4 1 2 18958.94 19790.29 164.54 o -3 1 2 56.43 77.78 2.33 o -2 1 2 4119.62 4220.36 38.41 o -1 1 2 1816.04 1773.18 19.71 o 0 1 2 17821.58 17777.13 196.77 o 1 1 2 1829.52 1811.35 17.07 o 2 1 2 4129.23 4329.98 40.24 o 3 1 2 53.60 82.85 2.67 o 4 1 2 19119.27 19988.79 166.44 o 5 1 2 27.92 44.60 2.73 o 6 1 2 107.15 121.08 7.71 o 7 1 2 97.44 116.77 6.09 o 8 1 2 3328.56 3322.50 48.41 o 9 1 2 15.21 18.59 5.06 o 10 1 2 249.52 293.53 12.03 o -9 2 2 425.21 462.36 14.13 o -8 2 2 10.15 14.13 4.16 o -7 2 2 3205.54 3378.97 39.39 o -6 2 2 205.04 213.03 6.60 o -5 2 2 5412.28 5479.98 51.98 o -4 2 2 2683.34 2978.29 32.31 o -3 2 2 9614.54 10054.88 97.44 o -2 2 2 1554.98 1492.57 15.45 o -1 2 2 7421.44 7476.65 62.63 o 0 2 2 1905.74 2018.42 23.52 o 1 2 2 7293.59 7331.99 71.26 o 2 2 2 1580.92 1537.19 14.42 o 3 2 2 9679.73 10208.87 77.12 o 4 2 2 2672.31 2935.00 26.08 o 5 2 2 5411.55 5467.57 49.06 o 6 2 2 212.81 226.94 5.67 o 7 2 2 3199.60 3341.61 41.52 o 8 2 2 9.70 16.97 4.72 o 9 2 2 424.60 461.62 14.06 o 10 2 2 27.04 54.98 6.85 o -10 3 2 92.59 124.00 10.34 o -9 3 2 142.57 163.73 9.13 o -8 3 2 2977.89 2953.91 38.85 o -7 3 2 434.27 495.95 12.28 o -6 3 2 14.79 22.93 3.21 o -5 3 2 484.58 461.62 9.88 o -4 3 2 14660.76 15465.64 140.29 o -3 3 2 2485.15 2353.20 22.35 o -2 3 2 1007.31 1050.71 10.85 o -1 3 2 144.30 148.90 2.71 o 0 3 2 5778.15 5969.74 50.57 o 1 3 2 135.40 139.58 3.89 o 2 3 2 1006.43 1027.21 10.61 o 3 3 2 2487.49 2327.59 21.80 o 4 3 2 14808.96 15612.39 130.98 o 5 3 2 501.52 469.40 7.24 o 6 3 2 13.13 20.31 2.72 o 7 3 2 444.97 489.95 9.94 o 8 3 2 2980.56 2927.76 43.87 o 9 3 2 140.06 166.97 9.19 o 10 3 2 92.50 138.16 9.11 o -10 4 2 183.14 205.87 16.91 o -9 4 2 328.02 316.16 20.72 o -8 4 2 470.06 460.30 12.58 o -7 4 2 2887.23 2961.66 35.64 o -6 4 2 703.07 737.59 11.57 o -5 4 2 2434.97 2461.01 25.00 o -4 4 2 103.26 105.47 3.59 o -3 4 2 4695.26 4943.43 43.79 o -2 4 2 3928.83 4177.47 36.83 o -1 4 2 5645.59 5515.56 47.49 o 0 4 2 981.75 954.02 9.81 o 1 4 2 5631.07 5388.90 49.93 o 2 4 2 3936.40 4190.64 37.07 o 3 4 2 4738.96 5001.97 44.16 o 4 4 2 102.47 94.92 3.37 o 5 4 2 2406.40 2404.66 25.59 o 6 4 2 698.88 692.54 14.73 o 7 4 2 2866.04 2898.98 37.22 o 8 4 2 466.74 453.39 13.26 o 9 4 2 321.67 333.72 12.05 o 10 4 2 183.10 189.72 10.09 o -9 5 2 432.42 406.27 19.52 o -8 5 2 1470.36 1401.50 25.36 o -7 5 2 437.71 481.65 12.40 o -6 5 2 35.87 40.46 3.57 o -5 5 2 1006.78 995.61 12.86 o -4 5 2 3049.18 3039.12 29.31 o -3 5 2 2343.72 2198.03 21.64 o -2 5 2 77.10 96.24 2.71 o -1 5 2 1533.89 1477.95 17.45 o 0 5 2 9451.46 9715.20 82.11 o 1 5 2 1507.73 1466.93 14.59 o 2 5 2 75.12 98.09 3.90 o 3 5 2 2382.23 2214.04 21.82 o 4 5 2 3044.20 3055.93 29.27 o 5 5 2 1011.48 979.91 23.15 o 6 5 2 33.19 35.63 3.87 o 7 5 2 446.31 474.87 11.36 o 8 5 2 1479.53 1444.22 26.19 o 9 5 2 431.94 409.31 15.39 o -9 6 2 125.67 129.15 12.49 o -8 6 2 19.80 19.35 5.86 o -7 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