#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/24/2222468.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222468_Fobs loop_ _publ_author_name 'Yap, Quai Ling' 'Lo, Kong Mun' 'Ng, Seik Weng' _publ_section_title ; Trimethylphenylammonium dibromidotriphenylstannate(IV) ; _journal_coeditor_code TK2456 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m714 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.003 _cell_angle_gamma 90.000 _cell_length_a 9.0010 _cell_length_b 16.7778 _cell_length_c 9.2448 _exptl_crystal_F_000 636.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file tk2456Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 193.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -21 0 114.33 121.22 11.86 o 2 -21 0 198.92 234.38 17.85 o 0 -20 0 3894.98 3997.56 75.85 o 1 -20 0 269.38 275.55 12.94 o 2 -20 0 769.78 805.48 25.92 o 3 -20 0 1769.45 1729.28 41.34 o 4 -20 0 110.19 111.30 14.91 o 1 -19 0 588.65 637.64 23.25 o 2 -19 0 579.23 550.38 26.02 o 3 -19 0 563.50 536.18 22.77 o 4 -19 0 1473.69 1454.19 36.62 o 5 -19 0 84.39 83.29 13.11 o 0 -18 0 6284.41 6178.38 107.08 o 1 -18 0 90.86 98.38 11.63 o 2 -18 0 129.75 130.32 8.82 o 3 -18 0 2761.95 2703.00 65.85 o 4 -18 0 861.51 812.71 25.88 o 5 -18 0 731.63 692.37 17.03 o 6 -18 0 590.93 579.70 16.61 o 1 -17 0 2185.55 2147.64 44.32 o 2 -17 0 615.77 585.28 14.25 o 3 -17 0 922.65 868.69 17.48 o 4 -17 0 1074.77 1032.09 24.47 o 5 -17 0 131.30 130.32 14.46 o 6 -17 0 575.84 557.45 15.73 o 1 -16 0 652.37 635.78 14.69 o 2 -16 0 2.15 2.89 5.56 o 3 -16 0 2933.77 2820.75 30.59 o 4 -16 0 1635.78 1590.02 28.74 o 5 -16 0 548.94 509.36 23.34 o 6 -16 0 1505.62 1422.73 24.75 o 7 -16 0 1704.27 1706.16 28.75 o 1 -15 0 3022.78 2906.48 38.20 o 2 -15 0 3415.31 3253.05 51.49 o 3 -15 0 681.89 656.89 14.11 o 4 -15 0 1039.25 1005.50 18.35 o 5 -15 0 52.29 58.27 8.28 o 6 -15 0 962.82 895.04 18.22 o 7 -15 0 405.46 392.36 13.89 o 1 -14 0 4574.25 4403.09 53.55 o 2 -14 0 1107.62 1069.85 19.12 o 3 -14 0 1699.91 1580.60 23.50 o 4 -14 0 4865.25 4646.89 45.90 o 5 -14 0 2484.93 2409.89 33.49 o 6 -14 0 1997.12 1918.29 29.13 o 7 -14 0 1045.29 1012.15 24.78 o 8 -14 0 674.86 673.93 17.22 o 1 -13 0 3982.11 3773.22 46.25 o 2 -13 0 2521.82 2401.67 33.97 o 3 -13 0 258.72 235.36 8.69 o 4 -13 0 1600.40 1560.90 18.55 o 5 -13 0 6.67 19.60 11.27 o 6 -13 0 908.06 879.64 17.32 o 7 -13 0 10.71 14.38 6.57 o 8 -13 0 1272.78 1188.74 28.96 o 1 -12 0 2692.09 2583.68 26.50 o 2 -12 0 5067.76 4900.03 47.35 o 3 -12 0 839.94 798.89 11.41 o 4 -12 0 3012.56 2932.25 30.24 o 5 -12 0 6750.03 6520.77 76.15 o 6 -12 0 1495.20 1427.61 23.01 o 7 -12 0 1044.00 981.85 18.85 o 8 -12 0 1983.11 1926.35 30.16 o 9 -12 0 434.55 422.88 14.53 o 1 -11 0 9500.73 9164.24 154.72 o 2 -11 0 4711.17 4551.98 43.42 o 3 -11 0 66.20 67.42 3.90 o 4 -11 0 986.74 958.37 12.75 o 5 -11 0 44.36 54.28 6.06 o 6 -11 0 110.90 113.00 7.11 o 7 -11 0 87.77 94.80 17.25 o 8 -11 0 1443.96 1360.04 23.77 o 9 -11 0 1214.23 1199.00 23.38 o 0 -10 0 1088.90 992.85 22.39 o 1 -10 0 1372.91 1340.34 18.32 o 2 -10 0 9297.84 9159.41 83.10 o 3 -10 0 751.85 699.67 9.85 o 4 -10 0 312.39 314.82 6.98 o 5 -10 0 13392.00 13237.28 145.07 o 6 -10 0 347.64 321.05 10.37 o 7 -10 0 63.40 57.65 6.41 o 8 -10 0 2977.57 2951.51 40.53 o 9 -10 0 139.75 156.08 10.09 o 1 -9 0 8144.55 8147.55 89.82 o 2 -9 0 4178.76 4039.06 47.87 o 3 -9 0 212.26 181.55 5.09 o 4 -9 0 1721.37 1672.95 18.33 o 5 -9 0 477.74 491.09 8.60 o 6 -9 0 358.18 333.99 10.05 o 7 -9 0 227.21 211.23 9.27 o 8 -9 0 577.26 570.39 27.42 o 9 -9 0 1112.79 1127.60 21.46 o 0 -8 0 377.20 380.26 12.46 o 1 -8 0 4998.69 5067.44 56.83 o 2 -8 0 9240.09 9000.01 98.81 o 3 -8 0 480.44 465.58 7.22 o 4 -8 0 2331.78 2287.27 23.34 o 5 -8 0 11770.25 11843.34 145.31 o 6 -8 0 182.48 170.87 9.66 o 7 -8 0 86.27 82.62 6.64 o 8 -8 0 4077.97 3968.06 50.50 o 9 -8 0 370.61 384.05 13.30 o 10 -8 0 93.70 84.14 13.36 o 1 -7 0 2972.52 2825.05 36.62 o 2 -7 0 9872.07 10327.43 92.39 o 3 -7 0 3191.69 3278.56 38.47 o 4 -7 0 1985.66 1919.77 19.90 o 5 -7 0 782.41 777.66 8.54 o 6 -7 0 2954.29 2845.96 36.28 o 7 -7 0 547.39 557.39 24.59 o 8 -7 0 738.09 727.70 15.45 o 9 -7 0 1335.12 1303.86 22.83 o 10 -7 0 189.18 173.23 10.82 o 0 -6 0 2882.78 2993.39 34.01 o 1 -6 0 14080.88 14294.29 305.87 o 2 -6 0 9439.59 9415.22 89.22 o 3 -6 0 448.85 446.35 12.53 o 4 -6 0 6313.69 6401.16 50.05 o 5 -6 0 8774.27 8651.47 67.29 o 6 -6 0 2577.30 2467.10 25.23 o 7 -6 0 1317.69 1296.03 20.47 o 8 -6 0 1382.15 1416.96 33.20 o 9 -6 0 1724.54 1689.09 26.90 o 10 -6 0 325.89 316.58 13.42 o 1 -5 0 3999.54 3799.72 34.91 o 2 -5 0 1896.13 1836.53 22.69 o 3 -5 0 4312.60 4282.13 33.73 o 4 -5 0 5186.49 5175.05 40.85 o 5 -5 0 93.27 106.64 3.51 o 6 -5 0 3950.58 3968.51 32.80 o 7 -5 0 933.76 916.40 12.59 o 8 -5 0 1142.96 1155.46 29.22 o 9 -5 0 1112.33 1111.53 20.41 o 10 -5 0 9.38 3.86 6.96 o 0 -4 0 12731.14 12488.49 143.92 o 1 -4 0 22659.09 22813.08 251.86 o 2 -4 0 2404.09 2444.55 19.63 o 3 -4 0 5179.93 5177.21 40.36 o 4 -4 0 8447.32 8394.64 74.47 o 5 -4 0 1193.75 1201.57 11.63 o 6 -4 0 3954.67 4019.89 33.18 o 7 -4 0 2494.07 2445.25 25.69 o 8 -4 0 636.81 628.77 11.03 o 9 -4 0 2218.29 2179.48 31.77 o 10 -4 0 1432.99 1419.65 24.50 o 1 -3 0 5815.45 5219.79 284.64 o 2 -3 0 3040.67 3253.48 25.65 o 3 -3 0 7129.46 7292.17 56.36 o 4 -3 0 5298.70 5174.12 40.72 o 5 -3 0 480.22 513.66 6.45 o 6 -3 0 4948.94 4981.03 46.58 o 7 -3 0 3450.79 3386.79 33.71 o 8 -3 0 131.92 132.91 5.73 o 9 -3 0 853.47 796.20 16.66 o 10 -3 0 298.71 302.36 12.32 o 0 -2 0 21817.37 20245.45 256.03 o 1 -2 0 8364.76 8748.20 76.57 o 2 -2 0 3566.67 3722.22 33.65 o 3 -2 0 15590.01 15977.38 145.36 o 4 -2 0 1261.65 1201.05 14.29 o 5 -2 0 352.50 375.84 7.99 o 6 -2 0 2833.36 2865.50 35.86 o 7 -2 0 2801.46 2779.63 34.84 o 8 -2 0 418.07 371.94 8.89 o 9 -2 0 1000.02 1007.15 15.02 o 10 -2 0 2635.52 2689.34 37.96 o 1 -1 0 8008.73 8469.31 61.21 o 2 -1 0 3711.62 3945.61 35.48 o 3 -1 0 11236.01 11218.54 161.79 o 4 -1 0 11121.63 11461.06 125.27 o 5 -1 0 223.50 251.40 13.70 o 6 -1 0 4203.28 4213.90 93.54 o 7 -1 0 4039.34 3941.00 83.77 o 8 -1 0 316.68 317.35 10.10 o 9 -1 0 325.53 303.08 10.82 o 10 -1 0 260.67 287.65 9.85 o 1 0 0 105.49 106.00 4.01 o 2 0 0 877.53 867.32 9.12 o 3 0 0 24904.64 25830.48 257.62 o 4 0 0 877.62 931.90 21.73 o 5 0 0 2370.58 2395.92 29.08 o 6 0 0 570.19 616.83 11.45 o 7 0 0 3359.52 3404.48 41.34 o 8 0 0 174.78 184.32 8.80 o 9 0 0 138.45 121.04 14.21 o 10 0 0 4507.98 4536.65 70.48 o 1 1 0 8337.04 8974.10 104.85 o 2 1 0 4517.64 4797.44 45.12 o 3 1 0 12215.46 12523.97 173.80 o 4 1 0 11308.18 11537.58 106.94 o 5 1 0 286.73 317.76 5.48 o 6 1 0 4272.69 4370.83 41.46 o 7 1 0 4052.88 4080.99 39.67 o 8 1 0 417.77 420.43 11.16 o 9 1 0 328.01 318.29 10.98 o 10 1 0 188.47 232.22 11.16 o 0 2 0 22371.59 20197.58 439.47 o 1 2 0 7088.41 7372.95 54.26 o 2 2 0 2959.27 3151.12 25.73 o 3 2 0 15436.87 15884.87 175.46 o 4 2 0 1861.83 1843.29 19.16 o 5 2 0 209.37 246.34 5.37 o 6 2 0 3228.45 3345.18 29.04 o 7 2 0 3167.83 3197.92 39.17 o 8 2 0 273.03 259.18 9.42 o 9 2 0 904.45 930.49 17.51 o 10 2 0 2711.79 2713.68 53.03 o 1 3 0 6603.35 6559.55 54.81 o 2 3 0 2811.35 3041.75 24.91 o 3 3 0 6388.80 6596.49 53.65 o 4 3 0 4964.42 4947.73 40.40 o 5 3 0 541.87 600.29 7.43 o 6 3 0 4632.45 4733.06 39.74 o 7 3 0 3254.09 3243.57 33.72 o 8 3 0 222.64 199.33 13.44 o 9 3 0 866.22 850.98 24.35 o 10 3 0 319.79 329.55 18.38 o 0 4 0 13238.12 13420.10 239.00 o 1 4 0 21086.50 21656.94 380.71 o 2 4 0 2540.27 2644.08 21.87 o 3 4 0 5571.60 5646.80 45.43 o 4 4 0 9220.44 9420.49 75.68 o 5 4 0 1148.27 1176.35 11.79 o 6 4 0 4122.66 4260.56 36.05 o 7 4 0 2846.84 2828.90 57.27 o 8 4 0 531.47 529.34 12.99 o 9 4 0 2121.97 2107.14 43.01 o 10 4 0 1422.22 1488.42 36.12 o 1 5 0 4523.88 4411.23 51.03 o 2 5 0 2312.63 2331.47 32.11 o 3 5 0 4202.11 4331.14 35.33 o 4 5 0 4925.59 4986.71 40.79 o 5 5 0 105.98 123.45 4.21 o 6 5 0 3444.17 3575.89 30.74 o 7 5 0 832.10 844.05 13.70 o 8 5 0 1305.74 1293.66 22.48 o 9 5 0 1057.95 1043.46 27.51 o 10 5 0 5.04 1.51 10.62 o 0 6 0 2683.93 2937.64 54.75 o 1 6 0 13324.46 13867.76 300.02 o 2 6 0 9291.10 9596.00 137.31 o 3 6 0 580.33 582.59 7.34 o 4 6 0 6399.64 6694.89 54.08 o 5 6 0 8839.00 8946.79 71.82 o 6 6 0 3046.23 3026.04 44.89 o 7 6 0 1477.93 1436.92 23.19 o 8 6 0 1448.65 1470.71 24.75 o 9 6 0 1599.94 1630.98 27.50 o 10 6 0 299.89 330.66 19.52 o 1 7 0 2967.97 2849.45 29.07 o 2 7 0 11350.33 11985.98 121.90 o 3 7 0 2565.68 2698.91 26.49 o 4 7 0 1813.11 1822.45 19.14 o 5 7 0 843.37 847.46 9.27 o 6 7 0 2577.69 2547.78 34.81 o 7 7 0 406.32 410.82 12.18 o 8 7 0 854.00 879.02 18.27 o 9 7 0 1350.21 1431.60 25.74 o 10 7 0 207.05 203.54 14.48 o 0 8 0 81.94 96.71 8.24 o 1 8 0 4831.67 5056.00 54.84 o 2 8 0 9019.31 9011.75 83.49 o 3 8 0 300.39 312.82 7.89 o 4 8 0 2432.60 2423.53 30.26 o 5 8 0 12290.31 12559.04 144.55 o 6 8 0 295.21 292.74 9.71 o 7 8 0 41.21 39.81 5.90 o 8 8 0 3848.79 3865.01 51.79 o 9 8 0 299.43 303.12 13.02 o 10 8 0 28.10 24.90 8.45 o 1 9 0 8381.71 8612.23 137.44 o 2 9 0 4153.87 4040.23 40.95 o 3 9 0 104.35 96.10 8.12 o 4 9 0 1562.84 1581.35 23.08 o 5 9 0 555.95 577.38 13.09 o 6 9 0 275.54 245.86 9.39 o 7 9 0 144.91 139.23 8.11 o 8 9 0 523.93 541.25 15.42 o 9 9 0 1141.02 1132.56 22.93 o 0 10 0 849.43 832.03 12.92 o 1 10 0 1488.49 1525.31 22.17 o 2 10 0 9348.09 9694.49 78.46 o 3 10 0 452.37 434.99 10.04 o 4 10 0 290.48 313.76 9.13 o 5 10 0 13234.28 13424.63 154.74 o 6 10 0 282.80 286.29 13.44 o 7 10 0 42.00 49.57 6.82 o 8 10 0 3192.79 3241.87 45.76 o 9 10 0 154.59 155.48 11.77 o 1 11 0 9326.88 9598.21 89.55 o 2 11 0 4554.26 4558.52 56.57 o 3 11 0 143.16 142.71 5.97 o 4 11 0 932.50 971.81 21.74 o 5 11 0 52.36 57.49 6.00 o 6 11 0 143.85 147.38 8.26 o 7 11 0 24.75 28.98 6.50 o 8 11 0 1400.95 1441.77 29.63 o 9 11 0 1282.28 1350.10 26.35 o 0 12 0 141.17 163.14 6.44 o 1 12 0 3110.30 3257.70 32.97 o 2 12 0 5482.59 5597.30 56.38 o 3 12 0 592.53 580.92 10.67 o 4 12 0 2683.69 2699.42 36.38 o 5 12 0 7263.44 7399.67 89.09 o 6 12 0 1437.05 1430.32 24.33 o 7 12 0 793.64 801.15 17.95 o 8 12 0 2123.48 2179.93 34.68 o 9 12 0 548.59 568.32 17.10 o 1 13 0 3881.78 4023.54 41.97 o 2 13 0 2410.15 2417.33 27.44 o 3 13 0 465.08 475.61 9.77 o 4 13 0 1688.55 1743.00 22.24 o 5 13 0 13.59 17.47 5.69 o 6 13 0 1147.15 1151.53 25.07 o 7 13 0 5.82 27.94 9.59 o 8 13 0 1229.32 1255.06 33.89 o 0 14 0 5502.87 5835.58 69.49 o 1 14 0 4326.94 4467.31 46.42 o 2 14 0 1303.15 1354.78 18.07 o 3 14 0 1647.43 1653.71 27.42 o 4 14 0 4317.50 4368.55 64.00 o 5 14 0 2441.25 2527.37 36.94 o 6 14 0 1865.66 1880.36 30.11 o 7 14 0 901.46 952.45 20.63 o 8 14 0 750.43 800.74 20.04 o 1 15 0 3004.79 3136.58 34.39 o 2 15 0 3286.53 3365.25 36.91 o 3 15 0 779.66 833.26 14.75 o 4 15 0 1166.35 1218.10 18.22 o 5 15 0 57.68 62.61 6.15 o 6 15 0 1139.92 1205.31 19.61 o 7 15 0 472.43 486.16 15.68 o 0 16 0 3424.28 3604.09 74.08 o 1 16 0 1094.81 1135.52 22.75 o 2 16 0 12.95 11.31 4.68 o 3 16 0 3056.65 3195.28 38.19 o 4 16 0 1605.31 1711.29 25.50 o 5 16 0 420.24 427.34 11.99 o 6 16 0 1559.93 1683.31 24.43 o 7 16 0 1548.52 1724.08 25.85 o 1 17 0 1970.95 2052.69 66.38 o 2 17 0 399.58 415.42 10.44 o 3 17 0 1111.80 1133.02 17.62 o 4 17 0 1236.81 1306.86 26.99 o 5 17 0 103.71 111.01 7.61 o 6 17 0 673.76 745.44 21.04 o 0 18 0 6509.85 6577.39 125.72 o 1 18 0 99.84 108.34 12.47 o 2 18 0 50.15 54.99 8.77 o 3 18 0 2895.02 3078.53 36.01 o 4 18 0 803.22 848.80 16.12 o 5 18 0 445.16 459.40 14.32 o 6 18 0 493.49 572.78 16.92 o 1 19 0 480.22 516.99 17.28 o 2 19 0 457.90 467.94 16.53 o 3 19 0 636.60 654.97 18.96 o 4 19 0 1533.38 1642.72 23.77 o 5 19 0 110.57 108.77 8.57 o 0 20 0 4147.97 4260.38 88.06 o 1 20 0 236.67 232.60 13.32 o 2 20 0 624.89 678.88 18.95 o 3 20 0 1754.98 1876.56 34.49 o 4 20 0 135.06 139.70 12.12 o 1 21 0 94.70 100.48 10.39 o 2 21 0 133.35 143.56 11.47 o -3 -21 1 601.50 576.65 17.68 o -2 -21 1 486.40 443.78 23.22 o -1 -21 1 1215.49 1263.04 24.94 o 0 -21 1 73.90 91.34 9.51 o 1 -21 1 753.36 786.43 27.14 o 2 -21 1 114.93 107.16 13.55 o -4 -20 1 2.14 -1.30 11.69 o -3 -20 1 584.27 558.15 16.83 o -2 -20 1 223.91 256.30 19.92 o -1 -20 1 756.87 747.43 18.42 o 0 -20 1 1830.32 1757.66 41.83 o 1 -20 1 3.28 -11.41 10.26 o 2 -20 1 981.77 938.61 27.92 o 3 -20 1 1358.70 1393.19 37.47 o -5 -19 1 68.83 60.50 8.43 o -4 -19 1 3011.25 2917.09 58.46 o -3 -19 1 608.60 594.05 22.02 o -2 -19 1 253.74 266.68 9.86 o -1 -19 1 3066.03 3074.31 42.82 o 0 -19 1 82.24 104.13 11.95 o 1 -19 1 922.88 917.20 27.36 o 2 -19 1 344.23 332.32 13.21 o 3 -19 1 1391.21 1311.76 34.56 o 4 -19 1 466.18 458.09 21.52 o -6 -18 1 483.09 503.62 15.39 o -5 -18 1 763.36 696.22 29.35 o -4 -18 1 170.08 162.47 9.25 o -3 -18 1 1468.02 1406.04 34.23 o -2 -18 1 725.87 712.88 14.07 o -1 -18 1 468.64 474.04 19.28 o 0 -18 1 2204.10 2222.62 46.98 o 1 -18 1 129.79 137.94 11.63 o 2 -18 1 1868.96 1766.85 28.15 o 3 -18 1 2332.53 2215.13 32.80 o 4 -18 1 339.55 313.08 18.27 o 5 -18 1 816.93 816.48 27.34 o -7 -17 1 1451.69 1392.43 25.49 o -6 -17 1 251.31 225.02 11.22 o -5 -17 1 300.63 275.30 16.28 o -4 -17 1 5320.08 5227.84 63.80 o -3 -17 1 732.58 701.56 15.27 o -2 -17 1 304.45 314.98 11.61 o -1 -17 1 4121.24 4034.88 74.07 o 0 -17 1 2769.81 2728.60 53.85 o 1 -17 1 286.82 265.79 15.82 o 2 -17 1 3021.61 2935.64 40.04 o 3 -17 1 1857.27 1700.56 37.03 o 4 -17 1 176.28 172.06 13.81 o 5 -17 1 1035.82 956.84 28.37 o 6 -17 1 2281.35 2347.63 50.78 o -7 -16 1 466.40 496.29 27.94 o -6 -16 1 992.76 942.79 19.13 o -5 -16 1 2075.57 1931.51 29.16 o -4 -16 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5063.55 56.20 o 1 -2 2 3859.91 4015.81 53.12 o 2 -2 2 20652.17 20661.85 231.45 o 3 -2 2 4956.99 4952.25 45.67 o 4 -2 2 1125.52 1158.01 11.29 o 5 -2 2 6121.23 6084.24 55.60 o 6 -2 2 887.44 870.21 10.33 o 7 -2 2 51.50 54.99 4.51 o 8 -2 2 1030.55 1029.05 20.35 o 9 -2 2 1051.05 1065.04 19.95 o 10 -2 2 68.23 63.40 9.53 o -11 -1 2 964.00 991.39 20.21 o -10 -1 2 7.30 13.86 6.23 o -9 -1 2 228.71 214.00 9.50 o -8 -1 2 82.77 77.25 6.32 o -7 -1 2 1679.23 1616.02 22.65 o -6 -1 2 94.09 105.45 5.58 o -5 -1 2 1505.27 1442.11 19.39 o -4 -1 2 17197.49 17628.17 199.45 o -3 -1 2 558.64 515.37 6.88 o -2 -1 2 5178.25 5327.71 48.89 o -1 -1 2 28296.12 29090.76 326.05 o 0 -1 2 7083.64 7334.73 64.79 o 1 -1 2 1472.73 1501.50 19.05 o 2 -1 2 1998.29 2043.66 20.43 o 3 -1 2 3680.35 3674.67 38.16 o 4 -1 2 420.00 440.24 10.60 o 5 -1 2 1581.74 1576.47 14.97 o 6 -1 2 5947.40 5868.53 47.72 o 7 -1 2 206.08 209.82 6.11 o 8 -1 2 2044.20 2088.09 20.81 o 9 -1 2 3696.57 3743.07 48.04 o 10 -1 2 190.35 198.64 10.83 o -11 0 2 2581.62 2613.12 68.97 o -10 0 2 90.75 94.90 18.21 o -9 0 2 329.34 301.99 10.56 o -8 0 2 12340.29 12320.59 185.57 o -7 0 2 495.51 480.15 11.06 o -6 0 2 95.30 83.41 4.93 o -5 0 2 6962.85 6854.67 75.86 o -4 0 2 484.48 494.24 11.16 o -3 0 2 4948.30 5204.53 47.24 o -2 0 2 6914.51 7335.27 58.22 o -1 0 2 7926.32 7990.88 92.61 o 0 0 2 10.89 15.25 1.08 o 1 0 2 1432.78 1598.98 13.83 o 2 0 2 37420.72 37066.44 526.67 o 3 0 2 2448.13 2519.11 19.41 o 4 0 2 20.65 26.98 2.05 o 5 0 2 10033.48 10027.09 65.31 o 6 0 2 31.97 32.44 3.59 o 7 0 2 23.58 28.63 3.67 o 8 0 2 400.01 415.09 11.37 o 9 0 2 310.94 334.97 10.89 o 10 0 2 98.27 113.18 12.92 o -11 1 2 989.23 1070.32 21.10 o -10 1 2 44.33 46.51 7.10 o -9 1 2 316.93 331.49 11.26 o -8 1 2 87.85 81.30 6.38 o -7 1 2 1784.80 1754.10 24.16 o -6 1 2 146.54 164.58 12.12 o -5 1 2 1507.43 1454.40 19.46 o -4 1 2 16286.76 16468.83 149.30 o -3 1 2 572.72 541.77 6.55 o -2 1 2 5372.56 5392.44 42.66 o -1 1 2 26398.35 27037.30 305.62 o 0 1 2 7266.06 7677.54 176.80 o 1 1 2 1298.05 1335.57 13.34 o 2 1 2 2101.77 2166.58 25.94 o 3 1 2 3804.02 3901.24 38.66 o 4 1 2 167.60 168.75 4.36 o 5 1 2 1549.92 1567.23 15.46 o 6 1 2 6174.70 6117.76 51.10 o 7 1 2 163.56 167.49 6.63 o 8 1 2 1973.49 2049.22 31.87 o 9 1 2 3695.03 3784.25 39.18 o 10 1 2 220.78 215.49 14.26 o -11 2 2 2203.53 2324.43 49.11 o -10 2 2 566.69 527.30 13.87 o -9 2 2 260.19 267.82 10.13 o -8 2 2 7793.78 7705.69 87.26 o -7 2 2 2505.24 2520.34 32.28 o -6 2 2 343.93 372.97 8.35 o -5 2 2 9197.64 9285.38 101.28 o -4 2 2 3183.23 3327.23 32.52 o -3 2 2 106.90 132.51 7.86 o -2 2 2 4150.53 4420.32 35.72 o -1 2 2 15035.58 15690.45 150.83 o 0 2 2 4359.01 4538.88 44.99 o 1 2 2 3183.30 3351.13 32.80 o 2 2 2 20874.28 21638.15 207.88 o 3 2 2 4462.92 4538.99 58.31 o 4 2 2 850.91 896.19 11.29 o 5 2 2 6225.11 6215.31 59.81 o 6 2 2 1043.73 1029.68 13.99 o 7 2 2 91.82 91.65 5.28 o 9 2 2 1176.09 1206.69 49.83 o 10 2 2 24.89 17.33 10.51 o -11 3 2 1027.19 992.99 29.64 o -10 3 2 639.51 666.35 15.32 o -9 3 2 762.35 762.80 35.08 o -8 3 2 374.23 390.81 10.64 o -7 3 2 2990.40 3044.31 37.65 o -6 3 2 413.77 409.14 9.92 o -5 3 2 4815.40 4806.10 46.33 o -4 3 2 4675.68 4638.09 44.17 o -3 3 2 473.71 447.98 6.39 o -2 3 2 7551.00 7753.81 89.54 o -1 3 2 17285.84 17694.49 166.53 o 0 3 2 8878.52 9079.59 78.97 o 1 3 2 1048.93 1075.19 15.00 o 2 3 2 1287.70 1295.41 17.89 o 3 3 2 6306.40 6615.55 79.35 o 4 3 2 65.26 64.83 4.41 o 5 3 2 3690.06 3701.45 31.88 o 6 3 2 4064.34 4041.86 35.04 o 7 3 2 148.67 147.84 5.60 o 8 3 2 1664.33 1621.87 26.03 o 9 3 2 2392.03 2388.03 48.03 o -11 4 2 576.90 566.56 23.53 o -10 4 2 1639.71 1551.46 35.84 o -9 4 2 1406.80 742.23 20.21 o -8 4 2 1985.64 2002.10 39.64 o -7 4 2 4524.02 4434.11 55.61 o -6 4 2 227.94 200.30 7.94 o -5 4 2 6744.46 6797.22 81.08 o -4 4 2 6936.18 7244.27 83.70 o -3 4 2 2294.82 2320.45 28.70 o -2 4 2 16628.38 17299.28 201.28 o -1 4 2 5566.60 5862.55 48.47 o 0 4 2 5539.60 5748.04 57.22 o 1 4 2 8375.27 8632.48 102.02 o 2 4 2 12088.56 12141.64 146.84 o 3 4 2 6370.17 6512.65 78.31 o 4 4 2 853.63 890.72 19.19 o 5 4 2 3790.12 3823.42 44.11 o 6 4 2 2520.64 2528.22 23.36 o 7 4 2 1047.38 1016.52 18.88 o 8 4 2 1318.09 1332.57 23.55 o 9 4 2 406.09 423.33 19.65 o -11 5 2 407.34 437.09 21.67 o -10 5 2 320.19 346.97 17.55 o -9 5 2 983.00 966.18 26.66 o -8 5 2 377.32 371.29 9.00 o -7 5 2 975.61 1000.43 15.28 o -6 5 2 2006.69 2008.04 22.13 o -5 5 2 1919.37 1842.40 20.09 o -4 5 2 3895.48 3845.38 37.32 o -3 5 2 581.22 593.14 10.43 o -2 5 2 9285.61 9465.43 109.06 o -1 5 2 2820.23 2757.32 27.58 o 0 5 2 5956.09 6381.76 79.09 o 1 5 2 4034.91 3978.09 49.02 o 2 5 2 467.46 450.43 8.85 o 3 5 2 5814.43 6082.65 73.62 o 4 5 2 2692.27 2796.48 36.46 o 5 5 2 3656.16 3612.60 48.28 o 6 5 2 2319.29 2293.11 32.12 o 7 5 2 231.79 241.14 10.16 o 8 5 2 2618.75 2574.33 37.52 o 9 5 2 403.14 394.05 13.80 o -11 6 2 23.77 22.21 10.99 o -10 6 2 1483.25 1420.96 34.73 o -9 6 2 1170.03 1163.23 29.26 o -8 6 2 376.24 396.27 21.76 o -7 6 2 5704.20 5821.02 56.87 o -6 6 2 3792.30 3838.42 38.43 o -5 6 2 2150.68 2173.01 23.08 o -4 6 2 5223.40 5445.85 51.64 o -3 6 2 8224.99 8221.41 75.76 o -2 6 2 8308.43 8510.16 97.42 o -1 6 2 2151.67 2318.42 24.97 o 0 6 2 6468.99 6599.79 68.29 o 1 6 2 3169.07 3097.20 41.34 o 2 6 2 1524.00 1557.51 37.66 o 3 6 2 5658.24 5793.59 70.60 o 4 6 2 2491.45 2533.90 33.69 o 5 6 2 321.51 324.40 7.45 o 6 6 2 1282.06 1295.89 16.89 o 7 6 2 2509.94 2434.76 34.97 o 8 6 2 855.20 882.72 18.89 o 9 6 2 233.45 222.57 11.62 o -10 7 2 517.85 525.91 21.36 o -9 7 2 2365.76 2384.93 46.67 o -8 7 2 348.03 342.14 11.69 o -7 7 2 805.19 822.90 12.33 o -6 7 2 4889.89 5026.64 51.23 o -5 7 2 1754.92 1823.86 20.10 o -4 7 2 1976.76 1992.74 21.11 o -3 7 2 1681.31 1816.59 23.90 o -2 7 2 6503.66 6823.79 78.41 o -1 7 2 921.94 947.91 11.44 o 0 7 2 5657.56 6095.27 70.57 o 1 7 2 8133.61 8368.63 82.62 o 2 7 2 1213.35 1248.38 18.56 o 3 7 2 3755.45 3855.41 48.68 o 4 7 2 6004.79 6044.72 74.15 o 5 7 2 1850.11 1867.61 21.57 o 6 7 2 228.00 249.78 7.64 o 7 7 2 1186.81 1160.91 21.29 o 8 7 2 1738.25 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704.16 722.75 14.18 o 3 9 2 2981.29 3004.82 39.70 o 4 9 2 7670.66 7779.38 74.86 o 5 9 2 184.04 182.92 7.00 o 6 9 2 245.61 258.33 10.96 o 7 9 2 662.10 696.69 16.70 o 8 9 2 475.94 480.84 15.17 o 9 9 2 103.62 87.96 9.70 o -10 10 2 1247.73 1244.59 24.98 o -9 10 2 435.05 469.94 15.30 o -8 10 2 104.26 106.80 8.03 o -7 10 2 501.42 530.58 15.10 o -6 10 2 5598.03 5805.15 71.31 o -5 10 2 992.59 1017.36 17.31 o -4 10 2 342.39 336.48 6.76 o -3 10 2 16547.35 16866.39 178.67 o -2 10 2 460.59 451.29 8.08 o -1 10 2 1457.69 1565.13 17.95 o 0 10 2 11215.53 11785.27 112.37 o 1 10 2 313.13 315.65 9.26 o 2 10 2 848.69 883.83 16.59 o 3 10 2 1143.91 1127.55 28.77 o 4 10 2 2940.16 2937.66 31.49 o 5 10 2 87.73 101.67 5.54 o 6 10 2 99.74 110.38 7.94 o 7 10 2 4255.77 4369.50 58.09 o 8 10 2 198.83 202.92 33.16 o -9 11 2 2222.36 2230.11 35.37 o -8 11 2 302.02 285.40 23.22 o -7 11 2 1482.08 1535.84 25.40 o -6 11 2 2790.53 2831.55 56.08 o -5 11 2 80.05 81.16 5.79 o -4 11 2 80.89 89.33 6.54 o -3 11 2 654.53 667.04 10.92 o -2 11 2 1816.16 1893.73 21.72 o -1 11 2 259.81 247.96 6.17 o 0 11 2 2376.08 2462.29 26.30 o 1 11 2 9133.43 9554.41 120.50 o 2 11 2 4.92 7.58 4.69 o 3 11 2 4535.70 4670.66 62.79 o 4 11 2 6923.62 7033.05 84.76 o 5 11 2 57.44 62.33 6.47 o 6 11 2 185.17 199.12 10.23 o 7 11 2 551.96 602.33 16.27 o 8 11 2 313.17 318.10 13.53 o -9 12 2 577.48 629.23 17.50 o -8 12 2 153.90 173.77 9.90 o -7 12 2 543.66 536.01 14.45 o -6 12 2 2636.91 2714.64 37.80 o -5 12 2 1005.80 1009.97 20.39 o -4 12 2 826.99 865.68 13.51 o -3 12 2 10624.66 10974.17 106.41 o -2 12 2 3223.68 3357.07 35.53 o -1 12 2 550.56 553.14 15.79 o 0 12 2 6965.26 7295.01 74.14 o 1 12 2 859.24 870.08 17.02 o 2 12 2 246.09 253.07 9.70 o 3 12 2 2037.34 1950.93 46.78 o 4 12 2 1734.65 1761.03 27.41 o 5 12 2 448.79 450.65 12.86 o 6 12 2 943.42 971.27 19.97 o 7 12 2 2837.13 2955.05 47.81 o 8 12 2 1014.63 1035.05 22.84 o -9 13 2 1466.82 1505.24 27.66 o -8 13 2 299.19 317.83 15.11 o -7 13 2 954.20 985.27 19.89 o -6 13 2 2259.61 2330.09 33.99 o -5 13 2 1523.95 1578.02 24.70 o -4 13 2 671.51 673.95 20.84 o -3 13 2 443.89 456.97 9.48 o -2 13 2 3216.71 3295.00 35.40 o -1 13 2 91.24 96.93 4.59 o 0 13 2 2533.70 2634.95 55.63 o 1 13 2 4861.71 5120.88 70.57 o 2 13 2 140.58 143.42 8.67 o 3 13 2 3860.72 3910.35 42.26 o 4 13 2 4051.43 4182.01 64.13 o 5 13 2 759.87 760.99 17.15 o 6 13 2 933.67 963.98 20.08 o 7 13 2 235.63 276.25 13.14 o -8 14 2 1008.73 1030.71 21.87 o -7 14 2 1321.49 1372.23 25.57 o -6 14 2 857.66 852.89 20.56 o -5 14 2 2107.38 2230.31 27.51 o -4 14 2 1499.26 1539.45 20.51 o -3 14 2 1867.43 1937.02 23.50 o -2 14 2 5505.00 5738.72 72.72 o -1 14 2 842.56 848.75 25.58 o 0 14 2 1894.65 1995.40 31.61 o 1 14 2 2746.28 2840.89 81.68 o 2 14 2 1606.62 1647.75 27.93 o 3 14 2 1392.46 1479.60 20.06 o 4 14 2 513.48 600.76 15.30 o 5 14 2 1245.55 1272.49 23.77 o 6 14 2 1199.84 1258.82 24.27 o 7 14 2 1850.79 1977.17 33.21 o -8 15 2 254.55 257.45 13.66 o -7 15 2 1027.63 1048.06 21.13 o -6 15 2 934.78 919.72 16.82 o -5 15 2 625.25 654.13 13.12 o -4 15 2 1827.07 1851.21 23.73 o -3 15 2 28.91 38.46 4.88 o -2 15 2 738.52 772.87 12.72 o -1 15 2 2010.43 2041.45 32.48 o 0 15 2 2289.47 2342.23 48.33 o 1 15 2 875.98 892.41 18.99 o 2 15 2 316.98 309.16 10.62 o 3 15 2 3411.47 3488.07 48.68 o 4 15 2 1141.45 1165.02 21.95 o 5 15 2 697.85 737.27 17.83 o 6 15 2 1275.50 1403.42 26.39 o 7 15 2 21.06 21.69 9.31 o -7 16 2 883.73 951.88 17.93 o -6 16 2 21.93 18.14 6.51 o -5 16 2 2897.26 2989.21 35.22 o -4 16 2 1245.86 1309.68 19.18 o -3 16 2 1038.20 1089.46 16.44 o -2 16 2 2938.54 3046.66 71.85 o -1 16 2 2721.69 2766.67 41.97 o 0 16 2 284.27 305.14 16.87 o 1 16 2 1150.71 1189.16 17.15 o 2 16 2 2264.42 2310.59 28.05 o 3 16 2 955.90 979.67 27.95 o 4 16 2 59.96 63.68 8.06 o 5 16 2 1345.08 1404.41 25.95 o 6 16 2 843.13 927.89 41.10 o -7 17 2 1219.31 1301.30 24.43 o -6 17 2 271.35 271.59 18.06 o -5 17 2 592.42 629.10 14.05 o -4 17 2 2080.61 2185.91 27.70 o -3 17 2 40.54 48.00 7.76 o -2 17 2 923.59 948.74 20.76 o -1 17 2 2649.36 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