#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/20/2222016.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222016_Fobs loop_ _publ_author_name 'Thomas, Lynne H.' 'Boyle, Bryan' 'Clive, Lesley A.' 'Collins, Anna' 'Currie, Lynsey D.' 'Gogol, Malgorzata' 'Hastings, Claire' 'Jones, Andrew O. F.' 'Kennedy, Jennifer L.' 'Kerr, Graham B.' 'Kidd, Alastair' 'Lawton, Lorreta M.' 'Macintyre, Susan J.' 'MacLean, Niall M.' 'Martin, Alan R. G.' 'McGonagle, Kate' 'Melrose, Samantha' 'Rew, Gaius A.' 'Robinson, Colin W.' 'Schmidtmann, Marc' 'Turnbull, Felicity B.' 'Williams, Lewis G.' 'Wiseman, Alan Y.' 'Wocial, Malgorzata H.' 'Wilson, Chick C.' _publ_section_title ; 2-Acetylpyridinium bromanilate ; _journal_coeditor_code HB2948 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1218 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.396 _cell_angle_gamma 90.000 _cell_length_a 9.1323 _cell_length_b 13.3821 _cell_length_c 12.2287 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file hb2948Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BA_2AP in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 298.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 37545.05 38861.35 727.98 o 3 0 0 9576.16 10058.52 154.15 o 4 0 0 10495.14 10974.88 125.49 o 5 0 0 9.39 45.93 24.70 o 6 0 0 13.61 14.90 8.57 o 7 0 0 20.57 1.16 19.47 o 8 0 0 938.43 1005.53 85.94 o 9 0 0 541.76 605.93 66.92 o 10 0 0 182.50 211.57 46.67 o 2 1 0 5321.31 5632.64 69.19 o 3 1 0 1462.02 1318.31 20.80 o 4 1 0 28.03 35.75 6.43 o 5 1 0 516.52 558.04 9.16 o 6 1 0 50.19 49.77 5.92 o 7 1 0 1574.78 1524.67 52.54 o 8 1 0 4577.21 4802.40 126.17 o 9 1 0 2729.28 2999.45 94.22 o 10 1 0 2041.74 2168.16 82.58 o 0 2 0 516.09 523.52 11.36 o 1 2 0 86.89 100.26 4.45 o 2 2 0 5874.31 5791.44 42.46 o 3 2 0 3547.09 3679.12 28.62 o 4 2 0 7443.31 7986.97 85.37 o 5 2 0 10198.28 10012.37 86.76 o 6 2 0 4052.34 4101.11 45.23 o 7 2 0 5019.25 4922.11 69.97 o 8 2 0 4639.42 4535.11 193.14 o 9 2 0 4672.57 4979.17 148.64 o 10 2 0 64.94 64.64 28.21 o 1 3 0 1700.73 1629.09 17.96 o 2 3 0 9960.76 9838.24 86.71 o 3 3 0 10131.50 10131.26 88.03 o 4 3 0 18727.78 19634.34 231.31 o 5 3 0 1999.13 1991.97 24.53 o 6 3 0 2529.45 2535.77 38.83 o 7 3 0 154.19 143.00 12.39 o 8 3 0 889.68 852.82 31.03 o 9 3 0 1314.37 1240.42 38.65 o 10 3 0 1547.55 1684.28 86.50 o 0 4 0 115.54 115.59 45.96 o 1 4 0 5337.36 5167.66 56.39 o 2 4 0 387.40 364.18 7.60 o 3 4 0 0.94 7.29 4.26 o 4 4 0 1791.90 1914.20 21.95 o 5 4 0 924.80 898.34 15.63 o 6 4 0 1627.49 1695.13 14.71 o 7 4 0 669.25 684.31 27.50 o 8 4 0 336.77 318.26 15.42 o 9 4 0 371.38 335.87 20.71 o 10 4 0 17.65 -2.32 23.61 o 1 5 0 9854.20 10074.22 124.31 o 2 5 0 851.66 787.74 10.96 o 3 5 0 90.81 69.94 6.11 o 4 5 0 1771.76 1722.96 18.01 o 5 5 0 2374.41 2405.74 25.61 o 6 5 0 242.64 253.24 12.49 o 7 5 0 179.59 175.63 12.55 o 8 5 0 128.85 118.37 11.21 o 9 5 0 111.32 89.00 11.99 o 10 5 0 37.51 47.21 44.70 o 0 6 0 668.42 655.12 32.08 o 1 6 0 295.73 271.81 10.85 o 2 6 0 41.19 54.83 5.93 o 3 6 0 5704.11 5858.67 62.63 o 4 6 0 5056.36 4915.73 65.68 o 5 6 0 4439.44 4196.38 43.05 o 6 6 0 8760.59 8696.68 98.48 o 7 6 0 12260.29 12428.60 162.71 o 8 6 0 4897.58 5166.66 86.33 o 9 6 0 1190.67 1245.81 73.49 o 10 6 0 273.00 181.55 40.58 o 1 7 0 435.79 419.32 12.47 o 2 7 0 4665.04 4643.77 49.59 o 3 7 0 3884.12 3737.09 43.55 o 4 7 0 1992.14 1978.69 25.54 o 5 7 0 4169.83 4011.80 46.86 o 6 7 0 3148.96 3043.35 36.93 o 7 7 0 554.61 546.94 18.04 o 8 7 0 438.41 432.02 19.83 o 9 7 0 21.06 23.64 14.70 o 10 7 0 8.48 23.44 27.88 o 0 8 0 21073.63 20348.23 475.13 o 1 8 0 13675.25 13573.84 203.62 o 2 8 0 20944.21 20721.13 302.60 o 3 8 0 2507.10 2423.55 33.25 o 4 8 0 3316.19 3317.84 45.50 o 5 8 0 1503.64 1437.81 22.71 o 6 8 0 1372.70 1437.10 26.46 o 7 8 0 26.06 40.10 11.68 o 8 8 0 387.41 362.00 33.34 o 9 8 0 616.15 740.04 43.49 o 1 9 0 3743.38 3733.28 66.37 o 2 9 0 4033.01 3835.22 49.48 o 3 9 0 6639.47 6600.02 90.38 o 4 9 0 1224.92 1189.65 29.45 o 5 9 0 897.84 914.07 25.43 o 6 9 0 54.33 37.46 10.15 o 7 9 0 386.58 413.44 15.99 o 8 9 0 1701.71 1848.50 62.12 o 9 9 0 2767.59 2904.01 98.32 o 0 10 0 5674.28 5527.40 129.72 o 1 10 0 9420.75 9130.72 151.85 o 2 10 0 9539.97 9353.58 127.32 o 3 10 0 5039.16 4917.24 70.62 o 4 10 0 1624.37 1590.32 29.65 o 5 10 0 297.66 316.17 16.72 o 6 10 0 8.17 -0.22 10.94 o 7 10 0 77.44 78.97 14.01 o 8 10 0 28.03 4.53 21.65 o 1 11 0 477.71 459.57 21.54 o 2 11 0 1830.69 1861.03 44.02 o 3 11 0 1947.13 1899.94 44.66 o 4 11 0 634.48 649.06 27.31 o 5 11 0 452.87 425.04 18.35 o 6 11 0 1054.15 1072.08 34.51 o 7 11 0 84.45 94.88 17.75 o 8 11 0 51.22 69.15 23.16 o 0 12 0 233.09 231.59 31.14 o 1 12 0 5808.36 5588.63 102.36 o 2 12 0 49.90 66.37 12.99 o 3 12 0 171.47 155.35 16.89 o 4 12 0 566.80 567.58 29.93 o 5 12 0 1861.11 1856.60 39.59 o 6 12 0 3470.08 3465.67 68.32 o 7 12 0 3120.67 3236.84 78.99 o 1 13 0 1069.73 1031.38 42.42 o 2 13 0 239.84 229.94 17.97 o 3 13 0 575.19 572.50 24.39 o 4 13 0 585.77 586.33 30.00 o 5 13 0 18.82 29.16 14.29 o 6 13 0 137.53 129.08 21.36 o 7 13 0 161.57 167.79 20.20 o 0 14 0 153.04 176.76 43.35 o 1 14 0 642.18 649.65 31.70 o 2 14 0 699.20 672.09 35.36 o 3 14 0 690.90 642.30 40.06 o 4 14 0 461.79 458.67 28.22 o 5 14 0 1162.18 1151.06 38.02 o 6 14 0 921.42 876.83 40.06 o 1 15 0 477.48 476.88 26.79 o 2 15 0 1721.61 1697.32 56.61 o 3 15 0 2468.68 2421.46 59.21 o 4 15 0 943.55 907.55 38.01 o 5 15 0 1934.94 1933.84 58.03 o 0 16 0 325.97 286.89 94.24 o 1 16 0 511.47 522.44 39.34 o 2 16 0 630.12 647.30 32.19 o 3 16 0 624.15 622.86 38.81 o 4 16 0 1284.57 1231.55 53.96 o 1 17 0 33.03 22.56 21.69 o 2 17 0 124.05 122.31 25.37 o -11 1 1 1249.50 1285.69 77.70 o -10 1 1 118.68 109.39 28.75 o -9 1 1 54.50 63.27 36.43 o -8 1 1 11.56 22.88 9.23 o -7 1 1 238.76 239.94 9.17 o -6 1 1 3499.56 3464.88 34.57 o -5 1 1 12270.04 12733.22 126.40 o -4 1 1 11977.66 12014.36 115.06 o -3 1 1 31444.27 32642.31 425.11 o -2 1 1 9922.42 10174.67 89.92 o 1 1 1 2293.34 2158.28 26.24 o 2 1 1 15.82 21.76 3.10 o 3 1 1 5455.86 5716.25 54.27 o 4 1 1 4611.89 4587.46 41.07 o 5 1 1 192.10 157.64 10.01 o 6 1 1 12.99 19.11 3.38 o 7 1 1 14.21 20.71 18.70 o 8 1 1 309.31 325.24 29.54 o 9 1 1 3725.38 4027.04 145.83 o 10 1 1 801.97 892.11 74.43 o -11 2 1 73.72 64.33 38.84 o -10 2 1 2.69 8.80 27.55 o -9 2 1 1764.22 1822.69 69.64 o -8 2 1 2187.21 2230.25 36.88 o -7 2 1 2851.86 2880.51 36.74 o -6 2 1 3086.06 2891.36 25.72 o -5 2 1 2960.96 2686.04 25.80 o -4 2 1 253.27 233.07 5.05 o -3 2 1 8112.52 8737.43 82.75 o -2 2 1 2731.77 2877.70 20.71 o -1 2 1 2795.31 2772.28 18.19 o 0 2 1 54.50 67.33 3.47 o 1 2 1 3770.00 3837.91 44.92 o 2 2 1 78.39 90.15 4.33 o 3 2 1 8.64 17.80 4.72 o 4 2 1 6595.77 6667.81 67.07 o 5 2 1 8720.58 8934.64 101.37 o 6 2 1 7787.25 7592.50 112.28 o 7 2 1 4095.67 4091.49 45.65 o 8 2 1 2017.63 2201.50 128.10 o 9 2 1 1128.07 1339.47 58.75 o 10 2 1 2100.24 2284.69 85.46 o -11 3 1 623.13 867.32 102.45 o -10 3 1 909.26 1039.25 53.80 o -9 3 1 868.15 877.92 45.34 o -8 3 1 1201.47 1195.96 28.63 o -7 3 1 3245.67 3213.06 60.00 o -6 3 1 6396.67 6337.89 61.88 o -5 3 1 2674.11 2547.87 28.95 o -4 3 1 3287.88 2971.48 30.03 o -3 3 1 12563.11 12814.14 124.12 o -2 3 1 6185.47 6235.07 50.03 o -1 3 1 495.09 446.37 6.74 o 0 3 1 7750.07 7662.57 73.66 o 1 3 1 13705.63 14065.39 160.23 o 2 3 1 4914.67 4977.99 42.79 o 3 3 1 8743.02 9102.68 74.93 o 4 3 1 4771.40 4907.11 42.30 o 5 3 1 1989.32 2029.72 29.84 o 6 3 1 1809.59 1840.11 47.08 o 7 3 1 567.72 559.88 31.89 o 8 3 1 45.54 34.54 12.29 o 9 3 1 188.89 213.62 38.68 o 10 3 1 182.48 147.95 34.62 o -10 4 1 543.56 548.34 49.18 o -9 4 1 86.79 91.21 22.12 o -8 4 1 901.97 948.99 30.47 o -7 4 1 2330.04 2435.79 48.97 o -6 4 1 5466.49 5491.76 55.77 o -5 4 1 13.13 23.27 8.14 o -4 4 1 384.72 409.65 9.85 o -3 4 1 5223.69 5241.61 45.72 o -2 4 1 5841.67 5743.78 47.28 o -1 4 1 11289.65 11374.86 128.01 o 0 4 1 9621.39 9321.11 106.90 o 1 4 1 28035.28 29355.29 493.81 o 2 4 1 12713.56 12798.91 140.12 o 3 4 1 6585.86 6506.09 69.04 o 4 4 1 947.88 955.25 16.80 o 5 4 1 672.72 787.59 18.78 o 6 4 1 1.28 9.36 9.23 o 7 4 1 13.08 14.55 10.34 o 8 4 1 0.92 0.64 6.03 o 9 4 1 452.93 485.89 38.63 o 10 4 1 736.87 673.62 72.08 o -10 5 1 2942.77 3149.15 139.39 o -9 5 1 3245.00 3382.45 55.58 o -8 5 1 6233.44 5912.90 125.34 o -7 5 1 2053.06 2050.58 31.76 o -6 5 1 2157.22 2170.08 27.60 o -5 5 1 328.61 314.99 11.00 o -4 5 1 88.79 97.40 9.96 o -3 5 1 8.57 9.54 4.87 o -2 5 1 1539.77 1452.68 17.35 o -1 5 1 3148.12 3098.90 33.91 o 0 5 1 1301.86 1205.33 16.29 o 1 5 1 15875.69 15877.89 218.72 o 2 5 1 14268.13 13353.48 154.18 o 3 5 1 15223.20 14907.30 173.30 o 4 5 1 10698.45 10214.93 104.41 o 5 5 1 7741.15 7613.91 74.41 o 6 5 1 3110.81 3250.48 51.66 o 7 5 1 65.25 80.54 14.41 o 8 5 1 3.16 15.38 11.26 o 9 5 1 144.20 200.90 33.34 o 10 5 1 307.09 271.48 48.20 o -10 6 1 2.03 -33.82 33.82 o -9 6 1 108.64 128.25 18.34 o -8 6 1 29.83 24.91 13.73 o -7 6 1 396.90 413.28 20.32 o -6 6 1 53.38 60.50 9.94 o -5 6 1 94.10 140.53 9.66 o -4 6 1 1838.97 1823.17 20.60 o -3 6 1 44.13 71.07 7.13 o -2 6 1 864.05 874.87 20.64 o -1 6 1 308.26 345.94 14.51 o 0 6 1 10578.31 10812.31 139.65 o 1 6 1 886.60 849.44 13.93 o 2 6 1 3181.10 3115.56 34.94 o 3 6 1 416.32 481.09 10.25 o 4 6 1 4429.27 4465.59 50.94 o 5 6 1 1034.95 1056.35 31.22 o 6 6 1 591.69 628.49 20.06 o 7 6 1 14.64 5.47 10.22 o 8 6 1 965.21 1036.94 31.69 o 9 6 1 210.70 182.48 29.41 o -10 7 1 209.49 231.03 34.88 o -9 7 1 568.61 594.92 28.91 o -8 7 1 458.00 379.84 12.79 o -7 7 1 329.87 313.03 12.90 o -6 7 1 1416.12 1294.73 23.21 o -5 7 1 2758.27 2679.11 35.20 o -4 7 1 11665.75 11506.43 149.09 o -3 7 1 11282.62 10938.64 156.19 o -2 7 1 1352.73 1282.47 21.30 o -1 7 1 2421.63 2375.27 32.59 o 0 7 1 1748.56 1646.60 27.52 o 1 7 1 299.39 336.87 17.10 o 2 7 1 2152.13 2134.01 28.69 o 3 7 1 666.31 651.69 13.10 o 4 7 1 2087.86 2003.00 32.92 o 5 7 1 844.43 882.74 23.46 o 6 7 1 486.51 449.28 16.39 o 7 7 1 872.15 814.17 24.17 o 8 7 1 575.66 574.92 27.61 o 9 7 1 301.64 280.42 18.83 o -9 8 1 767.76 838.12 75.92 o -8 8 1 1640.70 1778.51 43.18 o -7 8 1 2156.30 2146.32 31.37 o -6 8 1 1200.49 1182.46 27.40 o -5 8 1 2072.82 2051.87 31.95 o -4 8 1 426.72 429.45 14.39 o -3 8 1 79.43 72.45 10.96 o -2 8 1 7094.95 7088.92 84.72 o -1 8 1 5416.94 5244.04 75.52 o 0 8 1 3494.32 3303.72 49.54 o 1 8 1 952.99 916.18 18.28 o 2 8 1 2426.78 2268.72 36.96 o 3 8 1 353.32 370.67 10.79 o 4 8 1 972.34 947.50 18.32 o 5 8 1 1085.53 1070.15 18.75 o 6 8 1 2288.63 2240.51 29.06 o 7 8 1 1523.65 1677.79 32.74 o 8 8 1 1245.01 1336.63 37.00 o 9 8 1 667.53 560.35 31.21 o -9 9 1 240.30 192.69 27.87 o -8 9 1 3.26 7.26 13.91 o -7 9 1 234.25 248.81 16.05 o -6 9 1 163.10 156.61 22.86 o -5 9 1 186.91 176.41 13.26 o -4 9 1 1246.03 1279.51 29.03 o -3 9 1 390.96 365.70 16.68 o -2 9 1 72.13 88.14 10.05 o -1 9 1 408.22 371.21 23.61 o 0 9 1 1470.40 1458.96 31.19 o 1 9 1 23.13 15.12 9.70 o 2 9 1 778.55 758.55 17.85 o 3 9 1 690.73 685.96 18.24 o 4 9 1 557.91 576.62 16.72 o 5 9 1 266.27 257.59 14.72 o 6 9 1 9.63 18.16 10.23 o 7 9 1 184.79 129.06 13.46 o 8 9 1 2.29 -12.98 18.71 o 9 9 1 18.21 19.50 20.91 o -9 10 1 59.43 60.08 26.37 o -8 10 1 429.29 443.07 28.78 o -7 10 1 1241.68 1282.14 52.43 o -6 10 1 2032.32 2047.13 47.16 o -5 10 1 760.70 756.40 23.82 o -4 10 1 5.49 14.79 11.77 o -3 10 1 240.94 256.21 14.50 o -2 10 1 3511.76 3374.15 49.62 o -1 10 1 663.91 668.94 22.89 o 0 10 1 779.52 742.67 22.67 o 1 10 1 1032.43 991.51 35.56 o 2 10 1 226.42 239.59 28.08 o 3 10 1 569.35 582.44 19.00 o 4 10 1 1489.69 1489.94 25.82 o 5 10 1 1873.17 1958.01 37.48 o 6 10 1 5019.14 5214.50 78.59 o 7 10 1 2604.90 2614.81 80.18 o 8 10 1 2373.98 2721.87 159.41 o -8 11 1 630.60 638.61 36.11 o -7 11 1 1608.22 1668.79 34.52 o -6 11 1 4805.68 4940.82 78.38 o -5 11 1 8498.69 8496.96 159.04 o -4 11 1 11651.15 11635.34 190.04 o -3 11 1 1956.05 1834.22 35.61 o -2 11 1 7181.92 7175.72 113.92 o -1 11 1 7310.38 7068.80 111.80 o 0 11 1 1551.20 1524.58 34.34 o 1 11 1 663.37 669.29 24.83 o 2 11 1 3.20 0.04 12.14 o 3 11 1 178.64 198.33 16.27 o 4 11 1 7.61 7.35 10.72 o 5 11 1 144.13 135.12 16.87 o 6 11 1 5.99 7.43 11.69 o 7 11 1 674.75 648.09 27.09 o 8 11 1 1351.64 1511.74 157.09 o -8 12 1 99.47 113.44 25.74 o -7 12 1 339.46 291.85 28.29 o -6 12 1 26.98 -5.19 13.36 o -5 12 1 1.18 16.29 14.34 o -4 12 1 37.40 49.48 14.24 o -3 12 1 1624.23 1644.03 40.74 o -2 12 1 85.17 65.45 16.87 o -1 12 1 487.01 499.59 27.64 o 0 12 1 670.64 678.51 31.28 o 1 12 1 1449.34 1349.94 37.83 o 2 12 1 2257.29 2225.08 42.71 o 3 12 1 1362.34 1364.23 33.38 o 4 12 1 715.43 767.99 29.52 o 5 12 1 144.10 135.57 18.29 o 6 12 1 297.04 333.17 20.15 o 7 12 1 647.40 688.99 47.23 o -7 13 1 1580.33 1702.72 63.61 o -6 13 1 390.28 345.66 21.88 o -5 13 1 114.87 80.61 26.82 o -4 13 1 121.10 115.19 17.50 o -3 13 1 0.71 24.50 14.67 o -2 13 1 151.19 156.73 17.60 o -1 13 1 1138.81 1109.42 42.17 o 0 13 1 3238.67 3167.87 78.05 o 1 13 1 748.74 777.86 44.28 o 2 13 1 4734.34 4555.38 78.07 o 3 13 1 6896.36 6810.87 115.45 o 4 13 1 5545.79 5559.14 97.45 o 5 13 1 1787.69 1783.10 44.50 o 6 13 1 163.23 180.46 18.94 o -6 14 1 443.51 462.95 27.45 o -5 14 1 215.47 231.56 23.62 o -4 14 1 29.98 18.60 17.79 o -3 14 1 90.02 70.56 20.74 o -2 14 1 3285.10 3315.93 74.17 o -1 14 1 2272.73 2200.63 59.00 o 0 14 1 3905.56 3848.91 89.64 o 1 14 1 428.56 412.22 48.51 o 2 14 1 2479.88 2422.63 74.17 o 3 14 1 406.42 426.57 32.04 o 4 14 1 210.32 204.85 21.11 o 5 14 1 4.16 10.95 20.42 o 6 14 1 4.29 16.66 15.07 o -5 15 1 246.45 222.78 26.64 o -4 15 1 243.66 249.10 24.60 o -3 15 1 101.37 103.51 19.34 o -2 15 1 505.46 503.00 29.43 o -1 15 1 110.12 128.40 22.60 o 0 15 1 538.79 557.33 30.60 o 1 15 1 362.47 376.32 25.53 o 2 15 1 380.00 380.97 24.35 o 3 15 1 164.05 145.14 23.61 o 4 15 1 145.85 140.07 27.58 o 5 15 1 283.78 350.78 28.96 o -4 16 1 10.31 0.80 20.02 o -3 16 1 102.92 108.35 26.59 o -2 16 1 28.40 62.31 27.01 o -1 16 1 489.66 486.11 33.89 o 0 16 1 1048.31 1063.24 137.58 o 1 16 1 456.85 391.49 37.56 o 2 16 1 242.70 217.81 21.98 o 3 16 1 24.49 4.39 16.50 o -2 17 1 135.09 124.21 25.48 o -1 17 1 1.07 9.13 20.77 o 0 17 1 166.33 152.09 29.91 o 1 17 1 788.74 792.53 79.44 o -11 0 2 577.30 600.51 79.30 o -10 0 2 1630.09 1548.67 116.97 o -9 0 2 4720.83 4261.41 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