#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:06:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181141 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/20/2222072.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222072_Fobs loop_ _publ_author_name 'Guo, Min' _publ_section_title ; 4,5-Bis(1H-tetrazol-5-yl)-1H-imidazole monohydrate ; _journal_coeditor_code IM2114 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1403 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.130 _cell_angle_gamma 90.000 _cell_length_a 15.6070 _cell_length_b 3.6706 _cell_length_c 18.1270 _exptl_crystal_F_000 455.76 _reflns_d_resolution_high 0.8108 _cod_data_source_file im2114Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 55 in Pn P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 7349.49 6617.57 100.45 o 4 0 0 550.41 547.29 12.05 o 5 0 0 467.26 442.21 11.68 o 6 0 0 198.45 265.77 8.89 o 7 0 0 1975.65 1977.19 39.93 o 8 0 0 1620.69 1781.70 55.32 o 9 0 0 10.62 8.12 2.66 o 10 0 0 787.80 859.49 24.03 o 11 0 0 185.71 167.61 10.09 o 12 0 0 1436.13 1245.19 57.83 o 13 0 0 799.78 725.69 31.12 o 14 0 0 57.62 79.69 28.17 o 15 0 0 46.91 57.18 11.46 o 16 0 0 0.00 6.95 9.58 o 1 1 0 5115.39 6012.67 63.42 o 2 1 0 844.43 875.21 18.23 o 3 1 0 94.75 78.01 2.05 o 4 1 0 32.23 23.72 1.75 o 5 1 0 22.10 36.54 2.69 o 6 1 0 116.66 147.66 5.14 o 7 1 0 166.98 165.68 5.86 o 8 1 0 48.72 41.91 5.39 o 9 1 0 133.76 135.71 6.40 o 10 1 0 329.95 319.11 15.00 o 11 1 0 2.71 0.00 2.51 o 12 1 0 237.28 229.87 11.79 o 13 1 0 394.73 349.05 32.43 o 14 1 0 0.00 2.06 4.04 o 15 1 0 51.99 67.83 8.83 o 16 1 0 14.96 28.99 9.97 o 0 2 0 3464.02 2965.39 78.45 o 1 2 0 602.87 712.70 14.22 o 2 2 0 100.47 73.60 3.09 o 3 2 0 7.62 25.97 3.05 o 4 2 0 255.85 235.30 5.43 o 5 2 0 108.46 98.38 3.20 o 6 2 0 90.08 73.97 5.07 o 7 2 0 365.90 387.76 14.49 o 8 2 0 256.44 237.10 11.67 o 9 2 0 183.18 197.40 11.83 o 10 2 0 2.96 1.61 3.77 o 11 2 0 331.37 352.64 17.24 o 12 2 0 5.10 31.64 7.03 o 13 2 0 146.31 157.25 12.65 o 14 2 0 104.57 124.22 11.91 o 15 2 0 0.01 14.36 7.12 o 1 3 0 33.44 38.44 3.66 o 2 3 0 51.77 62.39 5.72 o 3 3 0 267.87 260.34 10.33 o 4 3 0 12.79 24.86 7.38 o 5 3 0 10.10 17.48 3.96 o 6 3 0 36.96 40.31 6.42 o 7 3 0 1.82 3.57 4.29 o 8 3 0 36.40 29.19 5.55 o 9 3 0 79.83 82.66 9.05 o 10 3 0 27.50 44.92 7.99 o 11 3 0 0.05 0.00 5.74 o 12 3 0 50.74 42.73 8.79 o 0 4 0 8.06 23.02 10.51 o 1 4 0 18.60 23.60 5.54 o 2 4 0 8.54 7.79 4.19 o 3 4 0 2.34 6.02 5.46 o 4 4 0 11.06 23.20 6.33 o 5 4 0 17.62 22.17 6.79 o 6 4 0 10.67 20.33 6.45 o 7 4 0 38.96 43.41 9.01 o -16 1 1 2.24 5.75 5.27 o -15 1 1 29.12 2.58 4.98 o -14 1 1 97.56 106.12 8.94 o -13 1 1 23.49 29.01 5.90 o -12 1 1 0.02 7.04 3.83 o -11 1 1 625.10 635.46 17.57 o -10 1 1 109.24 108.28 5.99 o -9 1 1 378.60 360.29 10.53 o -8 1 1 519.17 532.89 13.09 o -7 1 1 62.12 35.94 2.63 o -6 1 1 0.10 11.17 2.21 o -5 1 1 3.78 8.40 1.45 o -4 1 1 1938.16 1621.70 23.63 o -3 1 1 14.80 34.94 2.00 o -2 1 1 3905.45 3559.91 35.17 o -1 1 1 10549.99 10256.04 88.13 o 0 1 1 1389.49 1546.15 18.68 o 1 1 1 37.32 47.13 3.20 o 2 1 1 10091.22 9859.79 92.18 o 3 1 1 2202.43 1962.98 24.50 o 4 1 1 44.26 37.63 3.82 o 5 1 1 1860.15 1751.96 28.73 o 6 1 1 346.16 357.67 9.14 o 7 1 1 1365.04 1418.31 28.21 o 8 1 1 59.45 55.20 5.56 o 9 1 1 2.15 11.50 4.22 o 10 1 1 176.21 180.90 10.44 o 11 1 1 131.20 128.44 7.62 o 12 1 1 52.10 41.02 11.67 o 13 1 1 130.59 111.09 10.93 o 14 1 1 257.44 256.42 12.89 o 15 1 1 26.11 41.35 9.45 o -15 2 1 0.09 0.00 7.49 o -14 2 1 60.05 69.49 9.01 o -13 2 1 156.92 152.27 11.92 o -12 2 1 1.75 0.00 4.15 o -11 2 1 264.95 218.69 12.25 o -10 2 1 121.90 128.19 9.58 o -9 2 1 142.53 160.26 11.24 o -8 2 1 453.73 555.45 19.37 o -7 2 1 144.35 138.33 10.04 o -6 2 1 0.75 6.18 3.21 o -5 2 1 62.05 64.20 6.43 o -4 2 1 366.59 358.66 8.61 o -3 2 1 3.27 16.95 2.91 o -2 2 1 106.46 109.89 4.79 o -1 2 1 612.11 629.01 19.97 o 0 2 1 0.39 0.00 1.43 o 1 2 1 69.06 49.36 2.85 o 2 2 1 82.61 107.22 4.09 o 3 2 1 0.07 3.33 1.59 o 4 2 1 13.85 16.27 1.92 o 5 2 1 2.26 4.22 2.55 o 6 2 1 16.32 12.60 2.55 o 7 2 1 110.09 102.69 5.24 o 8 2 1 36.06 53.91 7.90 o 9 2 1 211.16 186.49 11.16 o 10 2 1 53.43 65.50 7.13 o 11 2 1 99.49 97.91 8.36 o 12 2 1 17.09 28.79 6.05 o 13 2 1 4.16 8.14 7.98 o 14 2 1 14.45 18.28 7.05 o -12 3 1 3.13 6.92 5.44 o -11 3 1 3.33 13.57 10.35 o -10 3 1 0.60 5.25 4.70 o -9 3 1 10.89 26.00 5.74 o -8 3 1 44.89 51.72 6.07 o -7 3 1 61.71 67.19 6.70 o -6 3 1 22.91 26.38 4.02 o -5 3 1 1.37 4.76 3.07 o -4 3 1 119.89 98.03 12.48 o -3 3 1 95.42 86.94 6.13 o -2 3 1 0.02 0.59 2.76 o -1 3 1 17.01 17.34 3.25 o 0 3 1 46.17 36.91 4.20 o 1 3 1 0.15 2.67 2.52 o 2 3 1 7.43 6.95 2.63 o 3 3 1 59.55 47.17 4.35 o 4 3 1 0.08 7.15 3.21 o 5 3 1 254.97 293.30 13.76 o 6 3 1 193.69 187.66 11.55 o 7 3 1 142.01 128.42 10.29 o 8 3 1 57.00 50.82 7.00 o 9 3 1 89.39 94.59 9.83 o 10 3 1 12.29 12.59 5.84 o 11 3 1 41.23 52.52 8.57 o 12 3 1 25.48 54.51 9.56 o -8 4 1 154.96 164.12 14.16 o -7 4 1 51.44 57.28 9.36 o -6 4 1 0.21 0.00 4.96 o -5 4 1 9.08 22.12 6.67 o -4 4 1 13.30 14.08 6.08 o -3 4 1 3.04 8.34 4.75 o -2 4 1 8.08 5.22 4.35 o -1 4 1 0.55 5.28 4.37 o 0 4 1 0.44 0.00 4.91 o 1 4 1 21.61 40.06 5.86 o 2 4 1 5.57 8.66 6.07 o 3 4 1 14.42 21.65 6.28 o 4 4 1 1.28 3.67 8.45 o 5 4 1 65.39 64.51 9.27 o 6 4 1 45.20 53.19 8.24 o 7 4 1 7.36 15.27 7.45 o -17 0 2 78.70 94.25 15.58 o -16 0 2 163.14 177.13 17.06 o -15 0 2 49.30 80.45 13.06 o -14 0 2 223.86 166.44 12.09 o -13 0 2 29.95 31.00 5.22 o -12 0 2 289.24 233.99 11.40 o -11 0 2 241.00 215.64 10.20 o -10 0 2 17.94 21.87 6.12 o -9 0 2 217.51 203.60 8.31 o -8 0 2 240.43 150.42 7.16 o -7 0 2 2093.56 2202.90 42.52 o -6 0 2 26.82 36.08 2.84 o -5 0 2 933.23 875.41 48.01 o -4 0 2 9092.86 10575.87 185.55 o -3 0 2 1005.78 766.89 27.20 o 1 0 2 543.18 550.76 18.21 o 2 0 2 3.63 9.45 1.08 o 3 0 2 393.69 273.94 6.43 o 4 0 2 40.11 37.06 2.67 o 5 0 2 189.77 355.31 9.37 o 6 0 2 65.53 59.78 5.59 o 7 0 2 167.04 171.90 9.19 o 8 0 2 3632.81 3275.67 70.40 o 9 0 2 1.76 2.57 3.04 o 10 0 2 484.44 477.83 16.36 o 11 0 2 700.10 688.18 30.39 o 12 0 2 54.47 61.80 7.25 o 13 0 2 393.65 322.12 23.39 o 14 0 2 15.25 23.03 15.90 o 15 0 2 10.41 12.81 10.29 o -17 1 2 11.99 2.46 5.93 o -16 1 2 26.37 27.83 6.64 o -15 1 2 36.28 43.17 6.50 o -14 1 2 245.19 242.59 10.82 o -13 1 2 54.70 66.37 6.07 o -12 1 2 8.29 7.64 3.35 o -11 1 2 106.95 82.30 5.57 o -10 1 2 0.86 1.02 2.92 o -9 1 2 422.20 441.19 9.30 o -8 1 2 115.18 81.01 3.29 o -7 1 2 0.72 0.00 1.39 o -6 1 2 70.55 100.15 4.26 o -5 1 2 1903.00 1780.12 25.43 o -4 1 2 86.85 77.74 3.04 o -3 1 2 541.18 434.77 8.32 o -2 1 2 5484.50 5772.06 91.24 o -1 1 2 5681.03 6328.64 106.63 o 0 1 2 90.17 25.69 2.52 o 1 1 2 83.41 117.37 7.86 o 2 1 2 702.86 772.22 12.77 o 3 1 2 112.92 72.97 4.03 o 4 1 2 22.62 28.23 3.18 o 5 1 2 398.62 441.40 12.20 o 6 1 2 37.06 49.52 4.17 o 7 1 2 28.48 18.88 5.03 o 8 1 2 364.01 379.61 14.85 o 9 1 2 251.35 233.22 9.64 o 10 1 2 99.01 94.65 7.08 o 11 1 2 1.14 0.00 3.06 o 12 1 2 179.33 194.01 9.94 o 13 1 2 13.39 19.21 4.94 o 14 1 2 0.87 10.65 5.83 o 15 1 2 0.08 0.00 6.34 o -15 2 2 74.75 88.85 13.57 o -14 2 2 88.37 123.39 11.52 o -13 2 2 8.78 15.06 6.21 o -12 2 2 4.19 18.08 7.43 o -11 2 2 9.43 11.02 7.11 o -10 2 2 9.34 28.34 5.61 o -9 2 2 36.97 49.65 6.18 o -8 2 2 66.53 88.21 6.58 o -7 2 2 331.86 329.22 9.09 o -6 2 2 181.08 194.07 6.62 o -5 2 2 452.75 392.49 10.27 o -4 2 2 0.11 1.66 1.57 o -3 2 2 1492.66 1462.47 23.73 o -2 2 2 947.30 831.62 14.40 o -1 2 2 315.04 265.12 6.52 o 0 2 2 254.54 334.55 7.45 o 1 2 2 265.94 385.63 15.86 o 2 2 2 166.51 125.91 4.06 o 3 2 2 0.24 7.71 3.44 o 4 2 2 278.94 292.95 7.91 o 5 2 2 10.08 16.68 2.81 o 6 2 2 179.10 194.66 7.56 o 7 2 2 537.44 536.60 15.25 o 8 2 2 4.31 0.97 2.52 o 9 2 2 1.10 6.34 4.96 o 10 2 2 12.59 24.16 5.22 o 11 2 2 28.96 45.07 7.18 o 12 2 2 164.85 172.26 13.01 o 13 2 2 52.75 49.93 8.59 o 14 2 2 0.29 0.55 5.60 o -13 3 2 81.97 92.19 11.14 o -12 3 2 135.69 142.11 25.76 o -11 3 2 155.41 160.12 20.88 o -10 3 2 236.01 208.50 14.58 o -9 3 2 290.86 245.63 14.07 o -8 3 2 77.58 75.54 8.12 o -7 3 2 16.71 28.02 5.22 o -6 3 2 23.45 29.68 8.87 o -5 3 2 1.25 2.95 2.87 o -4 3 2 0.01 2.83 3.37 o -3 3 2 482.46 462.64 17.29 o -2 3 2 39.42 32.82 3.80 o -1 3 2 27.73 34.84 3.94 o 0 3 2 3.73 0.49 3.16 o 1 3 2 6.54 7.65 3.53 o 2 3 2 19.10 25.55 3.30 o 3 3 2 0.08 3.94 5.03 o 4 3 2 0.12 0.00 3.10 o 5 3 2 28.29 34.19 6.11 o 6 3 2 8.35 15.61 6.47 o 7 3 2 17.36 21.91 5.22 o 8 3 2 82.68 82.80 8.41 o 9 3 2 70.17 64.69 8.03 o 10 3 2 7.54 13.85 7.42 o 11 3 2 131.68 122.30 17.13 o -8 4 2 62.39 63.87 9.56 o -7 4 2 2.53 4.19 5.80 o -6 4 2 1.67 0.91 6.56 o -5 4 2 0.06 0.00 4.82 o -4 4 2 14.73 20.32 5.84 o -3 4 2 0.33 0.00 3.88 o -2 4 2 75.06 75.00 9.09 o -1 4 2 13.08 22.16 5.37 o 0 4 2 4.51 0.00 5.14 o 1 4 2 123.69 125.39 13.70 o 2 4 2 4.68 11.06 4.63 o 3 4 2 26.48 44.41 7.71 o 4 4 2 70.58 53.75 8.60 o 5 4 2 11.18 21.27 6.52 o 6 4 2 53.21 58.45 14.06 o -17 1 3 19.18 8.42 5.79 o -16 1 3 5.51 9.11 7.64 o -15 1 3 314.29 333.75 20.01 o -14 1 3 121.63 145.60 11.73 o -13 1 3 0.02 2.00 2.85 o -12 1 3 113.62 118.50 8.14 o -11 1 3 340.64 305.64 12.40 o -10 1 3 96.68 83.49 3.89 o -9 1 3 1998.81 2243.16 41.61 o -8 1 3 14.73 55.86 2.78 o -7 1 3 250.48 232.61 9.19 o -6 1 3 329.06 374.81 10.90 o -5 1 3 10.23 85.71 3.32 o -4 1 3 22.25 18.93 1.93 o -3 1 3 393.00 364.86 7.42 o -2 1 3 22449.23 21171.29 219.10 o -1 1 3 2277.50 2652.51 32.60 o 0 1 3 2499.76 2834.29 35.42 o 1 1 3 72.00 48.76 5.52 o 2 1 3 10.60 9.94 2.12 o 3 1 3 558.14 527.12 10.34 o 4 1 3 677.20 692.74 40.36 o 5 1 3 164.41 118.75 4.95 o 6 1 3 656.10 891.65 23.10 o 7 1 3 350.25 411.35 12.61 o 8 1 3 49.57 57.32 5.15 o 9 1 3 11.22 6.53 3.17 o 10 1 3 885.53 884.80 24.86 o 11 1 3 689.82 641.43 20.22 o 12 1 3 148.68 143.05 8.85 o 13 1 3 0.00 0.00 4.21 o 14 1 3 21.22 22.61 6.87 o -16 2 3 28.53 32.64 10.97 o -15 2 3 122.67 97.74 12.72 o -14 2 3 21.38 20.89 6.10 o -13 2 3 3.86 11.03 5.48 o -12 2 3 152.22 161.58 11.33 o -11 2 3 425.99 423.47 18.28 o -10 2 3 9.50 0.00 5.86 o -9 2 3 120.80 117.50 5.55 o -8 2 3 90.15 92.11 4.59 o -7 2 3 0.07 0.94 2.38 o -6 2 3 134.28 131.92 6.22 o -5 2 3 328.69 309.83 12.63 o -4 2 3 148.90 153.89 5.30 o -3 2 3 5503.13 5826.91 76.62 o -2 2 3 8.09 2.72 1.75 o -1 2 3 84.01 117.16 4.29 o 0 2 3 973.81 987.68 17.58 o 1 2 3 7.00 0.00 1.24 o 2 2 3 0.43 3.95 2.16 o 3 2 3 14.04 12.27 2.10 o 4 2 3 38.15 43.27 4.16 o 5 2 3 141.94 144.33 7.27 o 6 2 3 5.72 3.66 2.86 o 7 2 3 23.71 21.99 5.72 o 8 2 3 43.12 46.19 4.73 o 9 2 3 107.26 82.42 9.01 o 10 2 3 473.83 511.69 23.42 o 11 2 3 9.27 14.13 5.91 o 12 2 3 74.03 66.19 7.92 o 13 2 3 46.01 45.34 8.81 o -13 3 3 3.36 4.00 5.96 o -12 3 3 1.22 14.10 8.72 o -11 3 3 65.69 80.08 9.27 o -10 3 3 136.12 134.80 10.74 o -9 3 3 73.72 87.56 8.54 o -8 3 3 31.48 40.99 6.58 o -7 3 3 57.43 46.16 4.71 o -6 3 3 7.06 10.52 3.82 o -5 3 3 13.95 10.34 3.56 o -4 3 3 226.15 208.24 11.14 o -3 3 3 5.94 1.19 2.27 o -2 3 3 3.64 4.36 4.57 o -1 3 3 16.50 22.61 3.14 o 0 3 3 65.05 61.85 4.21 o 1 3 3 39.51 40.00 4.59 o 2 3 3 43.87 41.89 4.74 o 3 3 3 83.24 88.92 5.41 o 4 3 3 219.66 208.35 10.83 o 5 3 3 74.13 81.97 8.29 o 6 3 3 17.39 14.62 5.60 o 7 3 3 14.84 23.90 6.75 o 8 3 3 15.14 19.38 6.30 o 9 3 3 7.94 2.18 5.39 o 10 3 3 10.72 11.78 6.57 o 11 3 3 11.73 18.37 7.68 o -8 4 3 0.02 0.00 5.61 o -7 4 3 6.20 18.23 9.40 o -6 4 3 2.22 2.90 5.22 o -5 4 3 11.17 6.88 7.38 o -4 4 3 54.84 49.51 6.73 o -3 4 3 140.61 122.48 10.11 o -2 4 3 0.01 4.59 4.44 o -1 4 3 0.61 6.03 5.41 o 0 4 3 86.38 85.95 9.17 o 1 4 3 13.69 13.03 6.57 o 2 4 3 1.73 5.89 5.14 o 3 4 3 52.38 53.43 8.25 o 4 4 3 17.29 20.61 6.96 o 5 4 3 9.83 16.30 10.52 o 6 4 3 22.46 22.26 7.78 o -18 0 4 0.46 0.00 6.83 o -17 0 4 36.65 64.35 11.97 o -16 0 4 380.21 359.97 33.19 o -15 0 4 46.61 42.42 6.62 o -14 0 4 29.21 24.88 4.98 o -13 0 4 995.72 933.72 30.37 o -12 0 4 82.85 82.17 7.24 o -11 0 4 175.96 250.73 10.73 o -10 0 4 1790.79 2204.16 51.98 o -9 0 4 115.59 76.96 7.65 o -8 0 4 106.15 81.07 6.25 o -7 0 4 3912.81 4169.45 80.37 o -6 0 4 710.35 800.41 18.90 o -5 0 4 956.63 801.75 15.87 o -4 0 4 1813.43 1563.02 31.46 o -3 0 4 420.34 331.73 10.23 o -2 0 4 9400.02 7986.76 75.88 o -1 0 4 385.75 328.33 13.00 o 0 0 4 5084.87 4595.29 57.87 o 1 0 4 4436.30 4814.44 86.30 o 2 0 4 9.51 18.59 3.61 o 3 0 4 99.70 53.43 3.37 o 4 0 4 1098.70 1432.98 48.44 o 5 0 4 2697.17 3072.48 61.65 o 6 0 4 1710.95 1816.43 41.13 o 7 0 4 193.41 204.32 8.79 o 8 0 4 227.82 220.04 9.61 o 9 0 4 59.02 102.26 7.39 o 10 0 4 281.16 222.39 15.52 o 11 0 4 174.13 183.90 18.82 o 12 0 4 85.05 95.31 18.93 o 13 0 4 153.97 184.37 18.99 o 14 0 4 0.03 12.33 9.31 o -17 1 4 29.81 40.06 9.50 o -16 1 4 34.42 36.92 7.31 o -15 1 4 0.75 0.00 4.10 o -14 1 4 74.50 54.45 5.42 o -13 1 4 4.46 6.33 3.28 o -12 1 4 136.36 125.77 5.33 o -11 1 4 211.97 242.53 7.27 o -10 1 4 258.52 324.26 13.94 o -9 1 4 34.45 39.20 2.63 o -8 1 4 1.35 0.00 1.27 o -7 1 4 6.82 18.69 1.80 o -6 1 4 1608.06 1667.90 19.47 o -5 1 4 169.74 203.60 3.58 o -4 1 4 382.46 493.71 8.97 o -3 1 4 351.21 318.24 5.54 o -2 1 4 1203.99 1470.24 17.57 o -1 1 4 429.36 484.13 7.37 o 0 1 4 672.12 802.16 12.73 o 1 1 4 38.40 18.63 1.70 o 2 1 4 117.24 102.56 3.11 o 3 1 4 419.45 507.20 8.24 o 4 1 4 19.44 12.28 1.53 o 5 1 4 265.89 265.13 9.94 o 6 1 4 592.80 648.23 28.61 o 7 1 4 130.15 139.68 7.08 o 8 1 4 132.79 160.31 8.31 o 9 1 4 19.21 19.74 4.30 o 10 1 4 520.40 478.84 16.26 o 11 1 4 20.74 24.77 5.60 o 12 1 4 5.54 9.08 4.59 o 13 1 4 15.12 12.81 10.23 o 14 1 4 29.74 35.36 10.09 o -16 2 4 33.14 22.51 7.67 o -15 2 4 110.30 99.78 10.41 o -14 2 4 95.03 106.01 9.46 o -13 2 4 258.62 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