#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/22/2222297.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222297_Fobs loop_ _publ_author_name 'Kim, Nam-Ho' 'Ha, Kwang' _publ_section_title ; [(2,3,5,6-\h)-Bicyclo[2.2.1]hepta-2,5-diene]dibromidopalladium(II) ; _journal_coeditor_code EZ2172 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m727 _journal_volume 65 _journal_year 2009 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.7579 _cell_length_b 7.4313 _cell_length_c 9.0138 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.8006 _[local]_cod_data_source_file ez2172Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Pd(nbd)Br2] in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 409.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13440.76 13476.91 159.58 o 4 0 0 7011.52 6843.91 108.52 o 6 0 0 17306.52 16820.86 235.99 o 8 0 0 31782.35 30551.85 547.10 o 10 0 0 4083.09 3857.96 132.08 o 12 0 0 4948.19 4414.21 304.72 o 14 0 0 1390.05 1328.34 216.03 o 2 1 0 26482.24 27631.09 195.25 o 4 1 0 3871.89 4078.90 86.57 o 6 1 0 16484.51 16279.85 195.55 o 8 1 0 84.95 73.29 36.21 o 10 1 0 4460.75 4296.40 132.55 o 12 1 0 446.67 428.80 69.79 o 14 1 0 2694.10 2761.54 189.94 o 0 2 0 167402.02 144298.64 878.32 o 2 2 0 4959.12 5174.14 74.16 o 4 2 0 3351.55 3345.73 71.76 o 6 2 0 11478.05 11825.12 139.70 o 8 2 0 26278.98 25042.83 290.86 o 10 2 0 1734.46 1665.47 96.03 o 12 2 0 2432.79 2485.82 119.87 o 14 2 0 1421.34 1358.05 154.21 o 2 3 0 4671.10 4601.92 82.08 o 4 3 0 1369.55 1397.47 50.07 o 6 3 0 12070.29 11803.86 225.76 o 8 3 0 350.42 387.11 61.20 o 10 3 0 1701.61 1911.31 110.01 o 12 3 0 713.65 704.14 84.63 o 14 3 0 2378.95 2604.14 162.92 o 0 4 0 52059.54 51383.96 421.63 o 2 4 0 1571.82 1571.58 59.43 o 4 4 0 2311.03 2212.31 64.25 o 6 4 0 10247.76 10659.60 206.15 o 8 4 0 15325.96 15535.84 265.96 o 10 4 0 411.34 415.04 72.71 o 12 4 0 695.23 753.74 92.68 o 14 4 0 1117.17 1164.23 114.94 o 2 5 0 2230.96 2153.40 77.99 o 4 5 0 116.70 107.08 35.32 o 6 5 0 5233.97 5438.25 162.84 o 8 5 0 25.63 22.61 47.52 o 10 5 0 679.32 779.20 95.30 o 12 5 0 416.42 422.24 82.61 o 0 6 0 23380.52 21992.81 498.95 o 2 6 0 869.75 878.37 62.90 o 4 6 0 1393.88 1363.83 71.89 o 6 6 0 6089.39 6025.62 155.55 o 8 6 0 6629.30 7179.70 186.61 o 10 6 0 236.10 359.97 122.83 o 12 6 0 446.76 267.96 190.92 o 2 7 0 1494.79 1535.76 107.84 o 4 7 0 30.38 88.33 87.83 o 6 7 0 1761.03 1711.40 192.07 o 8 7 0 6.11 -71.06 71.06 o 10 7 0 472.14 107.85 265.38 o 0 8 0 7895.50 8227.26 326.83 o 2 8 0 342.32 358.09 91.76 o 4 8 0 281.79 321.06 116.87 o 6 8 0 1274.02 1123.76 268.24 o 8 8 0 2197.00 423.27 948.51 o 2 9 0 398.92 524.43 135.05 o 1 0 1 44302.81 42360.36 256.84 o 2 0 1 12300.59 12867.23 211.29 o 3 0 1 1156.91 1175.71 48.43 o 4 0 1 27029.68 27010.52 164.58 o 5 0 1 2572.93 2380.04 55.39 o 6 0 1 527.22 496.63 32.66 o 7 0 1 28964.65 29110.36 209.65 o 8 0 1 1818.78 1909.27 64.93 o 9 0 1 3904.85 3589.81 87.39 o 10 0 1 2715.79 2577.55 90.65 o 11 0 1 2222.57 2183.50 155.12 o 12 0 1 1586.73 1503.51 141.84 o 13 0 1 1242.48 1135.70 134.17 o 14 0 1 385.37 389.64 97.83 o 15 0 1 1710.33 567.59 806.88 o 0 1 1 612.84 675.50 29.39 o 1 1 1 4133.99 3996.00 41.05 o 2 1 1 10126.13 10022.51 90.37 o 3 1 1 1170.19 1310.65 39.68 o 4 1 1 270.14 288.78 23.98 o 5 1 1 2151.19 2128.57 37.23 o 6 1 1 476.17 414.89 23.22 o 7 1 1 10315.48 9808.23 92.25 o 8 1 1 272.26 244.07 25.12 o 9 1 1 1041.27 982.35 44.92 o 10 1 1 1616.27 1601.23 64.56 o 11 1 1 989.00 1035.96 57.05 o 12 1 1 191.00 177.68 37.34 o 13 1 1 2408.64 2386.33 126.91 o 14 1 1 363.32 420.26 74.79 o 15 1 1 307.62 83.74 100.46 o 1 2 1 47867.80 47685.16 262.92 o 2 2 1 2101.51 2096.49 35.47 o 3 2 1 953.97 891.98 25.63 o 4 2 1 21946.98 22764.08 174.32 o 5 2 1 4363.43 4676.28 74.20 o 6 2 1 188.04 172.00 28.06 o 7 2 1 25514.15 25707.64 202.91 o 8 2 1 736.09 665.89 45.98 o 9 2 1 2563.84 2369.15 75.74 o 10 2 1 1387.09 1370.24 65.02 o 11 2 1 2524.66 2526.71 83.76 o 12 2 1 1802.02 1801.09 77.40 o 13 2 1 1196.41 1125.77 71.27 o 14 2 1 191.95 231.37 62.29 o 15 2 1 1349.78 280.73 361.16 o 0 3 1 6706.30 6670.06 94.74 o 1 3 1 3972.25 3976.99 53.79 o 2 3 1 3260.78 3071.36 47.49 o 3 3 1 44.06 52.23 16.16 o 4 3 1 108.71 119.04 17.89 o 5 3 1 1571.56 1614.11 51.42 o 6 3 1 828.44 854.31 43.94 o 7 3 1 5199.02 5090.35 92.43 o 8 3 1 153.59 143.89 35.64 o 9 3 1 1233.90 1272.98 65.64 o 10 3 1 2387.28 2342.44 82.83 o 11 3 1 719.85 746.74 59.41 o 12 3 1 25.74 25.29 31.99 o 13 3 1 1445.22 1505.04 79.90 o 14 3 1 389.29 454.64 58.99 o 15 3 1 163.08 134.83 86.63 o 1 4 1 24582.45 25157.28 147.38 o 2 4 1 249.26 207.19 23.84 o 3 4 1 357.17 351.67 26.04 o 4 4 1 14777.59 15317.33 117.17 o 5 4 1 2294.23 2293.45 57.40 o 6 4 1 103.16 99.21 31.19 o 7 4 1 13995.99 14410.73 184.31 o 8 4 1 429.33 409.20 48.23 o 9 4 1 1348.08 1343.94 69.92 o 10 4 1 285.30 345.80 48.74 o 11 4 1 1659.94 1624.48 79.76 o 12 4 1 1336.79 1305.56 78.50 o 13 4 1 844.83 883.69 71.13 o 14 4 1 111.58 162.15 44.78 o 0 5 1 2641.04 2503.58 81.10 o 1 5 1 1620.87 1548.64 47.75 o 2 5 1 1434.27 1362.27 45.70 o 3 5 1 25.99 53.14 23.98 o 4 5 1 7.89 20.91 22.43 o 5 5 1 731.96 731.67 40.05 o 6 5 1 1781.14 1828.26 69.46 o 7 5 1 2635.66 2764.10 84.74 o 8 5 1 50.30 75.59 37.70 o 9 5 1 579.54 601.49 57.36 o 10 5 1 1344.17 1340.23 75.64 o 11 5 1 474.94 475.46 56.57 o 12 5 1 38.36 22.60 37.13 o 13 5 1 896.72 903.75 74.70 o 1 6 1 8158.05 8117.45 121.08 o 2 6 1 346.01 350.27 42.09 o 3 6 1 103.99 99.88 34.22 o 4 6 1 6921.40 7001.25 119.61 o 5 6 1 562.78 581.02 65.68 o 6 6 1 76.67 122.64 49.58 o 7 6 1 5366.78 5454.47 140.60 o 8 6 1 366.56 414.23 63.61 o 9 6 1 766.09 794.51 75.94 o 10 6 1 131.53 124.02 51.77 o 11 6 1 519.29 540.43 72.27 o 12 6 1 519.03 369.47 104.35 o 0 7 1 278.54 373.76 74.94 o 1 7 1 509.45 520.88 55.80 o 2 7 1 680.82 715.65 60.66 o 3 7 1 10.80 0.33 38.65 o 4 7 1 16.47 31.61 58.72 o 5 7 1 313.38 295.92 79.50 o 6 7 1 649.14 537.50 94.77 o 7 7 1 1087.76 995.33 118.06 o 8 7 1 12.35 -37.08 53.74 o 9 7 1 220.84 94.51 70.65 o 10 7 1 364.44 63.35 112.23 o 1 8 1 2629.18 2641.65 100.47 o 2 8 1 158.19 192.72 55.38 o 3 8 1 30.93 32.87 61.02 o 4 8 1 1714.41 1849.57 142.40 o 5 8 1 243.02 259.24 79.05 o 6 8 1 10.30 21.01 64.23 o 7 8 1 1930.19 312.21 562.59 o 0 9 1 22.63 64.69 57.31 o 1 9 1 229.90 253.07 61.79 o 2 9 1 193.27 270.50 77.87 o 3 9 1 47.88 74.23 65.63 o 0 0 2 7107.23 7476.47 188.84 o 1 0 2 747.68 762.02 62.23 o 2 0 2 5699.82 5525.53 231.40 o 3 0 2 47509.80 48067.94 474.66 o 4 0 2 4650.79 4805.07 153.50 o 5 0 2 20728.92 21318.29 413.69 o 6 0 2 17775.39 18566.61 243.41 o 7 0 2 3602.67 3279.94 93.97 o 8 0 2 2682.89 2409.11 87.05 o 9 0 2 891.06 864.62 63.71 o 10 0 2 4.82 7.51 37.72 o 11 0 2 8595.58 8712.42 294.30 o 12 0 2 198.09 306.86 86.24 o 13 0 2 362.96 257.80 88.21 o 14 0 2 747.15 720.41 133.05 o 15 0 2 980.40 224.06 467.82 o 1 1 2 1366.03 1335.38 36.64 o 2 1 2 20.59 -0.01 16.65 o 3 1 2 14557.62 14330.47 113.37 o 4 1 2 3978.81 4138.60 64.00 o 5 1 2 4126.31 4151.83 68.86 o 6 1 2 1285.80 1234.18 43.28 o 7 1 2 39.77 37.49 18.16 o 8 1 2 58.49 75.60 21.23 o 9 1 2 2793.43 2825.20 79.93 o 10 1 2 9.35 15.36 28.39 o 11 1 2 3991.78 3840.62 104.96 o 12 1 2 1257.66 1244.51 89.19 o 13 1 2 1191.76 1222.75 101.39 o 14 1 2 304.57 317.48 69.98 o 15 1 2 498.51 262.11 192.36 o 0 2 2 17174.60 17924.08 188.24 o 1 2 2 10.45 14.48 11.42 o 2 2 2 5046.18 5012.17 65.71 o 3 2 2 52476.35 54446.30 333.38 o 4 2 2 2351.24 2414.25 57.99 o 5 2 2 17114.18 17104.99 161.43 o 6 2 2 11449.64 11866.12 133.61 o 7 2 2 5050.71 4957.98 95.76 o 8 2 2 2213.36 2248.34 73.02 o 9 2 2 1509.78 1471.03 64.91 o 10 2 2 21.83 16.03 29.90 o 11 2 2 7010.71 6873.25 131.22 o 12 2 2 487.65 493.60 52.25 o 13 2 2 147.75 141.52 44.85 o 14 2 2 586.40 568.76 71.27 o 15 2 2 983.94 289.83 324.30 o 1 3 2 234.24 229.60 28.36 o 2 3 2 478.63 530.50 23.96 o 3 3 2 9523.24 9168.46 82.39 o 4 3 2 747.44 748.13 36.81 o 5 3 2 4903.12 4939.15 79.75 o 6 3 2 883.97 895.00 46.03 o 7 3 2 52.18 42.08 29.11 o 8 3 2 42.16 46.32 30.12 o 9 3 2 1200.18 1163.75 63.10 o 10 3 2 219.32 244.01 43.06 o 11 3 2 1715.01 1733.34 79.65 o 12 3 2 761.98 763.74 61.79 o 13 3 2 1159.53 1155.39 73.72 o 14 3 2 204.78 170.91 46.54 o 0 4 2 15030.62 15787.09 222.83 o 1 4 2 8.87 0.88 26.00 o 2 4 2 3061.93 2949.62 49.54 o 3 4 2 27263.46 27912.55 163.49 o 4 4 2 620.50 624.11 31.30 o 5 4 2 9182.52 9145.70 113.39 o 6 4 2 3214.39 3312.62 77.54 o 7 4 2 3203.36 3186.60 80.85 o 8 4 2 1323.35 1342.03 66.16 o 9 4 2 1054.03 1072.28 64.30 o 10 4 2 97.06 84.75 37.36 o 11 4 2 4361.13 4200.43 115.52 o 12 4 2 745.48 736.58 65.41 o 13 4 2 93.39 74.54 39.41 o 14 4 2 323.28 242.08 57.09 o 1 5 2 40.18 53.02 32.80 o 2 5 2 287.36 341.69 42.07 o 3 5 2 4721.38 4612.02 83.21 o 4 5 2 111.31 122.13 27.67 o 5 5 2 1482.87 1524.99 61.17 o 6 5 2 532.51 532.14 43.37 o 7 5 2 15.65 15.66 30.12 o 8 5 2 45.95 51.60 34.30 o 9 5 2 664.12 663.67 56.58 o 10 5 2 364.24 372.53 50.50 o 11 5 2 983.15 1040.67 89.65 o 12 5 2 419.34 496.95 66.03 o 13 5 2 691.05 784.33 79.44 o 0 6 2 4882.65 4674.03 139.54 o 1 6 2 30.25 36.00 33.60 o 2 6 2 1129.86 1147.98 59.01 o 3 6 2 8344.95 8359.56 125.38 o 4 6 2 154.37 123.08 42.47 o 5 6 2 3516.93 3614.78 103.02 o 6 6 2 964.08 1082.78 87.81 o 7 6 2 826.31 778.38 80.48 o 8 6 2 657.70 648.99 72.47 o 9 6 2 266.69 319.45 61.70 o 10 6 2 32.62 61.03 49.23 o 11 6 2 2166.39 2063.99 313.36 o 1 7 2 8.21 -5.61 33.17 o 2 7 2 69.40 78.11 36.13 o 3 7 2 1650.71 1721.06 85.24 o 4 7 2 102.56 91.63 48.78 o 5 7 2 388.94 477.50 72.42 o 6 7 2 215.34 158.09 56.45 o 7 7 2 7.36 7.49 47.85 o 8 7 2 4.73 7.67 46.81 o 9 7 2 416.65 99.23 108.06 o 10 7 2 138.09 70.84 54.72 o 0 8 2 1105.66 1183.13 112.11 o 1 8 2 2.13 -25.01 41.05 o 2 8 2 328.88 363.62 66.15 o 3 8 2 2835.27 3008.78 167.41 o 4 8 2 81.30 56.72 64.25 o 5 8 2 1210.80 1299.47 145.11 o 6 8 2 656.49 231.77 176.35 o 7 8 2 244.17 66.80 64.53 o 1 9 2 44.60 45.57 50.47 o 2 9 2 19.13 72.94 64.53 o 1 0 3 264.65 254.94 57.05 o 2 0 3 21955.00 21793.59 209.20 o 3 0 3 5774.22 6008.16 146.61 o 4 0 3 84702.84 83078.41 1071.19 o 5 0 3 4902.83 4939.27 136.10 o 6 0 3 14.99 4.33 37.65 o 7 0 3 240.87 332.22 60.27 o 8 0 3 5749.00 5746.48 137.42 o 9 0 3 422.24 438.54 56.83 o 10 0 3 5449.97 5149.79 224.14 o 11 0 3 64.39 22.58 60.09 o 12 0 3 3478.84 3435.78 205.26 o 13 0 3 566.67 605.25 120.28 o 14 0 3 706.44 650.66 124.06 o 15 0 3 48.09 49.33 30.37 o 0 1 3 4416.96 4845.46 123.43 o 1 1 3 5236.70 5230.38 88.72 o 2 1 3 8307.46 8111.92 102.54 o 3 1 3 1080.45 1101.60 44.91 o 4 1 3 10.76 11.26 21.82 o 5 1 3 939.25 932.62 48.83 o 6 1 3 4786.13 5133.06 99.63 o 7 1 3 1062.95 1162.61 58.60 o 8 1 3 360.17 384.33 35.00 o 9 1 3 733.76 751.10 58.38 o 10 1 3 6338.53 6357.32 138.83 o 11 1 3 687.65 725.72 69.41 o 12 1 3 35.94 38.63 46.72 o 13 1 3 154.41 239.67 62.20 o 14 1 3 1279.61 1258.50 128.77 o 15 1 3 122.99 39.03 31.08 o 1 2 3 472.14 460.37 31.31 o 2 2 3 14312.72 14026.33 111.57 o 3 2 3 3814.93 3721.16 67.49 o 4 2 3 52400.36 53950.55 272.62 o 5 2 3 2161.69 2006.98 54.08 o 6 2 3 23.96 17.77 22.23 o 7 2 3 338.64 338.03 43.45 o 8 2 3 3435.62 3650.65 101.08 o 9 2 3 106.70 110.33 35.56 o 10 2 3 5178.07 5214.92 115.29 o 11 2 3 283.14 299.94 45.15 o 12 2 3 3145.56 3101.60 115.43 o 13 2 3 338.39 367.26 70.94 o 14 2 3 472.80 333.78 151.54 o 0 3 3 297.07 325.99 48.69 o 1 3 3 4050.99 3941.24 80.72 o 2 3 3 5077.46 5125.44 71.83 o 3 3 3 43.67 18.41 19.22 o 4 3 3 287.79 327.41 31.30 o 5 3 3 565.97 563.40 40.38 o 6 3 3 884.66 942.08 49.85 o 7 3 3 218.24 213.02 38.43 o 8 3 3 306.33 348.78 42.05 o 9 3 3 962.38 1101.18 63.56 o 10 3 3 4284.35 4156.52 108.42 o 11 3 3 508.58 504.95 55.01 o 12 3 3 17.41 27.81 34.94 o 13 3 3 210.71 259.33 49.93 o 14 3 3 925.55 522.40 258.74 o 1 4 3 577.60 604.47 46.14 o 2 4 3 9130.02 9047.12 145.52 o 3 4 3 1322.33 1292.66 42.80 o 4 4 3 23142.43 24357.18 205.92 o 5 4 3 1438.39 1484.64 58.50 o 6 4 3 43.54 14.39 27.10 o 7 4 3 85.67 85.16 33.32 o 8 4 3 1614.38 1702.99 70.64 o 9 4 3 5.51 3.89 29.45 o 10 4 3 4409.94 4424.67 135.89 o 11 4 3 297.82 297.02 49.71 o 12 4 3 1965.91 1945.39 92.37 o 13 4 3 126.04 141.72 41.90 o 0 5 3 85.14 134.21 57.53 o 1 5 3 1332.32 1307.53 65.28 o 2 5 3 2761.44 2755.41 88.02 o 3 5 3 220.06 212.34 41.79 o 4 5 3 150.72 138.80 49.20 o 5 5 3 308.98 351.87 57.72 o 6 5 3 163.62 189.22 51.78 o 7 5 3 199.58 247.82 54.98 o 8 5 3 269.18 319.04 59.41 o 9 5 3 314.02 384.46 63.50 o 10 5 3 1736.42 1773.57 105.18 o 11 5 3 204.46 169.78 54.86 o 12 5 3 101.71 130.22 55.82 o 1 6 3 22.67 62.46 39.21 o 2 6 3 4333.63 4147.93 102.96 o 3 6 3 411.50 460.35 55.69 o 4 6 3 9962.28 10000.21 186.30 o 5 6 3 1201.99 1176.44 81.47 o 6 6 3 26.85 14.08 49.34 o 7 6 3 1.30 11.48 50.52 o 8 6 3 887.49 953.24 91.91 o 9 6 3 15.97 47.77 51.12 o 10 6 3 2405.33 2833.51 153.36 o 11 6 3 47.53 21.73 32.57 o 0 7 3 74.17 106.15 53.90 o 1 7 3 330.64 329.92 47.06 o 2 7 3 1134.86 1113.43 70.02 o 3 7 3 195.10 230.58 51.22 o 4 7 3 8.84 23.19 41.69 o 5 7 3 129.37 128.15 55.07 o 6 7 3 311.23 287.73 66.38 o 7 7 3 142.67 181.25 61.41 o 8 7 3 186.29 53.60 51.10 o 9 7 3 71.37 29.66 33.59 o 1 8 3 6.15 -37.77 42.07 o 2 8 3 1210.04 1185.18 95.64 o 3 8 3 176.34 215.40 61.90 o 4 8 3 3632.09 3552.96 204.55 o 5 8 3 252.29 192.60 73.89 o 6 8 3 18.36 30.88 25.79 o 0 0 4 20225.79 20744.85 462.09 o 1 0 4 7220.35 7132.27 193.44 o 2 0 4 78.06 87.30 47.15 o 3 0 4 30572.55 32156.84 296.51 o 4 0 4 620.94 634.26 58.38 o 5 0 4 8407.55 8854.49 251.25 o 6 0 4 2569.75 2691.91 124.77 o 7 0 4 340.77 347.82 69.31 o 8 0 4 8592.04 8565.74 238.44 o 9 0 4 7105.69 7543.27 209.78 o 10 0 4 523.73 549.22 104.35 o 11 0 4 4314.46 3991.92 209.10 o 12 0 4 40.83 83.29 70.90 o 13 0 4 26.78 62.11 71.81 o 14 0 4 363.21 149.01 109.44 o 1 1 4 2629.35 2559.55 76.21 o 2 1 4 2707.23 2742.39 86.35 o 3 1 4 1793.23 1753.38 59.07 o 4 1 4 1642.83 1485.20 54.38 o 5 1 4 256.26 258.39 36.25 o 6 1 4 3823.79 4130.32 118.09 o 7 1 4 691.58 714.87 56.20 o 8 1 4 57.33 39.31 39.37 o 9 1 4 3509.04 3500.18 122.86 o 10 1 4 210.30 292.45 49.57 o 11 1 4 342.63 386.17 70.27 o 12 1 4 104.04 163.35 58.55 o 13 1 4 444.18 369.22 74.08 o 14 1 4 532.96 301.95 147.62 o 0 2 4 16464.36 16556.63 247.08 o 1 2 4 5874.44 5325.19 121.19 o 2 2 4 286.05 269.30 37.99 o 3 2 4 22606.58 21367.10 177.86 o 4 2 4 2.84 16.94 31.41 o 5 2 4 7177.25 7613.45 122.39 o 6 2 4 414.93 386.79 42.46 o 7 2 4 152.73 131.19 42.29 o 8 2 4 7239.48 7361.86 164.75 o 9 2 4 5491.32 5600.36 135.39 o 10 2 4 249.63 253.13 48.75 o 11 2 4 3716.74 3798.96 123.43 o 12 2 4 56.02 19.71 48.85 o 13 2 4 38.15 52.05 50.84 o 14 2 4 312.64 300.77 70.69 o 1 3 4 486.89 508.09 41.59 o 2 3 4 1260.65 1202.84 49.68 o 3 3 4 537.48 512.89 34.74 o 4 3 4 3777.24 3674.24 98.97 o 5 3 4 150.14 169.23 34.76 o 6 3 4 3286.97 3117.11 82.30 o 7 3 4 735.70 883.08 56.33 o 8 3 4 50.00 47.43 33.54 o 9 3 4 3329.08 3243.45 91.93 o 10 3 4 345.53 416.67 54.67 o 11 3 4 468.02 443.23 58.92 o 12 3 4 33.72 39.24 37.82 o 13 3 4 212.39 126.41 70.16 o 0 4 4 13093.73 13557.83 241.95 o 1 4 4 3156.29 2933.11 109.73 o 2 4 4 134.31 99.86 48.00 o 3 4 4 12157.52 12051.81 201.41 o 4 4 4 26.85 30.79 46.23 o 5 4 4 4180.48 4060.34 132.31 o 6 4 4 9.86 12.50 27.99 o 7 4 4 38.62 52.01 31.79 o 8 4 4 4484.59 4712.59 104.76 o 9 4 4 3198.99 3411.02 99.55 o 10 4 4 204.60 256.22 46.79 o 11 4 4 2241.74 2156.10 100.42 o 12 4 4 153.01 124.66 49.05 o 13 4 4 24.29 -8.59 45.17 o 1 5 4 343.57 312.23 48.02 o 2 5 4 1425.82 1483.49 80.96 o 3 5 4 114.63 114.30 53.90 o 4 5 4 1748.58 1825.03 101.41 o 5 5 4 15.43 11.02 46.33 o 6 5 4 1552.71 1605.39 91.69 o 7 5 4 768.79 813.21 76.68 o 8 5 4 1.07 26.62 46.98 o 9 5 4 1909.24 1947.44 107.74 o 10 5 4 496.78 558.60 74.24 o 11 5 4 214.68 222.89 62.90 o 12 5 4 33.98 33.79 43.10 o 0 6 4 7031.07 7284.30 231.24 o 1 6 4 1431.49 1493.22 79.74 o 2 6 4 9.47 31.08 35.33 o 3 6 4 5811.85 5825.96 166.29 o 4 6 4 9.79 17.77 48.97 o 5 6 4 1904.13 2021.79 104.38 o 6 6 4 14.27 14.29 45.22 o 7 6 4 35.03 0.07 48.65 o 8 6 4 2047.32 1949.82 118.77 o 9 6 4 1573.44 1499.05 121.97 o 10 6 4 219.68 87.41 67.05 o 1 7 4 254.38 301.18 53.14 o 2 7 4 741.61 761.44 71.91 o 3 7 4 72.78 80.84 52.00 o 4 7 4 311.40 344.55 64.81 o 5 7 4 19.22 -14.81 48.75 o 6 7 4 486.00 570.08 81.54 o 7 7 4 361.05 249.35 61.52 o 8 7 4 24.90 25.72 24.81 o 0 8 4 1641.42 1696.42 140.72 o 1 8 4 412.49 391.69 61.67 o 2 8 4 4.25 38.46 44.01 o 3 8 4 1785.88 1912.22 109.41 o 4 8 4 5.92 7.47 47.16 o 5 8 4 685.17 256.52 157.31 o 1 0 5 23236.88 23071.38 447.07 o 2 0 5 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