#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:07:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181143 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/22/2222265.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222265_Fobs loop_ _publ_author_name 'Narendra Babu, Shivanagere Nagojappa' 'Abdul Rahim, Aisyah Saad' 'Osman, Hasnah' 'Jebas, Samuel Robinson' 'Fun, Hoong-Kun' _publ_section_title ; 4-(But-3-enylamino)-3-nitrobenzoic acid ; _journal_coeditor_code CI2814 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1560 _journal_page_last o1561 _journal_volume 65 _journal_year 2009 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.632 _cell_angle_gamma 90.000 _cell_length_a 13.3461 _cell_length_b 66.7772 _cell_length_c 15.0195 _exptl_crystal_F_000 5952.00 _reflns_d_resolution_high 0.6873 _cod_data_source_file ci2814Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nb12am in Cc (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 2827.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4958.28 -317.11 317.11 o 4 0 0 7994292.50 7492179.00 303255.44 o 6 0 0 2113.05 1875.21 132.76 o 8 0 0 234640.09 221961.48 9059.10 o 10 0 0 454.90 620.59 144.58 o 12 0 0 9218.99 17668.05 1347.22 o 14 0 0 1183.57 1277.73 243.18 o 16 0 0 18112.74 18863.19 1211.51 o 18 0 0 903.20 871.89 328.10 o 1 1 0 181.98 19.00 8.04 o 3 1 0 169.94 18.42 24.42 o 5 1 0 754.37 586.78 44.33 o 7 1 0 480.47 414.05 45.87 o 9 1 0 3830.40 3474.11 205.01 o 11 1 0 1202.85 934.01 114.73 o 13 1 0 4098.11 4128.27 231.85 o 15 1 0 1445.82 1427.16 181.97 o 17 1 0 1845.59 1907.95 291.22 o 19 1 0 759.87 306.53 209.74 o 0 2 0 0.12 0.00 80.70 o 2 2 0 738.89 194.06 25.34 o 4 2 0 1914100.75 1502169.00 46262.96 o 6 2 0 599.62 313.61 49.47 o 8 2 0 663601.50 647565.81 18161.90 o 10 2 0 630.17 451.01 71.65 o 12 2 0 85522.08 86774.95 3001.52 o 14 2 0 179.79 296.38 86.35 o 16 2 0 2820.16 5091.73 583.42 o 18 2 0 37.38 17.37 173.70 o 1 3 0 2570.09 2456.54 244.49 o 3 3 0 10715.19 11239.55 337.19 o 5 3 0 2780.07 2880.79 97.90 o 7 3 0 1317.06 1167.83 66.49 o 9 3 0 2491.50 3821.54 141.32 o 11 3 0 1889.15 1918.78 188.18 o 13 3 0 369.14 1218.95 229.45 o 15 3 0 1965.81 1981.98 201.14 o 17 3 0 1791.86 1643.51 270.25 o 19 3 0 1891.17 2518.07 329.40 o 0 4 0 11.72 8.74 3.44 o 2 4 0 158.95 -17.71 17.71 o 4 4 0 134565.05 94337.47 2693.15 o 6 4 0 516.15 648.10 58.36 o 8 4 0 204402.08 162752.98 5357.52 o 10 4 0 440.71 761.40 76.47 o 12 4 0 87886.74 89970.97 3210.70 o 14 4 0 697.77 888.17 133.87 o 16 4 0 15394.62 17852.57 837.13 o 18 4 0 111.95 206.43 185.44 o 1 5 0 461.20 163.10 29.48 o 3 5 0 9298.34 6331.98 244.04 o 5 5 0 8253.59 6841.16 215.42 o 7 5 0 7918.45 6657.88 215.95 o 9 5 0 15229.59 14361.54 409.60 o 11 5 0 6932.70 7808.62 403.28 o 13 5 0 4887.44 5872.98 269.68 o 15 5 0 1336.39 1393.09 160.95 o 17 5 0 525.29 1034.06 295.88 o 19 5 0 154.77 744.40 238.60 o 0 6 0 479356.66 235365.94 24614.80 o 2 6 0 6748.88 7761.20 221.82 o 4 6 0 424035.94 428938.75 11148.37 o 6 6 0 2428.37 2356.95 85.70 o 8 6 0 61191.58 51698.01 1369.32 o 10 6 0 263.67 357.17 70.16 o 12 6 0 30408.62 24833.09 853.13 o 14 6 0 1002.73 1375.85 241.10 o 16 6 0 19437.21 20021.58 926.02 o 18 6 0 487.02 157.02 196.14 o 1 7 0 1402.88 946.69 69.62 o 3 7 0 1731.77 1302.34 76.34 o 5 7 0 10454.91 8258.86 254.52 o 7 7 0 11464.46 10117.78 286.91 o 9 7 0 6840.85 7538.50 367.23 o 11 7 0 5942.89 6066.52 281.23 o 13 7 0 5492.28 6788.25 332.23 o 15 7 0 1397.76 1303.99 238.59 o 17 7 0 2615.88 2722.39 313.71 o 19 7 0 155.59 233.71 202.54 o 0 8 0 1.90 13.10 13.67 o 2 8 0 118.26 63.20 17.36 o 4 8 0 85219.97 77944.37 2377.03 o 6 8 0 2841.14 3070.54 104.18 o 8 8 0 63493.52 63347.12 1660.93 o 10 8 0 2641.04 2900.91 139.12 o 12 8 0 10705.58 11598.38 471.31 o 14 8 0 733.69 1092.69 144.69 o 16 8 0 784.26 1212.85 174.55 o 18 8 0 32.59 364.22 201.21 o 1 9 0 11334.68 12284.59 487.43 o 3 9 0 13604.12 14082.04 390.57 o 5 9 0 499.43 472.39 36.54 o 7 9 0 967.19 769.95 52.07 o 9 9 0 3425.08 2889.07 118.67 o 11 9 0 581.93 1221.43 113.24 o 13 9 0 3401.04 4097.34 332.60 o 15 9 0 3128.07 3768.41 285.92 o 17 9 0 3528.61 3360.95 349.76 o 19 9 0 2833.32 2611.97 429.23 o 0 10 0 0.13 -15.57 15.57 o 2 10 0 493.47 466.45 28.81 o 4 10 0 7576.47 6764.93 238.10 o 6 10 0 1056.50 884.57 49.99 o 8 10 0 28521.21 25169.45 748.51 o 10 10 0 2888.32 2991.09 148.92 o 12 10 0 17963.34 16744.92 633.38 o 14 10 0 2167.23 2106.53 174.97 o 16 10 0 6395.51 6143.68 421.38 o 18 10 0 77.43 146.29 197.70 o 1 11 0 273.30 171.47 18.77 o 3 11 0 6272.44 4011.51 191.51 o 5 11 0 231.06 94.08 28.30 o 7 11 0 1039.69 730.24 50.30 o 9 11 0 1650.80 2041.68 94.80 o 11 11 0 2074.29 2569.45 152.87 o 13 11 0 125.08 -16.73 90.74 o 15 11 0 56.54 193.98 118.10 o 17 11 0 717.82 710.79 203.68 o 19 11 0 368.38 584.40 264.12 o 0 12 0 3621.22 4813.90 189.25 o 2 12 0 737.70 810.81 40.13 o 4 12 0 28612.15 28560.94 785.98 o 6 12 0 249.26 296.20 35.98 o 8 12 0 7532.58 7116.69 290.72 o 10 12 0 351.54 352.65 71.77 o 12 12 0 15.37 1486.47 295.85 o 14 12 0 219.63 187.49 103.89 o 16 12 0 1048.46 1206.32 181.17 o 18 12 0 15.87 -61.51 171.76 o 1 13 0 1352.11 2016.96 278.40 o 3 13 0 7185.87 4134.45 270.60 o 5 13 0 9408.95 9492.47 395.09 o 7 13 0 4140.30 4518.19 201.03 o 9 13 0 4021.79 3633.36 135.16 o 11 13 0 4710.41 4881.44 242.69 o 13 13 0 329.02 320.49 105.49 o 15 13 0 2794.07 3096.99 225.74 o 17 13 0 127.49 135.52 172.89 o 0 14 0 3.85 -9.53 27.83 o 2 14 0 1034.96 711.12 42.29 o 4 14 0 3750.44 2747.22 162.74 o 6 14 0 730.04 615.94 51.70 o 8 14 0 13861.33 14963.74 487.54 o 10 14 0 455.26 577.58 84.15 o 12 14 0 5317.01 5389.41 265.35 o 14 14 0 896.90 1036.51 137.80 o 16 14 0 750.37 713.64 160.14 o 18 14 0 73.10 402.02 219.21 o 1 15 0 83507.10 85715.53 2463.45 o 3 15 0 130922.65 131837.88 3458.09 o 5 15 0 21123.51 18763.01 501.63 o 7 15 0 7587.88 6362.29 246.06 o 9 15 0 1637.50 1458.44 91.20 o 11 15 0 264.55 487.81 105.40 o 13 15 0 471.52 480.35 113.36 o 15 15 0 106.96 124.34 108.40 o 17 15 0 359.36 289.78 156.29 o 0 16 0 8.01 3.61 31.65 o 2 16 0 7151.61 6832.65 232.98 o 4 16 0 9391.92 8708.55 398.25 o 6 16 0 890.58 634.57 45.47 o 8 16 0 9626.85 9620.34 274.20 o 10 16 0 309.59 213.51 60.79 o 12 16 0 1300.71 1375.00 136.53 o 14 16 0 45.00 259.50 109.97 o 16 16 0 534.47 595.70 152.86 o 18 16 0 32.20 87.40 212.54 o 1 17 0 54.76 137.32 24.74 o 3 17 0 2802.67 2362.57 194.00 o 5 17 0 6623.11 5354.52 322.19 o 7 17 0 2869.08 2378.65 166.68 o 9 17 0 4777.54 4894.03 192.76 o 11 17 0 2853.72 3153.36 171.20 o 13 17 0 572.10 462.43 113.88 o 15 17 0 742.40 808.62 143.57 o 17 17 0 110.57 18.13 162.45 o 0 18 0 1331.05 1428.14 72.62 o 2 18 0 15.05 -8.74 19.32 o 4 18 0 31152.54 31183.40 771.35 o 6 18 0 843.07 880.65 55.73 o 8 18 0 3450.11 3295.99 127.21 o 10 18 0 226.40 304.14 73.17 o 12 18 0 387.58 287.60 104.38 o 14 18 0 199.74 356.93 130.06 o 16 18 0 259.65 487.27 149.34 o 18 18 0 59.73 172.49 175.33 o 1 19 0 2490.19 2994.71 124.89 o 3 19 0 11067.41 12368.93 583.76 o 5 19 0 21424.76 20012.21 523.00 o 7 19 0 9848.49 8269.79 274.68 o 9 19 0 3743.12 3463.09 171.03 o 11 19 0 4969.85 6052.91 336.27 o 13 19 0 323.95 252.32 97.73 o 15 19 0 1093.61 790.41 147.69 o 17 19 0 290.09 -7.85 157.38 o 0 20 0 7.67 24.66 31.65 o 2 20 0 1623.58 1705.15 78.44 o 4 20 0 1245.65 989.19 69.50 o 6 20 0 1029.53 897.03 52.44 o 8 20 0 2516.74 2903.42 134.55 o 10 20 0 318.52 268.99 71.29 o 12 20 0 9.16 -10.95 90.06 o 14 20 0 300.04 109.45 101.05 o 16 20 0 143.61 206.08 130.53 o 18 20 0 78.78 118.29 180.28 o 1 21 0 38174.41 38658.77 969.34 o 3 21 0 23136.00 21690.96 585.65 o 5 21 0 13375.72 10579.79 320.22 o 7 21 0 203.69 292.07 42.85 o 9 21 0 144.74 327.79 79.83 o 11 21 0 528.87 818.48 99.80 o 13 21 0 212.94 149.32 94.82 o 15 21 0 4.06 70.04 131.17 o 17 21 0 189.01 210.89 168.94 o 0 22 0 242.18 169.51 33.22 o 2 22 0 13178.66 13457.71 385.87 o 4 22 0 287.43 377.46 35.36 o 6 22 0 558.31 831.08 89.04 o 8 22 0 485.48 652.71 56.63 o 10 22 0 3064.42 2655.85 151.81 o 12 22 0 1173.88 989.11 131.37 o 14 22 0 190.97 466.95 114.39 o 16 22 0 602.64 651.03 167.13 o 18 22 0 157.12 79.96 174.73 o 1 23 0 537.67 775.16 44.16 o 3 23 0 358.55 343.91 37.91 o 5 23 0 3136.12 3464.35 139.37 o 7 23 0 7591.32 7174.54 244.56 o 9 23 0 1396.12 1562.33 109.02 o 11 23 0 11238.12 11283.80 415.91 o 13 23 0 147.04 44.11 93.47 o 15 23 0 2237.65 2890.65 236.44 o 17 23 0 51.44 -147.34 147.34 o 0 24 0 99402.46 107928.48 3556.76 o 2 24 0 1912.23 1967.71 69.17 o 4 24 0 3416.65 2538.93 87.23 o 6 24 0 16323.55 14534.29 413.00 o 8 24 0 239.20 292.14 56.85 o 10 24 0 3651.67 3774.46 188.43 o 12 24 0 221.63 265.71 90.49 o 14 24 0 1720.86 1711.36 193.70 o 16 24 0 210.90 467.86 176.58 o 18 24 0 231.31 20.79 171.88 o 1 25 0 234.32 256.29 26.30 o 3 25 0 14260.71 17153.80 496.53 o 5 25 0 5445.36 5775.63 169.61 o 7 25 0 23966.74 24189.38 683.20 o 9 25 0 260.85 255.99 68.33 o 11 25 0 8294.17 8816.18 359.13 o 13 25 0 3.83 0.78 101.00 o 15 25 0 288.66 213.42 142.44 o 17 25 0 0.22 -120.50 161.13 o 0 26 0 194.11 841.98 70.98 o 2 26 0 1413.75 1075.69 47.87 o 4 26 0 9654.09 9492.47 273.30 o 6 26 0 8690.95 7908.84 232.09 o 8 26 0 7611.04 7247.38 249.87 o 10 26 0 4834.59 4718.41 234.85 o 12 26 0 1732.56 1979.00 202.63 o 14 26 0 510.70 872.76 146.99 o 16 26 0 725.90 260.89 174.86 o 18 26 0 107.87 5.03 187.47 o 1 27 0 44611.18 45358.35 1095.82 o 3 27 0 32247.59 29293.16 797.89 o 5 27 0 5813.29 5350.48 157.54 o 7 27 0 9024.82 7433.75 292.90 o 9 27 0 464.41 501.17 109.70 o 11 27 0 125.65 1359.82 217.01 o 13 27 0 684.20 818.57 159.83 o 15 27 0 314.17 536.47 167.81 o 17 27 0 484.56 264.11 188.82 o 0 28 0 167.86 198.79 38.83 o 2 28 0 27558.20 29390.99 740.15 o 4 28 0 5410.47 5095.57 151.84 o 6 28 0 22180.28 22710.11 627.87 o 8 28 0 6131.77 5820.98 227.54 o 10 28 0 3417.54 3747.16 205.65 o 12 28 0 2085.56 2108.01 164.20 o 14 28 0 811.31 1102.98 178.80 o 16 28 0 121.63 197.62 166.50 o 18 28 0 68.64 265.27 190.09 o 1 29 0 812.12 895.25 72.86 o 3 29 0 1999.46 2390.29 83.08 o 5 29 0 6792.14 7568.32 209.20 o 7 29 0 10710.66 11537.68 374.83 o 9 29 0 3104.48 2791.22 166.56 o 11 29 0 4316.61 4300.52 229.74 o 13 29 0 1624.00 1449.26 168.75 o 15 29 0 149.90 109.87 133.70 o 17 29 0 223.42 265.43 187.83 o 0 30 0 6503.15 7869.85 302.90 o 2 30 0 10969.99 10732.11 272.89 o 4 30 0 1138.30 1182.20 59.84 o 6 30 0 2712.23 2527.30 101.62 o 8 30 0 2070.43 1994.44 107.96 o 10 30 0 492.09 1247.89 159.75 o 12 30 0 2279.61 2493.10 294.29 o 14 30 0 1133.61 1149.45 187.77 o 16 30 0 717.04 946.78 210.23 o 18 30 0 259.42 165.53 190.86 o 1 31 0 204.84 193.51 28.40 o 3 31 0 1291.12 2133.42 139.93 o 5 31 0 4197.48 4109.46 133.26 o 7 31 0 8193.27 8127.85 286.27 o 9 31 0 1502.76 1545.27 119.28 o 11 31 0 4169.22 4600.12 232.70 o 13 31 0 539.98 271.04 131.28 o 15 31 0 275.39 387.54 154.92 o 17 31 0 53.67 123.43 173.02 o 0 32 0 31.06 28.29 36.22 o 2 32 0 491.13 692.80 44.77 o 4 32 0 651.25 761.41 48.88 o 6 32 0 4162.44 4627.43 148.74 o 8 32 0 61.13 382.45 68.58 o 10 32 0 2812.28 2492.42 158.57 o 12 32 0 190.31 359.46 99.90 o 14 32 0 1620.09 1615.83 262.01 o 16 32 0 224.96 267.97 167.41 o 18 32 0 268.43 221.47 228.31 o 1 33 0 8775.88 9448.44 245.00 o 3 33 0 70408.05 74649.35 1800.12 o 5 33 0 206.64 203.41 41.53 o 7 33 0 9104.56 8421.88 257.80 o 9 33 0 88.88 153.32 91.62 o 11 33 0 684.29 736.72 107.31 o 13 33 0 4.39 245.09 122.39 o 15 33 0 245.56 515.44 163.55 o 17 33 0 268.09 189.07 181.75 o 0 34 0 4.98 3.27 35.84 o 2 34 0 946.61 1451.08 68.62 o 4 34 0 338.59 1106.90 103.21 o 6 34 0 2435.00 2206.75 96.58 o 8 34 0 2326.59 2769.77 127.37 o 10 34 0 4599.44 4444.80 363.88 o 12 34 0 946.46 795.95 141.64 o 14 34 0 2629.21 2772.86 251.21 o 16 34 0 627.63 610.06 195.36 o 1 35 0 376.62 416.17 37.38 o 3 35 0 16033.48 21226.40 599.27 o 5 35 0 1008.48 1268.31 68.68 o 7 35 0 10774.38 11969.84 366.75 o 9 35 0 478.10 478.74 84.55 o 11 35 0 3559.33 3590.01 230.75 o 13 35 0 300.95 326.14 136.49 o 15 35 0 744.27 705.77 168.10 o 17 35 0 3.26 137.70 186.23 o 0 36 0 3645.02 3977.92 174.78 o 2 36 0 251.13 285.24 32.24 o 4 36 0 11149.04 11256.25 302.57 o 6 36 0 204.93 126.60 42.45 o 8 36 0 3421.96 3098.77 161.24 o 10 36 0 4.54 201.98 84.66 o 12 36 0 487.63 349.56 164.59 o 14 36 0 575.13 396.99 145.14 o 16 36 0 100.69 151.84 171.29 o 1 37 0 1814.49 2130.08 98.18 o 3 37 0 1193.28 1371.49 61.41 o 5 37 0 735.35 918.30 58.78 o 7 37 0 3752.46 5271.51 218.85 o 9 37 0 1798.06 1535.47 135.29 o 11 37 0 2050.47 2278.29 175.05 o 13 37 0 294.55 272.63 132.65 o 15 37 0 1611.04 1780.49 256.40 o 17 37 0 238.42 461.32 198.94 o 0 38 0 0.16 91.84 41.48 o 2 38 0 271.24 263.04 32.80 o 4 38 0 55.37 113.44 32.10 o 6 38 0 1665.15 1718.58 86.44 o 8 38 0 955.66 1121.36 119.98 o 10 38 0 1943.17 1883.36 156.10 o 12 38 0 87.02 99.21 142.95 o 14 38 0 752.99 977.29 174.63 o 16 38 0 347.38 359.78 188.81 o 1 39 0 129.04 129.38 28.33 o 3 39 0 7114.54 7866.23 207.91 o 5 39 0 1014.17 919.85 66.82 o 7 39 0 3520.19 3305.91 152.54 o 9 39 0 622.32 589.24 127.76 o 11 39 0 521.85 657.46 122.78 o 13 39 0 554.30 552.80 147.12 o 15 39 0 1086.29 1104.21 209.83 o 17 39 0 839.38 602.02 204.42 o 0 40 0 24.95 83.97 41.92 o 2 40 0 1944.81 1937.72 74.26 o 4 40 0 133.12 134.12 35.25 o 6 40 0 4001.24 3460.05 138.41 o 8 40 0 828.04 1010.51 97.92 o 10 40 0 501.90 492.53 104.70 o 12 40 0 115.01 253.26 114.20 o 14 40 0 464.13 453.33 182.66 o 16 40 0 263.89 298.31 183.20 o 1 41 0 1356.33 1508.94 69.53 o 3 41 0 1065.16 1241.03 58.44 o 5 41 0 1261.54 1347.70 72.27 o 7 41 0 311.17 362.54 61.15 o 9 41 0 2840.33 3114.13 189.54 o 11 41 0 83.25 190.13 109.02 o 13 41 0 817.13 658.83 151.26 o 15 41 0 24.71 254.54 168.57 o 17 41 0 321.57 580.24 234.19 o 0 42 0 10265.44 11657.94 445.13 o 2 42 0 609.29 562.70 44.08 o 4 42 0 271.52 357.89 42.75 o 6 42 0 298.87 433.81 59.17 o 8 42 0 177.18 301.26 76.62 o 10 42 0 322.73 315.10 96.95 o 12 42 0 230.33 257.74 115.49 o 14 42 0 1792.98 1962.38 234.99 o 16 42 0 70.45 -20.61 172.60 o 1 43 0 926.30 946.21 56.91 o 3 43 0 456.71 347.38 39.16 o 5 43 0 1416.16 1726.81 88.81 o 7 43 0 51.73 -6.85 52.13 o 9 43 0 1039.84 1064.57 135.21 o 11 43 0 535.20 573.42 123.02 o 13 43 0 589.97 541.74 261.07 o 15 43 0 93.61 115.52 167.81 o 17 43 0 330.69 257.33 205.60 o 0 44 0 23.76 183.17 52.01 o 2 44 0 832.07 920.32 54.49 o 4 44 0 29.83 103.64 41.38 o 6 44 0 460.90 496.85 60.63 o 8 44 0 233.28 256.02 73.53 o 10 44 0 709.14 575.01 132.71 o 12 44 0 9.14 -60.31 100.85 o 14 44 0 15.05 -124.89 124.89 o 16 44 0 8.80 -38.90 296.40 o 1 45 0 133.55 139.46 39.44 o 3 45 0 236.87 208.77 38.53 o 5 45 0 1370.46 1173.81 99.86 o 7 45 0 438.56 414.02 75.40 o 9 45 0 2467.43 2561.64 197.65 o 11 45 0 108.64 257.41 122.16 o 13 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