#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222092.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222092_Fobs loop_ _publ_author_name 'Meng, Lin' 'Yang, Lin Yan' 'Shi, Jing Min' _publ_section_title ; Tetra-\m-acetato-\k^8^O:O'-bis[(N^2^,N^2^-dimethylpyrazin-2-amine-\kN^4^)copper(II)] ; _journal_coeditor_code LH2807 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m646 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 67.826 _cell_angle_beta 80.013 _cell_angle_gamma 87.328 _cell_length_a 8.1052 _cell_length_b 8.1775 _cell_length_c 10.6534 _exptl_crystal_F_000 314.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file lh2807Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 90106em in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2831.07 3064.96 56.83 o 2 0 0 96.92 116.09 1.97 o 3 0 0 43.34 59.77 1.46 o 4 0 0 87.32 107.27 2.45 o 5 0 0 217.38 200.12 4.54 o 6 0 0 885.74 947.08 18.21 o 7 0 0 117.71 107.87 4.86 o 8 0 0 18.69 16.44 2.20 o 9 0 0 146.60 152.41 6.64 o -9 1 0 187.11 199.82 8.13 o -8 1 0 303.97 309.72 10.63 o -7 1 0 176.14 173.01 6.67 o -6 1 0 114.39 107.99 4.58 o -5 1 0 168.59 168.11 3.16 o -4 1 0 160.25 162.15 2.95 o -3 1 0 4736.26 5148.37 75.92 o -2 1 0 5570.97 5774.87 85.33 o -1 1 0 3882.37 4164.28 75.07 o 0 1 0 4516.80 4758.21 92.69 o 1 1 0 817.27 924.05 17.01 o 2 1 0 835.20 999.43 26.16 o 3 1 0 229.49 233.31 6.85 o 4 1 0 4.93 9.00 1.04 o 5 1 0 748.54 761.05 20.72 o 6 1 0 1151.13 1207.86 22.94 o 7 1 0 463.67 487.72 10.23 o 8 1 0 4.00 4.61 1.60 o 9 1 0 22.59 20.58 2.57 o -9 2 0 300.85 326.02 11.55 o -8 2 0 496.06 479.79 15.14 o -7 2 0 51.17 55.00 3.50 o -6 2 0 15.56 16.93 1.97 o -5 2 0 186.41 176.78 4.32 o -4 2 0 2853.02 3124.90 46.36 o -3 2 0 5357.48 5781.93 118.96 o -2 2 0 967.92 976.95 18.13 o -1 2 0 15.49 9.70 0.42 o 0 2 0 1761.41 2021.20 36.74 o 1 2 0 2327.42 2614.22 67.52 o 2 2 0 140.38 148.73 3.11 o 3 2 0 318.47 290.23 8.47 o 4 2 0 356.26 327.22 9.68 o 5 2 0 962.10 992.57 26.85 o 6 2 0 1092.48 1087.78 29.51 o 7 2 0 410.41 399.42 12.22 o 8 2 0 9.16 7.95 1.27 o 9 2 0 10.78 11.48 2.18 o -9 3 0 111.69 107.08 5.79 o -8 3 0 35.88 39.68 3.45 o -7 3 0 52.60 48.76 2.33 o -6 3 0 279.22 280.68 9.93 o -5 3 0 226.58 243.27 5.70 o -4 3 0 624.54 627.35 12.42 o -3 3 0 1785.77 1789.36 33.01 o -2 3 0 370.94 320.74 11.18 o -1 3 0 172.95 174.25 4.12 o 0 3 0 66.73 76.89 2.13 o 1 3 0 321.53 327.66 9.10 o 2 3 0 214.54 221.10 4.61 o 3 3 0 2589.59 2740.53 49.88 o 4 3 0 828.92 834.40 22.85 o 5 3 0 590.21 567.11 16.30 o 6 3 0 525.30 507.94 15.05 o 7 3 0 2.42 1.48 1.48 o 8 3 0 11.31 12.27 2.20 o 9 3 0 78.46 78.18 3.66 o -8 4 0 8.28 6.97 2.11 o -7 4 0 123.32 113.58 3.79 o -6 4 0 177.13 171.47 4.72 o -5 4 0 6.05 4.62 1.00 o -4 4 0 218.29 204.31 4.98 o -3 4 0 548.21 550.23 11.05 o -2 4 0 683.93 722.01 20.43 o -1 4 0 83.72 88.32 2.36 o 0 4 0 191.98 191.74 4.28 o 1 4 0 417.81 482.24 9.51 o 2 4 0 1337.57 1456.11 27.00 o 3 4 0 3489.77 3656.06 66.44 o 4 4 0 1013.71 981.44 26.92 o 5 4 0 91.15 84.65 4.19 o 6 4 0 6.27 5.67 1.74 o 7 4 0 21.25 14.21 2.27 o 8 4 0 58.08 57.32 4.07 o -8 5 0 10.16 11.13 2.34 o -7 5 0 53.71 52.09 2.66 o -6 5 0 108.34 109.48 6.78 o -5 5 0 442.76 440.97 10.46 o -4 5 0 137.41 133.15 3.83 o -3 5 0 8.79 8.54 1.71 o -2 5 0 7.96 9.65 1.69 o -1 5 0 455.84 507.59 10.16 o 0 5 0 228.91 207.27 4.78 o 1 5 0 777.45 829.47 15.97 o 2 5 0 1910.83 2090.90 109.94 o 3 5 0 640.43 644.59 18.43 o 4 5 0 311.84 287.36 9.54 o 5 5 0 28.22 22.94 2.48 o 6 5 0 194.47 178.29 7.13 o 7 5 0 44.43 47.85 3.82 o 8 5 0 227.58 219.84 8.75 o -7 6 0 63.97 65.12 4.28 o -6 6 0 283.34 264.68 6.83 o -5 6 0 331.41 305.10 7.42 o -4 6 0 0.50 1.02 1.57 o -3 6 0 0.65 0.00 1.39 o -2 6 0 273.93 268.77 9.12 o -1 6 0 427.36 401.54 8.49 o 0 6 0 959.20 992.87 19.11 o 1 6 0 548.11 529.95 40.05 o 2 6 0 225.47 227.53 8.38 o 3 6 0 1.97 0.00 1.30 o 4 6 0 22.61 19.19 2.38 o 5 6 0 55.18 50.51 3.70 o 6 6 0 93.52 94.79 5.30 o 7 6 0 83.76 87.29 5.21 o -6 7 0 104.55 94.84 5.76 o -5 7 0 2.45 0.58 1.94 o -4 7 0 8.03 9.58 2.27 o -3 7 0 43.03 42.85 3.47 o -2 7 0 232.61 207.04 7.82 o -1 7 0 499.68 470.26 14.38 o 0 7 0 465.65 467.96 9.89 o 1 7 0 32.91 39.80 2.05 o 2 7 0 12.73 8.06 1.85 o 3 7 0 19.44 17.01 2.41 o 4 7 0 82.80 76.57 4.54 o 5 7 0 117.65 118.06 5.95 o 6 7 0 58.56 52.59 4.26 o -5 8 0 19.04 18.50 3.15 o -4 8 0 78.62 80.83 5.14 o -3 8 0 110.45 108.43 5.72 o -2 8 0 23.84 24.40 2.85 o -1 8 0 98.30 94.44 4.88 o 0 8 0 55.94 60.14 3.80 o 1 8 0 23.07 24.21 1.83 o 2 8 0 82.00 81.02 4.56 o 3 8 0 15.27 13.15 2.41 o 4 8 0 51.70 48.26 3.98 o -2 9 0 19.41 20.88 2.92 o -1 9 0 1.43 2.38 1.99 o 0 9 0 20.78 24.38 2.94 o 0 -9 1 23.68 22.06 2.87 o 1 -9 1 28.39 26.41 3.13 o -4 -8 1 54.73 60.69 4.63 o -3 -8 1 60.80 59.58 4.21 o -2 -8 1 25.01 27.52 2.92 o -1 -8 1 199.86 196.64 7.55 o 0 -8 1 10.23 14.86 2.50 o 1 -8 1 5.56 5.51 2.04 o 2 -8 1 24.71 27.89 3.06 o 3 -8 1 183.23 185.53 7.94 o 4 -8 1 198.01 191.32 8.36 o -5 -7 1 116.77 110.16 5.88 o -4 -7 1 181.13 173.03 7.34 o -3 -7 1 90.23 93.54 4.88 o -2 -7 1 265.95 259.33 9.17 o -1 -7 1 2.18 2.31 1.13 o 0 -7 1 117.58 120.82 4.27 o 1 -7 1 451.80 443.08 13.82 o 2 -7 1 330.27 306.00 10.53 o 3 -7 1 91.40 93.43 5.12 o 4 -7 1 168.69 169.89 7.48 o 5 -7 1 22.83 21.57 3.06 o 6 -7 1 1.07 0.00 2.01 o -6 -6 1 90.91 84.70 5.12 o -5 -6 1 237.14 224.49 8.61 o -4 -6 1 328.12 324.79 10.95 o -3 -6 1 33.21 29.12 2.69 o -2 -6 1 5.73 3.13 1.44 o -1 -6 1 277.65 262.20 6.09 o 0 -6 1 751.88 753.40 14.91 o 1 -6 1 1057.92 1053.99 26.06 o 2 -6 1 482.01 466.51 14.31 o 3 -6 1 46.32 42.27 3.36 o 4 -6 1 3.51 5.37 1.92 o 5 -6 1 40.10 39.17 3.59 o 6 -6 1 22.67 22.57 2.42 o 7 -6 1 53.13 50.51 2.84 o -7 -5 1 290.78 262.80 9.81 o -6 -5 1 114.42 104.05 5.30 o -5 -5 1 110.36 91.94 4.72 o -4 -5 1 7.05 9.21 1.88 o -3 -5 1 106.75 106.64 4.79 o -2 -5 1 399.92 433.38 23.94 o -1 -5 1 404.12 446.92 11.16 o 0 -5 1 1088.25 1111.04 21.09 o 1 -5 1 413.48 379.87 13.74 o 2 -5 1 572.52 569.84 11.36 o 3 -5 1 107.14 89.21 4.40 o 4 -5 1 2.67 4.31 1.69 o 5 -5 1 6.63 4.76 1.41 o 6 -5 1 362.99 342.26 8.16 o 7 -5 1 155.59 159.07 4.92 o 8 -5 1 88.59 100.58 5.46 o -8 -4 1 184.64 173.84 7.34 o -7 -4 1 297.84 272.64 9.70 o -6 -4 1 27.04 28.01 2.69 o -5 -4 1 2.99 1.99 1.50 o -4 -4 1 195.65 225.63 7.82 o -3 -4 1 177.69 184.40 6.55 o -2 -4 1 1660.18 1827.04 51.25 o -1 -4 1 1544.23 1570.80 29.13 o 0 -4 1 132.72 104.50 2.76 o 1 -4 1 156.71 135.81 3.51 o 2 -4 1 247.37 249.36 5.34 o 3 -4 1 113.51 113.09 3.25 o 4 -4 1 23.15 19.29 1.39 o 5 -4 1 569.98 554.15 11.57 o 6 -4 1 192.19 186.27 5.06 o 7 -4 1 340.40 319.95 7.68 o 8 -4 1 190.79 175.79 7.29 o -8 -3 1 63.60 66.55 4.14 o -7 -3 1 5.56 3.98 1.74 o -6 -3 1 196.91 178.13 6.64 o -5 -3 1 1.22 0.74 1.16 o -4 -3 1 443.66 473.52 13.84 o -3 -3 1 1186.30 1263.86 23.44 o -2 -3 1 2420.40 2589.40 49.04 o -1 -3 1 779.38 738.19 18.24 o 0 -3 1 152.82 134.21 3.12 o 1 -3 1 460.41 532.73 18.48 o 2 -3 1 277.93 273.68 8.43 o 3 -3 1 272.86 274.03 9.05 o 4 -3 1 507.23 498.18 10.17 o 5 -3 1 1358.63 1358.45 25.72 o 6 -3 1 201.55 193.29 7.15 o 7 -3 1 374.90 375.99 8.51 o 8 -3 1 90.35 84.28 4.65 o 9 -3 1 0.65 0.97 1.44 o -9 -2 1 131.85 126.23 6.02 o -8 -2 1 44.39 42.36 2.26 o -7 -2 1 31.37 28.98 2.50 o -6 -2 1 2.21 1.92 1.25 o -5 -2 1 192.60 163.38 5.74 o -4 -2 1 301.78 263.22 8.17 o -3 -2 1 1780.24 1923.76 50.23 o -2 -2 1 217.50 174.63 3.68 o -1 -2 1 314.66 303.43 9.65 o 0 -2 1 1365.75 1311.00 37.60 o 1 -2 1 83.20 105.95 3.66 o 2 -2 1 1403.72 1460.04 26.85 o 3 -2 1 5515.57 5987.46 107.86 o 4 -2 1 2449.60 2617.02 38.98 o 5 -2 1 948.77 993.79 19.02 o 6 -2 1 350.10 336.92 10.29 o 7 -2 1 1.48 0.00 1.02 o 8 -2 1 0.36 0.00 1.20 o 9 -2 1 75.97 78.57 4.72 o -9 -1 1 63.43 54.68 3.87 o -8 -1 1 53.23 50.16 3.43 o -7 -1 1 8.71 7.46 1.68 o -6 -1 1 838.61 766.05 21.13 o -5 -1 1 312.44 303.66 9.10 o -4 -1 1 538.47 505.93 14.07 o -3 -1 1 462.03 467.69 8.87 o -2 -1 1 1209.37 1268.40 23.24 o -1 -1 1 5.52 5.30 0.53 o 0 -1 1 300.60 359.98 9.68 o 1 -1 1 1586.37 1600.45 29.06 o 2 -1 1 3156.61 3265.45 48.24 o 3 -1 1 4618.21 4863.66 71.68 o 4 -1 1 3953.95 4283.52 74.08 o 5 -1 1 31.24 24.47 1.00 o 6 -1 1 5.34 5.39 0.87 o 7 -1 1 30.61 33.82 2.73 o 8 -1 1 119.31 112.34 5.37 o 9 -1 1 194.03 193.40 7.96 o -9 0 1 5.41 2.31 1.67 o -8 0 1 1.82 1.23 1.41 o -7 0 1 9.24 9.38 1.69 o -6 0 1 951.19 1052.18 28.17 o -5 0 1 1443.21 1575.01 23.74 o -4 0 1 987.10 1038.51 19.18 o -3 0 1 539.96 523.51 9.83 o -2 0 1 68.19 83.83 1.86 o -1 0 1 4019.68 4243.29 109.47 o 0 0 1 1343.20 1409.10 36.39 o 1 0 1 9543.06 8639.85 128.48 o 2 0 1 2207.65 2226.33 32.97 o 3 0 1 34.42 23.77 0.89 o 4 0 1 502.99 545.94 8.56 o 5 0 1 17.48 23.69 0.99 o 6 0 1 34.30 32.33 1.68 o 7 0 1 35.28 34.58 2.71 o 8 0 1 377.87 384.45 12.43 o 9 0 1 126.38 146.71 6.57 o -9 1 1 29.65 29.65 3.08 o -8 1 1 57.58 59.17 3.80 o -7 1 1 143.03 146.25 6.02 o -6 1 1 972.92 1070.58 29.26 o -5 1 1 1256.44 1375.01 20.84 o -4 1 1 56.31 85.88 2.57 o -3 1 1 233.84 254.63 4.17 o -2 1 1 1142.82 1251.16 18.67 o -1 1 1 695.61 724.87 13.28 o 0 1 1 7008.96 6823.23 332.17 o 1 1 1 5288.93 5559.93 114.55 o 2 1 1 26.76 18.44 1.81 o 3 1 1 8.16 5.50 0.87 o 4 1 1 458.73 546.98 10.68 o 5 1 1 16.78 28.24 1.44 o 6 1 1 391.94 428.27 8.94 o 7 1 1 328.98 357.20 11.30 o 8 1 1 178.89 185.95 7.18 o 9 1 1 129.47 135.83 6.11 o -9 2 1 210.68 223.91 9.00 o -8 2 1 188.55 211.92 8.33 o -7 2 1 589.73 566.88 17.04 o -6 2 1 136.45 139.74 4.05 o -5 2 1 35.70 30.95 1.55 o -4 2 1 72.86 54.77 1.51 o -3 2 1 649.29 651.31 12.44 o -2 2 1 3.17 4.61 0.47 o -1 2 1 430.06 366.76 5.71 o 0 2 1 5774.40 5905.26 106.76 o 1 2 1 5.79 5.16 0.51 o 2 2 1 37.60 37.31 2.56 o 3 2 1 3.91 5.42 0.93 o 4 2 1 103.53 98.80 3.77 o 5 2 1 214.05 219.54 7.13 o 6 2 1 968.15 978.89 26.78 o 7 2 1 1019.54 1037.23 20.19 o 8 2 1 125.49 129.07 3.94 o 9 2 1 84.20 86.69 4.77 o -9 3 1 220.80 232.99 9.24 o -8 3 1 298.82 312.02 11.02 o -7 3 1 185.26 179.79 7.13 o -6 3 1 4.79 7.01 1.06 o -5 3 1 1.45 1.99 0.76 o -4 3 1 1.11 4.01 2.48 o -3 3 1 1954.91 2064.22 37.84 o -2 3 1 597.32 543.88 10.51 o -1 3 1 58.33 45.12 1.07 o 0 3 1 9.39 24.75 0.96 o 1 3 1 106.31 98.19 2.33 o 2 3 1 209.03 210.45 4.35 o 3 3 1 86.80 82.80 3.45 o 4 3 1 255.78 240.49 7.66 o 5 3 1 1084.90 1042.51 28.33 o 6 3 1 859.57 843.62 23.54 o 7 3 1 1018.50 1009.06 28.08 o 8 3 1 42.37 44.43 3.60 o 9 3 1 18.10 16.55 1.94 o -8 4 1 124.87 121.95 6.02 o -7 4 1 6.17 5.41 1.25 o -6 4 1 30.49 28.12 1.82 o -5 4 1 90.20 80.80 2.80 o -4 4 1 74.01 65.55 4.77 o -3 4 1 564.65 570.94 11.35 o -2 4 1 1520.51 1540.37 23.18 o -1 4 1 600.29 611.75 11.73 o 0 4 1 69.65 61.68 1.83 o 1 4 1 3.43 6.61 1.48 o 2 4 1 100.21 94.87 2.45 o 3 4 1 660.29 664.03 12.73 o 4 4 1 1830.92 1844.25 48.84 o 5 4 1 694.56 654.59 18.77 o 6 4 1 243.41 240.93 8.33 o 7 4 1 0.81 3.70 1.69 o 8 4 1 0.09 0.21 1.81 o 9 4 1 49.73 47.78 2.99 o -8 5 1 6.97 6.37 2.01 o -7 5 1 13.17 12.86 1.62 o -6 5 1 60.74 58.76 2.65 o -5 5 1 4.86 6.68 1.12 o -4 5 1 369.92 361.11 13.31 o -3 5 1 440.16 425.78 8.93 o -2 5 1 974.71 982.00 26.76 o -1 5 1 890.05 885.74 16.88 o 0 5 1 37.85 33.54 1.50 o 1 5 1 427.27 429.47 8.71 o 2 5 1 1029.46 1022.17 19.34 o 3 5 1 1499.23 1560.73 41.71 o 4 5 1 604.74 624.29 18.10 o 5 5 1 45.69 46.64 3.33 o 6 5 1 14.06 13.47 2.20 o 7 5 1 180.99 164.51 6.94 o 8 5 1 0.38 0.00 1.99 o -7 6 1 46.78 44.71 2.62 o -6 6 1 148.39 147.36 4.60 o -5 6 1 98.17 87.33 3.20 o -4 6 1 831.78 815.82 39.62 o -3 6 1 274.99 260.51 9.00 o -2 6 1 24.55 21.41 2.29 o -1 6 1 102.08 106.13 4.61 o 0 6 1 293.59 297.07 6.76 o 1 6 1 204.99 204.05 5.00 o 2 6 1 502.80 543.75 17.70 o 3 6 1 283.15 281.11 9.40 o 4 6 1 1.38 0.00 1.44 o 5 6 1 7.09 6.34 1.90 o 6 6 1 14.73 13.75 2.48 o 7 6 1 13.12 11.25 2.34 o -6 7 1 217.63 207.93 9.80 o -5 7 1 497.15 452.13 14.88 o -4 7 1 42.08 32.43 3.19 o -3 7 1 2.76 1.50 1.74 o -2 7 1 115.46 113.31 5.23 o -1 7 1 311.11 294.75 9.79 o 0 7 1 76.94 80.38 3.84 o 1 7 1 86.06 92.83 6.32 o 2 7 1 30.24 37.50 2.94 o 3 7 1 45.14 46.74 3.40 o 4 7 1 8.58 9.17 2.15 o 5 7 1 1.27 1.16 1.78 o 6 7 1 20.66 17.41 2.75 o -5 8 1 40.35 36.02 3.73 o -4 8 1 35.72 40.23 3.80 o -3 8 1 1.65 2.41 2.04 o -2 8 1 11.58 10.76 2.25 o -1 8 1 64.12 67.69 4.10 o 0 8 1 127.73 137.34 5.86 o 1 8 1 116.59 124.84 3.90 o 2 8 1 68.81 66.30 4.14 o 3 8 1 5.40 6.92 2.04 o 4 8 1 0.07 2.04 1.90 o 5 8 1 51.81 53.31 4.24 o -3 9 1 17.82 19.40 3.08 o -2 9 1 1.82 2.57 2.01 o -1 9 1 74.34 84.19 4.93 o 0 9 1 165.83 175.05 7.27 o 3 9 1 18.49 16.53 2.82 o -3 -8 2 39.95 41.81 3.80 o -2 -8 2 175.48 179.35 7.50 o -1 -8 2 42.10 47.55 3.80 o 0 -8 2 83.72 89.01 4.91 o 1 -8 2 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61.69 2.90 o 4 5 11 0.44 0.95 1.23 o 5 5 11 76.73 79.51 3.43 o 6 5 11 162.76 163.43 7.73 o -3 6 11 19.08 22.66 2.96 o -2 6 11 145.22 139.14 6.44 o -1 6 11 99.49 110.16 5.53 o 0 6 11 116.08 115.79 5.67 o 1 6 11 55.84 58.73 2.81 o 2 6 11 15.60 14.02 1.70 o 3 6 11 6.26 4.49 1.99 o 4 6 11 55.17 52.55 4.17 o 5 6 11 147.38 148.98 7.27 o -2 7 11 84.09 89.35 5.16 o -1 7 11 69.22 66.04 4.31 o 0 7 11 31.69 27.78 3.06 o 1 7 11 1.19 0.12 1.23 o 2 7 11 1.67 2.53 1.37 o 3 7 11 110.88 108.08 3.98 o 4 7 11 119.25 119.93 6.39 o 0 8 11 3.03 0.86 1.97 o 1 8 11 11.25 13.29 2.52 o 2 8 11 65.79 69.15 3.17 o 3 8 11 71.86 72.51 4.90 o 1 0 12 111.11 99.03 5.74 o 2 0 12 85.14 77.13 5.09 o 3 0 12 37.72 37.11 3.68 o -1 1 12 123.81 111.99 6.13 o 0 1 12 118.46 109.03 5.90 o 1 1 12 96.21 95.09 5.49 o 2 1 12 10.54 11.76 2.55 o 3 1 12 8.61 6.81 2.29 o 4 1 12 12.80 11.02 2.52 o -2 2 12 115.25 156.00 8.43 o -1 2 12 84.15 98.15 6.06 o 0 2 12 133.06 144.54 7.04 o 1 2 12 48.42 51.20 4.12 o 2 2 12 8.26 8.59 2.34 o 3 2 12 169.63 157.25 7.18 o 4 2 12 58.01 59.19 4.33 o 5 2 12 49.55 55.35 4.26 o -2 3 12 91.74 181.92 11.06 o -1 3 12 88.65 117.71 7.38 o 0 3 12 12.72 14.51 3.10 o 1 3 12 24.27 28.17 3.43 o 2 3 12 21.95 24.33 3.08 o 3 3 12 133.75 144.63 6.78 o 4 3 12 99.68 97.71 5.44 o 5 3 12 77.77 86.07 3.77 o -2 4 12 159.29 835.65 40.25 o -1 4 12 31.26 63.84 7.27 o 0 4 12 21.33 25.23 4.10 o 1 4 12 30.44 35.46 3.87 o 2 4 12 79.08 86.55 5.21 o 3 4 12 16.14 17.22 2.75 o 4 4 12 154.81 147.50 7.85 o 5 4 12 55.36 56.99 3.12 o -2 5 12 60.72 59.17 4.35 o -1 5 12 2.13 2.55 2.01 o 1 5 12 151.16 204.17 9.24 o 2 5 12 56.39 64.91 4.70 o 3 5 12 42.15 41.17 2.63 o 4 5 12 85.22 82.90 3.56 o 5 5 12 11.41 9.92 1.76 o -1 6 12 9.30 11.50 2.50 o 0 6 12 48.59 46.76 3.91 o 1 6 12 193.52 177.55 7.52 o 2 6 12 75.66 78.22 4.79 o 3 6 12 48.98 47.74 3.30 o 4 6 12 5.95 5.23 1.55 o 0 7 12 71.54 72.73 4.72 o 1 7 12 95.87 99.86 8.85 o 2 7 12 27.81 29.68 4.75 o 3 7 12 1.67 1.37 2.01 o 1 3 13 140.23 162.89 7.94 o 2 3 13 55.64 56.94 4.58 o 1 4 13 52.46 59.12 5.09 o 2 4 13 7.55 7.45 2.75 o 3 4 13 93.36 97.11 5.74 o 2 5 13 17.24 19.68 3.40 o