#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/24/2222408.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222408_Fobs loop_ _publ_author_name 'Ciborska, Anna' 'Baranowska, Katarzyna' 'Wojnowski, Wies\/law' _publ_section_title ; Bis(3,5-dimethylpyridine-\kN)bis(tri-tert-butoxysilanethiolato-\kS)chromium(II) toluene solvate ; _journal_coeditor_code NG2589 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m763 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.047 _cell_angle_gamma 90.000 _cell_length_a 19.6147 _cell_length_b 17.1521 _cell_length_c 17.2221 _exptl_crystal_F_000 1984.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ng2589Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 529.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 175277.61 185234.42 487.47 o 6 0 0 27797.83 24019.43 69.81 o 8 0 0 84758.60 107095.80 1666.97 o 10 0 0 22146.40 23386.67 55.83 o 12 0 0 21105.85 21156.22 124.32 o 14 0 0 334.23 366.27 24.15 o 16 0 0 7906.22 8547.88 450.25 o 18 0 0 9245.42 10265.84 150.93 o 20 0 0 617.24 725.25 101.15 o 22 0 0 2.34 55.88 36.58 o 3 1 0 41593.55 41978.55 346.15 o 5 1 0 346.61 169.61 13.43 o 7 1 0 14338.03 13970.36 74.64 o 9 1 0 31400.15 39513.42 362.31 o 11 1 0 12184.60 11614.67 123.34 o 13 1 0 4736.75 4726.41 55.85 o 15 1 0 32.01 41.64 14.86 o 17 1 0 2291.67 2565.42 86.01 o 19 1 0 2593.20 2645.85 93.66 o 21 1 0 182.78 239.99 39.88 o 2 2 0 6352.15 4385.51 56.60 o 4 2 0 65417.77 80009.41 400.66 o 6 2 0 4151.06 7704.93 53.01 o 8 2 0 3586.63 4817.74 37.77 o 10 2 0 3808.49 3631.36 37.75 o 12 2 0 2615.64 2064.22 34.03 o 14 2 0 2614.68 2525.21 37.85 o 16 2 0 4623.94 4903.33 193.17 o 18 2 0 4476.53 4847.92 164.10 o 20 2 0 62.39 105.14 33.91 o 22 2 0 120.73 162.15 35.98 o 1 3 0 23777.04 27434.44 148.49 o 3 3 0 96427.75 102607.64 729.07 o 5 3 0 91.82 279.77 17.23 o 7 3 0 10874.59 10712.82 93.74 o 9 3 0 3625.64 4772.67 42.65 o 11 3 0 2444.38 2038.86 36.22 o 13 3 0 6.29 26.45 11.01 o 15 3 0 5867.55 5450.31 45.87 o 17 3 0 8823.50 8954.90 138.10 o 19 3 0 733.63 691.47 46.53 o 21 3 0 209.59 127.81 32.04 o 0 4 0 96186.87 108197.67 675.32 o 2 4 0 76361.82 94567.44 655.13 o 4 4 0 2420.87 3220.58 23.02 o 6 4 0 10477.14 7938.88 135.77 o 8 4 0 1561.84 2119.15 31.43 o 10 4 0 9331.12 9266.61 87.15 o 12 4 0 599.33 437.48 15.62 o 14 4 0 2.44 27.23 14.09 o 16 4 0 2529.92 2394.82 87.45 o 18 4 0 5207.21 5066.98 267.31 o 20 4 0 8.90 53.87 22.93 o 22 4 0 563.57 689.76 49.15 o 1 5 0 138.36 111.86 9.10 o 3 5 0 63983.71 68374.23 697.30 o 5 5 0 4290.61 2115.71 50.59 o 7 5 0 2173.31 2198.77 42.14 o 9 5 0 2408.88 2597.65 47.58 o 11 5 0 761.05 592.93 36.26 o 13 5 0 6.60 9.50 13.30 o 15 5 0 4473.91 4313.01 119.05 o 17 5 0 4568.61 4505.56 232.72 o 19 5 0 2.84 53.85 21.31 o 21 5 0 4.59 24.83 22.01 o 0 6 0 81401.19 83595.45 709.60 o 2 6 0 4417.08 5258.07 46.08 o 4 6 0 153.69 267.20 17.78 o 6 6 0 20093.82 19105.15 207.87 o 8 6 0 1514.81 1888.76 38.32 o 10 6 0 1873.86 1668.45 60.62 o 12 6 0 6002.51 5326.34 138.91 o 14 6 0 20.10 28.85 19.49 o 16 6 0 1021.54 1070.69 61.25 o 18 6 0 4432.00 4534.47 174.35 o 20 6 0 432.55 519.99 30.91 o 1 7 0 5170.78 5476.17 67.70 o 3 7 0 3774.34 4520.22 51.25 o 5 7 0 2607.15 1566.75 67.14 o 7 7 0 27853.10 30235.74 704.21 o 9 7 0 56.72 65.95 18.09 o 11 7 0 7588.04 7343.33 73.23 o 13 7 0 231.32 138.47 28.28 o 15 7 0 14.72 33.56 21.92 o 17 7 0 2443.98 2474.43 160.88 o 19 7 0 426.68 279.26 27.89 o 21 7 0 168.96 132.15 27.64 o 0 8 0 58672.13 63489.24 724.78 o 2 8 0 151.86 405.41 12.93 o 4 8 0 1303.46 1167.02 17.12 o 6 8 0 6724.27 6280.68 107.47 o 8 8 0 571.87 765.50 59.76 o 10 8 0 39.61 37.78 18.12 o 12 8 0 4527.20 4470.26 50.26 o 14 8 0 387.86 402.53 30.12 o 16 8 0 962.15 1019.17 38.42 o 18 8 0 3569.05 3803.93 47.98 o 20 8 0 711.45 773.19 45.40 o 1 9 0 22.29 14.94 8.34 o 3 9 0 12685.95 12375.80 121.84 o 5 9 0 2438.75 2029.85 31.85 o 7 9 0 1280.11 1246.26 35.85 o 9 9 0 180.37 234.04 46.24 o 11 9 0 967.97 907.02 31.60 o 13 9 0 17.16 32.63 20.41 o 15 9 0 883.39 790.54 55.19 o 17 9 0 702.35 703.16 69.22 o 19 9 0 27.68 60.59 21.09 o 0 10 0 8726.41 7312.71 179.11 o 2 10 0 216.28 320.16 17.10 o 4 10 0 1039.63 1224.55 22.09 o 6 10 0 10025.15 10335.32 41.87 o 8 10 0 2471.58 2381.88 47.70 o 10 10 0 4366.40 4331.29 117.49 o 12 10 0 106.41 113.69 24.18 o 14 10 0 215.18 215.96 32.61 o 16 10 0 706.45 701.35 31.83 o 18 10 0 962.53 1020.33 54.97 o 1 11 0 2248.76 2290.57 37.43 o 3 11 0 10531.96 10406.59 100.40 o 5 11 0 6830.46 6616.35 123.79 o 7 11 0 3.16 30.84 16.97 o 9 11 0 19.40 37.73 20.07 o 11 11 0 1020.43 1100.23 35.30 o 13 11 0 100.65 136.37 25.88 o 15 11 0 1.30 21.72 17.96 o 17 11 0 1934.28 2105.69 127.75 o 19 11 0 148.49 143.89 43.44 o 0 12 0 2059.39 1573.14 112.04 o 2 12 0 610.22 467.88 37.38 o 4 12 0 3092.07 3205.20 36.44 o 6 12 0 8613.42 8822.49 145.08 o 8 12 0 4787.15 5038.17 62.53 o 10 12 0 1153.43 1112.85 39.74 o 12 12 0 37.34 46.59 17.94 o 14 12 0 2.55 24.92 22.17 o 16 12 0 24.50 27.95 24.69 o 18 12 0 176.62 195.99 47.52 o 1 13 0 294.69 318.40 25.19 o 3 13 0 2477.28 2304.59 38.08 o 5 13 0 1394.34 1340.83 25.36 o 7 13 0 1.72 31.33 16.53 o 9 13 0 709.09 773.14 59.96 o 11 13 0 327.45 304.06 25.79 o 13 13 0 119.91 109.38 24.35 o 15 13 0 1001.70 1064.08 74.49 o 17 13 0 2.93 29.06 27.17 o 0 14 0 4050.96 3750.60 60.62 o 2 14 0 3119.00 3100.53 61.10 o 4 14 0 123.97 80.96 13.27 o 6 14 0 113.87 157.76 18.29 o 8 14 0 651.71 666.54 64.92 o 10 14 0 1289.75 1290.86 49.00 o 12 14 0 609.78 633.45 63.52 o 14 14 0 912.36 909.01 48.15 o 16 14 0 32.91 29.27 33.36 o 1 15 0 14.53 38.36 18.00 o 3 15 0 724.66 653.51 29.42 o 5 15 0 320.34 268.98 21.54 o 7 15 0 38.65 36.99 13.22 o 9 15 0 5116.46 5675.29 82.61 o 11 15 0 748.79 863.12 42.41 o 13 15 0 8.52 28.85 23.45 o 15 15 0 9.82 10.72 21.39 o 0 16 0 6.17 57.43 71.16 o 2 16 0 3035.80 2900.85 31.99 o 4 16 0 362.68 299.72 21.62 o 6 16 0 207.39 180.77 24.64 o 8 16 0 768.63 868.06 50.58 o 10 16 0 900.14 969.44 62.77 o 12 16 0 1172.41 1190.12 91.90 o 14 16 0 333.52 350.57 39.93 o 1 17 0 1196.50 1044.29 30.32 o 3 17 0 805.92 788.24 34.36 o 5 17 0 218.96 225.97 27.91 o 7 17 0 94.50 121.82 56.01 o 9 17 0 5095.84 5471.15 72.93 o 11 17 0 1.25 50.32 31.62 o 13 17 0 181.34 141.98 35.87 o 0 18 0 3522.84 3487.07 97.86 o 2 18 0 1683.19 1766.14 53.12 o 4 18 0 88.45 90.13 24.23 o 6 18 0 401.94 390.04 30.27 o 8 18 0 2904.18 3132.95 70.90 o 10 18 0 3900.06 4423.57 82.67 o 1 19 0 300.82 289.36 29.21 o 3 19 0 104.64 77.21 21.86 o 5 19 0 1502.18 1483.98 56.02 o 7 19 0 137.52 115.62 26.83 o 9 19 0 3318.71 3783.44 69.63 o 0 20 0 3565.84 3830.37 105.88 o 2 20 0 1820.71 1806.94 42.42 o 4 20 0 25.63 41.64 19.65 o 6 20 0 1000.92 1070.53 44.86 o 1 21 0 804.02 735.72 46.54 o -21 1 1 486.78 460.06 63.91 o -19 1 1 1846.12 1901.41 105.87 o -17 1 1 187.85 163.61 28.83 o -15 1 1 2784.26 2824.32 66.89 o -13 1 1 90.43 101.42 17.32 o -11 1 1 7249.02 7198.52 26.84 o -9 1 1 1844.36 1814.22 46.05 o -7 1 1 3400.41 3126.71 49.18 o -5 1 1 1363.42 1408.89 39.01 o -3 1 1 356.61 381.86 10.31 o 3 1 1 1827.56 1655.83 11.90 o 5 1 1 6165.25 6086.31 74.47 o 7 1 1 3498.01 3870.03 48.26 o 9 1 1 1557.81 1969.40 28.72 o 11 1 1 1379.18 1439.97 21.17 o 13 1 1 238.68 271.08 17.80 o 15 1 1 158.26 199.64 19.83 o 17 1 1 438.41 362.66 76.97 o 19 1 1 15.81 92.75 33.75 o 21 1 1 32.19 71.97 31.03 o -22 2 1 263.61 236.72 39.17 o -20 2 1 658.47 686.19 70.52 o -18 2 1 1033.30 977.44 76.44 o -16 2 1 0.77 85.34 53.10 o -14 2 1 117.31 155.82 19.19 o -12 2 1 2640.70 2317.24 35.81 o -10 2 1 581.08 753.63 13.81 o -8 2 1 4565.73 4720.64 32.57 o -6 2 1 12383.87 15430.47 114.78 o -4 2 1 81.88 156.00 28.15 o -2 2 1 443.83 228.97 9.93 o 0 2 1 2813.49 3396.85 8.54 o 2 2 1 162.48 114.19 7.74 o 4 2 1 1721.46 2213.07 47.05 o 6 2 1 829.52 783.22 47.61 o 8 2 1 359.22 416.57 30.40 o 10 2 1 957.99 956.38 25.05 o 12 2 1 89.16 75.17 10.89 o 14 2 1 1664.14 1558.50 45.16 o 16 2 1 495.08 490.98 30.69 o 18 2 1 774.06 832.40 64.73 o 20 2 1 32.55 84.66 29.76 o -21 3 1 3.95 26.35 24.90 o -19 3 1 67.38 107.29 57.00 o -17 3 1 29.66 80.16 36.36 o -15 3 1 5471.84 5711.84 136.12 o -13 3 1 59.06 42.85 9.69 o -11 3 1 81.92 49.81 10.34 o -9 3 1 368.86 518.39 11.65 o -7 3 1 259.59 275.86 14.52 o -5 3 1 2227.33 2681.08 114.84 o -3 3 1 25.73 11.80 6.81 o -1 3 1 87.07 200.55 6.66 o 1 3 1 38.41 48.26 5.97 o 3 3 1 1728.68 2349.41 32.87 o 5 3 1 5186.77 6959.59 73.30 o 7 3 1 5970.77 6851.28 64.81 o 9 3 1 311.55 479.29 25.43 o 11 3 1 10.19 31.83 12.77 o 13 3 1 130.70 98.45 20.88 o 15 3 1 101.58 98.52 20.29 o 17 3 1 1788.14 1697.37 110.76 o 19 3 1 31.44 34.80 18.85 o 21 3 1 21.95 59.61 23.80 o -22 4 1 67.71 30.67 24.01 o -20 4 1 134.32 134.39 26.60 o -18 4 1 641.69 549.62 71.06 o -16 4 1 73.13 66.38 34.93 o -14 4 1 0.64 8.41 11.47 o -12 4 1 4366.89 4121.23 38.88 o -10 4 1 338.83 303.56 20.90 o -8 4 1 20016.76 20832.89 237.79 o -6 4 1 8592.99 11049.70 295.40 o -4 4 1 5226.22 5150.19 55.19 o -2 4 1 17475.39 21704.25 223.32 o 0 4 1 21028.49 25796.46 175.43 o 2 4 1 2240.85 1830.95 27.71 o 4 4 1 1611.62 1439.95 46.98 o 6 4 1 1581.19 1533.39 22.57 o 8 4 1 6897.07 7726.34 63.21 o 10 4 1 1961.26 1699.86 38.36 o 12 4 1 495.74 428.35 15.31 o 14 4 1 2878.58 2759.05 59.87 o 16 4 1 2043.24 2030.64 77.00 o 18 4 1 75.19 62.71 24.08 o 20 4 1 517.41 479.09 43.59 o -21 5 1 1075.48 1188.71 65.33 o -19 5 1 7.71 53.53 24.31 o -17 5 1 786.84 819.35 72.52 o -15 5 1 6683.58 6460.48 102.50 o -13 5 1 2931.32 2630.70 107.25 o -11 5 1 190.16 159.36 14.66 o -9 5 1 5048.27 5113.57 119.62 o -7 5 1 15.05 90.33 23.04 o -5 5 1 3900.32 4954.58 55.32 o -3 5 1 2558.09 2614.14 24.47 o -1 5 1 247.72 112.95 10.41 o 1 5 1 1373.85 1536.08 13.42 o 3 5 1 3215.01 4183.55 34.98 o 5 5 1 57.85 183.04 13.42 o 7 5 1 14629.63 16462.06 187.20 o 9 5 1 1794.67 1785.52 16.65 o 11 5 1 64.77 68.20 11.27 o 13 5 1 1575.21 1299.05 35.99 o 15 5 1 636.01 561.05 21.30 o 17 5 1 41.24 36.94 13.80 o 19 5 1 416.36 398.50 37.33 o 21 5 1 479.45 421.44 28.25 o -20 6 1 2356.60 2310.80 71.34 o -18 6 1 141.92 155.90 27.89 o -16 6 1 678.34 606.76 83.47 o -14 6 1 232.73 195.19 35.22 o -12 6 1 3358.20 3094.19 108.15 o -10 6 1 3002.70 2889.97 145.00 o -8 6 1 380.58 335.55 19.61 o -6 6 1 10.69 132.07 17.32 o -4 6 1 1174.46 944.48 23.70 o -2 6 1 6429.45 7417.28 90.62 o 0 6 1 73427.89 87162.71 539.77 o 2 6 1 18.83 95.75 8.52 o 4 6 1 163.51 337.73 21.07 o 6 6 1 320.75 228.17 15.21 o 8 6 1 8549.97 8955.57 113.15 o 10 6 1 610.90 530.45 32.79 o 12 6 1 46.27 35.21 11.65 o 14 6 1 18.63 28.36 19.91 o 16 6 1 5522.86 5502.49 83.44 o 18 6 1 1312.04 1404.10 83.31 o 20 6 1 121.43 98.81 27.42 o -21 7 1 2766.82 2852.64 122.28 o -19 7 1 969.62 783.66 32.76 o -17 7 1 26.06 26.69 21.26 o -15 7 1 63.69 24.93 15.30 o -13 7 1 1588.39 1585.94 71.11 o -11 7 1 2114.12 2268.35 48.82 o -9 7 1 20227.66 21650.78 288.11 o -7 7 1 2761.84 2600.76 140.37 o -5 7 1 12085.39 11371.15 87.73 o -3 7 1 12.66 16.72 6.95 o -1 7 1 53742.59 62291.34 534.57 o 1 7 1 4208.91 4036.67 31.36 o 3 7 1 6.96 142.35 13.56 o 5 7 1 3825.58 3222.40 31.73 o 7 7 1 6843.88 6966.36 81.14 o 9 7 1 17302.91 18030.35 219.56 o 11 7 1 677.74 654.60 23.39 o 13 7 1 3389.77 3187.85 101.44 o 15 7 1 4193.10 4028.43 138.08 o 17 7 1 1669.77 1701.39 109.21 o 19 7 1 1854.23 1717.58 78.00 o -20 8 1 1786.09 1762.67 120.47 o -18 8 1 3022.29 3108.24 158.50 o -16 8 1 1977.94 1892.72 53.39 o -14 8 1 1655.28 1613.66 54.49 o -12 8 1 12066.14 11878.69 184.68 o -10 8 1 9836.39 9806.68 146.10 o -8 8 1 4454.95 4505.14 121.06 o -6 8 1 2551.73 2268.30 53.96 o -4 8 1 5726.41 6334.55 47.29 o -2 8 1 5939.55 6621.06 74.23 o 0 8 1 113642.24 139933.83 1318.97 o 2 8 1 318.95 334.51 12.09 o 4 8 1 329.48 243.41 17.38 o 6 8 1 5484.20 5715.94 153.59 o 8 8 1 15831.79 16530.60 167.23 o 10 8 1 6421.62 6430.75 65.29 o 12 8 1 959.65 826.75 28.17 o 14 8 1 991.41 1065.24 66.20 o 16 8 1 2138.18 1972.89 75.13 o 18 8 1 4033.05 4300.16 155.53 o 20 8 1 1.32 70.67 33.45 o -19 9 1 1409.68 1368.69 59.88 o -17 9 1 60.90 70.89 17.71 o -15 9 1 8.13 20.31 16.88 o -13 9 1 41.84 53.13 18.88 o -11 9 1 2257.44 2249.21 94.23 o -9 9 1 1566.07 1700.52 61.81 o -7 9 1 7.01 11.50 11.42 o -5 9 1 873.10 1166.59 19.08 o -3 9 1 4956.65 5671.41 56.49 o -1 9 1 3726.36 3539.67 43.54 o 1 9 1 591.68 377.79 14.54 o 3 9 1 6762.89 7055.26 45.46 o 5 9 1 209.37 141.85 15.26 o 7 9 1 12816.35 12808.57 133.95 o 9 9 1 18094.48 19286.67 350.62 o 11 9 1 752.94 649.19 29.97 o 13 9 1 954.83 818.91 30.53 o 15 9 1 811.26 741.99 39.20 o 17 9 1 7691.73 8735.59 260.13 o 19 9 1 1079.73 1129.77 54.72 o -20 10 1 937.35 934.56 112.55 o -18 10 1 1387.99 1325.96 43.77 o -16 10 1 94.10 96.01 22.60 o -14 10 1 744.19 801.03 66.18 o -12 10 1 1563.58 1512.99 48.23 o -10 10 1 1128.33 985.00 63.62 o -8 10 1 1516.98 1249.34 60.29 o -6 10 1 148.89 207.63 23.37 o -4 10 1 61.79 114.53 12.34 o -2 10 1 13603.84 13508.97 157.38 o 0 10 1 23694.20 25235.45 142.05 o 2 10 1 1197.22 1058.93 20.75 o 4 10 1 6237.83 6968.06 49.54 o 6 10 1 1288.27 1201.47 37.28 o 8 10 1 2728.94 2728.52 53.91 o 10 10 1 10147.96 10574.62 194.09 o 12 10 1 3905.68 3951.47 47.73 o 14 10 1 748.51 856.43 27.00 o 16 10 1 4981.36 5177.22 312.92 o 18 10 1 5393.75 5725.13 353.84 o -19 11 1 555.26 540.68 50.14 o -17 11 1 9.34 36.67 21.54 o -15 11 1 406.09 353.34 29.86 o -13 11 1 47.50 72.04 22.32 o -11 11 1 7056.78 7191.76 118.41 o -9 11 1 1076.94 1041.77 51.82 o -7 11 1 3156.22 3194.93 75.95 o -5 11 1 259.65 260.76 15.73 o -3 11 1 6.82 23.09 9.77 o -1 11 1 4891.58 5051.82 86.87 o 1 11 1 8620.54 9141.64 168.55 o 3 11 1 11542.05 12494.42 118.16 o 5 11 1 1357.08 1325.62 49.59 o 7 11 1 6177.65 6399.84 135.38 o 9 11 1 12746.62 13105.86 154.99 o 11 11 1 423.25 378.19 28.94 o 13 11 1 1118.35 1018.77 50.52 o 15 11 1 20.16 21.54 24.34 o 17 11 1 2808.92 2909.49 174.69 o -18 12 1 1560.12 1660.49 62.21 o -16 12 1 19.12 13.31 21.87 o -14 12 1 3123.07 3243.97 53.78 o -12 12 1 1116.56 1093.49 34.94 o -10 12 1 8422.64 8646.69 93.58 o -8 12 1 397.57 465.84 29.43 o -6 12 1 1324.14 1490.56 37.86 o -4 12 1 23.81 42.32 13.94 o -2 12 1 16242.86 17913.05 169.01 o 0 12 1 30169.88 32929.42 369.33 o 2 12 1 818.82 904.88 27.06 o 4 12 1 72.17 73.11 14.40 o 6 12 1 1480.74 1662.14 61.00 o 8 12 1 6847.44 6948.50 102.57 o 10 12 1 3569.15 3694.36 54.47 o 12 12 1 1392.43 1191.87 46.94 o 14 12 1 607.29 542.67 67.30 o 16 12 1 1645.81 1727.45 80.52 o 18 12 1 751.03 696.14 50.11 o -17 13 1 151.26 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