#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:08:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181145 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/24/2222445.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222445_Fobs loop_ _publ_author_name 'Ferreira, Valquiria B. N.' 'Fiedler, Haidi D.' 'Nome, Faruk' 'Bortoluzzi, Adailton J.' _publ_section_title ; 2-Allyloxy-5-nitrobenzoic acid ; _journal_coeditor_code RZ2336 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1718 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.227 _cell_angle_gamma 90.000 _cell_length_a 3.9438 _cell_length_b 9.0409 _cell_length_c 28.8036 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.8116 _cod_data_source_file rz2336Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '2-Allyloxy-5-Nitrobenzoic Acid' _shelx_refln_list_code 4 _shelx_f_calc_maximum 152.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 39.39 39.96 0.86 o 4 0 0 3.21 4.22 0.75 o 1 1 0 3957.11 3656.19 71.46 o 2 1 0 21.46 22.24 0.60 o 3 1 0 29.22 31.75 1.52 o 4 1 0 1.10 0.82 1.02 o 0 2 0 2358.69 1935.24 35.12 o 1 2 0 95.95 118.54 2.17 o 2 2 0 1.17 0.59 0.55 o 3 2 0 41.15 40.97 1.86 o 4 2 0 0.00 0.79 0.73 o 1 3 0 53.75 57.33 1.68 o 2 3 0 95.55 97.85 3.79 o 3 3 0 6.40 4.31 2.24 o 4 3 0 1.16 1.24 1.00 o 0 4 0 28.17 22.40 0.65 o 1 4 0 56.41 49.69 1.88 o 2 4 0 29.14 29.37 0.76 o 3 4 0 0.08 0.31 0.78 o 4 4 0 2.19 4.21 1.26 o 1 5 0 96.73 120.44 3.40 o 2 5 0 95.20 92.41 1.85 o 3 5 0 12.90 13.58 0.85 o 4 5 0 0.02 0.98 1.95 o 0 6 0 174.56 164.57 3.76 o 1 6 0 50.97 53.16 1.20 o 2 6 0 605.69 564.84 10.09 o 3 6 0 1.13 2.62 0.79 o 4 6 0 0.46 -1.50 1.96 o 1 7 0 214.02 205.11 3.79 o 2 7 0 131.85 130.53 2.84 o 3 7 0 0.09 1.02 0.95 o 0 8 0 101.04 96.03 2.42 o 1 8 0 98.83 89.00 1.95 o 2 8 0 23.90 25.67 1.45 o 3 8 0 4.49 5.49 2.63 o 1 9 0 11.41 14.36 0.88 o 2 9 0 4.27 4.48 0.80 o 0 10 0 28.34 27.56 1.59 o 1 10 0 4.37 5.21 2.13 o 2 10 0 0.22 1.34 1.87 o -3 0 1 25.04 21.30 1.08 o -1 0 1 1532.10 1564.80 9.27 o 1 0 1 5274.08 5020.66 61.20 o 3 0 1 5.19 5.26 0.78 o -4 1 1 14.60 13.64 1.26 o -3 1 1 0.12 0.90 1.75 o -2 1 1 35.31 34.69 0.95 o -1 1 1 4880.72 4799.85 62.04 o 0 1 1 1889.00 1754.64 24.10 o 1 1 1 120.66 132.15 3.01 o 2 1 1 42.62 49.13 1.38 o 3 1 1 14.76 12.40 0.95 o 4 1 1 42.02 42.01 1.69 o -4 2 1 9.19 12.20 1.25 o -3 2 1 122.77 115.42 3.66 o -2 2 1 54.85 54.08 1.69 o -1 2 1 88.23 73.10 1.74 o 0 2 1 446.65 439.17 4.61 o 1 2 1 1.20 0.87 1.15 o 2 2 1 350.12 331.16 6.68 o 3 2 1 33.76 38.09 1.39 o 4 2 1 25.30 25.40 1.50 o -4 3 1 13.37 13.22 1.27 o -3 3 1 0.37 -0.79 2.19 o -2 3 1 41.82 38.51 1.15 o -1 3 1 35.18 34.34 1.15 o 0 3 1 53.62 46.52 1.42 o 1 3 1 3.71 1.14 0.40 o 2 3 1 23.93 23.19 0.96 o 3 3 1 30.15 30.06 1.31 o 4 3 1 2.38 1.66 2.71 o -4 4 1 1.36 1.88 1.04 o -3 4 1 0.37 1.38 0.82 o -2 4 1 28.04 26.45 1.07 o -1 4 1 1422.95 1475.89 13.12 o 0 4 1 35.70 36.61 1.22 o 1 4 1 3.14 2.34 0.56 o 2 4 1 7.69 7.80 0.76 o 3 4 1 0.04 0.57 0.87 o 4 4 1 1.09 -2.93 2.93 o -4 5 1 0.45 -1.54 2.63 o -3 5 1 9.73 12.00 1.09 o -2 5 1 111.92 109.88 3.51 o -1 5 1 156.78 149.25 3.42 o 0 5 1 185.77 192.89 5.12 o 1 5 1 6.72 5.55 0.65 o 2 5 1 70.42 76.66 2.08 o 3 5 1 8.29 6.83 1.12 o 4 5 1 14.12 15.44 1.48 o -4 6 1 0.16 2.04 1.08 o -3 6 1 2.34 1.53 2.80 o -2 6 1 6.60 6.61 1.20 o -1 6 1 0.24 0.65 1.78 o 0 6 1 5.57 6.83 0.74 o 1 6 1 60.98 55.15 1.72 o 2 6 1 171.57 180.69 4.77 o 3 6 1 179.78 178.18 5.30 o 4 6 1 0.54 -2.32 2.90 o -3 7 1 11.92 10.72 1.27 o -2 7 1 177.58 166.92 4.97 o -1 7 1 0.14 0.58 2.61 o 0 7 1 34.69 34.81 1.26 o 1 7 1 66.92 60.70 1.66 o 2 7 1 4.15 3.99 1.17 o 3 7 1 0.18 -2.26 2.36 o -3 8 1 3.92 4.79 1.19 o -2 8 1 0.92 1.81 2.30 o -1 8 1 31.79 32.67 1.49 o 0 8 1 52.82 49.87 1.69 o 1 8 1 23.44 28.29 1.47 o 2 8 1 6.30 9.33 1.15 o 3 8 1 3.81 2.82 1.20 o -2 9 1 2.92 3.87 1.11 o -1 9 1 28.82 34.95 1.56 o 0 9 1 2.17 -0.25 2.11 o 1 9 1 20.75 17.53 1.40 o 2 9 1 0.02 1.77 2.50 o -2 10 1 3.27 4.93 1.27 o -1 10 1 0.04 1.20 2.51 o 0 10 1 2.38 3.14 1.08 o 1 10 1 11.60 14.63 1.34 o 2 10 1 2.50 1.88 1.12 o 0 11 1 6.98 6.42 1.21 o -4 0 2 0.16 0.26 2.29 o -2 0 2 62.79 63.06 1.74 o 0 0 2 183.88 188.13 1.70 o 2 0 2 9.17 8.15 0.66 o 4 0 2 4.22 4.70 1.05 o -4 1 2 18.19 12.82 1.24 o -3 1 2 1.88 0.72 2.19 o -2 1 2 359.10 358.29 6.61 o -1 1 2 38.64 36.50 1.21 o 0 1 2 1817.19 1725.59 25.33 o 1 1 2 9606.67 9114.90 87.19 o 2 1 2 454.38 436.28 7.36 o 3 1 2 1.95 3.09 0.80 o 4 1 2 9.17 8.52 1.13 o -4 2 2 1.58 1.59 2.25 o -3 2 2 181.91 184.47 4.55 o -2 2 2 5.19 4.48 0.63 o -1 2 2 2128.01 2018.44 12.27 o 0 2 2 2063.38 1829.34 9.52 o 1 2 2 3259.45 2951.38 14.92 o 2 2 2 838.86 859.87 10.73 o 3 2 2 31.63 35.60 1.35 o 4 2 2 1.35 0.27 2.28 o -4 3 2 13.99 9.92 1.26 o -3 3 2 31.85 30.99 1.27 o -2 3 2 287.77 304.33 6.75 o -1 3 2 1074.10 1016.35 9.78 o 0 3 2 388.11 337.95 5.04 o 1 3 2 47.71 40.59 1.24 o 2 3 2 57.93 57.97 1.85 o 3 3 2 35.33 36.03 1.43 o 4 3 2 1.55 -0.28 2.53 o -4 4 2 3.81 3.53 1.12 o -3 4 2 4.50 0.43 2.52 o -2 4 2 21.38 19.47 0.96 o -1 4 2 1.18 1.77 0.55 o 0 4 2 155.19 166.28 4.20 o 1 4 2 949.31 903.78 10.34 o 2 4 2 72.20 75.52 2.28 o 3 4 2 55.91 62.38 1.75 o 4 4 2 0.18 -0.29 3.02 o -4 5 2 1.06 1.08 1.11 o -3 5 2 3.72 -0.23 2.60 o -2 5 2 53.58 62.96 1.93 o -1 5 2 0.37 0.41 1.52 o 0 5 2 331.86 315.12 6.45 o 1 5 2 92.67 94.00 2.77 o 2 5 2 139.64 147.47 3.88 o 3 5 2 4.30 5.81 1.21 o 4 5 2 10.92 6.77 1.46 o -4 6 2 2.38 3.97 1.23 o -3 6 2 1.62 2.60 1.04 o -2 6 2 0.79 -0.20 2.12 o -1 6 2 39.33 38.79 1.25 o 0 6 2 11.26 12.43 0.83 o 1 6 2 4.07 4.45 0.76 o 2 6 2 4.16 5.28 1.03 o 3 6 2 88.05 104.65 3.16 o 4 6 2 8.31 7.64 1.39 o -3 7 2 4.29 3.95 1.13 o -2 7 2 64.08 62.76 1.90 o -1 7 2 437.61 409.81 9.62 o 0 7 2 6.32 7.35 0.83 o 1 7 2 14.76 14.64 1.08 o 2 7 2 150.12 144.51 3.85 o 3 7 2 6.67 5.01 1.27 o -3 8 2 0.26 0.26 1.20 o -2 8 2 3.05 1.56 2.62 o -1 8 2 1.45 1.28 0.95 o 0 8 2 302.40 318.22 8.80 o 1 8 2 49.62 53.86 1.77 o 2 8 2 0.07 -2.71 2.71 o 3 8 2 0.03 -2.20 2.86 o -2 9 2 18.59 23.48 1.55 o -1 9 2 0.57 1.31 2.39 o 0 9 2 7.15 7.96 1.06 o 1 9 2 1.96 1.05 2.78 o 2 9 2 0.21 -2.36 2.77 o -2 10 2 0.91 0.33 2.60 o -1 10 2 0.07 2.11 2.68 o 0 10 2 6.20 6.05 1.15 o 1 10 2 1.90 1.81 2.45 o 2 10 2 3.88 1.00 3.00 o 0 11 2 7.82 9.60 1.37 o -3 0 3 4.70 1.31 0.69 o -1 0 3 2.67 1.74 0.33 o 1 0 3 17622.38 16403.07 114.75 o 3 0 3 23.18 24.63 1.16 o -4 1 3 4.47 4.67 1.04 o -3 1 3 0.76 0.33 0.77 o -2 1 3 1.42 0.58 1.39 o -1 1 3 1419.77 1358.44 9.27 o 0 1 3 494.12 472.41 3.92 o 1 1 3 6878.57 6558.35 75.67 o 2 1 3 71.49 67.15 1.99 o 3 1 3 11.67 11.29 0.96 o 4 1 3 3.63 4.90 1.06 o -4 2 3 15.90 11.74 1.15 o -3 2 3 2.34 3.03 0.89 o -2 2 3 170.69 190.61 5.20 o -1 2 3 138.65 130.89 3.31 o 0 2 3 2497.50 2353.59 11.09 o 1 2 3 74.35 81.07 1.95 o 2 2 3 716.28 712.39 9.83 o 3 2 3 5.39 4.21 1.01 o 4 2 3 14.73 14.99 1.32 o -4 3 3 4.84 3.18 1.19 o -3 3 3 2.05 1.52 0.87 o -2 3 3 250.71 259.78 6.32 o -1 3 3 257.06 275.30 5.22 o 0 3 3 74.05 76.27 1.82 o 1 3 3 29.45 38.27 1.23 o 2 3 3 0.70 2.67 0.66 o 3 3 3 46.48 45.56 1.52 o 4 3 3 0.13 1.67 2.65 o -4 4 3 0.62 0.82 1.10 o -3 4 3 54.56 58.31 1.70 o -2 4 3 52.23 52.26 1.62 o -1 4 3 23.78 27.55 0.89 o 0 4 3 692.64 684.04 8.40 o 1 4 3 87.08 93.92 2.49 o 2 4 3 2.54 2.66 0.61 o 3 4 3 7.23 11.31 1.12 o 4 4 3 0.04 -0.88 2.64 o -4 5 3 4.21 -0.62 2.99 o -3 5 3 3.34 0.93 2.33 o -2 5 3 73.34 72.33 2.07 o -1 5 3 311.29 345.51 7.22 o 0 5 3 1.23 3.23 0.56 o 1 5 3 26.72 30.42 1.00 o 2 5 3 9.01 11.77 0.93 o 3 5 3 138.22 153.47 4.70 o 4 5 3 0.14 -0.31 3.13 o -4 6 3 0.00 -3.42 3.42 o -3 6 3 26.10 28.23 1.46 o -2 6 3 44.12 52.04 1.75 o -1 6 3 86.96 82.91 2.38 o 0 6 3 12.49 12.12 0.82 o 1 6 3 125.57 134.98 3.64 o 2 6 3 10.93 13.00 1.03 o 3 6 3 54.98 60.50 2.04 o 4 6 3 0.07 1.67 2.81 o -3 7 3 0.01 0.28 2.79 o -2 7 3 51.05 49.00 1.73 o -1 7 3 676.46 629.88 11.86 o 0 7 3 5.19 4.31 0.78 o 1 7 3 6.71 6.49 0.95 o 2 7 3 156.71 149.00 4.60 o 3 7 3 0.81 0.85 2.66 o -3 8 3 0.61 0.31 3.18 o -2 8 3 4.34 3.99 1.07 o -1 8 3 64.65 55.80 1.78 o 0 8 3 142.00 142.80 4.43 o 1 8 3 39.12 38.33 1.54 o 2 8 3 0.02 -1.05 2.51 o 3 8 3 0.05 1.26 2.64 o -2 9 3 0.89 -1.18 2.64 o -1 9 3 18.43 19.85 1.35 o 0 9 3 79.46 76.64 2.36 o 1 9 3 46.84 47.78 1.77 o 2 9 3 0.41 1.48 2.79 o -2 10 3 1.83 -1.00 2.77 o -1 10 3 4.57 6.49 1.25 o 0 10 3 0.41 2.38 1.00 o 1 10 3 3.24 4.44 1.13 o 2 10 3 0.01 -1.67 3.40 o 0 11 3 0.95 1.67 2.56 o -4 0 4 2.53 0.86 0.99 o -2 0 4 240.11 204.43 5.08 o 0 0 4 2748.39 2481.88 31.34 o 2 0 4 0.56 0.12 1.41 o 4 0 4 0.44 -2.27 2.27 o -4 1 4 0.97 2.82 1.00 o -3 1 4 129.72 151.09 4.05 o -2 1 4 62.29 61.64 1.73 o -1 1 4 89.96 86.15 2.56 o 0 1 4 410.65 417.97 4.02 o 1 1 4 8926.59 8353.80 87.40 o 2 1 4 1434.90 1442.24 13.55 o 3 1 4 9.35 12.21 1.04 o 4 1 4 1.37 -2.68 2.68 o -4 2 4 1.99 1.87 2.71 o -3 2 4 157.53 134.24 4.01 o -2 2 4 717.30 717.21 9.76 o -1 2 4 1007.69 1040.85 9.09 o 0 2 4 24.05 22.34 0.68 o 1 2 4 15.60 15.81 0.56 o 2 2 4 45.70 44.71 1.38 o 3 2 4 74.72 80.29 2.28 o 4 2 4 8.93 11.41 1.15 o -4 3 4 4.60 9.24 1.19 o -3 3 4 19.51 20.62 1.14 o -2 3 4 275.10 288.70 6.70 o -1 3 4 16.73 15.91 0.61 o 0 3 4 123.28 118.27 3.19 o 1 3 4 97.05 87.04 2.23 o 2 3 4 74.13 72.42 2.09 o 3 3 4 11.88 8.92 1.02 o 4 3 4 1.70 1.68 2.48 o -4 4 4 0.65 1.12 1.06 o -3 4 4 7.67 8.42 1.00 o -2 4 4 15.86 14.72 0.87 o -1 4 4 23.79 23.57 0.82 o 0 4 4 1672.32 1730.91 13.38 o 1 4 4 10.48 8.95 0.68 o 2 4 4 33.96 30.72 1.13 o 3 4 4 23.80 26.69 1.38 o 4 4 4 0.28 2.06 2.52 o -4 5 4 0.95 -0.62 3.10 o -3 5 4 22.72 23.70 1.34 o -2 5 4 26.49 28.25 1.13 o -1 5 4 694.54 709.30 10.38 o 0 5 4 225.87 226.23 5.60 o 1 5 4 3.35 5.72 0.61 o 2 5 4 27.92 28.66 1.22 o 3 5 4 0.10 1.46 1.10 o 4 5 4 14.33 17.70 1.71 o -4 6 4 7.86 8.46 1.36 o -3 6 4 1.15 1.80 2.29 o -2 6 4 122.19 112.95 3.70 o -1 6 4 26.22 35.74 1.26 o 0 6 4 69.67 67.95 2.13 o 1 6 4 32.64 35.29 1.23 o 2 6 4 5.70 4.35 0.96 o 3 6 4 24.02 30.20 1.71 o 4 6 4 10.06 9.11 1.50 o -3 7 4 11.62 10.42 1.32 o -2 7 4 5.84 5.25 1.00 o -1 7 4 403.11 362.64 9.09 o 0 7 4 4.04 4.66 0.93 o 1 7 4 18.47 15.84 1.12 o 2 7 4 8.95 9.11 1.18 o 3 7 4 7.18 5.30 1.22 o -3 8 4 0.10 0.26 1.03 o -2 8 4 11.33 12.98 1.24 o -1 8 4 29.97 32.62 1.48 o 0 8 4 4.68 4.10 1.25 o 1 8 4 34.33 34.28 1.58 o 2 8 4 0.51 -0.26 2.80 o 3 8 4 0.84 2.43 1.10 o -2 9 4 0.17 1.83 0.98 o -1 9 4 0.07 0.97 0.97 o 0 9 4 19.10 18.35 1.29 o 1 9 4 26.47 24.34 1.61 o 2 9 4 22.42 19.16 1.56 o -2 10 4 0.56 1.50 1.21 o -1 10 4 0.36 -2.12 2.76 o 0 10 4 1.81 -1.76 2.58 o 1 10 4 0.46 0.91 2.73 o 2 10 4 2.79 5.66 1.26 o 0 11 4 0.21 -0.28 1.16 o -3 0 5 3.56 1.09 0.76 o -1 0 5 1770.05 1682.26 10.50 o 1 0 5 23231.12 20716.88 137.18 o 3 0 5 24.80 15.12 1.01 o -4 1 5 1.06 1.27 0.96 o -3 1 5 16.93 14.45 1.08 o -2 1 5 13.79 20.31 0.85 o -1 1 5 127.62 144.80 3.28 o 0 1 5 5121.80 4627.37 52.15 o 1 1 5 51.88 53.90 1.72 o 2 1 5 2340.56 2259.69 17.07 o 3 1 5 0.62 -1.50 2.09 o 4 1 5 1.66 0.00 2.36 o -4 2 5 0.27 0.49 1.00 o -3 2 5 22.41 18.06 1.19 o -2 2 5 262.01 271.93 6.15 o -1 2 5 28.61 26.56 0.79 o 0 2 5 92.27 95.76 2.54 o 1 2 5 20.90 21.07 0.64 o 2 2 5 687.92 675.98 9.76 o 3 2 5 121.46 109.47 2.99 o 4 2 5 10.67 10.27 1.31 o -4 3 5 12.13 9.38 1.35 o -3 3 5 5.38 5.24 0.85 o -2 3 5 372.20 382.42 7.65 o -1 3 5 262.23 297.64 5.60 o 0 3 5 1109.45 1108.44 9.53 o 1 3 5 387.66 388.23 6.38 o 2 3 5 23.17 23.90 1.01 o 3 3 5 7.24 7.93 1.06 o 4 3 5 13.40 12.88 1.43 o -4 4 5 9.28 8.69 1.27 o -3 4 5 5.87 7.98 1.00 o -2 4 5 0.01 -1.90 1.90 o -1 4 5 22.17 25.87 0.87 o 0 4 5 25.92 27.62 0.94 o 1 4 5 9.03 19.48 0.80 o 2 4 5 14.81 16.98 0.94 o 3 4 5 1.25 0.88 0.85 o 4 4 5 5.04 4.81 1.37 o -4 5 5 3.05 4.56 1.20 o -3 5 5 0.02 0.08 0.91 o -2 5 5 8.61 7.76 0.83 o -1 5 5 220.36 253.16 6.37 o 0 5 5 0.67 4.20 0.64 o 1 5 5 83.42 93.14 2.84 o 2 5 5 5.69 5.08 0.83 o 3 5 5 0.08 1.44 2.42 o 4 5 5 33.28 32.91 1.98 o -4 6 5 0.66 2.72 1.22 o -3 6 5 7.07 7.81 1.15 o -2 6 5 0.66 1.42 1.88 o -1 6 5 14.14 12.03 0.91 o 0 6 5 48.36 45.94 1.42 o 1 6 5 1.40 -0.17 1.71 o 2 6 5 8.29 12.15 1.09 o 3 6 5 162.59 159.26 5.25 o 4 6 5 8.25 6.69 1.50 o -3 7 5 12.08 12.94 1.26 o -2 7 5 56.86 48.65 1.72 o -1 7 5 33.87 37.07 1.46 o 0 7 5 316.74 320.50 8.16 o 1 7 5 7.43 6.71 0.90 o 2 7 5 23.33 23.03 1.38 o 3 7 5 5.50 2.31 3.19 o -3 8 5 0.66 0.32 2.81 o -2 8 5 0.17 0.22 0.98 o -1 8 5 0.07 2.57 0.90 o 0 8 5 290.51 304.82 8.90 o 1 8 5 199.05 197.15 5.23 o 2 8 5 2.47 2.47 1.05 o 3 8 5 3.00 3.46 1.19 o -2 9 5 11.39 11.11 1.38 o -1 9 5 36.82 34.70 1.63 o 0 9 5 0.02 -1.79 2.64 o 1 9 5 50.55 47.53 1.95 o 2 9 5 0.72 -0.30 2.42 o -2 10 5 14.29 14.00 1.47 o -1 10 5 3.38 3.61 1.10 o 0 10 5 7.29 6.63 1.16 o 1 10 5 0.05 0.00 1.98 o 2 10 5 13.45 13.13 1.52 o 0 11 5 0.64 -2.36 3.39 o -4 0 6 7.97 8.72 1.16 o -2 0 6 35.87 44.72 1.33 o 0 0 6 247.19 268.44 3.53 o 2 0 6 175.41 169.22 4.89 o 4 0 6 0.00 1.92 0.95 o -4 1 6 3.90 4.79 1.11 o -3 1 6 10.44 1.67 2.11 o -2 1 6 15.44 15.18 0.78 o -1 1 6 320.77 315.84 4.93 o 0 1 6 1969.08 1881.43 9.74 o 1 1 6 4.18 2.08 0.42 o 2 1 6 984.32 984.86 11.54 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