#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/20/2222043.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222043_Fobs loop_ _publ_author_name 'Momeni, Badri Z.' 'Rominger, Frank' 'Hosseini, Simin S.' _publ_section_title ; Tetrachlorido(1,10-phenanthroline-\k^2^N,N')tin(IV) 1,2-dichloroethane hemisolvate ; _journal_coeditor_code HG2511 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m690 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.4478 _cell_length_b 12.3681 _cell_length_c 18.3551 _exptl_crystal_F_000 1896.00 _reflns_d_resolution_high 0.7710 _[local]_cod_data_source_file hg2511Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sba57 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 537.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6234.72 9391.44 196.78 o 4 0 0 288903.56 297131.06 8193.60 o 6 0 0 4953.91 5750.75 154.27 o 8 0 0 73774.34 71306.55 1707.26 o 10 0 0 3676.38 3768.08 199.90 o 12 0 0 18822.27 19124.95 924.12 o 14 0 0 14940.05 14128.54 597.32 o 16 0 0 4510.41 4174.96 365.90 o 18 0 0 284.65 113.49 128.67 o 2 1 0 112319.85 122768.17 1957.95 o 4 1 0 105.11 62.05 14.18 o 6 1 0 167785.83 155678.00 3256.99 o 8 1 0 14045.72 12207.51 218.96 o 10 1 0 10236.83 10742.13 310.14 o 12 1 0 4867.87 5010.25 183.55 o 14 1 0 10748.11 9991.08 317.83 o 16 1 0 948.53 1075.01 110.58 o 18 1 0 3124.85 3087.35 182.21 o 0 2 0 119234.14 111246.88 3525.34 o 2 2 0 17337.60 17660.05 388.40 o 4 2 0 64077.64 66539.89 1129.72 o 6 2 0 2687.60 3315.08 72.46 o 8 2 0 24426.95 23763.44 445.97 o 10 2 0 2131.61 2347.29 102.76 o 12 2 0 10017.54 10084.18 307.87 o 14 2 0 869.31 739.57 84.56 o 16 2 0 1343.48 1392.32 120.50 o 18 2 0 2.21 32.03 106.44 o 2 3 0 88197.30 88280.31 1900.20 o 4 3 0 14194.98 14334.66 295.09 o 6 3 0 61711.68 60852.85 1291.58 o 8 3 0 385.16 422.64 34.99 o 10 3 0 25967.28 25409.06 570.23 o 12 3 0 146.42 100.34 65.45 o 14 3 0 5425.31 5771.54 268.58 o 16 3 0 558.19 643.87 106.53 o 18 3 0 1933.79 1704.62 181.39 o 0 4 0 1623.81 1007.48 51.61 o 2 4 0 183.12 434.84 28.85 o 4 4 0 3203.91 3187.51 82.70 o 6 4 0 22668.16 21614.68 485.58 o 8 4 0 10091.90 10165.30 212.69 o 10 4 0 1294.74 1323.28 63.29 o 12 4 0 6017.60 6466.53 224.41 o 14 4 0 774.99 884.73 96.33 o 16 4 0 1287.83 1421.13 149.41 o 18 4 0 128.08 175.55 105.93 o 2 5 0 34198.39 33945.51 1075.34 o 4 5 0 3665.63 2713.37 77.38 o 6 5 0 4157.52 4782.15 121.69 o 8 5 0 26.61 135.90 30.93 o 10 5 0 1460.82 1534.03 69.80 o 12 5 0 4868.19 5175.86 194.72 o 14 5 0 6.70 94.25 97.63 o 16 5 0 916.74 957.86 110.79 o 0 6 0 3261.32 3947.06 144.83 o 2 6 0 0.72 -6.69 24.56 o 4 6 0 9861.38 8264.93 189.17 o 6 6 0 5928.71 5875.77 156.61 o 8 6 0 7722.10 7784.35 176.05 o 10 6 0 177.95 154.56 40.18 o 12 6 0 1162.06 1481.02 124.05 o 14 6 0 405.52 446.13 85.84 o 16 6 0 229.51 401.37 98.53 o 2 7 0 1651.17 1401.12 56.65 o 4 7 0 5964.17 5943.71 147.83 o 6 7 0 25.85 -10.29 28.99 o 8 7 0 2463.48 2444.33 93.67 o 10 7 0 1232.11 1240.01 86.79 o 12 7 0 2718.56 2825.35 128.32 o 14 7 0 1050.65 1069.57 108.41 o 16 7 0 189.60 142.22 94.85 o 0 8 0 2693.92 2708.17 146.67 o 2 8 0 119.31 160.99 32.89 o 4 8 0 651.28 984.86 63.77 o 6 8 0 0.72 -31.65 31.65 o 8 8 0 1087.54 1119.79 64.19 o 10 8 0 56.38 71.55 48.38 o 12 8 0 2239.31 2206.48 120.31 o 14 8 0 135.46 72.59 80.99 o 16 8 0 1926.83 1816.37 167.95 o 2 9 0 5351.54 5622.38 147.19 o 4 9 0 1997.92 2004.61 93.82 o 6 9 0 3545.40 3617.95 124.72 o 8 9 0 0.32 80.39 58.68 o 10 9 0 14009.30 13505.40 324.32 o 12 9 0 2.88 -25.00 68.80 o 14 9 0 1447.17 1190.24 122.69 o 0 10 0 2100.23 2291.88 121.92 o 2 10 0 55.39 90.25 48.25 o 4 10 0 37472.43 37171.93 843.51 o 6 10 0 1024.98 1100.00 73.17 o 8 10 0 24797.61 24580.56 583.55 o 10 10 0 395.15 473.21 71.18 o 12 10 0 8837.98 8474.89 298.19 o 14 10 0 188.53 332.69 109.41 o 2 11 0 37574.71 35002.35 728.45 o 4 11 0 2727.79 2685.42 102.51 o 6 11 0 9445.80 9271.44 260.46 o 8 11 0 1106.66 862.96 83.87 o 10 11 0 11929.56 12706.67 461.05 o 12 11 0 2470.84 2718.61 174.52 o 0 12 0 26021.59 27377.79 1368.20 o 2 12 0 1588.10 1623.82 111.54 o 4 12 0 21748.46 22115.80 603.40 o 6 12 0 7.93 -37.66 69.52 o 8 12 0 13830.07 13930.52 417.87 o 10 12 0 91.64 169.47 144.73 o 12 12 0 3767.93 3246.15 394.04 o 2 13 0 23129.06 22588.26 620.76 o 4 13 0 509.54 366.08 87.61 o 6 13 0 10226.18 9768.94 322.76 o 8 13 0 121.85 309.25 171.83 o 10 13 0 3917.48 3353.70 276.18 o 0 14 0 6890.56 7139.91 373.23 o 2 14 0 13.40 197.16 89.00 o 4 14 0 4214.47 3715.69 185.02 o 6 14 0 247.68 427.40 127.69 o 8 14 0 2882.63 2963.98 300.17 o 2 15 0 4013.89 3903.16 235.58 o 4 15 0 27.35 -110.54 110.54 o 6 15 0 4232.24 4623.28 265.61 o 0 16 0 5011.01 5976.29 537.90 o 1 1 1 4797.91 5083.85 54.68 o 2 1 1 2832.49 3807.27 53.60 o 3 1 1 2.74 34.70 7.28 o 4 1 1 20973.46 19828.85 250.66 o 5 1 1 1199.97 1353.86 30.65 o 6 1 1 3373.51 3719.60 64.18 o 7 1 1 181.30 223.88 18.71 o 8 1 1 2410.14 3020.17 53.75 o 9 1 1 605.85 677.85 26.61 o 10 1 1 2129.14 1914.45 53.58 o 11 1 1 7.89 -0.90 38.69 o 12 1 1 504.21 525.29 48.31 o 13 1 1 32.92 45.58 38.07 o 14 1 1 315.22 284.94 49.48 o 15 1 1 567.96 480.01 57.80 o 16 1 1 18.64 -51.48 51.48 o 17 1 1 0.65 -50.00 54.39 o 18 1 1 566.52 536.87 76.70 o 0 2 1 56240.49 56638.78 1074.63 o 1 2 1 3619.20 3306.78 44.72 o 2 2 1 115.24 23.73 7.21 o 3 2 1 1678.95 2197.85 45.07 o 4 2 1 19.01 39.32 12.75 o 5 2 1 2274.22 2666.76 46.56 o 6 2 1 20156.90 20077.87 277.48 o 7 2 1 7069.05 7127.70 145.92 o 8 2 1 488.40 602.65 21.90 o 9 2 1 1575.37 1709.51 44.97 o 10 2 1 2189.50 2083.31 51.92 o 11 2 1 3157.57 3083.75 105.04 o 12 2 1 2294.82 2221.05 81.58 o 13 2 1 764.91 744.26 61.06 o 14 2 1 577.65 550.03 55.97 o 15 2 1 963.57 855.12 67.68 o 16 2 1 743.70 453.80 63.03 o 17 2 1 0.33 68.71 57.45 o 18 2 1 74.93 147.34 71.13 o 1 3 1 45.17 60.94 10.17 o 2 3 1 34349.18 38569.45 537.35 o 3 3 1 5617.51 5602.73 91.01 o 4 3 1 18761.37 17321.60 275.89 o 5 3 1 87.87 78.97 14.53 o 6 3 1 24173.78 22852.58 306.37 o 7 3 1 4066.57 4083.00 68.86 o 8 3 1 196.64 93.01 21.26 o 9 3 1 1605.34 1766.59 45.74 o 10 3 1 551.50 749.46 34.61 o 11 3 1 103.64 99.33 31.80 o 12 3 1 545.03 612.98 50.26 o 13 3 1 993.13 950.70 64.12 o 14 3 1 4818.99 4802.71 145.64 o 15 3 1 221.74 199.16 53.62 o 16 3 1 171.79 24.28 52.20 o 17 3 1 199.40 284.13 67.38 o 18 3 1 2455.70 2670.82 122.29 o 0 4 1 86292.83 78199.27 1420.06 o 1 4 1 186.14 145.69 15.44 o 2 4 1 3199.33 2973.03 53.29 o 3 4 1 3806.48 3796.47 65.34 o 4 4 1 42335.61 44284.95 651.06 o 5 4 1 385.76 489.04 24.02 o 6 4 1 17.44 38.88 15.76 o 7 4 1 1178.57 1208.10 35.09 o 8 4 1 31751.60 30364.54 441.32 o 9 4 1 204.91 249.57 23.63 o 10 4 1 1101.91 1061.39 51.00 o 11 4 1 3147.09 3083.74 79.80 o 12 4 1 20664.92 19784.64 384.62 o 13 4 1 627.93 626.26 59.32 o 14 4 1 861.94 980.40 67.89 o 15 4 1 476.98 524.10 64.47 o 16 4 1 3218.82 3073.56 119.61 o 17 4 1 638.38 659.62 77.26 o 18 4 1 49.75 -22.89 82.56 o 1 5 1 8650.67 8491.03 137.04 o 2 5 1 85804.73 84388.45 1171.07 o 3 5 1 9169.11 9510.01 150.77 o 4 5 1 3534.69 3719.57 71.05 o 5 5 1 18465.28 17363.18 268.07 o 6 5 1 72638.79 70375.95 1031.48 o 7 5 1 3268.17 3425.25 66.39 o 8 5 1 1895.39 1823.34 50.89 o 9 5 1 5352.62 5376.57 103.04 o 10 5 1 30340.17 29206.70 454.32 o 11 5 1 3690.57 3729.77 93.10 o 12 5 1 1118.77 1209.78 65.88 o 13 5 1 2936.16 2836.53 108.09 o 14 5 1 12666.56 12985.26 280.70 o 15 5 1 906.49 929.13 73.54 o 16 5 1 380.55 236.39 64.17 o 17 5 1 558.75 737.14 81.00 o 0 6 1 46066.96 46875.30 932.62 o 1 6 1 895.30 1205.29 35.32 o 2 6 1 373.44 420.14 24.90 o 3 6 1 11856.79 12744.02 203.67 o 4 6 1 52097.76 48153.30 712.12 o 5 6 1 168.93 202.30 22.77 o 6 6 1 7363.29 7482.07 124.82 o 7 6 1 1823.71 2014.78 53.54 o 8 6 1 50109.29 48544.07 694.88 o 9 6 1 264.39 336.92 29.85 o 10 6 1 61.24 102.55 28.05 o 11 6 1 66.11 91.66 34.05 o 12 6 1 14405.55 14361.41 280.12 o 13 6 1 1332.35 1182.29 71.55 o 14 6 1 70.84 93.81 55.32 o 15 6 1 249.90 235.02 83.67 o 16 6 1 5692.25 5909.43 173.07 o 17 6 1 716.83 734.30 83.10 o 1 7 1 1846.18 1990.48 47.53 o 2 7 1 33576.80 32310.19 485.12 o 3 7 1 8.61 -3.94 18.34 o 4 7 1 4310.39 4082.76 86.00 o 5 7 1 717.14 747.39 37.84 o 6 7 1 25548.29 25812.53 413.82 o 7 7 1 280.26 197.42 27.36 o 8 7 1 181.15 156.04 32.48 o 9 7 1 3929.16 3813.02 92.05 o 10 7 1 28016.90 27124.30 428.24 o 11 7 1 295.38 261.99 39.64 o 12 7 1 1334.12 1457.91 72.05 o 13 7 1 1274.43 1269.75 72.37 o 14 7 1 8169.38 7901.39 197.89 o 15 7 1 792.42 689.38 92.71 o 16 7 1 4.95 -30.03 64.05 o 0 8 1 8137.60 9623.17 219.89 o 1 8 1 1048.82 1177.31 38.82 o 2 8 1 1637.29 1454.66 43.48 o 3 8 1 6221.23 6540.71 119.71 o 4 8 1 26947.42 27210.52 612.78 o 5 8 1 1830.83 1886.56 56.37 o 6 8 1 587.20 659.26 35.99 o 7 8 1 7526.32 7390.77 137.24 o 8 8 1 18789.70 18302.39 294.32 o 9 8 1 268.89 323.73 34.45 o 10 8 1 6.75 -15.20 40.24 o 11 8 1 2781.05 2768.69 80.34 o 12 8 1 9047.05 8999.42 212.79 o 13 8 1 632.82 574.88 61.65 o 14 8 1 759.87 1110.25 80.47 o 15 8 1 1569.63 1641.18 104.20 o 16 8 1 4773.83 5041.45 163.53 o 1 9 1 331.61 344.91 30.18 o 2 9 1 6278.16 6497.44 121.15 o 3 9 1 179.63 116.11 24.97 o 4 9 1 4.87 -2.06 24.30 o 5 9 1 109.59 131.73 28.19 o 6 9 1 3523.43 3484.65 78.73 o 7 9 1 13.94 0.85 29.97 o 8 9 1 2363.42 2344.60 71.66 o 9 9 1 1406.73 1442.33 58.92 o 10 9 1 8703.70 8584.06 175.45 o 11 9 1 433.00 453.50 54.00 o 12 9 1 133.21 83.76 48.85 o 13 9 1 462.75 485.03 61.26 o 14 9 1 3674.92 3584.45 125.19 o 15 9 1 171.94 235.20 75.21 o 0 10 1 4629.81 4684.68 132.49 o 1 10 1 69.04 60.18 28.70 o 2 10 1 947.00 911.61 41.40 o 3 10 1 1.87 17.97 25.96 o 4 10 1 4159.95 4256.00 90.83 o 5 10 1 16.00 12.52 39.05 o 6 10 1 1588.27 1597.20 57.37 o 7 10 1 436.05 470.21 40.54 o 8 10 1 1774.67 1764.48 64.90 o 9 10 1 187.56 215.52 43.76 o 10 10 1 175.25 274.34 56.02 o 11 10 1 1258.47 1312.20 74.07 o 12 10 1 1289.64 1154.32 81.51 o 13 10 1 364.83 325.40 72.24 o 14 10 1 62.73 -44.84 77.47 o 1 11 1 2499.54 2529.64 81.89 o 2 11 1 6460.04 6691.05 148.65 o 3 11 1 88.56 -4.74 35.12 o 4 11 1 1157.24 1207.16 58.29 o 5 11 1 780.87 815.00 49.24 o 6 11 1 5738.70 5547.38 132.39 o 7 11 1 205.17 282.40 44.67 o 8 11 1 657.77 424.49 58.12 o 9 11 1 1565.11 1517.50 68.95 o 10 11 1 588.19 640.62 68.39 o 11 11 1 46.48 67.01 60.95 o 12 11 1 0.02 46.61 104.36 o 13 11 1 691.28 691.01 115.59 o 0 12 1 14443.85 15402.59 450.20 o 1 12 1 1239.22 1134.72 76.45 o 2 12 1 100.43 34.37 46.71 o 3 12 1 941.47 942.47 71.20 o 4 12 1 989.83 809.63 69.87 o 5 12 1 130.66 74.84 49.83 o 6 12 1 325.99 354.65 59.14 o 7 12 1 648.19 690.46 76.97 o 8 12 1 399.55 409.36 66.02 o 9 12 1 90.13 174.79 90.89 o 10 12 1 61.25 -49.28 90.14 o 11 12 1 159.49 92.14 113.07 o 12 12 1 340.76 556.04 122.98 o 1 13 1 323.85 248.17 57.51 o 2 13 1 7.91 -49.96 49.96 o 3 13 1 526.75 448.79 67.57 o 4 13 1 27.31 8.54 52.84 o 5 13 1 25.48 114.34 65.31 o 6 13 1 623.24 742.12 80.67 o 7 13 1 299.93 229.98 80.50 o 8 13 1 272.58 464.97 80.37 o 9 13 1 45.31 -38.60 79.65 o 10 13 1 25.82 -24.36 107.84 o 0 14 1 659.22 479.60 97.38 o 1 14 1 56.27 156.77 62.17 o 2 14 1 41.07 -1.00 70.53 o 3 14 1 40.08 7.78 63.17 o 4 14 1 1559.75 1682.11 103.95 o 5 14 1 291.93 178.68 71.25 o 6 14 1 0.48 -26.40 66.18 o 7 14 1 34.25 -8.31 82.85 o 8 14 1 54.83 -77.23 77.23 o 9 14 1 111.93 -13.46 113.32 o 1 15 1 678.51 611.88 99.07 o 2 15 1 5472.53 5891.27 187.52 o 3 15 1 825.88 983.41 97.72 o 4 15 1 98.07 9.26 81.60 o 5 15 1 21.73 -49.83 84.81 o 6 15 1 1586.05 1623.76 129.96 o 0 16 1 7775.32 8623.41 465.39 o 1 16 1 344.52 175.29 106.13 o 0 0 2 84689.55 77123.59 1650.79 o 1 0 2 35297.85 33793.49 928.26 o 2 0 2 4281.19 3418.89 74.09 o 3 0 2 13526.51 15337.62 254.23 o 4 0 2 33375.23 35627.98 1016.38 o 5 0 2 83373.45 84474.70 2201.96 o 6 0 2 11105.84 11167.25 262.66 o 7 0 2 52991.36 56015.63 1481.64 o 8 0 2 13677.85 13606.15 358.40 o 9 0 2 23693.73 22465.62 733.26 o 10 0 2 968.80 1074.92 57.93 o 11 0 2 7990.90 7778.22 245.33 o 12 0 2 12445.37 12447.20 364.53 o 13 0 2 6191.74 6522.62 226.75 o 14 0 2 4872.62 4685.72 188.07 o 15 0 2 1253.91 1077.55 101.87 o 16 0 2 3309.83 3271.48 167.74 o 17 0 2 544.74 639.58 101.02 o 18 0 2 529.14 561.36 167.92 o 1 1 2 69088.42 67616.91 704.14 o 2 1 2 103893.20 104541.16 1472.26 o 3 1 2 65804.96 72038.69 951.85 o 4 1 2 10107.01 9225.06 125.15 o 5 1 2 3303.63 3055.19 50.77 o 6 1 2 92165.19 88531.66 1179.31 o 7 1 2 41979.74 39302.33 555.23 o 8 1 2 112.42 291.92 17.13 o 9 1 2 8.99 -17.25 21.37 o 10 1 2 14455.33 14950.84 276.71 o 11 1 2 7784.13 8054.90 190.64 o 12 1 2 61.61 91.77 37.10 o 13 1 2 1246.02 1384.22 69.85 o 14 1 2 12947.97 12551.57 269.29 o 15 1 2 2849.65 2940.63 108.04 o 16 1 2 667.20 711.67 70.36 o 17 1 2 209.12 286.75 68.82 o 18 1 2 3464.50 3492.99 135.02 o 0 2 2 119046.52 114689.66 2234.40 o 1 2 2 22294.94 22963.27 287.70 o 2 2 2 3431.05 4267.39 61.32 o 3 2 2 5633.87 6362.77 97.12 o 4 2 2 14573.09 16848.01 238.83 o 5 2 2 36795.88 38295.60 643.63 o 6 2 2 764.03 700.90 21.25 o 7 2 2 4765.84 4729.67 74.30 o 8 2 2 20575.91 20697.50 305.22 o 9 2 2 15239.54 16139.82 258.83 o 10 2 2 437.37 377.06 26.56 o 11 2 2 1398.65 1362.85 55.26 o 12 2 2 13865.03 14177.21 288.14 o 13 2 2 3868.29 3722.84 113.38 o 14 2 2 47.34 108.74 47.34 o 15 2 2 1207.31 966.77 74.35 o 16 2 2 4410.72 4195.87 136.18 o 17 2 2 329.24 316.75 68.17 o 18 2 2 55.82 -63.90 63.90 o 1 3 2 60986.20 62967.69 781.27 o 2 3 2 8486.57 8558.44 122.47 o 3 3 2 33857.57 33675.21 517.80 o 4 3 2 113.17 149.21 17.68 o 5 3 2 9541.53 9661.66 141.51 o 6 3 2 819.31 1183.85 36.64 o 7 3 2 14105.89 14441.27 217.28 o 8 3 2 1155.71 980.40 36.70 o 9 3 2 4694.45 4873.23 85.30 o 10 3 2 6407.57 6564.73 125.65 o 11 3 2 6915.52 7321.48 153.98 o 12 3 2 3.40 -39.58 39.58 o 13 3 2 931.80 1009.23 63.07 o 14 3 2 4179.98 3972.34 123.72 o 15 3 2 864.90 835.52 71.56 o 16 3 2 270.70 181.71 56.64 o 17 3 2 176.97 150.57 62.32 o 18 3 2 1166.42 1231.62 96.12 o 0 4 2 9284.57 8234.41 161.99 o 1 4 2 8920.32 10313.00 141.41 o 2 4 2 3843.19 3557.94 61.82 o 3 4 2 25403.92 24210.54 361.50 o 4 4 2 4953.88 4907.09 81.93 o 5 4 2 16346.20 16622.77 268.44 o 6 4 2 151.35 141.88 17.98 o 7 4 2 962.43 1102.02 37.16 o 8 4 2 12382.83 12209.99 184.84 o 9 4 2 1492.78 1643.57 45.56 o 10 4 2 4788.33 4626.09 91.78 o 11 4 2 2209.35 2105.22 68.42 o 12 4 2 4744.70 4688.83 126.95 o 13 4 2 1005.60 1050.25 65.18 o 14 4 2 3206.50 3232.26 110.78 o 15 4 2 294.30 325.42 59.12 o 16 4 2 2975.17 3242.54 122.00 o 17 4 2 664.57 752.35 78.42 o 18 4 2 19.13 47.11 71.62 o 1 5 2 18256.14 17665.31 246.54 o 2 5 2 396.14 611.79 24.08 o 3 5 2 831.65 571.86 23.81 o 4 5 2 3486.24 3167.07 60.65 o 5 5 2 481.94 566.25 25.55 o 6 5 2 159.02 74.72 21.22 o 7 5 2 278.80 243.40 22.88 o 8 5 2 3882.89 3765.46 76.02 o 9 5 2 7091.45 7051.70 115.14 o 10 5 2 6658.40 6597.66 128.33 o 11 5 2 182.05 119.09 34.32 o 12 5 2 67.88 45.32 42.41 o 13 5 2 120.13 77.09 45.40 o 14 5 2 1315.59 1435.77 80.44 o 15 5 2 232.25 295.09 58.21 o 16 5 2 129.48 40.30 57.45 o 17 5 2 73.14 81.27 66.00 o 0 6 2 8077.65 8020.85 179.56 o 1 6 2 2370.67 3004.55 58.91 o 2 6 2 3504.17 3432.06 65.28 o 3 6 2 17591.91 17825.18 263.60 o 4 6 2 2.17 -1.86 17.07 o 5 6 2 5454.44 5460.56 100.50 o 6 6 2 1692.50 1779.34 49.53 o 7 6 2 37.69 38.69 24.21 o 8 6 2 922.94 935.02 39.01 o 9 6 2 118.17 96.73 25.67 o 10 6 2 208.80 174.05 30.55 o 11 6 2 5910.83 5792.08 121.74 o 12 6 2 49.20 148.50 43.34 o 13 6 2 19.17 15.56 44.93 o 14 6 2 74.94 231.91 55.09 o 15 6 2 31.49 165.67 62.42 o 16 6 2 138.80 289.43 67.74 o 17 6 2 3.79 -3.78 74.17 o 1 7 2 622.17 661.77 29.38 o 2 7 2 9393.72 8992.82 144.36 o 3 7 2 598.39 505.63 28.00 o 4 7 2 140.33 195.57 22.95 o 5 7 2 3536.11 3510.61 75.19 o 6 7 2 1612.09 1639.94 49.77 o 7 7 2 191.99 205.52 27.71 o 8 7 2 736.35 671.45 35.21 o 9 7 2 59.86 65.62 26.31 o 10 7 2 438.29 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3949.88 3861.36 133.01 o 2 6 19 279.24 270.09 64.82 o 3 6 19 2989.79 2845.51 117.51 o 4 6 19 7049.77 7209.96 207.36 o 5 6 19 1167.52 1282.63 90.85 o 6 6 19 358.73 551.31 76.91 o 7 6 19 967.61 683.32 109.30 o 8 6 19 3387.30 3610.53 162.27 o 1 7 19 2184.21 2233.39 108.98 o 2 7 19 4200.35 4168.88 143.06 o 3 7 19 3140.12 3110.88 126.77 o 4 7 19 1075.90 1165.10 90.63 o 5 7 19 3082.48 3396.39 133.77 o 6 7 19 2185.52 2122.94 122.19 o 7 7 19 1954.80 1905.39 119.08 o 0 8 19 2640.57 2539.51 165.96 o 1 8 19 2796.65 2962.87 136.25 o 2 8 19 54.53 7.77 64.46 o 3 8 19 1929.88 1587.70 108.62 o 4 8 19 4330.60 4918.76 161.69 o 5 8 19 1113.07 1046.12 95.61 o 6 8 19 778.84 866.37 93.81 o 1 9 19 244.42 265.33 81.90 o 2 9 19 3432.11 3536.11 141.98 o 3 9 19 278.49 208.72 77.60 o 4 9 19 113.35 105.21 76.37 o 0 0 20 803.27 1013.25 155.89 o 1 0 20 5016.55 4629.88 197.26 o 2 0 20 207.23 303.23 86.36 o 3 0 20 4085.27 3826.79 207.62 o 4 0 20 1047.79 903.74 114.20 o 5 0 20 7187.43 7057.07 335.75 o 6 0 20 670.38 743.29 108.24 o 7 0 20 2726.30 2687.61 162.93 o 8 0 20 141.37 31.86 106.25 o 9 0 20 6021.67 6310.24 302.44 o 10 0 20 63.65 270.31 170.10 o 1 1 20 1631.68 1666.74 89.37 o 2 1 20 1825.91 1878.91 99.37 o 3 1 20 2924.62 3067.43 123.56 o 4 1 20 1203.23 1323.34 86.79 o 5 1 20 4556.12 4557.34 144.34 o 6 1 20 604.57 723.29 76.45 o 7 1 20 1670.04 1625.81 102.55 o 8 1 20 75.98 -45.62 123.09 o 9 1 20 3249.07 3711.93 179.76 o 10 1 20 178.94 126.53 89.25 o 0 2 20 1208.79 1246.58 138.33 o 1 2 20 885.89 783.31 89.24 o 2 2 20 0.01 -89.51 89.51 o 3 2 20 1675.92 1616.32 105.56 o 4 2 20 510.70 396.85 70.65 o 5 2 20 785.67 760.96 78.42 o 6 2 20 9.33 42.77 70.45 o 7 2 20 2040.73 1978.04 103.85 o 8 2 20 969.60 1162.94 114.05 o 9 2 20 1440.67 1272.11 118.66 o 1 3 20 1087.97 887.58 80.73 o 2 3 20 2.02 -58.37 58.37 o 3 3 20 291.65 221.90 64.33 o 4 3 20 123.12 159.07 63.56 o 5 3 20 1893.19 1938.08 108.02 o 6 3 20 185.68 135.22 68.99 o 7 3 20 489.36 412.18 84.93 o 8 3 20 10.62 81.83 88.55 o 9 3 20 1905.15 1878.68 144.03 o 0 4 20 164.86 368.77 93.15 o 1 4 20 555.75 549.39 68.18 o 2 4 20 64.47 17.31 70.76 o 3 4 20 1303.47 1161.36 95.48 o 4 4 20 230.35 283.00 70.62 o 5 4 20 107.88 333.46 73.60 o 6 4 20 107.66 138.49 72.45 o 7 4 20 1436.31 1435.97 112.16 o 8 4 20 793.39 951.53 141.76 o 9 4 20 35.76 -36.58 124.25 o 1 5 20 2.43 -38.94 55.08 o 2 5 20 8.99 106.36 82.81 o 3 5 20 218.13 251.97 71.27 o 4 5 20 1131.50 1198.56 90.35 o 5 5 20 1750.04 1788.46 109.56 o 6 5 20 29.60 48.89 76.95 o 7 5 20 3.44 -23.57 78.77 o 8 5 20 21.52 24.00 86.99 o 0 6 20 1010.18 974.95 132.24 o 1 6 20 63.59 32.24 65.93 o 2 6 20 316.42 274.08 70.71 o 3 6 20 394.61 399.97 74.03 o 4 6 20 1.80 88.22 72.47 o 5 6 20 494.36 629.88 89.58 o 6 6 20 137.61 -23.74 86.91 o 7 6 20 198.59 256.28 96.04 o 1 7 20 6.28 -61.36 61.36 o 2 7 20 2.19 -57.90 66.13 o 3 7 20 44.14 87.15 69.95 o 4 7 20 3.17 48.53 74.87 o 5 7 20 21.14 -15.11 68.87 o 6 7 20 104.02 121.42 74.48 o 0 8 20 0.79 52.75 100.80 o 1 8 20 825.80 965.99 94.16 o 2 8 20 70.88 57.49 73.15 o 3 8 20 596.78 641.15 88.53 o 4 8 20 38.30 -22.06 95.98 o 1 1 21 6.81 -0.39 62.82 o 2 1 21 12.55 -58.11 58.11 o 3 1 21 381.62 422.72 78.73 o 4 1 21 549.63 622.95 81.72 o 5 1 21 574.51 476.50 81.94 o 6 1 21 56.53 -30.98 71.84 o 7 1 21 67.80 121.54 79.87 o 8 1 21 1.29 38.65 101.95 o 0 2 21 488.90 658.70 124.58 o 1 2 21 113.67 105.41 71.72 o 2 2 21 1.43 21.24 69.08 o 3 2 21 2.05 -60.73 69.96 o 4 2 21 142.07 256.40 80.22 o 5 2 21 562.45 530.80 90.83 o 6 2 21 87.05 -38.30 78.52 o 7 2 21 12.03 113.53 97.48 o 8 2 21 41.06 220.18 109.17 o 1 3 21 766.97 789.81 91.71 o 2 3 21 1.22 -65.31 65.31 o 3 3 21 2476.42 2366.25 132.21 o 4 3 21 190.49 204.49 89.84 o 5 3 21 613.04 483.66 79.60 o 6 3 21 93.14 114.17 82.72 o 7 3 21 2391.42 2417.00 177.15 o 8 3 21 0.09 43.73 87.33 o 0 4 21 0.02 -12.12 108.92 o 1 4 21 3205.14 3173.72 133.09 o 2 4 21 22.62 -20.69 69.01 o 3 4 21 2005.60 2139.44 116.56 o 4 4 21 98.31 197.50 72.55 o 5 4 21 4768.83 4982.94 170.53 o 6 4 21 53.41 49.47 84.11 o 7 4 21 1575.84 1485.11 135.82 o 1 5 21 4606.20 4614.99 151.04 o 2 5 21 793.75 756.46 89.12 o 3 5 21 4682.48 4912.41 193.30 o 4 5 21 7.76 172.92 86.00 o 5 5 21 2079.89 2128.48 126.32 o 6 5 21 166.88 233.46 84.71 o 0 6 21 477.85 728.38 169.27 o 1 6 21 8349.73 8287.64 241.43 o 2 6 21 30.29 0.18 65.59 o 3 6 21 6442.49 6343.62 208.17 o 4 6 21 88.99 143.70 79.30 o 5 6 21 3810.88 4017.26 163.23 o 1 7 21 4690.37 4876.93 174.34 o 2 7 21 171.35 221.46 84.08 o 3 7 21 4013.80 3898.69 158.69 o 0 0 22 90.03 390.53 152.39 o 1 0 22 4452.32 4366.36 206.32 o 2 0 22 309.32 344.25 132.26 o 3 0 22 2516.49 2322.13 161.43 o 4 0 22 1137.15 1075.14 128.12 o 5 0 22 3144.53 3539.67 225.56 o 6 0 22 749.32 509.99 139.81 o 7 0 22 1187.59 1212.76 350.26 o 1 1 22 1945.92 1923.27 124.81 o 2 1 22 604.83 633.76 109.09 o 3 1 22 5390.52 5261.77 190.96 o 4 1 22 12.01 -74.61 74.61 o 5 1 22 1515.80 1516.46 126.48 o 6 1 22 382.01 335.44 96.27 o 7 1 22 7007.87 7581.35 400.43 o 0 2 22 2.28 63.37 112.48 o 1 2 22 3441.81 3553.68 157.61 o 2 2 22 56.88 20.38 77.41 o 3 2 22 1881.64 1810.23 153.50 o 4 2 22 260.92 231.84 111.25 o 5 2 22 3336.33 3269.96 172.16 o 6 2 22 155.95 197.30 91.92 o 1 3 22 1237.92 1383.21 130.07 o 2 3 22 1.23 -29.09 79.63 o 3 3 22 1536.93 1440.41 117.64 o 4 3 22 217.70 281.38 91.67 o 5 3 22 1562.08 1685.46 129.11 o 6 3 22 190.52 -20.19 108.62 o 0 4 22 322.92 242.38 122.75 o 1 4 22 1141.59 998.68 106.28 o 2 4 22 1.90 107.32 83.48 o 3 4 22 1261.52 1323.17 115.92 o 4 4 22 124.02 143.62 85.79 o 5 4 22 220.73 136.41 90.45 o 1 5 22 1346.08 1410.41 135.97 o 2 5 22 19.53 22.18 83.32 o 3 5 22 204.28 307.88 90.19 o 4 5 22 989.88 1181.66 114.57 o 0 6 22 72.30 -93.74 93.74 o 1 6 22 314.31 342.60 88.71 o 1 1 23 186.97 400.65 95.03 o 2 1 23 506.72 656.72 101.61 o 3 1 23 20.46 177.21 87.99 o 4 1 23 75.92 82.71 87.30 o 0 2 23 92.33 217.72 134.68 o 1 2 23 6.01 147.52 93.03 o 2 2 23 41.75 125.86 89.69 o 3 2 23 30.65 175.75 98.64 o 4 2 23 582.69 660.97 109.26 o 1 3 23 17.78 84.30 93.82 o 2 3 23 1317.48 1326.66 122.76 o 3 3 23 210.64 120.29 98.13 o 0 4 23 2355.05 2137.69 197.99 o 1 4 23 635.49 577.15 104.52 o