#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/24/2222476.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222476_Fobs loop_ _publ_author_name 'Lo, Kong Mun' 'Ng, Seik Weng' _publ_section_title ; Dihydronium hexakis[bromido/chlorido(0.75/0.25)]dicadmate(II)--triphenylphosphine oxide (1/6) ; _journal_coeditor_code TK2468 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m720 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.499 _cell_angle_beta 81.013 _cell_angle_gamma 79.605 _cell_length_a 11.1623 _cell_length_b 15.0677 _cell_length_c 16.0911 _exptl_crystal_F_000 1177.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file tk2468Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2074.55 2433.73 21.62 o 2 0 0 8915.73 9754.56 99.49 o 3 0 0 22297.59 22600.94 220.79 o 4 0 0 19064.87 19133.09 240.60 o 5 0 0 21807.29 21731.21 274.96 o 6 0 0 14815.43 14936.78 202.06 o 7 0 0 8073.90 8046.56 126.68 o 8 0 0 1687.54 1655.31 51.69 o 9 0 0 26.14 -3.68 43.31 o 10 0 0 2676.42 2662.61 127.73 o 11 0 0 1992.26 1914.42 118.55 o 12 0 0 158.33 153.21 73.01 o 13 0 0 91.67 103.76 76.16 o 14 0 0 85.27 -22.92 75.92 o -14 1 0 34.25 -28.51 81.27 o -13 1 0 41.06 62.82 77.65 o -12 1 0 309.17 493.22 90.00 o -11 1 0 2678.88 2663.43 142.64 o -10 1 0 471.59 512.13 75.37 o -9 1 0 1065.60 1088.73 86.62 o -8 1 0 563.65 568.57 33.69 o -7 1 0 270.52 300.76 25.65 o -6 1 0 19306.15 19403.67 202.60 o -5 1 0 3672.91 3598.72 52.20 o -4 1 0 20450.75 20626.13 206.05 o -3 1 0 7650.86 8200.94 88.32 o -2 1 0 10883.95 11329.73 113.90 o -1 1 0 29472.28 31494.82 339.52 o 0 1 0 4411.32 4122.31 222.58 o 1 1 0 10396.36 10983.79 197.70 o 2 1 0 6653.40 6630.24 90.93 o 3 1 0 5798.81 5647.78 118.43 o 4 1 0 2944.69 2674.10 51.61 o 5 1 0 13522.89 13639.15 182.76 o 6 1 0 9250.20 9366.45 138.24 o 7 1 0 6964.39 7124.10 116.32 o 8 1 0 429.31 379.79 35.09 o 9 1 0 431.83 455.45 61.44 o 10 1 0 614.79 701.04 77.21 o 11 1 0 1292.75 1318.17 103.14 o 12 1 0 319.85 186.04 68.93 o 13 1 0 2.10 35.78 71.03 o 14 1 0 5.20 -104.29 69.52 o -13 2 0 260.00 266.97 84.93 o -12 2 0 22.40 -47.06 59.79 o -11 2 0 0.26 -8.84 54.82 o -10 2 0 414.07 376.99 71.78 o -9 2 0 1048.76 1014.87 82.33 o -8 2 0 1454.99 1435.89 50.47 o -7 2 0 427.24 430.47 24.47 o -6 2 0 230.76 224.69 17.35 o -5 2 0 847.27 776.99 37.45 o -4 2 0 1376.05 1333.95 28.61 o -3 2 0 9744.14 10327.45 109.91 o -2 2 0 660.26 760.12 17.86 o -1 2 0 254.29 260.13 18.94 o 0 2 0 1419.98 1459.77 22.36 o 1 2 0 6650.54 7076.25 75.46 o 2 2 0 637.06 707.02 33.39 o 3 2 0 195.41 253.31 16.80 o 4 2 0 552.10 532.69 37.38 o 5 2 0 2654.76 2539.55 82.50 o 6 2 0 4151.05 3953.73 95.29 o 7 2 0 512.00 520.05 38.33 o 8 2 0 2479.14 2553.48 65.21 o 9 2 0 208.85 216.73 50.03 o 10 2 0 739.66 814.99 78.97 o 11 2 0 264.53 433.70 70.97 o 12 2 0 1466.22 1683.41 121.17 o 13 2 0 69.80 15.81 65.90 o 14 2 0 28.20 -101.45 67.63 o -13 3 0 863.93 861.98 109.65 o -12 3 0 1097.10 1285.14 118.46 o -11 3 0 72.60 91.20 62.39 o -10 3 0 1682.99 1887.72 114.65 o -9 3 0 595.59 619.59 75.19 o -8 3 0 7441.43 7273.66 106.38 o -7 3 0 3271.98 3239.53 57.38 o -6 3 0 960.00 1139.05 39.07 o -5 3 0 106.94 71.41 14.31 o -4 3 0 953.11 925.13 25.75 o -3 3 0 609.06 695.13 32.30 o -2 3 0 22.88 7.43 10.43 o -1 3 0 97.28 88.45 12.98 o 0 3 0 1884.56 1806.10 29.51 o 1 3 0 123.80 172.47 14.18 o 2 3 0 20.03 22.70 7.82 o 3 3 0 1979.48 1221.82 40.72 o 4 3 0 706.56 619.01 28.82 o 5 3 0 1528.88 1462.95 45.84 o 6 3 0 5091.83 5108.51 134.84 o 7 3 0 743.04 746.51 36.95 o 8 3 0 181.87 239.40 41.87 o 9 3 0 1245.92 1185.93 82.74 o 10 3 0 10.63 11.43 48.23 o 11 3 0 1746.26 1722.71 114.82 o 12 3 0 864.27 868.17 95.02 o 13 3 0 96.98 134.45 70.03 o 14 3 0 105.72 22.26 78.31 o -13 4 0 914.01 1055.13 117.47 o -12 4 0 339.37 353.37 89.25 o -11 4 0 704.49 619.49 87.05 o -10 4 0 243.91 197.14 62.04 o -9 4 0 1231.44 1000.63 84.89 o -8 4 0 5190.31 5275.25 82.42 o -7 4 0 1486.90 1526.27 41.26 o -6 4 0 188.41 148.90 18.22 o -5 4 0 1009.23 1059.04 47.93 o -4 4 0 341.55 393.48 19.24 o -3 4 0 2632.96 2551.61 42.64 o -2 4 0 2908.06 3105.71 48.97 o -1 4 0 25360.57 25527.91 309.00 o 0 4 0 9037.40 9390.61 105.60 o 1 4 0 5673.91 5880.84 89.47 o 2 4 0 148.56 109.83 19.80 o 3 4 0 143.33 145.56 15.75 o 4 4 0 3624.47 3675.43 69.50 o 5 4 0 617.74 632.29 31.45 o 6 4 0 1329.47 1268.45 46.72 o 7 4 0 587.70 474.73 46.44 o 8 4 0 6.98 12.64 33.18 o 9 4 0 1193.49 1187.83 85.45 o 10 4 0 553.24 553.48 67.15 o 11 4 0 1247.83 1208.23 96.66 o 12 4 0 36.46 75.15 60.76 o 13 4 0 2.19 -64.46 60.76 o 14 4 0 103.50 259.56 88.12 o -13 5 0 977.58 935.84 116.20 o -12 5 0 458.41 668.82 102.25 o -11 5 0 35.47 5.16 61.87 o -10 5 0 1067.16 1063.65 95.57 o -9 5 0 2758.50 2856.17 132.87 o -8 5 0 927.03 912.19 38.80 o -7 5 0 14339.99 14219.02 166.34 o -6 5 0 2245.91 2190.13 48.32 o -5 5 0 845.84 744.68 29.53 o -4 5 0 3140.79 3136.25 53.87 o -3 5 0 13792.26 14042.16 135.84 o -2 5 0 22859.38 22657.22 237.49 o -1 5 0 6747.36 6928.69 124.23 o 0 5 0 3165.97 3127.90 61.27 o 1 5 0 15182.89 14690.36 195.86 o 2 5 0 7708.96 7524.57 89.39 o 3 5 0 7456.65 7292.83 90.41 o 4 5 0 23064.04 23957.10 250.99 o 5 5 0 3196.38 3223.12 70.33 o 7 5 0 21.07 49.11 38.90 o 8 5 0 9293.92 8617.41 209.72 o 9 5 0 1283.52 1266.32 82.93 o 10 5 0 5.33 -12.36 47.75 o 11 5 0 1629.64 1810.96 116.24 o 12 5 0 13.74 38.11 58.46 o 13 5 0 562.22 697.90 98.09 o 14 5 0 401.30 419.87 95.42 o -12 6 0 632.36 501.82 95.27 o -11 6 0 1677.81 1456.52 117.35 o -10 6 0 112.60 140.70 65.12 o -9 6 0 1678.59 1502.20 109.46 o -8 6 0 8015.07 7828.85 139.72 o -7 6 0 10202.36 9969.81 129.55 o -6 6 0 5138.79 4681.98 101.26 o -5 6 0 3659.28 3598.00 63.02 o -4 6 0 7207.56 6787.40 82.06 o -3 6 0 29081.43 28505.73 299.83 o -2 6 0 34242.10 34304.01 491.98 o -1 6 0 36262.30 36772.56 372.46 o 0 6 0 11195.04 10964.19 158.42 o 1 6 0 3031.12 3180.01 65.76 o 2 6 0 18008.70 18362.13 245.69 o 3 6 0 29598.98 30506.62 309.93 o 4 6 0 5237.98 4785.90 72.11 o 5 6 0 4462.71 4305.97 70.73 o 6 6 0 2.62 9.07 22.41 o 8 6 0 568.73 500.60 54.15 o 9 6 0 2079.32 2120.03 100.94 o 10 6 0 1284.12 1050.01 83.76 o 11 6 0 353.15 345.45 68.41 o 12 6 0 58.30 20.72 61.44 o 13 6 0 71.59 114.03 72.48 o 14 6 0 365.85 361.23 92.31 o -12 7 0 1074.11 1172.13 122.21 o -11 7 0 79.48 155.89 79.34 o -10 7 0 33.18 28.11 62.67 o -9 7 0 336.83 389.05 72.21 o -8 7 0 2688.65 2834.90 132.60 o -7 7 0 3887.54 3819.10 83.90 o -6 7 0 1206.57 1265.57 43.21 o -5 7 0 1681.30 1678.16 41.58 o -4 7 0 3507.31 3544.39 82.14 o -3 7 0 612.89 634.02 29.14 o -2 7 0 9878.28 10107.23 150.27 o -1 7 0 1662.22 1616.47 42.49 o 0 7 0 673.40 820.52 37.62 o 1 7 0 5.13 -9.44 41.68 o 2 7 0 431.68 442.50 30.35 o 3 7 0 4086.09 3950.29 61.61 o 4 7 0 1106.05 1173.90 41.60 o 5 7 0 610.82 658.15 30.21 o 6 7 0 12.41 31.91 19.27 o 7 7 0 13.81 28.10 21.94 o 8 7 0 11.40 54.64 25.46 o 9 7 0 357.60 388.51 54.37 o 10 7 0 992.47 852.36 79.61 o 11 7 0 1267.49 1511.22 106.06 o 12 7 0 308.84 202.82 71.01 o 13 7 0 24.85 33.58 67.69 o -11 8 0 543.89 446.05 96.01 o -10 8 0 184.15 190.47 72.57 o -9 8 0 998.23 1044.41 95.73 o -8 8 0 21.82 41.18 57.44 o -7 8 0 160.95 137.63 24.70 o -6 8 0 626.57 627.39 31.48 o -5 8 0 267.07 261.94 23.89 o -4 8 0 4653.23 4618.91 68.80 o -3 8 0 97.50 84.30 20.46 o -2 8 0 47.06 61.36 18.37 o -1 8 0 1294.55 1233.45 73.19 o 0 8 0 15.98 13.16 20.01 o 1 8 0 3310.26 3488.89 79.06 o 2 8 0 1619.90 1767.50 65.46 o 3 8 0 1039.36 1299.49 51.83 o 4 8 0 25.21 28.66 15.56 o 5 8 0 1.73 -21.25 16.70 o 6 8 0 662.71 646.56 33.23 o 7 8 0 1391.55 1413.82 49.35 o 8 8 0 1153.00 1150.24 49.84 o 9 8 0 99.16 72.34 30.24 o 10 8 0 108.53 47.19 61.20 o 11 8 0 30.76 -3.08 42.24 o 12 8 0 57.79 49.44 48.61 o 13 8 0 129.92 86.83 88.26 o -11 9 0 634.53 619.62 104.12 o -10 9 0 2502.11 2514.94 112.28 o -9 9 0 798.78 864.72 71.97 o -8 9 0 1951.23 2074.07 90.84 o -7 9 0 24.77 18.26 23.40 o -6 9 0 360.53 388.22 29.18 o -5 9 0 4046.46 4032.44 69.34 o -4 9 0 552.60 582.07 41.53 o -3 9 0 662.53 662.74 45.67 o -2 9 0 105.85 95.46 24.84 o -1 9 0 46.91 76.07 25.22 o 0 9 0 509.60 533.81 37.67 o 1 9 0 137.85 104.08 25.60 o 2 9 0 561.12 596.24 60.86 o 3 9 0 13.68 41.44 25.35 o 4 9 0 3365.56 3356.56 130.59 o 5 9 0 212.19 226.31 23.20 o 6 9 0 29.86 32.08 20.82 o 7 9 0 1241.98 1201.55 53.86 o 8 9 0 1242.30 1232.30 51.52 o 9 9 0 216.88 193.80 35.38 o 10 9 0 6.17 4.72 59.88 o 11 9 0 403.88 386.31 88.62 o 12 9 0 341.24 316.01 87.98 o 13 9 0 123.84 17.91 88.34 o -10 10 0 1240.57 1403.36 123.84 o -9 10 0 2848.27 2761.63 140.33 o -8 10 0 258.90 263.66 53.68 o -7 10 0 9.34 -18.37 28.21 o -6 10 0 61.17 38.44 24.16 o -5 10 0 2406.47 2334.36 55.01 o -4 10 0 965.55 903.69 41.97 o -3 10 0 1595.16 1563.45 61.13 o -2 10 0 25.36 42.71 33.99 o -1 10 0 193.15 253.56 53.05 o 0 10 0 1643.43 1766.71 129.84 o 1 10 0 840.88 834.32 46.08 o 2 10 0 379.90 379.07 36.17 o 3 10 0 717.10 742.72 46.51 o 4 10 0 287.60 320.55 38.70 o 5 10 0 204.38 225.96 24.04 o 6 10 0 1042.04 1071.75 95.46 o 7 10 0 4.49 -16.84 34.27 o 8 10 0 190.72 164.33 44.18 o 9 10 0 155.58 84.04 49.94 o 10 10 0 82.45 129.32 49.66 o 11 10 0 14.73 -13.89 68.44 o 12 10 0 782.95 935.78 113.46 o 13 10 0 252.56 365.90 99.51 o -10 11 0 1567.90 1402.66 126.71 o -9 11 0 372.52 492.95 85.50 o -8 11 0 703.98 712.00 68.09 o -7 11 0 626.98 603.24 45.60 o -6 11 0 86.86 50.15 31.11 o -5 11 0 2481.93 2473.26 75.90 o -4 11 0 4119.28 4071.08 83.16 o -3 11 0 4401.58 4262.23 105.22 o -2 11 0 10.13 -30.28 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252.29 54.26 o 10 12 0 2.18 -7.36 47.07 o 11 12 0 366.97 459.90 97.85 o 12 12 0 2.30 -73.64 81.27 o -8 13 0 254.89 342.47 83.03 o -7 13 0 9.71 54.76 43.04 o -6 13 0 109.64 113.07 35.57 o -5 13 0 789.28 854.20 48.42 o -4 13 0 894.10 821.33 46.31 o -3 13 0 252.87 355.34 140.65 o -2 13 0 23.66 12.65 51.90 o -1 13 0 124.99 73.29 36.74 o 0 13 0 227.41 257.04 43.30 o 1 13 0 67.89 12.53 35.15 o 2 13 0 210.65 209.14 41.30 o 3 13 0 148.54 127.07 40.75 o 4 13 0 2107.40 2032.10 83.16 o 5 13 0 233.17 346.55 50.08 o 6 13 0 228.17 241.86 47.47 o 7 13 0 31.87 81.02 44.87 o 8 13 0 9.68 -28.26 41.64 o 9 13 0 534.55 593.52 68.49 o 10 13 0 141.06 170.43 56.79 o 11 13 0 631.08 716.89 81.12 o -6 14 0 788.79 772.39 88.96 o -5 14 0 118.20 196.97 93.43 o -4 14 0 239.48 208.69 58.64 o -3 14 0 72.33 18.09 37.81 o -2 14 0 106.05 196.28 61.28 o -1 14 0 1341.89 1271.48 73.16 o 0 14 0 1926.42 1731.73 81.07 o 1 14 0 85.08 72.66 85.40 o 2 14 0 4.55 -22.45 53.01 o 3 14 0 1859.17 1860.68 107.15 o 4 14 0 1112.62 1226.45 70.16 o 5 14 0 1305.10 1277.33 73.51 o 6 14 0 416.21 472.08 57.74 o 7 14 0 671.39 725.02 77.59 o 8 14 0 23.47 22.48 48.15 o 9 14 0 117.97 130.69 80.25 o 10 14 0 600.83 625.60 96.43 o 11 14 0 464.99 461.99 111.86 o -6 15 0 496.54 375.78 81.12 o -5 15 0 617.97 523.70 85.43 o -4 15 0 132.80 124.27 48.02 o -3 15 0 79.81 148.29 47.94 o -2 15 0 115.85 143.22 69.41 o -1 15 0 1281.21 1530.89 116.11 o 0 15 0 152.94 16.97 41.65 o 1 15 0 86.93 128.20 93.62 o 2 15 0 252.31 206.54 47.80 o 3 15 0 418.56 386.82 59.58 o 4 15 0 10.05 -4.34 41.01 o 5 15 0 109.50 173.98 48.82 o 6 15 0 214.00 214.70 52.24 o 7 15 0 157.94 166.38 54.79 o 8 15 0 85.40 154.90 54.37 o 9 15 0 259.68 285.07 61.93 o 10 15 0 160.04 188.23 100.43 o -5 16 0 337.69 463.08 86.93 o -4 16 0 561.90 616.66 89.83 o -3 16 0 102.50 212.29 53.33 o -2 16 0 19.02 30.78 61.90 o -1 16 0 1.01 9.69 64.35 o 0 16 0 127.95 175.79 65.32 o 1 16 0 70.90 99.87 48.05 o 2 16 0 65.37 75.10 46.57 o 3 16 0 12.60 81.86 46.58 o 4 16 0 40.18 1.24 45.17 o 5 16 0 767.74 909.68 71.83 o 6 16 0 28.97 22.57 47.21 o 7 16 0 78.49 71.21 53.22 o 8 16 0 256.01 250.79 115.72 o 9 16 0 10.75 -72.17 53.48 o -4 17 0 47.40 84.26 78.05 o -3 17 0 124.17 103.52 76.77 o -2 17 0 3.77 19.23 49.78 o -1 17 0 746.68 738.41 101.26 o 0 17 0 438.88 488.34 63.14 o 1 17 0 19.99 76.79 51.68 o 2 17 0 172.59 181.23 54.01 o 3 17 0 0.05 -33.24 47.53 o 4 17 0 839.09 911.74 75.97 o 5 17 0 379.86 372.24 61.21 o 6 17 0 260.84 271.18 60.89 o 7 17 0 407.37 529.18 71.72 o 8 17 0 37.22 28.33 83.31 o -2 18 0 342.79 438.48 94.01 o -1 18 0 9.05 212.75 81.51 o 0 18 0 532.25 564.91 69.56 o 1 18 0 3.66 7.19 51.72 o 2 18 0 11.70 -9.65 51.57 o 3 18 0 173.99 144.82 101.74 o 4 18 0 16.66 99.37 56.99 o 5 18 0 318.94 343.13 66.43 o 6 18 0 49.97 14.53 53.91 o -5 -18 1 245.97 210.68 94.30 o -4 -18 1 204.73 187.35 83.01 o -3 -18 1 91.88 81.39 59.90 o -2 -18 1 64.16 103.21 57.59 o -1 -18 1 81.10 78.36 57.19 o 0 -18 1 390.97 385.02 67.32 o 1 -18 1 214.94 275.19 90.38 o -7 -17 1 87.00 19.00 60.19 o -6 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