#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222246.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222246_Fobs loop_ _publ_author_name 'Ward, Antony J.' 'Arrow, Gregory J.' 'Maschmeyer, Thomas' 'Masters, Anthony F.' 'Turner, Peter' 'Clegg, Jack K.' _publ_section_title ; Tetraammonium diaquadiperoxidooctamolybdate(VI) tetrahydrate ; _journal_coeditor_code BR2108 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i53 _journal_page_last i54 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.991 _cell_angle_gamma 90.000 _cell_length_a 10.4055 _cell_length_b 7.8706 _cell_length_c 18.0634 _exptl_crystal_F_000 1328.00 _reflns_d_resolution_high 0.7491 _[local]_cod_data_source_file br2108Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' afm106 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 486.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 15.49 66.21 4.08 o 4 0 0 3181.00 3381.54 45.47 o 6 0 0 624.86 666.92 31.68 o 8 0 0 829.81 859.27 26.70 o 10 0 0 14970.56 15532.42 316.77 o 12 0 0 10645.21 11502.85 199.43 o 1 1 0 27404.32 26547.82 365.33 o 2 1 0 8051.00 8509.41 130.28 o 3 1 0 101.69 166.22 5.14 o 4 1 0 5938.91 5955.53 51.54 o 5 1 0 1001.58 960.37 21.70 o 6 1 0 23279.99 23113.05 206.31 o 7 1 0 41314.95 41740.21 568.11 o 8 1 0 347.80 321.15 13.82 o 9 1 0 3141.77 3245.60 33.66 o 10 1 0 15545.31 16335.77 125.04 o 11 1 0 36.12 40.49 11.20 o 12 1 0 8105.61 8204.97 146.95 o 13 1 0 3731.16 3769.17 88.71 o 0 2 0 0.22 33.09 9.53 o 1 2 0 38849.10 37208.83 740.60 o 2 2 0 7798.99 7735.48 118.15 o 3 2 0 280.85 203.50 7.43 o 4 2 0 1071.49 1344.28 18.47 o 5 2 0 2107.78 2053.56 38.62 o 6 2 0 48318.32 47450.42 858.61 o 7 2 0 3170.37 3277.11 34.93 o 8 2 0 3548.53 3487.55 32.35 o 9 2 0 16952.52 17825.88 100.16 o 10 2 0 238.36 311.94 29.36 o 11 2 0 206.10 237.39 17.07 o 12 2 0 2406.02 2449.55 87.91 o 13 2 0 227.86 230.67 20.65 o 1 3 0 49.22 43.00 6.38 o 2 3 0 633.04 619.00 10.20 o 3 3 0 17142.07 17343.45 170.18 o 4 3 0 37194.66 37060.17 510.79 o 5 3 0 4225.04 4046.15 66.32 o 6 3 0 1904.44 1916.38 30.69 o 7 3 0 1069.29 993.08 25.40 o 8 3 0 5592.80 5548.66 56.15 o 9 3 0 3051.10 3134.34 83.56 o 10 3 0 1220.41 1257.48 28.22 o 11 3 0 30.40 43.12 10.64 o 12 3 0 7395.02 7284.61 128.31 o 13 3 0 13023.45 13032.49 240.09 o 0 4 0 368.78 403.94 12.68 o 1 4 0 220.82 242.55 9.59 o 2 4 0 32370.81 32126.88 335.37 o 3 4 0 48558.57 47193.16 514.43 o 4 4 0 1012.31 995.40 24.18 o 5 4 0 1600.85 1550.15 26.28 o 6 4 0 1.60 25.50 5.90 o 7 4 0 5034.64 5147.61 129.22 o 8 4 0 3594.07 3536.41 39.51 o 9 4 0 76.06 108.99 12.24 o 10 4 0 1206.97 1098.64 27.52 o 11 4 0 327.19 346.55 20.54 o 12 4 0 2.86 4.60 11.26 o 1 5 0 7485.61 7453.01 80.24 o 2 5 0 3.16 37.64 10.21 o 3 5 0 38090.54 37756.41 498.92 o 4 5 0 27947.28 27488.44 300.39 o 5 5 0 2912.17 3061.92 68.40 o 6 5 0 453.58 528.05 23.02 o 7 5 0 2.96 19.02 6.76 o 8 5 0 13090.01 13067.37 203.94 o 9 5 0 3.12 39.62 17.99 o 10 5 0 12527.33 12100.89 318.74 o 11 5 0 2151.08 2025.46 66.21 o 0 6 0 1022.53 919.19 22.96 o 1 6 0 27.56 50.15 8.23 o 2 6 0 2823.20 2824.25 29.27 o 3 6 0 7296.83 7211.60 108.44 o 4 6 0 27444.25 26901.01 378.25 o 5 6 0 73.01 107.58 10.43 o 6 6 0 6036.54 6021.19 63.47 o 7 6 0 2585.58 2566.43 42.76 o 8 6 0 2871.14 2788.61 89.60 o 9 6 0 16433.62 15996.39 467.34 o 10 6 0 598.58 563.31 29.54 o 1 7 0 10975.27 11093.58 74.64 o 2 7 0 18338.12 18461.60 145.55 o 3 7 0 100.85 132.00 10.19 o 4 7 0 527.56 514.04 17.21 o 5 7 0 4990.67 4885.22 73.29 o 6 7 0 1049.58 1037.84 28.59 o 7 7 0 383.85 400.42 23.70 o 8 7 0 877.73 795.29 32.63 o 9 7 0 1049.19 976.09 37.34 o 10 7 0 1964.99 1953.15 86.09 o 0 8 0 6547.65 6440.43 130.43 o 1 8 0 854.44 911.69 42.52 o 2 8 0 1006.69 981.40 25.99 o 3 8 0 1602.42 1561.27 33.90 o 4 8 0 350.90 351.05 15.81 o 5 8 0 25580.08 25697.78 561.27 o 6 8 0 917.92 907.55 28.86 o 7 8 0 90.03 126.22 17.83 o 8 8 0 170.96 198.25 20.86 o 1 9 0 2024.52 2066.05 45.99 o 2 9 0 3358.10 3232.15 57.56 o 3 9 0 27.94 37.09 9.99 o 4 9 0 992.50 930.28 33.42 o 5 9 0 3350.85 3113.72 64.23 o 6 9 0 2199.74 2156.61 49.83 o 7 9 0 7951.92 8474.05 199.43 o 0 10 0 96.67 103.39 27.25 o 1 10 0 11518.89 11749.58 120.17 o 2 10 0 293.95 286.70 28.44 o 3 10 0 372.99 375.01 29.35 o 4 10 0 3559.44 3483.23 111.61 o -13 0 1 1.30 5.99 17.21 o -11 0 1 690.16 799.15 89.55 o -9 0 1 1337.20 1347.34 46.64 o -7 0 1 7948.52 8136.28 68.60 o -5 0 1 410.60 447.25 23.13 o -3 0 1 237075.06 184009.05 23992.23 o -1 0 1 36315.59 31469.62 1751.45 o 1 0 1 23757.03 23981.87 324.99 o 3 0 1 4576.44 4354.51 45.89 o 5 0 1 6674.23 6650.20 76.53 o 7 0 1 28333.91 28471.16 269.20 o 9 0 1 24693.74 26262.30 424.81 o 11 0 1 1286.26 1403.26 45.32 o 13 0 1 7.93 39.37 24.44 o -13 1 1 7665.83 7801.49 248.41 o -12 1 1 8361.94 8499.24 114.14 o -11 1 1 269.46 270.24 15.08 o -10 1 1 26145.45 26565.39 267.01 o -9 1 1 16251.53 16952.72 123.12 o -8 1 1 404.08 484.81 12.73 o -7 1 1 12886.53 13280.65 170.68 o -6 1 1 4949.76 5113.02 41.58 o -5 1 1 8.66 54.36 6.40 o -4 1 1 21831.35 21106.54 496.11 o -3 1 1 2773.69 2765.67 26.74 o -2 1 1 630.45 646.44 6.32 o -1 1 1 53291.69 48935.16 1515.65 o 0 1 1 97428.15 83061.52 2349.59 o 1 1 1 16416.55 17420.79 249.81 o 2 1 1 14302.61 14628.71 70.43 o 3 1 1 14971.39 15328.65 150.78 o 4 1 1 14016.93 13879.00 176.08 o 5 1 1 53.24 89.30 13.52 o 6 1 1 4159.04 4332.21 39.77 o 7 1 1 31823.44 32279.39 218.11 o 8 1 1 106.93 148.47 9.61 o 9 1 1 20105.49 20811.16 199.12 o 10 1 1 87.19 177.83 40.34 o 11 1 1 0.89 8.62 9.10 o 12 1 1 824.52 860.91 32.72 o 13 1 1 93.45 73.25 15.28 o -13 2 1 9859.45 10131.81 162.61 o -12 2 1 3749.54 3836.43 59.43 o -11 2 1 2083.52 2002.75 47.77 o -10 2 1 11151.86 11529.59 191.21 o -9 2 1 10231.63 10601.46 165.04 o -8 2 1 2299.09 2401.35 31.59 o -7 2 1 6154.14 6389.57 66.74 o -6 2 1 785.74 824.54 16.96 o -5 2 1 3193.68 3606.38 68.60 o -4 2 1 9469.06 9520.46 94.75 o -3 2 1 751.18 773.69 210.39 o -2 2 1 31705.02 30049.84 459.50 o -1 2 1 6570.02 6376.53 46.24 o 0 2 1 14663.78 14515.89 252.20 o 1 2 1 1281.88 1261.40 31.69 o 2 2 1 1063.08 1076.78 16.17 o 3 2 1 48428.92 48090.57 563.16 o 4 2 1 613.34 628.53 18.12 o 5 2 1 15521.53 16079.35 307.75 o 6 2 1 39498.29 40062.21 635.47 o 7 2 1 2740.18 2739.88 27.22 o 8 2 1 3059.35 3195.49 31.34 o 9 2 1 4472.15 4608.83 51.38 o 10 2 1 3700.77 3922.11 60.15 o 11 2 1 2.25 26.53 9.64 o 12 2 1 0.18 -0.57 10.04 o 13 2 1 10303.23 10151.53 230.62 o -13 3 1 400.07 399.80 34.56 o -12 3 1 949.71 972.15 32.05 o -11 3 1 3577.43 3440.10 80.55 o -10 3 1 507.43 518.28 19.11 o -9 3 1 184.82 224.68 12.07 o -8 3 1 7451.35 7228.83 92.89 o -7 3 1 35206.52 35268.50 422.75 o -6 3 1 21073.90 20998.93 430.19 o -5 3 1 551.22 558.52 12.94 o -4 3 1 7978.67 8086.96 85.46 o -3 3 1 26127.84 26240.29 319.42 o -2 3 1 4314.96 4113.79 60.72 o -1 3 1 7644.08 7442.08 92.49 o 0 3 1 2185.15 1878.92 27.15 o 1 3 1 829.63 820.93 18.41 o 2 3 1 2035.01 1890.82 16.45 o 3 3 1 10755.74 10287.51 135.59 o 4 3 1 1217.92 1358.78 17.59 o 5 3 1 508.48 533.62 9.73 o 6 3 1 15218.37 15271.92 187.21 o 7 3 1 743.02 824.36 33.81 o 8 3 1 1501.94 1528.40 29.78 o 9 3 1 1849.60 1843.17 28.44 o 10 3 1 15418.21 15603.34 338.83 o 11 3 1 589.53 589.14 24.54 o 12 3 1 896.88 973.34 32.66 o -12 4 1 1673.28 1529.18 57.64 o -11 4 1 51.54 40.12 12.53 o -10 4 1 2.45 16.61 17.68 o -9 4 1 3181.00 3116.76 108.81 o -8 4 1 112.48 130.39 13.55 o -7 4 1 1777.16 1681.72 41.30 o -6 4 1 22062.64 21530.59 166.78 o -5 4 1 2229.36 2358.46 27.12 o -4 4 1 37456.04 36244.57 654.62 o -3 4 1 1257.48 1258.23 11.32 o -2 4 1 19.68 37.20 3.46 o -1 4 1 21635.09 21431.91 175.92 o 0 4 1 22506.14 21662.04 221.58 o 1 4 1 16192.38 17057.28 249.16 o 2 4 1 5709.05 5467.82 71.98 o 3 4 1 125.37 183.24 7.95 o 4 4 1 47714.66 46195.34 706.89 o 5 4 1 2960.17 3060.47 39.69 o 6 4 1 248.27 290.75 12.79 o 7 4 1 3533.52 3558.50 56.63 o 8 4 1 343.19 367.94 16.05 o 9 4 1 43.88 58.70 15.98 o 10 4 1 981.61 1044.69 26.98 o 11 4 1 114.16 157.45 16.00 o 12 4 1 15118.89 14817.86 237.27 o -11 5 1 9804.83 9604.74 306.17 o -10 5 1 307.91 336.88 22.10 o -9 5 1 6076.66 5667.45 120.56 o -8 5 1 3352.60 3335.42 48.48 o -7 5 1 6062.56 6187.55 121.75 o -6 5 1 18559.66 18620.75 220.50 o -5 5 1 2315.40 2345.60 62.88 o -4 5 1 408.09 409.91 20.68 o -3 5 1 7950.50 7951.13 106.92 o -2 5 1 27029.80 26757.88 239.82 o -1 5 1 1044.61 1046.26 18.78 o 0 5 1 9637.64 9995.56 152.21 o 1 5 1 8185.10 7893.04 148.29 o 2 5 1 7743.79 7862.79 83.57 o 3 5 1 14694.85 14697.53 154.04 o 4 5 1 1293.56 1295.34 19.28 o 5 5 1 15393.80 15323.63 132.28 o 6 5 1 6135.22 6283.91 60.02 o 7 5 1 7759.04 7634.53 69.54 o 8 5 1 595.69 597.00 25.30 o 9 5 1 1418.73 1458.02 39.90 o 10 5 1 362.82 399.91 24.09 o 11 5 1 5610.29 5705.02 110.81 o -11 6 1 398.44 480.61 45.64 o -10 6 1 8157.37 7717.04 118.74 o -9 6 1 1227.03 1221.59 83.65 o -8 6 1 368.42 415.47 19.42 o -7 6 1 5291.99 5169.30 87.88 o -6 6 1 53.61 70.46 9.81 o -5 6 1 4227.33 4075.51 115.76 o -4 6 1 799.01 794.29 23.91 o -3 6 1 1232.35 1275.78 58.92 o -2 6 1 868.08 808.00 17.96 o -1 6 1 533.98 526.51 14.06 o 0 6 1 8621.65 8634.48 63.02 o 1 6 1 29256.20 29061.70 399.95 o 2 6 1 4904.90 4936.23 95.38 o 3 6 1 19625.15 19361.95 163.27 o 4 6 1 2246.06 2258.68 31.33 o 5 6 1 3577.36 3697.62 47.46 o 6 6 1 11703.08 11664.84 126.22 o 7 6 1 176.43 244.84 18.83 o 8 6 1 8666.38 8598.95 202.22 o 9 6 1 913.23 973.53 39.62 o 10 6 1 12115.75 12075.55 255.23 o -10 7 1 755.49 740.60 55.59 o -9 7 1 0.30 29.56 33.07 o -8 7 1 5767.60 5805.58 166.96 o -7 7 1 12.41 37.11 9.67 o -6 7 1 5056.38 4996.37 133.00 o -5 7 1 14773.31 14492.43 350.57 o -4 7 1 17086.68 17124.86 366.09 o -3 7 1 729.94 791.36 20.15 o -2 7 1 2151.46 2084.01 31.06 o -1 7 1 7500.38 7469.51 87.35 o 0 7 1 12329.50 12306.30 83.20 o 1 7 1 3830.71 3739.24 42.86 o 2 7 1 753.90 740.56 21.54 o 3 7 1 124.70 141.03 22.54 o 4 7 1 12497.37 12446.49 167.30 o 5 7 1 1910.72 1962.45 44.49 o 6 7 1 37.84 61.94 10.26 o 7 7 1 1318.93 1354.51 40.11 o 8 7 1 3.72 13.71 10.78 o 9 7 1 6759.20 6676.23 123.74 o 10 7 1 1456.00 1528.13 75.27 o -8 8 1 11601.00 11774.74 141.73 o -7 8 1 1922.64 1914.43 42.44 o -6 8 1 8037.84 8009.88 189.32 o -5 8 1 42.33 113.84 13.49 o -4 8 1 2521.63 2410.11 43.14 o -3 8 1 3016.66 3038.48 41.54 o -2 8 1 718.28 712.88 20.24 o -1 8 1 1780.48 1817.78 39.87 o 0 8 1 77.15 89.26 11.84 o 1 8 1 96.71 106.62 16.65 o 2 8 1 27525.12 26931.95 457.74 o 3 8 1 1867.05 1887.96 32.50 o 4 8 1 63.51 100.67 10.56 o 5 8 1 1170.54 1168.45 31.29 o 6 8 1 172.18 213.98 16.71 o 7 8 1 5409.75 5353.78 114.30 o 8 8 1 2.38 3.14 12.22 o -7 9 1 53.12 101.23 34.17 o -6 9 1 211.30 185.23 17.24 o -5 9 1 10305.59 10148.08 273.80 o -4 9 1 835.82 829.46 31.82 o -3 9 1 18.01 33.95 9.55 o -2 9 1 8292.27 8354.76 112.34 o -1 9 1 1646.77 1571.79 47.47 o 0 9 1 235.48 236.11 22.41 o 1 9 1 7354.02 7172.69 305.63 o 2 9 1 2143.72 2134.30 49.17 o 3 9 1 170.86 156.24 16.96 o 4 9 1 10069.20 9906.58 91.45 o 5 9 1 360.18 399.76 21.52 o 6 9 1 18.53 32.81 13.82 o 7 9 1 552.21 533.17 54.94 o -3 10 1 770.48 813.04 39.91 o -2 10 1 2430.14 2374.05 78.52 o -1 10 1 190.79 234.87 20.47 o 0 10 1 215.36 239.66 20.42 o 1 10 1 1058.57 1056.52 37.34 o 2 10 1 190.64 178.45 23.19 o 3 10 1 729.92 681.71 36.51 o 4 10 1 3146.11 3202.26 106.63 o -12 0 2 4442.98 4439.41 105.66 o -10 0 2 22942.68 24011.58 788.71 o -8 0 2 982.95 1022.85 25.55 o -6 0 2 18190.75 19342.62 1085.72 o -4 0 2 35122.73 32301.78 1417.11 o -2 0 2 1623.23 1633.93 19.42 o 0 0 2 64610.00 53408.66 3149.49 o 2 0 2 4200.37 4390.66 34.33 o 4 0 2 7259.04 6655.85 111.29 o 6 0 2 40668.07 41564.23 425.37 o 8 0 2 1731.44 1907.89 35.72 o 10 0 2 5714.68 5596.54 85.14 o 12 0 2 9340.53 9830.01 186.88 o -13 1 2 1606.28 1558.68 47.99 o -12 1 2 10967.63 10992.70 202.46 o -11 1 2 5387.55 5643.43 76.45 o -10 1 2 11663.92 11945.48 118.42 o -9 1 2 1224.40 1252.22 23.03 o -8 1 2 1958.89 2035.31 33.74 o -7 1 2 1927.97 2121.91 22.56 o -6 1 2 666.40 746.62 30.45 o -5 1 2 949.67 1028.66 12.72 o -4 1 2 956.97 591.85 16.70 o -3 1 2 114582.06 102372.73 2320.60 o -2 1 2 2929.51 3237.15 37.22 o -1 1 2 3445.77 3763.30 49.95 o 0 1 2 18.07 67.15 7.04 o 1 1 2 581.65 581.49 6.87 o 2 1 2 62.41 58.79 2.82 o 3 1 2 23070.06 23400.55 432.55 o 4 1 2 508.21 509.83 8.91 o 5 1 2 7209.52 7344.25 52.57 o 6 1 2 58472.95 58922.95 619.67 o 7 1 2 9849.87 10029.41 112.77 o 8 1 2 293.42 322.09 14.41 o 9 1 2 12440.27 12757.10 170.99 o 10 1 2 1658.10 1686.59 33.69 o 11 1 2 277.32 298.17 19.60 o 12 1 2 4906.93 5269.69 77.82 o 13 1 2 1698.41 1808.21 88.25 o -13 2 2 16268.52 15858.66 165.53 o -12 2 2 22.06 49.38 12.33 o -11 2 2 2906.95 2942.68 43.25 o -10 2 2 7576.21 7703.25 128.72 o -9 2 2 8859.76 8811.13 129.84 o -8 2 2 10.79 23.55 4.83 o -7 2 2 98.17 135.42 7.07 o -6 2 2 8351.72 8342.86 79.73 o -5 2 2 4967.83 5607.82 72.11 o -4 2 2 171.29 174.67 14.34 o -3 2 2 3943.17 4066.50 58.23 o -2 2 2 2438.87 2636.40 20.16 o -1 2 2 67613.52 63068.82 918.67 o 0 2 2 55768.42 54585.95 691.96 o 1 2 2 477.40 410.99 6.12 o 2 2 2 59689.03 58616.07 1223.36 o 3 2 2 29.04 192.67 25.67 o 4 2 2 6379.24 6126.32 61.54 o 5 2 2 35.41 57.81 11.71 o 6 2 2 457.47 500.55 11.29 o 7 2 2 3167.51 3422.42 30.39 o 8 2 2 14.61 36.04 7.26 o 9 2 2 1290.99 1303.90 33.29 o 10 2 2 14243.08 14789.24 192.00 o 11 2 2 456.92 477.08 24.13 o 12 2 2 6.95 15.23 10.28 o 13 2 2 4841.76 4803.65 167.85 o -13 3 2 1928.36 1871.48 63.62 o -12 3 2 337.43 331.06 30.20 o -11 3 2 675.86 695.95 22.93 o -10 3 2 5356.52 5344.15 115.21 o -9 3 2 18543.14 18466.62 187.40 o -8 3 2 5279.58 5248.77 46.95 o -7 3 2 0.46 72.00 26.88 o -6 3 2 38716.10 38421.80 572.34 o -5 3 2 5873.33 6192.77 123.57 o -4 3 2 4054.31 3960.01 69.88 o -3 3 2 234.08 184.20 6.77 o -2 3 2 6072.11 5951.41 58.94 o -1 3 2 563.36 474.35 11.76 o 0 3 2 3001.36 2402.36 39.69 o 1 3 2 116.07 129.63 5.60 o 2 3 2 980.36 946.40 10.85 o 3 3 2 33416.50 33336.67 220.49 o 4 3 2 11817.66 11744.36 97.59 o 5 3 2 10845.91 10522.64 142.92 o 6 3 2 6262.04 6435.76 83.76 o 7 3 2 12084.00 12355.08 120.93 o 8 3 2 20765.13 20827.26 198.41 o 9 3 2 3144.35 3139.11 37.19 o 10 3 2 1521.54 1628.46 77.14 o 11 3 2 829.39 886.63 29.61 o 12 3 2 7284.59 7144.89 99.93 o -12 4 2 3622.71 3793.48 89.08 o -11 4 2 1801.58 1889.06 47.81 o -10 4 2 24.47 47.18 11.93 o -9 4 2 1749.06 1671.97 34.88 o -8 4 2 562.32 571.50 22.26 o -7 4 2 54859.36 54436.71 811.12 o -6 4 2 502.71 518.08 21.29 o -5 4 2 4370.83 4431.21 53.67 o -4 4 2 8867.80 8604.64 52.08 o -3 4 2 1156.29 1167.60 28.81 o -2 4 2 28838.91 28875.48 171.08 o -1 4 2 197.54 220.60 9.74 o 0 4 2 1994.76 2065.77 19.56 o 1 4 2 4733.68 4680.74 64.63 o 2 4 2 1878.45 1928.25 19.27 o 3 4 2 9991.74 9952.68 88.11 o 4 4 2 4574.53 4533.96 50.84 o 5 4 2 2614.33 2561.01 29.17 o 6 4 2 28.06 38.40 5.12 o 7 4 2 2177.25 2124.17 41.52 o 8 4 2 1376.09 1390.04 28.12 o 9 4 2 24266.96 24151.08 405.63 o 10 4 2 143.90 134.78 14.52 o 11 4 2 42.53 64.27 12.53 o 12 4 2 30.51 40.45 25.96 o -11 5 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