#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222400.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222400_Fobs loop_ _publ_author_name 'Wu, Huilu' 'Yun, Ruirui' 'Li, Ke' 'Tao, Sun' 'Wang, Kaitong' _publ_section_title ; Bis[1,3-bis(1-benzyl-1H-benzimidazol-2-yl)-2-oxapropane]zinc(II) dipicrate dimethylformamide disolvate ; _journal_coeditor_code LH2840 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m786 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.267 _cell_angle_gamma 90.000 _cell_length_a 13.3235 _cell_length_b 18.1630 _cell_length_c 30.0144 _exptl_crystal_F_000 3296.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file lh2840Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' G0557 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 601.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 23733.41 20745.97 138.98 o 3 0 0 55.99 409.09 191.61 o 4 0 0 5154.34 4798.15 54.45 o 5 0 0 611.15 725.89 24.00 o 6 0 0 37.59 53.59 18.05 o 7 0 0 7273.58 6825.12 91.74 o 8 0 0 1349.13 1396.10 38.88 o 9 0 0 352.36 495.87 39.53 o 10 0 0 554.41 611.58 40.58 o 11 0 0 3689.59 3657.38 177.52 o 12 0 0 9.76 34.29 35.67 o 13 0 0 1242.30 1416.83 79.16 o 14 0 0 4337.94 4748.16 184.16 o 15 0 0 227.08 235.54 192.12 o 16 0 0 5.08 12.26 73.57 o 17 0 0 1147.16 1190.54 713.95 o 2 1 0 20154.01 18913.89 76.07 o 3 1 0 24570.15 23061.37 109.00 o 4 1 0 4542.60 3875.06 32.05 o 5 1 0 4996.65 4835.90 37.53 o 6 1 0 85.80 138.13 16.55 o 7 1 0 2684.14 2684.38 34.19 o 8 1 0 4240.38 4397.40 43.94 o 9 1 0 777.65 921.29 28.68 o 10 1 0 439.05 562.37 40.91 o 11 1 0 376.59 515.52 32.01 o 12 1 0 444.23 429.39 39.96 o 13 1 0 3.76 -3.66 27.05 o 14 1 0 1.06 -33.37 36.13 o 15 1 0 634.43 333.80 159.17 o 16 1 0 318.35 119.35 97.50 o 17 1 0 19.97 6.64 39.32 o 2 2 0 954.28 882.81 10.06 o 3 2 0 14686.17 13987.99 64.50 o 4 2 0 6827.70 6255.69 38.37 o 5 2 0 2295.10 1993.12 24.60 o 6 2 0 13321.97 13423.62 87.54 o 7 2 0 18120.28 17616.05 112.45 o 8 2 0 1122.31 1128.09 30.55 o 9 2 0 1.43 30.49 18.51 o 10 2 0 6154.50 6382.76 64.28 o 11 2 0 2813.38 2875.39 54.29 o 12 2 0 3172.77 3261.28 67.78 o 13 2 0 964.06 1042.43 54.75 o 14 2 0 774.48 780.76 62.09 o 15 2 0 493.36 385.73 152.13 o 16 2 0 1.38 4.05 39.81 o 17 2 0 6.00 -2.06 64.21 o 1 3 0 9673.51 8678.41 92.54 o 2 3 0 23.15 37.20 7.98 o 3 3 0 17605.13 16858.19 77.74 o 4 3 0 468.62 447.86 13.07 o 5 3 0 1641.57 1567.38 20.63 o 6 3 0 16770.81 16546.21 96.97 o 7 3 0 294.11 359.11 21.79 o 8 3 0 1729.96 1921.00 33.54 o 9 3 0 128.49 147.75 25.18 o 10 3 0 1213.44 1335.46 51.83 o 11 3 0 132.44 216.16 29.45 o 12 3 0 79.13 102.61 32.61 o 13 3 0 44.46 34.69 27.58 o 14 3 0 151.01 91.26 62.22 o 15 3 0 13.98 12.85 34.81 o 16 3 0 176.59 40.04 51.23 o 17 3 0 123.93 49.14 49.01 o 0 4 0 9580.53 8735.92 75.09 o 1 4 0 79746.30 82097.24 426.28 o 2 4 0 51862.43 51093.48 238.52 o 3 4 0 153.12 129.41 10.12 o 4 4 0 6688.82 5924.85 36.72 o 5 4 0 1930.31 2074.44 24.33 o 6 4 0 743.75 674.21 21.47 o 7 4 0 5912.17 5275.79 47.53 o 8 4 0 1941.72 2042.28 34.38 o 9 4 0 288.33 325.94 27.31 o 10 4 0 3017.78 3263.75 56.82 o 11 4 0 6488.53 6718.34 77.78 o 12 4 0 6301.18 7016.26 80.47 o 13 4 0 134.40 122.58 43.21 o 14 4 0 1491.00 1578.56 55.27 o 15 4 0 99.41 10.19 51.84 o 16 4 0 101.57 49.07 41.59 o 1 5 0 8295.79 7322.52 62.35 o 2 5 0 12715.35 12096.22 153.59 o 3 5 0 7072.57 6683.13 55.29 o 4 5 0 2408.26 2182.16 29.30 o 5 5 0 6739.49 6502.22 44.64 o 6 5 0 143.76 131.24 16.34 o 7 5 0 2405.68 2925.24 33.37 o 8 5 0 148.75 154.17 21.47 o 9 5 0 398.70 467.88 28.03 o 10 5 0 4581.68 4841.14 63.84 o 11 5 0 31.26 41.24 24.59 o 12 5 0 3160.97 3371.15 63.61 o 13 5 0 510.85 536.76 38.71 o 14 5 0 4.77 35.96 39.83 o 15 5 0 56.33 46.45 33.99 o 16 5 0 16.54 38.31 43.79 o 0 6 0 6453.01 5123.68 153.59 o 1 6 0 20003.55 19717.23 130.68 o 2 6 0 23.54 67.10 15.78 o 3 6 0 15200.49 14367.62 79.84 o 4 6 0 203.25 237.39 13.43 o 5 6 0 1173.40 1048.82 23.92 o 6 6 0 5041.30 5397.68 44.89 o 7 6 0 11384.49 11351.47 75.27 o 8 6 0 3060.24 3179.85 40.67 o 9 6 0 28.02 29.63 19.29 o 10 6 0 1022.39 1073.08 37.60 o 11 6 0 41.45 17.09 25.40 o 12 6 0 196.58 192.16 34.64 o 13 6 0 302.24 259.97 41.30 o 14 6 0 1294.51 1460.36 51.48 o 15 6 0 700.05 675.07 107.57 o 16 6 0 122.68 80.74 39.29 o 1 7 0 1095.75 1149.32 26.62 o 2 7 0 7823.70 7301.53 47.28 o 3 7 0 2881.23 2880.75 32.19 o 4 7 0 5644.84 5766.38 56.80 o 5 7 0 7758.67 7781.05 52.00 o 6 7 0 2923.50 2808.85 31.22 o 7 7 0 124.83 122.90 17.57 o 8 7 0 1261.38 1422.73 32.12 o 9 7 0 1181.37 1134.63 36.59 o 10 7 0 76.55 72.64 24.87 o 11 7 0 600.49 582.17 34.78 o 12 7 0 1239.99 1231.72 49.75 o 13 7 0 1211.74 1200.98 49.09 o 14 7 0 12.03 35.54 30.47 o 15 7 0 9.86 -13.02 30.22 o 16 7 0 103.82 99.75 52.38 o 0 8 0 21659.52 20885.94 177.61 o 1 8 0 6970.01 6415.13 59.31 o 2 8 0 6846.99 7201.43 56.14 o 3 8 0 21110.46 20145.82 129.29 o 4 8 0 938.75 750.30 20.42 o 5 8 0 948.96 947.88 28.09 o 6 8 0 4776.95 5153.25 46.34 o 7 8 0 5498.61 5512.33 51.59 o 8 8 0 1534.36 1671.89 38.12 o 9 8 0 43.71 32.51 18.83 o 10 8 0 1411.10 1567.51 44.33 o 11 8 0 4566.23 4605.76 64.67 o 12 8 0 284.83 267.28 35.72 o 13 8 0 174.55 172.85 36.17 o 14 8 0 520.26 437.05 51.95 o 15 8 0 363.87 344.90 49.89 o 16 8 0 0.86 -35.58 38.16 o 1 9 0 182.36 208.43 26.22 o 2 9 0 5564.02 5307.17 50.32 o 3 9 0 2337.31 2697.80 31.65 o 4 9 0 12573.65 13295.02 130.43 o 5 9 0 174.63 198.53 20.90 o 6 9 0 31.03 37.72 18.99 o 7 9 0 256.14 267.62 22.08 o 8 9 0 1390.03 1412.83 32.93 o 9 9 0 111.69 136.78 22.66 o 10 9 0 254.63 247.94 36.34 o 11 9 0 85.56 97.29 29.67 o 12 9 0 2394.22 2517.96 58.11 o 13 9 0 138.17 168.41 39.47 o 14 9 0 82.48 79.43 39.35 o 15 9 0 253.22 171.16 41.54 o 0 10 0 10863.44 10191.50 107.88 o 1 10 0 4251.99 4518.60 64.08 o 2 10 0 580.84 577.15 33.53 o 3 10 0 13026.33 12166.81 83.91 o 4 10 0 1772.94 1641.39 28.88 o 5 10 0 783.54 800.84 28.49 o 6 10 0 59.13 56.86 18.40 o 7 10 0 1745.47 1770.33 42.40 o 8 10 0 1354.48 1459.62 33.47 o 9 10 0 8.51 20.89 19.33 o 10 10 0 2848.19 2885.34 49.56 o 11 10 0 932.35 1106.79 54.56 o 12 10 0 191.72 266.12 34.56 o 13 10 0 393.23 397.49 41.22 o 14 10 0 327.32 258.24 57.46 o 15 10 0 761.07 581.14 136.66 o 1 11 0 11.81 17.10 19.72 o 2 11 0 4845.77 4830.52 53.22 o 3 11 0 6554.26 6801.76 58.05 o 4 11 0 4417.04 4385.50 51.31 o 5 11 0 9.35 16.68 18.27 o 6 11 0 424.62 466.85 29.42 o 7 11 0 181.93 203.29 26.58 o 8 11 0 4984.84 5126.92 65.71 o 9 11 0 936.75 1024.22 38.81 o 10 11 0 263.34 269.82 33.07 o 11 11 0 1.02 11.86 26.95 o 12 11 0 3.84 0.95 23.31 o 13 11 0 470.07 372.37 77.94 o 14 11 0 104.27 68.42 34.71 o 15 11 0 8.80 -2.21 28.27 o 0 12 0 563.29 464.03 52.13 o 1 12 0 364.50 387.33 28.91 o 2 12 0 664.25 609.28 26.55 o 3 12 0 136.70 129.68 21.69 o 4 12 0 3428.64 3281.05 46.48 o 5 12 0 332.54 381.50 23.34 o 6 12 0 179.33 160.93 26.61 o 7 12 0 5080.38 5050.59 82.50 o 8 12 0 22.91 10.55 20.28 o 9 12 0 410.37 397.12 33.56 o 10 12 0 573.64 564.53 38.72 o 11 12 0 205.74 247.85 47.87 o 12 12 0 301.92 268.08 42.72 o 13 12 0 238.43 139.33 37.26 o 14 12 0 1425.32 1320.21 89.69 o 1 13 0 88.28 96.71 26.03 o 2 13 0 3957.64 4033.92 51.64 o 3 13 0 753.10 677.59 26.56 o 4 13 0 2506.10 2620.35 41.41 o 5 13 0 13.10 7.65 16.95 o 6 13 0 661.05 663.74 32.48 o 7 13 0 1531.19 1614.40 48.42 o 8 13 0 294.48 300.17 41.30 o 9 13 0 109.93 104.35 35.24 o 10 13 0 189.24 190.49 33.82 o 11 13 0 96.74 89.23 32.86 o 12 13 0 128.12 78.96 39.88 o 13 13 0 6.99 14.90 41.90 o 14 13 0 43.84 1.87 52.80 o 0 14 0 3665.13 3388.96 106.42 o 1 14 0 992.51 1056.16 38.61 o 2 14 0 1854.12 1911.37 43.99 o 3 14 0 1740.26 1745.48 36.09 o 4 14 0 3399.44 3509.65 49.32 o 5 14 0 19.06 14.16 20.21 o 6 14 0 1487.79 1584.85 38.34 o 7 14 0 3997.81 4191.58 60.69 o 8 14 0 2275.61 2362.92 64.68 o 9 14 0 112.73 117.99 33.56 o 10 14 0 6.05 43.53 43.23 o 11 14 0 37.42 55.61 32.65 o 12 14 0 71.04 20.55 34.62 o 13 14 0 0.40 58.35 71.84 o 1 15 0 1536.71 1599.29 52.18 o 2 15 0 4300.12 4009.83 137.72 o 3 15 0 2748.46 2748.42 44.89 o 4 15 0 123.77 131.58 31.64 o 5 15 0 4076.94 4176.60 59.08 o 6 15 0 216.73 167.80 26.36 o 7 15 0 118.45 121.85 30.41 o 8 15 0 2224.95 2173.59 52.41 o 9 15 0 7555.79 7437.33 215.15 o 10 15 0 2440.08 2316.53 121.75 o 11 15 0 11.86 22.03 40.86 o 12 15 0 1152.00 1493.93 128.65 o 13 15 0 624.68 446.27 182.43 o 0 16 0 44.74 0.00 37.81 o 1 16 0 5992.94 5951.13 83.68 o 2 16 0 3607.72 3399.80 60.69 o 3 16 0 491.04 486.31 32.73 o 4 16 0 1706.98 1773.18 45.24 o 5 16 0 1268.71 1234.02 42.06 o 6 16 0 32.93 40.75 25.22 o 7 16 0 211.46 165.15 29.99 o 8 16 0 110.65 97.66 33.56 o 9 16 0 151.22 113.68 36.57 o 10 16 0 234.77 202.93 37.54 o 11 16 0 102.71 77.26 31.24 o 12 16 0 20.16 10.74 84.47 o 1 17 0 983.23 1087.29 55.35 o 2 17 0 1143.84 1190.16 45.48 o 3 17 0 131.86 131.59 27.51 o 4 17 0 1.78 -3.34 18.90 o 5 17 0 3231.31 3360.31 59.39 o 6 17 0 346.78 379.27 39.93 o 7 17 0 7.24 41.57 28.25 o 8 17 0 487.74 441.44 39.59 o 9 17 0 3979.72 3793.61 127.49 o 10 17 0 1142.44 1079.85 73.04 o 11 17 0 101.14 110.31 64.44 o 0 18 0 1620.09 1625.51 157.44 o 1 18 0 370.59 379.86 44.73 o 2 18 0 281.70 295.76 35.16 o 3 18 0 1016.44 983.36 40.14 o 4 18 0 560.01 592.98 37.09 o 5 18 0 794.96 804.88 51.15 o 6 18 0 406.83 347.36 41.35 o 7 18 0 2010.10 2145.02 72.29 o 8 18 0 3.80 3.19 28.88 o 9 18 0 439.04 311.85 42.04 o 10 18 0 60.03 153.69 68.17 o 11 18 0 68.95 91.02 65.52 o 1 19 0 172.01 145.83 43.75 o 2 19 0 655.11 638.82 43.17 o 3 19 0 2635.54 2651.57 69.65 o 4 19 0 448.36 508.14 41.45 o 5 19 0 830.33 865.85 47.23 o 6 19 0 195.91 149.35 35.95 o 7 19 0 0.51 -7.27 21.33 o 8 19 0 6.69 -13.44 32.14 o 9 19 0 1047.10 1211.21 85.64 o 10 19 0 1184.25 1250.46 91.60 o 0 20 0 9.28 4.46 33.59 o 1 20 0 19.76 39.74 36.30 o 2 20 0 44.78 -0.63 27.53 o 3 20 0 617.60 517.50 48.32 o 4 20 0 242.27 226.24 35.75 o 5 20 0 142.55 144.38 33.97 o 6 20 0 56.28 69.78 35.93 o 7 20 0 584.39 432.97 105.40 o 8 20 0 0.32 1.26 31.46 o 9 20 0 80.89 129.35 108.47 o 1 21 0 339.36 338.12 44.10 o 2 21 0 56.65 75.78 42.11 o 3 21 0 2282.66 2458.36 66.00 o 4 21 0 103.85 92.58 46.29 o 5 21 0 1126.52 1161.11 57.72 o 6 21 0 1148.17 1136.02 50.32 o 7 21 0 0.41 6.15 28.93 o 0 22 0 1010.10 1038.46 123.67 o 1 22 0 141.23 174.59 58.76 o 2 22 0 23.08 35.60 43.24 o 3 22 0 68.52 23.93 47.59 o 4 22 0 74.30 80.03 44.72 o 5 22 0 292.58 272.13 59.06 o 6 22 0 112.45 113.03 41.32 o 1 23 0 582.92 347.68 268.27 o 2 23 0 200.30 135.92 63.34 o 3 23 0 229.92 136.27 132.85 o -17 1 1 5.37 -6.65 37.90 o -16 1 1 760.47 4.09 73.59 o -15 1 1 636.28 642.91 448.15 o -14 1 1 93.38 98.07 45.07 o -13 1 1 171.62 193.44 40.30 o -12 1 1 562.18 706.70 37.48 o -11 1 1 2.04 11.25 21.77 o -10 1 1 9853.03 10609.99 90.67 o -9 1 1 21.21 34.15 18.96 o -8 1 1 3260.83 3333.72 41.67 o -7 1 1 1405.84 1769.27 29.64 o -6 1 1 1657.99 1793.58 32.12 o -5 1 1 52886.89 52626.90 262.95 o -4 1 1 1754.63 1556.04 22.48 o -3 1 1 50186.79 49759.32 232.17 o -2 1 1 30.77 68.13 14.20 o 2 1 1 16042.30 14695.32 59.28 o 3 1 1 5386.89 4985.33 33.08 o 4 1 1 6458.19 6002.78 40.44 o 5 1 1 67.49 79.51 12.81 o 6 1 1 5362.17 5106.26 43.17 o 7 1 1 2458.97 2699.96 32.65 o 8 1 1 892.36 857.15 28.92 o 9 1 1 11043.63 11046.27 80.70 o 10 1 1 1193.92 1254.30 35.17 o 11 1 1 1781.88 1898.37 52.97 o 12 1 1 2522.61 2773.38 62.00 o 13 1 1 1389.12 1602.98 48.42 o 14 1 1 97.19 71.60 41.75 o 15 1 1 47.59 38.62 37.67 o 16 1 1 112.55 -10.97 41.31 o 17 1 1 95.40 8.61 37.34 o -17 2 1 0.30 4.90 46.84 o -16 2 1 8.57 9.09 46.48 o -15 2 1 2.24 4.43 31.83 o -14 2 1 29.82 55.47 45.98 o -13 2 1 171.86 132.52 38.71 o -12 2 1 27.19 25.34 26.72 o -11 2 1 2942.10 3059.65 54.09 o -10 2 1 1428.89 1438.72 38.34 o -9 2 1 126.02 173.89 27.42 o -8 2 1 22.66 34.60 19.27 o -7 2 1 2665.21 2860.25 37.72 o -6 2 1 3255.51 3086.52 35.24 o -5 2 1 4151.82 3763.14 35.02 o -4 2 1 9386.27 9543.76 59.57 o -3 2 1 2545.19 2429.25 20.83 o -2 2 1 17423.58 16808.96 69.03 o 2 2 1 4167.99 3707.30 21.10 o 3 2 1 615.74 454.47 12.47 o 4 2 1 21.77 35.57 9.88 o 5 2 1 4783.52 4713.34 52.26 o 6 2 1 5137.85 5208.09 44.46 o 7 2 1 8069.65 8828.16 78.57 o 8 2 1 269.05 324.86 20.03 o 9 2 1 1648.75 1837.78 33.52 o 10 2 1 503.57 559.03 32.48 o 11 2 1 810.43 798.73 36.29 o 12 2 1 28.87 47.54 27.11 o 13 2 1 2.82 -27.59 30.29 o 14 2 1 1648.71 1699.25 60.77 o 15 2 1 33.85 32.04 34.67 o 16 2 1 6.74 16.59 36.92 o 17 2 1 41.24 17.48 48.04 o -17 3 1 173.37 90.46 86.59 o -16 3 1 791.34 1094.29 74.66 o -15 3 1 139.35 31.00 45.78 o -14 3 1 822.07 710.21 120.01 o -13 3 1 247.89 308.75 48.45 o -12 3 1 5496.24 6125.25 72.28 o -11 3 1 349.04 404.90 33.58 o -10 3 1 2666.98 2919.58 52.06 o -9 3 1 4673.31 4876.49 54.33 o -8 3 1 1952.92 2076.01 34.70 o -7 3 1 2124.75 2223.00 32.45 o -6 3 1 447.15 563.77 22.07 o -5 3 1 8886.25 8200.36 66.51 o -4 3 1 5897.22 5669.40 35.90 o -3 3 1 964.77 672.35 13.96 o -2 3 1 14290.72 13556.91 59.33 o -1 3 1 4949.60 4604.31 24.58 o 0 3 1 8803.75 8261.47 43.19 o 1 3 1 5769.55 5161.45 40.58 o 2 3 1 74625.84 75999.98 314.80 o 3 3 1 522.12 478.42 12.83 o 4 3 1 4163.67 3672.81 26.49 o 5 3 1 15911.73 15048.31 79.48 o 6 3 1 5351.67 6001.30 43.04 o 7 3 1 88.97 156.58 17.02 o 8 3 1 4573.97 4665.60 51.83 o 9 3 1 8402.44 8770.59 96.80 o 10 3 1 134.46 164.52 23.52 o 11 3 1 94.22 98.90 29.06 o 12 3 1 696.72 892.11 40.67 o 13 3 1 1912.80 2255.32 66.06 o 14 3 1 824.38 1090.91 66.14 o 15 3 1 112.55 -1.62 39.20 o 16 3 1 264.37 165.98 93.85 o -16 4 1 387.91 190.11 136.01 o -15 4 1 1.44 28.42 42.33 o -14 4 1 59.15 38.89 45.13 o -13 4 1 110.82 150.82 35.38 o -12 4 1 10.68 -21.98 26.97 o -11 4 1 752.32 831.44 38.68 o -10 4 1 287.59 322.46 29.24 o -9 4 1 52.44 62.94 22.16 o -8 4 1 530.66 480.52 24.65 o -7 4 1 6947.77 7106.69 59.82 o -6 4 1 9682.09 9851.99 66.34 o -5 4 1 1759.47 1636.12 22.51 o -4 4 1 1400.69 1527.84 18.96 o -3 4 1 416.24 565.79 24.38 o -2 4 1 330.11 339.21 10.28 o -1 4 1 1151.99 974.39 20.07 o 0 4 1 75294.73 75956.59 389.01 o 1 4 1 27458.66 25888.58 134.33 o 2 4 1 14640.78 14229.75 73.34 o 3 4 1 59832.54 60785.90 262.44 o 4 4 1 11673.30 10721.21 58.21 o 5 4 1 3182.84 3073.98 28.02 o 6 4 1 2161.07 2059.09 28.25 o 7 4 1 3070.75 2874.70 36.09 o 8 4 1 1483.30 1494.05 38.84 o 9 4 1 903.54 996.85 32.11 o 10 4 1 592.43 591.83 34.22 o 11 4 1 177.21 198.32 29.42 o 12 4 1 30.82 19.54 29.60 o 13 4 1 41.04 30.17 28.93 o 14 4 1 2328.53 2467.84 74.24 o 15 4 1 4.44 7.00 28.50 o 16 4 1 561.93 364.01 118.63 o -16 5 1 37.35 15.06 42.77 o -15 5 1 19.99 14.69 32.28 o -14 5 1 176.37 160.34 38.60 o -13 5 1 168.96 183.22 43.03 o -12 5 1 244.52 159.06 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