#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/23/2222353.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222353_Fobs loop_ _publ_author_name 'Temel, Ersin' 'Erer, Hakan' 'Ye\,silel, Okan Zafer' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; Diaquabis(1,3-propanediamine)nickel(II) squarate tetrahydrate ; _journal_coeditor_code HK2703 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m735 _journal_page_last m736 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.570 _cell_angle_gamma 90.000 _cell_length_a 8.0429 _cell_length_b 9.1752 _cell_length_c 14.6510 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.7688 _[local]_cod_data_source_file hk2703Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' okan31 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2014.67 2041.40 40.84 o 2 0 0 294.64 319.51 6.70 o 3 0 0 4592.44 4597.34 45.59 o 4 0 0 33.57 37.16 2.47 o 5 0 0 1547.36 1548.50 27.19 o 6 0 0 893.56 887.74 4.59 o 7 0 0 514.41 509.29 9.49 o 8 0 0 604.31 616.64 9.87 o 9 0 0 167.45 168.54 10.46 o 1 1 0 40.52 37.27 3.63 o 2 1 0 3006.60 3129.60 8.80 o 3 1 0 0.56 2.75 1.99 o 4 1 0 55.76 60.68 1.69 o 5 1 0 22.38 25.14 1.69 o 6 1 0 6.08 7.64 1.48 o 7 1 0 0.22 1.21 1.39 o 8 1 0 9.65 7.49 1.83 o 9 1 0 1.37 1.09 1.95 o 0 2 0 9373.63 8950.15 22.21 o 1 2 0 56.89 77.75 3.09 o 2 2 0 7.64 9.73 2.15 o 3 2 0 1267.31 1180.32 11.45 o 4 2 0 936.44 907.61 12.98 o 5 2 0 738.39 710.11 10.87 o 6 2 0 441.49 450.07 4.43 o 7 2 0 281.39 297.26 3.25 o 8 2 0 159.00 175.32 2.41 o 9 2 0 71.79 65.20 2.18 o 1 3 0 26.03 18.97 2.09 o 2 3 0 75.39 95.42 4.20 o 3 3 0 29.17 29.26 1.82 o 4 3 0 0.14 1.10 1.70 o 5 3 0 77.34 75.71 2.31 o 6 3 0 114.39 107.17 2.11 o 7 3 0 54.73 46.58 1.96 o 8 3 0 8.30 15.15 1.77 o 0 4 0 126.60 116.77 5.03 o 1 4 0 408.83 381.64 2.86 o 2 4 0 3074.99 3058.57 17.26 o 3 4 0 4217.38 4118.18 37.37 o 4 4 0 107.48 94.92 2.15 o 5 4 0 689.95 689.03 3.64 o 6 4 0 593.76 584.12 13.94 o 7 4 0 22.62 20.87 1.77 o 8 4 0 216.75 229.88 3.97 o 1 5 0 1901.80 1888.80 14.32 o 2 5 0 89.43 85.61 1.96 o 3 5 0 3.08 4.94 1.85 o 4 5 0 139.40 123.64 4.59 o 5 5 0 105.18 102.55 4.78 o 6 5 0 16.05 17.42 2.40 o 7 5 0 18.35 22.48 2.53 o 8 5 0 0.34 2.25 2.22 o 0 6 0 29.94 43.41 2.36 o 1 6 0 1337.49 1346.86 10.65 o 2 6 0 2351.76 2302.12 21.09 o 3 6 0 1552.40 1567.26 9.08 o 4 6 0 442.31 442.04 3.64 o 5 6 0 181.69 187.21 4.77 o 6 6 0 485.04 474.71 8.42 o 7 6 0 130.35 125.08 5.73 o 8 6 0 65.56 53.53 3.00 o 1 7 0 108.40 113.07 1.76 o 2 7 0 3.99 3.68 1.49 o 3 7 0 259.16 265.04 2.91 o 4 7 0 63.77 64.23 2.49 o 5 7 0 50.08 53.80 2.04 o 6 7 0 11.81 14.49 2.26 o 7 7 0 9.86 9.95 2.14 o 0 8 0 181.88 162.30 5.12 o 1 8 0 171.83 181.40 1.97 o 2 8 0 310.75 327.72 3.15 o 3 8 0 211.33 215.28 5.17 o 4 8 0 192.93 190.64 2.56 o 5 8 0 124.50 138.53 3.00 o 6 8 0 119.94 117.95 2.19 o 1 9 0 0.06 1.84 1.92 o 2 9 0 1.36 1.55 1.80 o 3 9 0 8.10 6.53 2.37 o 4 9 0 19.57 20.56 3.16 o 5 9 0 2.07 2.20 2.58 o 6 9 0 15.03 19.01 3.26 o 0 10 0 656.98 648.41 17.85 o 1 10 0 537.49 571.17 7.03 o 2 10 0 204.38 223.64 2.26 o 3 10 0 30.22 25.52 2.15 o 4 10 0 330.74 331.86 6.15 o 5 10 0 132.07 125.61 4.70 o 1 11 0 25.49 27.33 2.03 o 2 11 0 58.64 60.42 2.16 o 3 11 0 4.32 4.83 2.68 o -9 1 1 87.11 83.13 3.18 o -8 1 1 203.15 208.70 2.32 o -7 1 1 394.75 408.70 2.46 o -6 1 1 793.37 786.67 3.85 o -5 1 1 1244.72 1185.10 3.81 o -4 1 1 2788.12 2868.93 14.91 o -3 1 1 1409.29 1391.13 5.51 o -2 1 1 228.20 260.30 3.36 o -1 1 1 8599.03 8036.41 45.59 o 0 1 1 2143.09 2158.54 21.09 o 1 1 1 4120.44 4288.79 30.35 o 2 1 1 3751.73 3912.23 19.53 o 3 1 1 4527.15 4572.13 37.65 o 4 1 1 245.78 240.25 2.33 o 5 1 1 5.13 4.15 1.47 o 6 1 1 1125.60 1140.20 5.19 o 7 1 1 325.94 325.54 2.43 o 8 1 1 225.20 237.49 3.67 o -9 2 1 4.81 6.75 2.00 o -8 2 1 60.03 62.40 1.84 o -7 2 1 203.91 200.50 2.28 o -6 2 1 431.18 395.34 5.83 o -5 2 1 285.51 277.69 7.40 o -4 2 1 0.31 0.87 1.59 o -3 2 1 1030.82 1084.77 9.92 o -2 2 1 593.53 574.65 4.37 o -1 2 1 268.91 294.73 6.05 o 0 2 1 985.20 1011.87 8.31 o 1 2 1 65.77 58.38 2.67 o 2 2 1 1790.19 1774.12 6.19 o 3 2 1 2206.00 2324.76 19.96 o 4 2 1 570.21 539.85 11.23 o 5 2 1 207.04 206.79 2.11 o 6 2 1 1.05 0.15 1.60 o 7 2 1 192.01 183.99 2.24 o 8 2 1 11.55 15.25 1.91 o -9 3 1 118.23 124.45 2.52 o -8 3 1 116.27 121.56 2.08 o -7 3 1 145.08 156.59 2.41 o -6 3 1 236.07 236.52 3.79 o -5 3 1 656.18 620.15 8.71 o -4 3 1 573.25 586.07 7.16 o -3 3 1 1132.79 1057.53 4.85 o -2 3 1 1030.94 936.97 4.90 o -1 3 1 226.20 246.28 2.92 o 0 3 1 1128.24 1141.85 6.85 o 1 3 1 900.40 917.16 8.73 o 2 3 1 371.36 320.97 3.74 o 3 3 1 2575.34 2587.93 24.30 o 4 3 1 1192.82 1172.46 7.73 o 5 3 1 304.34 296.85 2.70 o 6 3 1 340.25 339.01 4.56 o 7 3 1 115.50 117.06 2.13 o 8 3 1 77.98 73.21 2.16 o -8 4 1 13.12 13.35 2.07 o -7 4 1 146.53 136.80 3.39 o -6 4 1 403.31 398.74 3.73 o -5 4 1 83.54 81.98 2.44 o -4 4 1 17.32 20.27 1.86 o -3 4 1 93.97 90.42 2.53 o -2 4 1 1092.51 1069.72 12.22 o -1 4 1 449.69 500.69 3.12 o 0 4 1 268.76 285.33 2.63 o 1 4 1 1479.52 1609.57 22.22 o 2 4 1 760.16 730.51 7.47 o 3 4 1 1.09 0.72 1.45 o 4 4 1 623.82 608.73 4.08 o 5 4 1 1.37 3.76 1.90 o 6 4 1 77.68 75.41 1.99 o 7 4 1 9.67 12.64 1.82 o 8 4 1 0.05 0.89 1.94 o -8 5 1 148.90 137.88 2.27 o -7 5 1 427.44 427.01 20.98 o -6 5 1 144.24 140.40 4.03 o -5 5 1 401.86 384.74 8.27 o -4 5 1 1447.33 1476.33 12.21 o -3 5 1 1652.60 1594.60 5.25 o -2 5 1 4132.06 4117.43 13.31 o -1 5 1 2133.53 2011.56 7.14 o 0 5 1 2572.92 2453.39 16.80 o 1 5 1 1317.27 1239.78 4.82 o 2 5 1 447.22 454.81 5.77 o 3 5 1 246.07 224.71 4.84 o 4 5 1 1730.32 1723.40 5.05 o 5 5 1 1083.02 1048.40 5.24 o 6 5 1 203.00 212.63 5.10 o 7 5 1 209.61 216.93 3.02 o 8 5 1 31.50 27.33 2.72 o -8 6 1 40.73 38.76 2.07 o -7 6 1 0.10 -1.92 2.49 o -6 6 1 21.02 23.61 1.99 o -5 6 1 1.64 3.21 2.87 o -4 6 1 148.36 154.06 3.83 o -3 6 1 7.04 4.15 1.89 o -2 6 1 19.76 23.03 1.65 o -1 6 1 232.78 222.73 2.16 o 0 6 1 24.01 25.01 1.47 o 1 6 1 34.21 40.98 1.77 o 2 6 1 159.26 158.26 2.56 o 3 6 1 316.62 296.96 3.06 o 4 6 1 0.48 2.98 4.39 o 5 6 1 101.55 95.23 2.50 o 6 6 1 5.95 5.17 2.42 o 7 6 1 0.90 1.00 2.14 o -7 7 1 160.59 158.63 9.46 o -6 7 1 232.56 247.92 12.77 o -5 7 1 234.21 245.48 4.51 o -4 7 1 42.84 43.06 2.40 o -3 7 1 510.24 513.46 3.80 o -2 7 1 559.12 565.81 6.22 o -1 7 1 292.58 270.76 4.40 o 0 7 1 1279.65 1296.75 3.86 o 1 7 1 304.15 289.35 3.56 o 2 7 1 373.60 404.13 2.76 o 3 7 1 382.52 391.17 7.31 o 4 7 1 74.98 84.63 2.63 o 5 7 1 513.62 514.56 6.62 o 6 7 1 256.20 256.94 6.86 o 7 7 1 25.65 22.67 1.97 o -7 8 1 6.50 4.31 2.15 o -6 8 1 0.22 0.58 2.85 o -5 8 1 114.66 114.82 5.01 o -4 8 1 12.22 9.74 1.72 o -3 8 1 439.31 434.04 6.17 o -2 8 1 175.48 164.82 2.65 o -1 8 1 21.49 22.80 1.71 o 0 8 1 28.19 29.27 1.69 o 1 8 1 146.15 148.57 1.92 o 2 8 1 74.21 65.47 1.71 o 3 8 1 270.67 273.90 3.00 o 4 8 1 4.80 8.37 2.47 o 5 8 1 155.30 158.07 2.89 o 6 8 1 16.99 17.32 1.85 o -6 9 1 231.72 206.68 2.73 o -5 9 1 120.93 127.32 2.88 o -4 9 1 105.62 107.73 4.17 o -3 9 1 101.16 115.27 4.32 o -2 9 1 170.02 183.03 2.31 o -1 9 1 609.58 615.53 2.98 o 0 9 1 123.51 131.45 2.02 o 1 9 1 616.28 635.44 5.09 o 2 9 1 478.92 495.39 5.40 o 3 9 1 98.73 106.32 3.49 o 4 9 1 64.10 67.25 3.32 o 5 9 1 122.59 131.02 7.95 o -5 10 1 0.32 2.34 2.74 o -4 10 1 17.12 16.69 2.15 o -3 10 1 30.29 28.73 3.80 o -2 10 1 2.10 1.74 1.73 o -1 10 1 69.02 69.44 2.02 o 0 10 1 1.40 1.35 1.74 o 1 10 1 1.54 0.03 1.76 o 2 10 1 25.03 27.67 2.02 o 3 10 1 2.29 6.63 2.54 o 4 10 1 4.76 4.39 2.15 o -3 11 1 316.94 317.77 20.86 o -2 11 1 233.74 235.02 7.47 o -1 11 1 168.00 160.20 4.29 o 0 11 1 286.42 286.40 5.63 o 1 11 1 160.74 172.64 3.19 o 2 11 1 125.10 124.89 2.22 o 3 11 1 212.90 213.52 2.76 o -9 0 2 182.10 180.64 4.92 o -8 0 2 1139.27 1154.13 13.47 o -7 0 2 289.41 314.60 6.69 o -6 0 2 37.37 37.09 3.30 o -5 0 2 7519.34 7465.71 118.89 o -4 0 2 1948.93 1904.56 12.99 o -3 0 2 62.02 54.42 2.96 o -2 0 2 13575.65 12623.34 27.66 o -1 0 2 3732.40 3613.09 37.50 o 0 0 2 11471.77 12535.84 44.75 o 1 0 2 395.90 383.59 5.31 o 2 0 2 128.99 109.25 2.58 o 3 0 2 2046.24 2069.77 20.71 o 4 0 2 946.25 900.46 5.79 o 5 0 2 1296.17 1323.80 5.06 o 6 0 2 172.58 175.75 4.48 o 7 0 2 168.37 167.39 5.04 o 8 0 2 216.96 222.97 3.33 o -9 1 2 0.98 1.63 1.84 o -8 1 2 6.77 9.23 1.58 o -7 1 2 9.67 12.63 1.49 o -6 1 2 4.73 5.12 1.45 o -5 1 2 71.22 64.70 2.07 o -4 1 2 28.95 34.07 1.82 o -3 1 2 4606.77 4660.52 24.58 o -2 1 2 42.13 32.05 2.01 o -1 1 2 156.34 146.24 3.23 o 0 1 2 144.12 163.14 3.14 o 1 1 2 76.61 88.89 2.83 o 2 1 2 3367.46 3593.21 19.62 o 3 1 2 43.64 42.95 1.62 o 4 1 2 45.85 44.21 1.78 o 5 1 2 91.19 92.19 1.70 o 6 1 2 38.99 34.31 1.80 o 7 1 2 5.76 5.92 1.44 o 8 1 2 8.90 9.82 1.71 o -9 2 2 96.01 100.12 2.24 o -8 2 2 361.75 384.09 4.34 o -7 2 2 374.22 386.69 4.87 o -6 2 2 54.80 48.68 1.60 o -5 2 2 1098.70 1116.96 11.38 o -4 2 2 794.78 741.42 5.80 o -3 2 2 73.99 101.41 2.02 o -2 2 2 2892.23 2897.58 39.34 o -1 2 2 3757.24 3906.57 68.76 o 0 2 2 1185.95 1230.89 10.85 o 1 2 2 2296.70 2302.37 12.11 o 2 2 2 1213.61 1223.63 10.60 o 3 2 2 578.40 577.50 7.77 o 4 2 2 1293.45 1247.62 16.37 o 5 2 2 654.27 682.68 7.83 o 6 2 2 180.42 184.60 2.17 o 7 2 2 332.79 326.08 2.54 o 8 2 2 182.32 173.81 3.66 o -9 3 2 11.19 12.88 1.89 o -8 3 2 16.85 17.26 1.96 o -7 3 2 9.10 8.77 1.72 o -6 3 2 197.66 195.98 3.03 o -5 3 2 188.75 179.36 2.41 o -4 3 2 19.60 20.03 1.80 o -3 3 2 850.29 829.05 6.79 o -2 3 2 458.98 497.88 8.81 o -1 3 2 9111.21 9043.74 117.04 o 0 3 2 4095.67 4171.21 33.69 o 1 3 2 191.95 236.74 2.68 o 2 3 2 256.16 280.24 4.07 o 3 3 2 186.32 191.47 3.70 o 4 3 2 0.66 2.28 1.46 o 5 3 2 150.29 139.89 2.04 o 6 3 2 32.30 31.13 1.56 o 7 3 2 180.13 183.68 3.94 o 8 3 2 27.99 33.37 2.06 o -9 4 2 21.77 18.89 3.45 o -8 4 2 285.85 306.73 3.24 o -7 4 2 162.59 155.78 2.18 o -6 4 2 426.31 436.31 14.19 o -5 4 2 714.23 716.35 12.57 o -4 4 2 112.49 97.27 2.10 o -3 4 2 4062.46 4011.18 19.66 o -2 4 2 4137.78 4033.84 45.61 o -1 4 2 347.29 307.36 2.64 o 0 4 2 998.94 1007.88 12.16 o 1 4 2 1555.54 1476.21 17.83 o 2 4 2 650.28 598.27 8.30 o 3 4 2 1977.77 1955.24 32.33 o 4 4 2 361.25 350.49 4.31 o 5 4 2 422.01 450.36 3.98 o 6 4 2 649.99 673.69 9.44 o 7 4 2 56.68 52.77 1.93 o 8 4 2 118.80 124.89 3.49 o -8 5 2 0.78 2.57 3.67 o -7 5 2 46.16 49.86 4.23 o -6 5 2 7.76 7.19 1.61 o -5 5 2 14.26 16.37 2.18 o -4 5 2 296.79 294.24 5.07 o -3 5 2 88.64 98.68 1.99 o -2 5 2 256.88 252.03 3.94 o -1 5 2 860.46 887.28 7.58 o 0 5 2 9.29 11.64 1.67 o 1 5 2 6.59 5.99 1.53 o 2 5 2 40.94 42.42 1.80 o 3 5 2 35.78 33.20 1.95 o 4 5 2 15.60 15.02 1.56 o 5 5 2 2.82 4.68 2.32 o 6 5 2 0.57 3.27 2.11 o 7 5 2 8.92 13.65 1.81 o -8 6 2 82.14 83.03 2.46 o -7 6 2 295.30 302.00 3.36 o -6 6 2 582.32 595.66 18.00 o -5 6 2 259.66 275.01 2.60 o -4 6 2 872.61 816.40 11.56 o -3 6 2 1534.72 1595.23 15.95 o -2 6 2 1283.74 1237.94 4.46 o -1 6 2 832.02 843.96 10.29 o 0 6 2 10.77 8.59 1.61 o 1 6 2 1932.22 1884.84 11.97 o 2 6 2 1145.05 1095.33 5.07 o 3 6 2 302.50 320.98 3.04 o 4 6 2 477.58 473.71 9.56 o 5 6 2 250.49 259.17 2.90 o 6 6 2 297.57 283.05 4.02 o 7 6 2 75.89 72.55 2.39 o -7 7 2 4.48 7.09 2.07 o -6 7 2 2.49 -1.56 1.87 o -5 7 2 18.09 19.35 2.94 o -4 7 2 76.53 76.92 1.91 o -3 7 2 162.94 151.13 3.21 o -2 7 2 695.90 668.29 6.66 o -1 7 2 55.19 55.54 1.58 o 0 7 2 451.38 450.71 2.66 o 1 7 2 155.55 146.33 1.84 o 2 7 2 670.31 664.12 3.49 o 3 7 2 100.18 102.43 2.11 o 4 7 2 1.53 0.80 1.67 o 5 7 2 0.21 0.36 1.73 o 6 7 2 32.67 29.87 2.73 o -7 8 2 172.48 175.70 6.88 o -6 8 2 142.98 139.19 2.45 o -5 8 2 167.66 171.79 7.27 o -4 8 2 180.67 200.52 2.84 o -3 8 2 39.02 40.91 2.36 o -2 8 2 104.00 102.09 3.94 o -1 8 2 133.61 141.68 1.97 o 0 8 2 646.90 647.16 3.87 o 1 8 2 957.47 973.86 8.50 o 2 8 2 670.99 685.11 7.14 o 3 8 2 126.78 133.47 2.33 o 4 8 2 117.37 127.94 2.46 o 5 8 2 125.46 129.44 3.29 o 6 8 2 55.09 53.50 2.38 o -6 9 2 2.30 3.35 2.14 o -5 9 2 14.25 14.85 2.13 o -4 9 2 5.04 9.35 2.43 o -3 9 2 72.73 73.20 2.37 o -2 9 2 45.75 48.38 2.06 o -1 9 2 34.54 30.80 1.75 o 0 9 2 26.44 28.82 1.74 o 1 9 2 21.82 21.64 1.49 o 2 9 2 165.98 167.89 2.39 o 3 9 2 8.07 6.70 1.99 o 4 9 2 1.56 1.16 2.50 o 5 9 2 9.93 9.13 3.63 o -5 10 2 160.51 146.35 2.66 o -4 10 2 448.24 460.98 24.93 o -3 10 2 155.50 167.44 3.54 o -2 10 2 125.10 134.03 2.79 o -1 10 2 279.03 285.38 3.39 o 0 10 2 523.47 550.62 6.36 o 1 10 2 176.10 177.55 2.57 o 2 10 2 130.25 133.78 2.79 o 3 10 2 122.87 123.29 3.30 o 4 10 2 222.38 219.16 2.92 o -3 11 2 31.73 33.07 2.88 o -2 11 2 5.95 7.56 1.97 o -1 11 2 3.26 3.86 1.64 o 0 11 2 22.94 26.70 1.74 o 1 11 2 1.06 1.93 1.89 o 2 11 2 3.64 5.98 1.87 o -9 1 3 108.16 107.60 2.00 o -8 1 3 61.39 66.57 1.88 o -7 1 3 459.16 453.71 3.92 o -6 1 3 2273.55 2312.19 16.46 o -5 1 3 2968.83 2863.71 25.54 o -4 1 3 1083.74 975.26 9.51 o -3 1 3 317.43 309.01 3.27 o -2 1 3 3832.25 3917.98 20.20 o -1 1 3 3237.12 3379.70 12.06 o 0 1 3 1209.22 1331.08 13.82 o 2 1 3 4208.98 4149.32 22.77 o 3 1 3 198.65 191.48 2.27 o 4 1 3 768.47 780.46 3.14 o 5 1 3 3.25 5.66 1.65 o 6 1 3 479.47 485.28 5.44 o 7 1 3 584.89 588.92 5.77 o 8 1 3 55.05 51.06 2.10 o -9 2 3 3.70 3.06 1.71 o -8 2 3 0.19 -1.08 1.87 o -7 2 3 87.95 84.19 1.94 o -6 2 3 78.67 73.68 1.70 o -5 2 3 93.32 100.89 1.71 o -4 2 3 29.25 27.27 1.64 o -3 2 3 1.14 2.02 1.66 o -2 2 3 5058.77 5111.39 84.00 o -1 2 3 446.17 509.73 7.07 o 0 2 3 1054.77 1116.91 11.55 o 1 2 3 5.45 5.36 1.80 o 2 2 3 14.54 10.66 1.84 o 3 2 3 223.24 219.46 4.90 o 4 2 3 45.90 43.22 1.67 o 5 2 3 114.82 120.27 1.87 o 6 2 3 0.29 0.98 1.78 o 7 2 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