#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222103.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222103_Fobs loop_ _publ_author_name 'Gabro, Milad' 'Lalancette, Roger A.' 'Bernal, Ivan' _publ_section_title ; Ethylenediammonium dichloride ; _journal_coeditor_code LH2823 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1352 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.192 _cell_angle_gamma 90.000 _cell_length_a 4.3807 _cell_length_b 6.8569 _cell_length_c 9.9464 _exptl_crystal_F_000 140.00 _reflns_d_resolution_high 0.8329 _[local]_cod_data_source_file lh2823Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 102307MG in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 70.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 999.45 1110.08 35.20 o 3 0 0 3.47 5.93 0.32 o 4 0 0 444.95 477.88 8.48 o 5 0 0 304.51 311.29 9.84 o 1 1 0 295.74 312.16 9.94 o 2 1 0 179.18 214.33 8.31 o 3 1 0 496.05 536.75 11.24 o 4 1 0 34.98 37.12 0.69 o 5 1 0 122.29 128.14 2.44 o 1 2 0 1454.11 1370.31 76.47 o 2 2 0 1.82 3.48 0.56 o 3 2 0 35.94 44.46 3.11 o 4 2 0 188.44 203.44 3.11 o 5 2 0 79.92 77.21 1.86 o 3 3 0 351.57 330.34 7.00 o 4 3 0 907.24 968.76 15.44 o 0 4 0 47.99 52.72 2.57 o 1 4 0 504.91 539.61 12.98 o 2 4 0 0.80 1.12 0.21 o 3 4 0 20.71 22.07 0.63 o 4 4 0 105.05 106.22 1.85 o 1 5 0 101.82 106.90 3.15 o 2 5 0 235.84 235.16 4.75 o 3 5 0 348.60 354.39 6.25 o 4 5 0 52.15 49.57 1.46 o 0 6 0 1917.01 1854.59 47.10 o 1 6 0 185.63 180.07 1.92 o 2 6 0 383.77 363.95 5.68 o 3 6 0 5.40 4.56 0.41 o 1 7 0 42.01 45.95 0.66 o 2 7 0 35.60 34.32 0.86 o 0 8 0 201.24 225.01 12.39 o 1 8 0 247.99 266.09 8.45 o -5 1 1 483.54 453.52 9.97 o -4 1 1 407.98 435.14 5.99 o -3 1 1 983.26 1023.94 17.18 o -2 1 1 438.24 500.52 13.51 o -1 1 1 120.08 121.25 3.99 o 0 1 1 19.02 27.80 1.25 o 1 1 1 2717.67 3107.26 189.46 o 2 1 1 1591.96 1961.61 99.29 o 3 1 1 449.66 477.97 10.05 o 4 1 1 266.32 285.13 4.02 o 5 1 1 38.72 38.55 0.75 o -5 2 1 204.37 193.72 6.02 o -4 2 1 16.59 17.95 0.42 o -3 2 1 258.74 244.69 4.34 o -2 2 1 403.00 429.66 13.95 o -1 2 1 2601.88 2672.26 115.95 o 0 2 1 1815.37 1933.08 79.13 o 1 2 1 87.98 90.98 5.01 o 2 2 1 55.91 62.78 3.84 o 3 2 1 331.41 356.73 12.73 o 4 2 1 486.23 484.02 6.42 o 5 2 1 301.06 254.51 7.92 o -4 3 1 1.12 3.34 0.23 o -3 3 1 5.37 5.71 0.49 o -1 3 1 15.29 18.95 1.01 o 0 3 1 1.29 1.41 0.22 o 3 3 1 0.10 0.34 0.09 o 4 3 1 6.21 6.91 0.22 o -4 4 1 35.62 37.61 0.66 o -3 4 1 325.07 314.82 5.59 o -2 4 1 290.14 299.23 5.31 o -1 4 1 1546.54 1746.56 41.84 o 0 4 1 1004.48 864.33 35.30 o 2 4 1 51.14 56.21 1.83 o 3 4 1 407.12 404.56 6.11 o 4 4 1 380.90 378.96 6.14 o -4 5 1 249.78 248.23 6.45 o -3 5 1 494.34 480.10 8.35 o 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975.71 1028.41 21.08 o 0 1 2 18.38 9.12 0.75 o 1 1 2 2439.14 2872.05 146.81 o 2 1 2 38.18 43.26 2.80 o 3 1 2 105.22 114.54 2.08 o 4 1 2 1.75 2.02 0.15 o 5 1 2 132.33 134.02 2.18 o -5 2 2 0.16 0.33 0.17 o -4 2 2 18.73 18.82 0.39 o -3 2 2 263.84 249.34 4.06 o -2 2 2 263.85 260.22 7.22 o -1 2 2 858.61 879.66 19.77 o 0 2 2 282.17 282.46 8.44 o 1 2 2 146.85 140.12 6.27 o 3 2 2 736.82 787.84 13.26 o 4 2 2 26.49 28.26 0.48 o 5 2 2 332.72 312.78 6.37 o -4 3 2 287.79 291.22 4.37 o -3 3 2 1034.60 962.38 27.34 o -2 3 2 256.22 248.07 6.14 o -1 3 2 5.91 9.42 0.59 o 0 3 2 2359.31 2413.56 98.18 o 3 3 2 352.20 360.48 7.50 o 4 3 2 6.65 7.02 0.23 o -4 4 2 1.45 1.69 0.14 o -3 4 2 177.00 172.80 3.20 o -2 4 2 135.71 138.26 2.58 o -1 4 2 184.73 201.25 4.99 o 0 4 2 119.28 125.24 2.80 o 2 4 2 7.63 9.28 0.54 o 3 4 2 465.26 437.41 6.59 o 4 4 2 8.45 8.64 0.35 o -4 5 2 235.10 196.96 5.15 o -3 5 2 60.16 57.45 1.48 o -2 5 2 20.52 22.59 0.62 o -1 5 2 235.26 238.54 6.06 o 0 5 2 38.86 38.31 1.03 o 1 5 2 847.48 846.82 21.68 o 2 5 2 73.79 75.06 1.76 o 3 5 2 125.47 107.10 2.52 o 4 5 2 0.79 1.02 0.15 o -3 6 2 259.35 256.06 7.99 o -2 6 2 661.26 686.77 9.35 o -1 6 2 1087.26 1042.94 13.67 o 0 6 2 42.22 40.74 0.66 o 1 6 2 96.57 91.40 1.28 o 2 6 2 390.37 369.95 7.24 o 3 6 2 414.73 399.08 11.41 o -2 7 2 36.07 36.99 0.74 o -1 7 2 97.49 101.87 1.39 o 0 7 2 8.95 9.66 0.23 o 1 7 2 232.68 238.18 3.05 o 2 7 2 16.90 16.38 0.78 o 0 8 2 58.63 62.43 0.99 o -5 1 3 204.34 213.41 6.82 o -4 1 3 394.58 388.68 5.95 o -3 1 3 6.54 8.64 0.42 o -2 1 3 357.18 352.47 8.01 o -1 1 3 498.65 521.21 10.40 o 0 1 3 3467.10 3085.30 132.53 o 1 1 3 1140.57 1058.50 118.03 o 2 1 3 260.87 284.19 10.58 o 3 1 3 23.09 22.90 0.56 o 4 1 3 336.88 361.02 4.41 o 5 1 3 258.58 251.16 3.91 o -4 2 3 447.80 461.09 6.70 o -3 2 3 437.01 437.93 5.85 o -2 2 3 1334.46 1323.06 23.41 o -1 2 3 245.18 238.08 7.84 o 0 2 3 0.78 3.39 0.30 o 1 2 3 30.91 27.46 1.53 o 3 2 3 560.61 552.63 18.43 o 4 2 3 357.49 389.26 5.70 o -4 3 3 1.76 3.07 0.26 o -3 3 3 0.25 0.31 0.10 o -2 3 3 6.39 8.94 0.77 o -1 3 3 5.93 6.98 0.53 o 0 3 3 19.21 18.89 1.14 o 1 3 3 16.26 18.79 1.24 o 3 3 3 4.43 3.84 0.24 o 4 3 3 8.45 6.99 0.24 o -4 4 3 478.78 482.80 15.24 o -3 4 3 368.95 350.53 7.87 o -2 4 3 1036.15 1015.81 22.15 o -1 4 3 303.65 268.14 6.61 o 0 4 3 2.02 2.87 0.24 o 2 4 3 852.54 844.55 21.58 o 3 4 3 588.89 572.41 14.71 o 4 4 3 352.20 363.77 7.71 o -3 5 3 10.30 9.81 0.29 o -2 5 3 154.78 153.03 2.14 o -1 5 3 245.84 258.06 5.24 o 0 5 3 1078.82 959.65 23.24 o 1 5 3 399.97 380.00 10.02 o 2 5 3 86.05 80.74 1.58 o 3 5 3 33.94 33.78 0.91 o -3 6 3 4.62 4.78 0.32 o -2 6 3 17.88 18.29 0.44 o -1 6 3 9.01 8.54 0.21 o 0 6 3 7.21 8.18 0.19 o 1 6 3 4.07 4.79 0.19 o 2 6 3 33.36 28.59 0.66 o 3 6 3 1.52 2.37 0.30 o -2 7 3 138.00 139.44 2.80 o -1 7 3 238.65 240.01 3.26 o 0 7 3 867.36 906.12 9.31 o 1 7 3 390.49 391.97 4.36 o 2 7 3 130.28 124.46 3.80 o -4 0 4 264.61 269.95 5.08 o -3 0 4 1503.68 1425.01 58.01 o -2 0 4 335.18 342.44 7.45 o -1 0 4 38.94 39.97 1.54 o 0 0 4 445.95 428.24 11.03 o 2 0 4 1818.38 2050.37 52.07 o 3 0 4 591.09 597.86 12.25 o 4 0 4 252.85 258.23 5.78 o -4 1 4 37.20 37.35 0.66 o -3 1 4 53.13 52.08 0.82 o -2 1 4 303.76 316.87 4.90 o -1 1 4 123.96 113.37 2.42 o 0 1 4 1426.61 1279.75 32.78 o 1 1 4 69.08 81.82 3.94 o 2 1 4 279.58 316.53 9.83 o 3 1 4 285.83 306.61 5.31 o 4 1 4 64.72 64.66 1.37 o -4 2 4 321.99 328.21 5.92 o -3 2 4 52.38 50.52 0.87 o -2 2 4 693.30 726.22 15.57 o -1 2 4 240.81 257.07 9.80 o 0 2 4 9.06 10.57 0.54 o 1 2 4 515.91 479.16 20.89 o 2 2 4 453.75 456.85 13.66 o 3 2 4 67.96 71.73 1.71 o 4 2 4 247.59 239.17 4.31 o -4 3 4 61.38 60.69 1.17 o -3 3 4 322.61 315.91 3.84 o -2 3 4 295.31 282.16 3.95 o -1 3 4 2073.66 1824.42 43.53 o 0 3 4 892.08 818.42 33.59 o 1 3 4 546.26 536.79 23.47 o 2 3 4 1.41 1.76 0.15 o 3 3 4 96.98 97.07 1.63 o 4 3 4 910.65 883.45 14.47 o -4 4 4 229.92 227.44 3.92 o -3 4 4 13.48 12.84 0.44 o -2 4 4 272.32 265.82 4.49 o -1 4 4 51.22 50.04 1.10 o 1 4 4 259.54 224.73 4.27 o 2 4 4 257.92 253.91 4.16 o 3 4 4 22.72 24.08 0.61 o 4 4 4 124.48 119.26 3.22 o -3 5 4 92.83 93.06 2.52 o -2 5 4 152.40 147.77 2.28 o -1 5 4 168.61 171.98 2.99 o 0 5 4 774.65 716.30 13.03 o 1 5 4 5.97 6.87 0.32 o 2 5 4 149.76 135.61 2.31 o 3 5 4 234.77 224.64 6.67 o -3 6 4 792.81 868.59 21.57 o -2 6 4 197.77 195.31 3.17 o -1 6 4 5.85 7.21 0.17 o 0 6 4 111.92 111.14 1.28 o 1 6 4 565.33 524.07 6.41 o 2 6 4 829.37 824.72 12.55 o 3 6 4 372.34 345.79 9.85 o -2 7 4 72.88 73.63 3.11 o -1 7 4 34.65 38.30 0.78 o 0 7 4 216.09 230.77 2.71 o 1 7 4 7.51 7.44 0.22 o 2 7 4 56.66 53.55 1.78 o -4 1 5 109.70 106.89 1.60 o -3 1 5 488.77 460.16 6.15 o -2 1 5 540.72 497.78 7.60 o -1 1 5 1699.80 1671.73 42.82 o 0 1 5 277.00 257.28 11.42 o 1 1 5 15.44 20.46 1.37 o 2 1 5 100.27 116.33 3.56 o 3 1 5 887.43 880.90 11.94 o 4 1 5 357.26 375.06 4.97 o -4 2 5 257.40 264.25 4.84 o -3 2 5 469.08 441.14 5.29 o -2 2 5 0.77 0.88 0.09 o -1 2 5 141.90 150.36 3.41 o 0 2 5 525.42 493.19 21.51 o 1 2 5 1648.58 1610.34 38.97 o 2 2 5 328.07 326.47 9.95 o 3 2 5 274.70 285.64 3.36 o 4 2 5 5.24 8.78 0.59 o -4 3 5 0.58 0.33 0.16 o -3 3 5 1.70 3.02 0.28 o -2 3 5 0.92 1.27 0.18 o -1 3 5 13.16 14.75 0.58 o 0 3 5 0.76 0.62 0.26 o 1 3 5 1.25 3.45 0.54 o 2 3 5 2.26 5.15 0.44 o 3 3 5 3.39 3.21 0.25 o 4 3 5 0.35 1.78 0.28 o -4 4 5 268.82 277.67 6.83 o -3 4 5 467.23 466.47 5.63 o -2 4 5 0.39 0.25 0.08 o -1 4 5 157.21 149.61 3.17 o 0 4 5 362.81 341.34 12.69 o 1 4 5 1219.06 1083.74 43.67 o 2 4 5 478.17 443.00 7.07 o 3 4 5 176.96 167.24 2.97 o -3 5 5 302.06 298.12 6.30 o -2 5 5 352.71 370.23 6.06 o -1 5 5 761.04 718.37 8.06 o 0 5 5 83.21 81.16 1.28 o 1 5 5 18.50 18.46 0.36 o 2 5 5 71.50 67.75 1.13 o 3 5 5 497.76 493.82 14.02 o -2 6 5 0.60 0.77 0.14 o -1 6 5 2.03 2.06 0.12 o 0 6 5 1.04 0.95 0.08 o 1 6 5 34.19 32.10 0.60 o 2 6 5 0.48 0.85 0.12 o -1 7 5 668.62 748.28 15.11 o 0 7 5 141.88 149.92 2.00 o 1 7 5 0.71 1.17 0.16 o -4 0 6 485.79 478.21 14.62 o -3 0 6 11.20 12.76 0.59 o -2 0 6 97.70 94.70 1.82 o 0 0 6 1038.51 1062.76 45.73 o 1 0 6 1900.40 1998.11 85.55 o 2 0 6 46.52 51.22 1.56 o 3 0 6 215.78 212.58 3.61 o 4 0 6 405.36 420.60 12.56 o -4 1 6 325.68 321.30 5.81 o -3 1 6 22.01 23.46 0.37 o -2 1 6 449.01 432.37 5.10 o -1 1 6 82.80 86.22 2.11 o 0 1 6 0.73 0.46 0.15 o 1 1 6 5.84 4.15 0.55 o 2 1 6 410.97 430.56 8.03 o 3 1 6 70.62 67.10 0.89 o 4 1 6 251.05 235.04 7.58 o -4 2 6 73.49 76.31 1.93 o -3 2 6 88.95 86.96 1.17 o -2 2 6 321.57 314.90 4.15 o -1 2 6 1.49 1.24 0.14 o 0 2 6 1002.32 886.36 38.35 o 1 2 6 66.58 63.60 3.37 o 2 2 6 232.48 245.48 5.25 o 3 2 6 0.07 0.24 0.08 o 4 2 6 53.42 51.09 1.15 o -4 3 6 303.67 306.56 9.53 o -3 3 6 716.36 696.92 10.38 o -2 3 6 732.76 703.11 13.62 o -1 3 6 634.15 603.77 9.38 o 0 3 6 2.21 3.56 0.31 o 1 3 6 72.03 71.00 1.46 o 2 3 6 710.29 700.88 9.78 o 3 3 6 1127.62 1129.35 16.39 o 4 3 6 164.25 166.05 3.37 o -3 4 6 43.79 41.04 0.77 o -2 4 6 134.78 128.26 2.07 o -1 4 6 1.27 2.50 0.16 o 0 4 6 557.77 522.96 9.63 o 1 4 6 17.01 16.81 0.43 o 2 4 6 134.31 127.50 2.00 o 3 4 6 2.43 1.75 0.16 o -3 5 6 32.66 27.51 0.96 o -2 5 6 448.09 479.55 9.40 o -1 5 6 92.14 90.97 1.42 o 0 5 6 1.94 1.94 0.29 o 1 5 6 0.31 0.46 0.08 o 2 5 6 411.46 363.35 11.60 o 3 5 6 92.71 97.36 3.00 o -2 6 6 72.12 81.32 2.33 o -1 6 6 443.88 471.46 7.23 o 0 6 6 562.02 587.12 6.70 o 1 6 6 1001.44 992.25 12.20 o 2 6 6 29.14 27.87 1.10 o 0 7 6 0.01 0.70 0.12 o -4 1 7 394.16 421.33 13.15 o -3 1 7 401.39 393.70 4.77 o -2 1 7 596.58 589.39 6.92 o -1 1 7 0.17 0.70 0.15 o 0 1 7 79.26 78.43 1.44 o 1 1 7 521.00 529.82 10.58 o 2 1 7 1105.54 1149.20 13.38 o 3 1 7 272.94 266.74 3.17 o 4 1 7 284.49 285.81 6.27 o -4 2 7 99.90 96.01 2.64 o -3 2 7 134.97 131.54 1.68 o -2 2 7 322.03 315.20 4.02 o -1 2 7 621.49 585.78 8.01 o 0 2 7 994.86 914.94 15.27 o 1 2 7 130.25 121.72 3.02 o 2 2 7 45.25 46.94 0.72 o 3 2 7 106.69 106.38 1.25 o 4 2 7 466.53 417.30 12.94 o -3 3 7 1.70 1.96 0.13 o -2 3 7 5.01 5.68 0.21 o -1 3 7 0.54 0.82 0.10 o 0 3 7 0.71 0.74 0.13 o 1 3 7 7.17 8.43 0.63 o 2 3 7 1.77 1.74 0.18 o 3 3 7 3.33 4.30 0.19 o -3 4 7 117.84 125.88 2.25 o -2 4 7 308.69 304.15 4.90 o -1 4 7 557.74 547.83 7.24 o 0 4 7 994.61 908.51 13.18 o 1 4 7 111.10 102.17 1.35 o 2 4 7 40.71 40.04 0.85 o 3 4 7 86.14 84.58 1.59 o -2 5 7 329.02 333.14 8.75 o -1 5 7 1.33 1.19 0.11 o 0 5 7 27.78 27.95 0.52 o 1 5 7 340.82 328.34 4.24 o 2 5 7 565.59 555.10 15.72 o -1 6 7 13.50 13.53 0.71 o 0 6 7 14.33 15.13 0.28 o 1 6 7 1.80 2.49 0.18 o -3 0 8 693.23 646.37 13.73 o -2 0 8 491.28 480.28 10.60 o -1 0 8 1137.20 1099.85 29.32 o 0 0 8 513.73 534.87 12.33 o 1 0 8 2.77 3.48 0.57 o 2 0 8 0.93 1.25 0.18 o 3 0 8 1311.14 1316.03 29.62 o -3 1 8 318.05 300.40 4.01 o -2 1 8 26.77 28.09 0.40 o -1 1 8 1.66 2.48 0.21 o 0 1 8 275.87 263.63 4.86 o 1 1 8 150.22 151.17 2.31 o 2 1 8 248.08 246.85 2.81 o 3 1 8 38.40 37.55 0.54 o -3 2 8 96.05 93.09 1.73 o -2 2 8 147.45 132.96 1.68 o -1 2 8 417.70 417.39 5.59 o 0 2 8 38.13 38.60 1.33 o 1 2 8 45.20 46.45 0.72 o 2 2 8 77.88 81.06 1.03 o 3 2 8 79.33 73.94 1.07 o -3 3 8 266.97 269.49 3.96 o -2 3 8 148.60 145.20 2.05 o -1 3 8 404.13 396.84 6.00 o 0 3 8 122.35 116.00 1.89 o 1 3 8 1676.00 1672.57 18.15 o 2 3 8 412.10 398.04 4.65 o 3 3 8 233.57 231.57 4.52 o -3 4 8 36.44 34.88 1.06 o -2 4 8 93.56 103.14 2.99 o -1 4 8 214.50 212.65 3.10 o 0 4 8 14.62 15.19 0.34 o 1 4 8 34.63 34.32 0.55 o 2 4 8 87.30 79.59 1.16 o -2 5 8 10.89 12.15 0.68 o -1 5 8 0.27 0.67 0.14 o 0 5 8 200.39 202.29 2.47 o 1 5 8 227.76 229.70 3.28 o 2 5 8 228.52 237.24 6.49 o 0 6 8 311.93 322.31 6.50 o -3 1 9 100.80 90.45 3.18 o -2 1 9 150.60 150.76 1.77 o -1 1 9 239.71 232.11 2.76 o 0 1 9 743.10 724.73 9.94 o 1 1 9 789.14 769.36 11.11 o 2 1 9 109.81 113.13 1.36 o 3 1 9 68.04 63.46 0.97 o -3 2 9 290.26 303.59 6.10 o -2 2 9 513.90 483.40 5.91 o -1 2 9 378.66 382.69 4.42 o 0 2 9 0.60 0.68 0.10 o 1 2 9 25.80 25.67 0.46 o 2 2 9 404.97 414.19 4.53 o 3 2 9 594.23 588.38 11.16 o -2 3 9 0.12 0.99 0.13 o -1 3 9 0.29 0.44 0.07 o 0 3 9 8.89 7.46 0.30 o 1 3 9 2.17 2.35 0.15 o 2 3 9 0.35 0.84 0.09 o -2 4 9 460.52 527.68 16.40 o -1 4 9 442.90 456.52 5.18 o 0 4 9 2.61 3.08 0.19 o 1 4 9 7.24 7.71 0.22 o 2 4 9 442.49 441.08 6.55 o -1 5 9 151.47 164.79 3.00 o 0 5 9 460.39 487.84 6.75 o 1 5 9 456.61 460.79 8.01 o -2 0 10 957.21 985.19 15.36 o -1 0 10 7.23 7.17 0.40 o 0 0 10 22.71 23.87 0.96 o 1 0 10 395.98 427.14 12.24 o 2 0 10 1144.35 1197.04 23.70 o -2 1 10 48.54 45.94 0.57 o -1 1 10 236.26 242.56 2.65 o 0 1 10 108.50 109.25 1.91 o 1 1 10 185.39 183.93 3.29 o 2 1 10 14.82 14.40 0.32 o -2 2 10 49.14 51.56 0.71 o -1 2 10 43.81 43.93 0.70 o 0 2 10 60.36 61.43 0.95 o 1 2 10 55.40 55.91 1.53 o 2 2 10 306.06 316.82 4.52 o -2 3 10 431.81 446.81 7.63 o -1 3 10 308.63 314.21 3.94 o 0 3 10 1416.86 1511.57 18.81 o 1 3 10 54.31 56.23 1.12 o 2 3 10 135.65 136.65 1.99 o -1 4 10 33.83 34.79 0.97 o 0 4 10 52.59 51.61 1.00 o 1 4 10 35.27 34.83 0.71 o -2 1 11 264.33 278.54 11.94 o -1 1 11 666.77 678.96 8.22 o 0 1 11 294.05 288.19 4.51 o 1 1 11 1.90 2.53 0.35 o -1 2 11 87.47 90.84 1.64 o 0 2 11 155.22 159.77 5.29 o 1 2 11 601.75 647.36 13.43 o 0 3 11 2.76 3.73 0.26 o