#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:08:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181145 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/24/2222477.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222477_Fobs loop_ _publ_author_name 'Tan, Chui Lian' 'Lo, Kong Mun' 'Ng, Seik Weng' _publ_section_title ; (2-Amido-3-oxidopyridinium-\k^2^N,O)dibenzylchloridotin(IV) ; _journal_coeditor_code TK2469 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m721 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.0457 _cell_length_b 16.8447 _cell_length_c 19.1227 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file tk2469Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 513.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 263277.59 254450.52 7196.00 o 4 0 0 57328.66 57297.26 409.91 o 6 0 0 132974.36 137228.91 1156.29 o 8 0 0 54813.25 54235.78 886.04 o 10 0 0 9764.85 9254.72 211.91 o 12 0 0 16585.32 16038.79 304.88 o 14 0 0 10738.10 10545.50 262.98 o 2 1 0 14553.46 14706.77 95.14 o 4 1 0 6045.86 6399.68 57.94 o 6 1 0 85.22 85.53 16.81 o 8 1 0 69.94 63.23 26.11 o 10 1 0 629.50 689.27 63.57 o 12 1 0 14.77 -24.16 30.46 o 14 1 0 31.86 2.71 36.65 o 0 2 0 84399.52 86403.84 676.54 o 2 2 0 95617.09 97931.30 838.37 o 4 2 0 24594.29 24256.61 177.11 o 6 2 0 84343.09 85369.27 499.17 o 8 2 0 29456.14 29168.67 262.35 o 10 2 0 11006.39 11033.43 158.94 o 12 2 0 16287.70 15806.74 215.32 o 14 2 0 15465.22 15779.57 233.59 o 2 3 0 27978.88 29924.18 222.33 o 4 3 0 3566.74 3626.46 34.50 o 6 3 0 284.81 369.17 20.84 o 8 3 0 1598.11 1640.91 49.97 o 10 3 0 1149.54 1100.19 55.67 o 12 3 0 1191.14 1172.23 63.58 o 14 3 0 1572.15 1432.60 91.30 o 0 4 0 118571.07 123510.98 892.10 o 2 4 0 18223.69 18952.78 153.70 o 4 4 0 40566.99 44105.35 386.37 o 6 4 0 30591.05 32317.21 221.09 o 8 4 0 4100.92 4055.19 71.08 o 10 4 0 1024.46 1087.80 55.44 o 12 4 0 3337.00 3375.02 97.59 o 14 4 0 2118.11 2251.39 91.26 o 2 5 0 13385.00 13828.71 112.96 o 4 5 0 2664.21 2481.61 48.59 o 6 5 0 1657.35 1802.88 45.79 o 8 5 0 6796.80 6896.04 96.51 o 10 5 0 704.56 761.89 49.71 o 12 5 0 0.70 6.24 30.80 o 0 6 0 2526.67 2379.28 40.30 o 2 6 0 2941.35 2880.68 89.74 o 4 6 0 4634.04 4819.89 93.39 o 6 6 0 2789.02 2660.25 68.03 o 8 6 0 433.80 462.87 32.31 o 10 6 0 31.08 90.98 32.60 o 12 6 0 2.67 33.15 32.90 o 2 7 0 4115.05 4077.91 60.56 o 4 7 0 11221.17 12307.25 116.96 o 6 7 0 746.24 715.59 28.52 o 8 7 0 7937.13 7700.10 119.58 o 10 7 0 2247.43 2099.32 74.48 o 12 7 0 306.79 247.92 42.03 o 0 8 0 60823.40 60533.62 454.26 o 2 8 0 24112.14 23794.15 205.83 o 4 8 0 33647.20 33799.06 256.93 o 6 8 0 21395.61 21013.26 181.26 o 8 8 0 16972.70 16436.15 196.87 o 10 8 0 13810.24 12754.32 183.13 o 12 8 0 6219.39 5849.54 132.25 o 2 9 0 3052.41 3095.49 51.09 o 4 9 0 322.98 285.41 24.06 o 6 9 0 0.01 5.98 19.75 o 8 9 0 145.64 153.16 37.50 o 10 9 0 4.36 -16.64 33.42 o 12 9 0 391.47 341.18 48.03 o 0 10 0 111203.69 113859.56 939.17 o 2 10 0 74437.01 75057.84 509.36 o 4 10 0 20885.05 20484.85 181.81 o 6 10 0 42465.57 41694.72 320.32 o 8 10 0 21064.29 20165.47 323.80 o 10 10 0 10102.87 10343.58 192.64 o 12 10 0 12555.07 12882.17 496.04 o 2 11 0 1607.08 1487.50 39.36 o 4 11 0 286.43 273.58 38.81 o 6 11 0 381.75 392.58 35.00 o 8 11 0 1433.79 1212.66 79.62 o 10 11 0 74.93 52.32 45.91 o 12 11 0 74.47 67.52 55.51 o 0 12 0 80878.11 79850.04 691.62 o 2 12 0 16892.99 16639.65 242.71 o 4 12 0 20137.85 20297.02 218.37 o 6 12 0 34641.82 34662.99 451.69 o 8 12 0 15780.73 16021.70 293.66 o 10 12 0 7886.67 7471.89 161.79 o 12 12 0 9573.69 9992.31 482.97 o 2 13 0 945.34 912.54 40.15 o 4 13 0 50.55 -7.13 27.62 o 6 13 0 3055.26 2962.89 96.67 o 8 13 0 15.46 -1.24 41.08 o 10 13 0 73.41 34.49 39.72 o 0 14 0 26418.50 26273.61 378.32 o 2 14 0 17595.83 17108.12 235.60 o 4 14 0 7027.87 6962.17 124.27 o 6 14 0 13704.16 13082.86 213.48 o 8 14 0 4086.60 3991.05 146.52 o 10 14 0 245.59 269.27 52.52 o 2 15 0 2219.75 2387.34 89.70 o 4 15 0 1393.31 1284.12 60.28 o 6 15 0 355.64 500.45 104.10 o 8 15 0 1737.69 1762.99 107.01 o 10 15 0 130.34 154.03 59.75 o 0 16 0 1309.85 1355.29 88.51 o 2 16 0 2.61 75.29 41.10 o 4 16 0 13.55 -2.64 33.40 o 6 16 0 3.90 -48.08 44.39 o 8 16 0 545.55 675.75 170.02 o 2 17 0 609.46 602.59 71.04 o 4 17 0 2344.39 2368.42 135.11 o 6 17 0 758.42 741.37 99.60 o 8 17 0 1068.22 1237.76 114.20 o 0 18 0 4557.33 4272.73 216.13 o 2 18 0 3177.38 2964.41 133.50 o 4 18 0 2344.53 2236.99 106.79 o 6 18 0 3003.09 3272.82 146.95 o 8 18 0 2837.53 2732.10 422.37 o 2 19 0 1408.28 1425.53 83.10 o 4 19 0 68.28 64.63 69.91 o 6 19 0 1.33 -35.57 51.69 o 0 20 0 18559.22 19498.86 520.19 o 2 20 0 6397.71 6810.24 170.83 o 4 20 0 3468.69 3773.70 129.22 o 2 21 0 426.04 434.35 65.21 o 4 21 0 894.64 926.09 77.35 o 1 1 1 22502.97 23984.67 112.76 o 2 1 1 12476.89 13061.96 64.30 o 3 1 1 8517.39 8653.48 52.38 o 4 1 1 25671.13 27702.86 124.57 o 5 1 1 9790.89 9539.35 62.35 o 6 1 1 6837.57 7542.18 53.97 o 7 1 1 16455.67 16076.70 99.06 o 8 1 1 1151.30 1031.98 32.80 o 9 1 1 2222.42 2276.07 48.39 o 10 1 1 44.23 45.76 22.72 o 11 1 1 1924.54 1898.49 50.21 o 12 1 1 1098.90 1050.96 42.70 o 13 1 1 6780.26 6826.52 100.12 o 14 1 1 252.44 344.37 35.32 o 0 2 1 96274.34 98066.76 734.21 o 1 2 1 52.87 39.80 5.16 o 2 2 1 54924.45 56850.04 266.60 o 3 2 1 1646.25 1788.20 18.43 o 4 2 1 19543.54 18881.16 97.31 o 5 2 1 10.93 -2.28 9.15 o 6 2 1 9490.16 9284.22 63.95 o 7 2 1 1.08 3.74 10.54 o 8 2 1 12323.96 12363.47 89.93 o 9 2 1 58.32 38.45 18.98 o 10 2 1 10783.94 10584.15 109.61 o 11 2 1 18.21 32.93 20.81 o 12 2 1 3745.45 3602.63 73.23 o 13 2 1 8.67 21.18 23.60 o 14 2 1 1382.85 1504.68 54.47 o 1 3 1 262.32 302.28 9.11 o 2 3 1 2713.38 2953.94 23.29 o 3 3 1 891.22 812.12 22.03 o 4 3 1 66.21 88.01 7.69 o 5 3 1 1368.65 1172.62 24.02 o 6 3 1 484.97 527.95 17.41 o 7 3 1 4646.86 4449.72 45.22 o 8 3 1 76.74 55.46 13.26 o 9 3 1 4131.34 4005.85 62.92 o 10 3 1 23.11 9.62 19.70 o 11 3 1 3349.14 3072.72 61.97 o 12 3 1 132.07 82.86 24.11 o 13 3 1 2210.11 2281.22 60.58 o 14 3 1 309.59 376.55 43.21 o 0 4 1 3777.64 3354.59 37.03 o 1 4 1 1656.89 1761.70 22.72 o 2 4 1 81869.03 83689.53 374.61 o 3 4 1 2106.06 2292.63 23.47 o 4 4 1 87159.25 88392.72 359.53 o 5 4 1 508.13 755.14 14.83 o 6 4 1 29768.62 29100.23 151.33 o 7 4 1 3628.77 3746.06 54.85 o 8 4 1 27564.96 27661.22 153.67 o 9 4 1 4638.81 4771.35 74.38 o 10 4 1 14913.70 15049.93 136.43 o 11 4 1 1396.89 1327.99 44.40 o 12 4 1 7287.13 7392.18 100.67 o 13 4 1 24.38 22.61 24.61 o 14 4 1 7410.03 7572.94 112.49 o 1 5 1 2472.00 2766.36 34.43 o 2 5 1 201.11 224.91 11.44 o 3 5 1 2947.47 3176.25 31.36 o 4 5 1 1321.86 1495.40 21.50 o 5 5 1 101.32 76.48 11.76 o 6 5 1 64.74 62.51 11.26 o 7 5 1 263.11 240.06 16.75 o 8 5 1 270.77 256.37 18.13 o 9 5 1 60.74 68.50 18.69 o 10 5 1 1053.97 1056.20 39.49 o 11 5 1 14.76 5.68 21.90 o 12 5 1 113.37 123.14 25.89 o 13 5 1 103.17 65.86 30.71 o 0 6 1 8576.88 7661.54 74.84 o 1 6 1 4436.14 4526.86 37.85 o 2 6 1 70563.09 71078.66 331.98 o 3 6 1 553.63 629.67 20.11 o 4 6 1 117412.36 120852.17 491.15 o 5 6 1 7150.83 7461.36 59.11 o 6 6 1 34975.68 35401.05 195.35 o 7 6 1 270.45 289.84 19.56 o 8 6 1 19964.63 19768.12 125.15 o 9 6 1 558.52 574.99 24.53 o 10 6 1 26239.86 25670.92 195.55 o 11 6 1 350.36 386.99 31.56 o 12 6 1 9836.00 9427.15 116.26 o 13 6 1 35.01 30.56 24.74 o 1 7 1 2678.91 2602.89 24.20 o 2 7 1 733.90 735.63 18.15 o 3 7 1 6391.47 6776.85 51.93 o 4 7 1 925.95 940.58 22.80 o 5 7 1 4261.40 4467.43 65.20 o 6 7 1 695.45 618.72 21.94 o 7 7 1 4156.32 4218.14 60.41 o 8 7 1 1101.37 1069.20 31.77 o 9 7 1 529.19 510.84 24.62 o 10 7 1 871.26 792.31 44.32 o 11 7 1 754.35 824.64 38.90 o 12 7 1 25.85 -6.39 22.32 o 13 7 1 1613.28 1570.91 55.38 o 0 8 1 18439.89 18678.47 126.14 o 1 8 1 233.16 209.36 10.26 o 2 8 1 43343.94 43387.37 230.30 o 3 8 1 80.60 64.36 11.60 o 4 8 1 23817.39 23500.68 128.50 o 5 8 1 1545.64 1445.49 31.32 o 6 8 1 5381.10 5294.35 53.63 o 7 8 1 0.28 -5.69 18.64 o 8 8 1 15681.88 15754.36 126.12 o 9 8 1 951.49 975.80 30.57 o 10 8 1 12853.13 12659.43 134.25 o 11 8 1 633.71 606.10 38.84 o 12 8 1 3426.25 3421.58 72.78 o 13 8 1 87.35 144.66 30.29 o 1 9 1 9945.26 10029.64 60.73 o 2 9 1 1659.54 1834.77 28.42 o 3 9 1 1863.72 1741.81 28.67 o 4 9 1 23.58 8.27 11.96 o 5 9 1 8435.42 8295.67 69.94 o 6 9 1 310.86 312.50 19.96 o 7 9 1 8290.03 8232.85 101.58 o 8 9 1 4.22 30.87 18.59 o 9 9 1 2704.30 2506.24 68.96 o 10 9 1 47.46 -11.04 23.10 o 11 9 1 2063.61 2121.83 61.02 o 12 9 1 406.97 473.26 39.07 o 13 9 1 4430.79 4618.85 94.44 o 0 10 1 34.02 55.78 18.87 o 1 10 1 915.78 992.99 19.38 o 2 10 1 247.25 194.91 22.70 o 3 10 1 111.29 90.03 12.64 o 4 10 1 307.30 281.57 17.92 o 5 10 1 356.76 389.73 20.24 o 6 10 1 190.42 210.44 23.93 o 7 10 1 79.47 67.33 23.85 o 8 10 1 429.58 568.18 48.51 o 9 10 1 0.10 0.29 20.74 o 10 10 1 382.55 385.56 40.33 o 11 10 1 169.14 211.86 34.16 o 12 10 1 17.17 79.30 32.02 o 1 11 1 13670.54 13504.75 84.88 o 2 11 1 0.17 -7.82 13.29 o 3 11 1 1409.33 1498.65 32.96 o 4 11 1 3021.83 3157.83 47.02 o 5 11 1 5589.52 5659.91 70.09 o 6 11 1 260.61 315.95 25.70 o 7 11 1 19569.31 19332.74 200.66 o 8 11 1 723.85 757.04 43.28 o 9 11 1 1832.91 1918.65 63.48 o 10 11 1 61.40 36.55 43.60 o 11 11 1 2751.63 2826.02 94.01 o 12 11 1 296.45 305.63 47.76 o 0 12 1 2064.50 1828.90 56.27 o 1 12 1 223.35 271.28 15.83 o 2 12 1 7786.61 7702.03 80.84 o 3 12 1 899.35 888.72 30.95 o 4 12 1 4855.50 4711.19 61.77 o 5 12 1 640.93 619.15 30.12 o 6 12 1 878.43 817.38 39.47 o 7 12 1 116.06 132.19 30.68 o 8 12 1 1255.95 1278.63 54.44 o 9 12 1 3.00 -32.56 28.08 o 10 12 1 4305.50 4454.50 88.40 o 11 12 1 117.97 126.57 47.44 o 1 13 1 2201.19 2153.67 45.50 o 2 13 1 2137.24 2226.41 51.40 o 3 13 1 390.52 333.18 25.33 o 4 13 1 2415.23 2403.21 51.60 o 5 13 1 2079.53 2035.72 50.71 o 6 13 1 743.02 720.35 44.73 o 7 13 1 3470.76 3305.82 82.09 o 8 13 1 128.32 152.89 32.68 o 9 13 1 1171.61 1045.91 59.90 o 10 13 1 364.07 422.85 38.85 o 11 13 1 511.60 545.52 70.48 o 0 14 1 12038.02 12038.43 189.07 o 1 14 1 64.08 88.55 25.85 o 2 14 1 16080.32 16080.39 134.47 o 3 14 1 1497.72 1436.15 36.82 o 4 14 1 24001.09 23763.32 198.67 o 5 14 1 5.34 11.72 22.34 o 6 14 1 14983.52 14969.88 179.85 o 7 14 1 1272.86 1198.46 54.84 o 8 14 1 9206.57 9012.05 138.45 o 9 14 1 521.32 565.56 51.37 o 10 14 1 7430.18 7681.45 133.89 o 11 14 1 86.80 221.03 44.33 o 1 15 1 2496.18 2469.32 63.28 o 2 15 1 117.81 82.93 26.90 o 3 15 1 3.91 -7.56 21.87 o 4 15 1 80.48 78.62 25.85 o 5 15 1 84.28 109.35 26.71 o 6 15 1 720.90 723.54 48.14 o 7 15 1 1447.99 1360.15 60.18 o 8 15 1 4.61 10.16 33.96 o 9 15 1 15.74 -11.19 35.00 o 10 15 1 147.66 199.55 38.21 o 0 16 1 10794.71 10545.17 185.00 o 1 16 1 190.12 195.00 31.04 o 2 16 1 26681.42 26084.51 233.72 o 3 16 1 13.96 56.32 25.50 o 4 16 1 20530.39 20637.82 196.56 o 5 16 1 0.84 24.47 25.62 o 6 16 1 7415.73 7460.43 129.59 o 7 16 1 25.17 42.22 38.55 o 8 16 1 12497.29 12044.66 194.01 o 9 16 1 585.52 625.63 71.99 o 1 17 1 648.73 559.62 47.52 o 2 17 1 341.53 313.67 37.90 o 3 17 1 1044.86 992.06 47.00 o 4 17 1 593.95 597.15 38.38 o 5 17 1 667.07 657.32 53.48 o 6 17 1 594.43 601.96 59.91 o 7 17 1 336.31 250.42 46.24 o 8 17 1 470.30 554.12 55.98 o 9 17 1 481.02 482.24 56.30 o 0 18 1 4672.95 4675.04 176.40 o 1 18 1 372.35 410.81 42.76 o 2 18 1 7201.70 7080.86 114.27 o 3 18 1 630.03 597.05 39.84 o 4 18 1 8384.73 8248.17 115.54 o 5 18 1 104.29 105.03 41.73 o 6 18 1 3885.08 3822.92 111.77 o 7 18 1 223.80 243.44 63.04 o 8 18 1 4523.48 4536.22 124.71 o 1 19 1 2278.27 2240.61 114.44 o 2 19 1 1066.97 1209.73 59.84 o 3 19 1 2598.36 2802.73 78.50 o 4 19 1 166.96 226.80 35.60 o 5 19 1 1305.84 1215.82 72.30 o 6 19 1 65.63 20.45 39.68 o 7 19 1 1051.57 1224.15 93.13 o 0 20 1 126.34 242.88 68.62 o 1 20 1 0.15 16.60 37.70 o 2 20 1 3211.96 3356.36 91.56 o 3 20 1 47.48 62.52 33.07 o 4 20 1 3625.37 3677.55 90.14 o 5 20 1 15.47 16.32 39.95 o 1 21 1 2778.47 2722.64 99.39 o 2 21 1 127.44 111.72 37.25 o 3 21 1 368.23 417.58 49.30 o 4 21 1 472.89 474.56 46.64 o 0 0 2 96256.21 94312.64 1326.52 o 1 0 2 133.99 180.34 12.44 o 2 0 2 107659.00 111868.78 654.94 o 3 0 2 165.65 110.81 12.63 o 4 0 2 7273.59 6635.41 73.78 o 5 0 2 2333.28 2260.60 29.73 o 6 0 2 20178.04 20433.14 131.20 o 7 0 2 490.12 551.52 19.39 o 8 0 2 16596.69 16547.78 183.81 o 9 0 2 1829.65 1760.17 62.16 o 10 0 2 22417.79 21657.11 306.46 o 11 0 2 2201.77 2137.01 74.96 o 12 0 2 7839.56 7472.63 141.17 o 13 0 2 375.44 424.03 58.55 o 14 0 2 4400.25 4474.79 121.83 o 1 1 2 6425.41 6808.69 38.72 o 2 1 2 1972.84 2276.66 23.17 o 3 1 2 10455.52 10607.49 62.16 o 4 1 2 4348.03 4680.22 36.75 o 5 1 2 989.29 889.97 16.97 o 6 1 2 1217.99 1493.38 29.33 o 7 1 2 1364.66 1253.69 21.54 o 8 1 2 8.72 4.64 12.25 o 9 1 2 7084.30 7024.26 82.64 o 10 1 2 1023.71 955.47 36.69 o 11 1 2 1366.61 1343.84 44.03 o 12 1 2 20.51 8.42 21.78 o 13 1 2 581.69 646.08 38.67 o 14 1 2 829.59 895.60 46.11 o 0 2 2 42807.95 44695.14 272.15 o 1 2 2 37.43 35.79 4.85 o 2 2 2 22423.71 22833.71 111.58 o 3 2 2 179.65 205.82 9.04 o 4 2 2 35870.28 37318.07 163.25 o 5 2 2 12115.82 12779.17 76.43 o 6 2 2 8742.44 8469.93 55.28 o 7 2 2 171.97 137.22 13.75 o 8 2 2 18175.57 18167.03 109.42 o 9 2 2 52.16 32.51 19.31 o 10 2 2 6334.18 6250.91 82.21 o 11 2 2 2598.43 2472.69 57.02 o 12 2 2 4934.31 4882.39 80.98 o 13 2 2 63.82 39.06 28.27 o 14 2 2 4260.28 4334.08 85.06 o 1 3 2 67850.77 70080.46 331.10 o 2 3 2 209.85 228.15 9.51 o 3 3 2 36114.90 36532.41 200.44 o 4 3 2 1264.57 1424.57 19.62 o 5 3 2 28162.77 28750.38 143.81 o 6 3 2 417.86 502.29 17.32 o 7 3 2 12258.76 12679.06 87.00 o 8 3 2 63.49 50.22 13.39 o 9 3 2 12669.79 12323.25 114.67 o 10 3 2 39.78 23.83 20.85 o 11 3 2 10231.95 10047.71 112.09 o 12 3 2 1360.97 1317.47 60.38 o 13 3 2 2266.83 2348.61 61.56 o 14 3 2 212.28 189.02 31.38 o 0 4 2 1659.10 1527.13 33.71 o 1 4 2 149.08 159.85 11.39 o 2 4 2 16602.22 17586.17 95.62 o 3 4 2 992.88 1037.74 20.45 o 4 4 2 11626.88 12591.72 76.20 o 5 4 2 1280.74 1490.48 22.69 o 6 4 2 7514.92 8039.71 57.00 o 7 4 2 223.91 212.86 15.94 o 8 4 2 22.02 31.58 13.63 o 9 4 2 5.04 14.11 19.62 o 10 4 2 285.42 342.17 27.62 o 11 4 2 136.16 86.91 23.85 o 12 4 2 759.81 782.15 38.83 o 13 4 2 37.00 21.59 24.29 o 14 4 2 728.37 803.94 45.02 o 1 5 2 15793.97 15316.85 92.19 o 2 5 2 185.13 247.24 13.00 o 3 5 2 95383.76 97268.74 436.84 o 4 5 2 105.69 107.38 10.51 o 5 5 2 47476.24 47889.30 220.07 o 6 5 2 60.47 71.49 12.03 o 7 5 2 14751.98 14222.40 95.34 o 8 5 2 232.33 214.62 17.47 o 9 5 2 47658.76 46663.62 309.22 o 10 5 2 1847.01 1843.88 48.75 o 11 5 2 25996.70 24805.91 196.79 o 12 5 2 205.73 173.77 27.09 o 13 5 2 4226.92 4240.43 80.72 o 0 6 2 627.69 570.35 23.28 o 1 6 2 279.95 342.69 13.82 o 2 6 2 621.64 724.13 16.18 o 3 6 2 674.60 757.69 20.97 o 4 6 2 7.20 1.06 12.32 o 5 6 2 214.54 264.71 18.14 o 6 6 2 2901.10 2996.96 36.79 o 7 6 2 335.43 339.46 18.88 o 8 6 2 223.59 164.80 18.39 o 9 6 2 334.62 389.36 21.70 o 10 6 2 734.25 705.64 34.93 o 11 6 2 56.80 100.83 24.55 o 12 6 2 8.12 8.02 22.20 o 13 6 2 1.90 -2.95 23.63 o 1 7 2 18444.85 18381.29 106.18 o 2 7 2 480.72 498.97 16.98 o 3 7 2 47218.90 46956.73 245.30 o 4 7 2 87.11 70.46 13.04 o 5 7 2 23255.35 23260.66 132.23 o 6 7 2 23.34 3.81 13.56 o 7 7 2 8853.35 8669.94 82.30 o 8 7 2 1950.54 1829.24 37.36 o 9 7 2 22449.96 21823.12 140.70 o 10 7 2 1542.98 1392.09 45.00 o 11 7 2 14576.89 14063.42 141.10 o 12 7 2 44.47 58.30 25.39 o 13 7 2 3133.84 3321.50 74.26 o 0 8 2 11623.96 11529.77 94.66 o 1 8 2 365.01 338.42 15.59 o 2 8 2 13378.50 13559.81 88.55 o 3 8 2 0.26 -2.61 10.49 o 4 8 2 10434.44 10277.91 79.97 o 5 8 2 3499.72 3525.34 50.57 o 6 8 2 13534.58 13319.64 98.75 o 7 8 2 238.06 247.02 21.64 o 8 8 2 5041.71 4896.78 74.11 o 9 8 2 60.99 64.50 17.43 o 10 8 2 5247.75 5113.26 81.71 o 11 8 2 1798.79 1901.57 72.46 o 12 8 2 2560.37 2582.83 63.95 o 13 8 2 47.04 2.19 31.14 o 1 9 2 3148.90 3120.68 37.93 o 2 9 2 1488.34 1718.10 30.02 o 3 9 2 18529.76 18476.08 122.59 o 4 9 2 24.92 57.13 20.66 o 5 9 2 11846.68 11806.50 85.76 o 6 9 2 103.73 113.18 17.92 o 7 9 2 1623.54 1582.34 51.86 o 8 9 2 108.85 77.10 20.95 o 9 9 2 8358.23 8342.47 90.58 o 10 9 2 53.35 94.80 24.22 o 11 9 2 7268.87 7056.32 186.35 o 12 9 2 130.84 116.20 29.56 o 13 9 2 531.61 637.41 44.76 o 0 10 2 25397.99 24899.53 226.16 o 1 10 2 858.03 818.50 22.79 o 2 10 2 17393.56 16901.26 113.15 o 3 10 2 199.67 189.72 19.81 o 4 10 2 9178.43 8869.05 78.83 o 5 10 2 887.58 919.95 30.29 o 6 10 2 1848.68 1832.07 40.61 o 7 10 2 1819.33 1895.15 52.98 o 8 10 2 8533.62 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11898.59 148.91 o 2 1 23 405.62 455.86 49.33 o 3 1 23 4852.92 4968.92 219.91 o 4 1 23 409.92 374.32 46.34 o 5 1 23 8917.04 8802.95 151.95 o 0 2 23 624.75 724.22 85.03 o 1 2 23 22.80 38.57 32.92 o 2 2 23 101.40 192.76 58.01 o 3 2 23 188.84 119.62 87.94 o 4 2 23 71.61 113.89 37.72 o 5 2 23 210.17 193.99 40.64 o 1 3 23 4681.41 4964.89 94.29 o 2 3 23 133.35 247.79 41.07 o 3 3 23 3469.80 3322.00 136.00 o 4 3 23 115.88 62.61 35.60 o 5 3 23 4426.60 4341.07 98.55 o 0 4 23 338.25 138.50 103.27 o 1 4 23 28.49 4.48 36.38 o 2 4 23 151.15 68.58 79.54 o 3 4 23 40.34 98.28 43.54 o 4 4 23 21.13 27.39 37.11 o 1 5 23 93.15 126.76 36.47 o 2 5 23 42.60 18.35 65.81 o 3 5 23 9.49 52.36 35.43 o 4 5 23 2.63 62.30 39.19 o 0 6 23 1506.11 1602.83 97.53 o 1 6 23 226.77 234.23 50.77 o 2 6 23 89.77 98.73 44.39 o 3 6 23 98.61 172.15 36.36 o 1 7 23 2868.77 2960.99 88.59 o 2 7 23 26.01 22.54 38.35 o 0 8 23 2071.16 2106.60 111.42 o 1 8 23 2.51 17.25 34.46 o 0 0 24 830.77 1000.71 105.11 o 1 0 24 100.52 183.93 59.10 o 2 0 24 368.92 508.59 60.46 o 3 0 24 7.11 50.76 59.59 o 1 1 24 234.72 328.58 79.76 o 2 1 24 109.72 99.64 36.39 o 3 1 24 187.99 265.13 64.10 o 0 2 24 3832.04 3999.49 191.87 o 1 2 24 2.02 30.61 47.52 o 2 2 24 591.98 592.99 48.22 o 3 2 24 4.62 28.11 47.60 o 1 3 24 7749.06 7769.49 160.67 o 2 3 24 165.55 168.86 41.14 o 3 3 24 5810.85 5946.64 155.01 o 0 4 24 558.81 708.38 111.23 o 1 4 24 0.67 -39.84 48.51 o 2 4 24 281.95 118.75 76.76 o 1 5 24 8429.28 8735.63 182.80 o