#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222505.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222505_Fobs loop_ _publ_author_name 'Ketuly, Kamal Aziz' 'A. Hadi, A. Hamid' 'Ng, Seik Weng' _publ_section_title ; (20S)-22-Acetoxymethyl-6{\b}-methoxy-3\a,5-dihydro-3'H-cyclopropa[3\a,5]-5\a-pregnane ; _journal_coeditor_code XU2534 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1486 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.604 _cell_angle_gamma 90.000 _cell_length_a 9.8222 _cell_length_b 7.6128 _cell_length_c 15.2309 _exptl_crystal_F_000 428.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file xu2534Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1116.32 1125.37 19.03 o 2 0 0 6933.27 6708.54 111.27 o 3 0 0 0.98 -0.48 0.43 o 4 0 0 558.49 582.53 10.02 o 5 0 0 67.00 74.78 1.73 o 6 0 0 618.88 653.86 7.87 o 7 0 0 3.13 5.86 0.64 o 8 0 0 265.52 280.43 4.45 o 9 0 0 21.21 27.12 1.22 o 10 0 0 16.59 20.90 1.67 o 11 0 0 43.95 48.92 2.33 o 12 0 0 11.36 14.73 2.32 o 1 1 0 8173.72 8078.38 308.80 o 2 1 0 4094.62 4048.36 38.57 o 3 1 0 397.77 411.95 3.75 o 4 1 0 27.04 28.75 0.87 o 5 1 0 187.07 199.86 2.05 o 6 1 0 44.88 41.31 1.04 o 7 1 0 201.50 202.74 2.38 o 8 1 0 160.74 161.50 2.06 o 9 1 0 33.13 34.49 1.10 o 10 1 0 18.13 19.97 0.91 o 11 1 0 0.40 -0.32 0.71 o 12 1 0 39.37 40.14 2.95 o 0 2 0 5587.86 5315.92 61.17 o 1 2 0 1235.82 1265.20 12.06 o 2 2 0 892.50 936.49 16.54 o 3 2 0 58.51 58.10 1.35 o 4 2 0 28.59 31.12 0.68 o 5 2 0 268.49 267.80 2.87 o 6 2 0 145.96 157.32 2.25 o 7 2 0 439.08 441.12 5.44 o 8 2 0 421.34 395.33 5.76 o 9 2 0 141.98 143.24 2.49 o 10 2 0 77.47 73.30 2.02 o 11 2 0 47.71 48.87 1.89 o 1 3 0 1956.08 2058.68 21.25 o 2 3 0 213.09 230.18 2.43 o 3 3 0 262.64 276.44 3.70 o 4 3 0 142.43 161.76 2.47 o 5 3 0 191.63 181.95 3.68 o 6 3 0 820.37 852.80 12.02 o 7 3 0 349.41 355.46 4.89 o 8 3 0 34.27 35.37 1.77 o 9 3 0 51.95 54.96 3.14 o 10 3 0 9.95 10.93 1.29 o 11 3 0 32.36 35.80 1.72 o 0 4 0 66.84 65.87 1.43 o 1 4 0 529.77 544.87 4.97 o 2 4 0 459.34 516.29 5.92 o 3 4 0 166.53 156.15 2.41 o 4 4 0 216.36 212.25 4.85 o 5 4 0 140.15 159.26 2.61 o 6 4 0 273.18 254.97 3.61 o 7 4 0 288.67 295.66 3.47 o 8 4 0 4.11 3.58 0.72 o 9 4 0 132.96 123.09 2.86 o 10 4 0 80.67 73.89 7.55 o 11 4 0 7.67 8.73 1.55 o 1 5 0 935.99 913.00 8.18 o 2 5 0 108.11 101.53 1.67 o 3 5 0 523.26 509.77 5.85 o 4 5 0 28.71 31.82 1.22 o 5 5 0 548.94 534.72 6.24 o 6 5 0 151.15 145.50 2.08 o 7 5 0 35.34 37.19 1.18 o 8 5 0 56.48 59.04 1.93 o 9 5 0 83.80 86.96 2.85 o 10 5 0 13.24 12.23 1.25 o 0 6 0 789.80 787.61 10.90 o 1 6 0 391.19 382.23 4.02 o 2 6 0 123.62 120.16 1.86 o 3 6 0 138.42 133.25 1.87 o 4 6 0 359.07 335.10 4.15 o 5 6 0 2.36 1.06 0.48 o 6 6 0 56.37 55.23 1.52 o 7 6 0 24.84 25.74 1.37 o 8 6 0 41.27 45.22 2.58 o 9 6 0 6.11 5.53 1.11 o 1 7 0 315.18 322.79 3.69 o 2 7 0 222.61 211.61 2.94 o 3 7 0 57.37 55.09 1.21 o 4 7 0 0.73 1.28 0.54 o 5 7 0 39.37 42.15 1.45 o 6 7 0 30.35 27.03 1.48 o 7 7 0 22.54 22.74 1.59 o 8 7 0 41.12 45.55 2.00 o 0 8 0 2.81 2.47 1.06 o 1 8 0 0.89 0.27 0.62 o 2 8 0 3.80 2.39 0.67 o 3 8 0 2.98 2.07 0.72 o 4 8 0 55.55 56.81 1.50 o 5 8 0 60.11 55.23 1.96 o 6 8 0 14.62 15.97 1.64 o 7 8 0 66.61 70.11 2.82 o 1 9 0 36.85 37.62 1.33 o 2 9 0 20.47 19.25 1.73 o 3 9 0 14.91 17.67 1.27 o 4 9 0 5.10 4.04 1.07 o 5 9 0 90.89 97.23 2.73 o -12 0 1 1.63 4.91 1.86 o -11 0 1 21.32 19.76 2.09 o -10 0 1 14.68 13.38 1.00 o -9 0 1 48.18 42.92 1.44 o -8 0 1 168.04 159.13 2.87 o -7 0 1 22.09 21.45 1.19 o -6 0 1 15.41 18.36 1.05 o -5 0 1 15.98 10.27 0.75 o -4 0 1 72.30 101.43 2.55 o -3 0 1 1406.91 1468.68 19.36 o -2 0 1 18608.69 15747.80 226.14 o -1 0 1 361.16 378.31 3.66 o 1 0 1 107.27 107.35 1.92 o 2 0 1 86.27 83.04 1.64 o 3 0 1 1382.63 1369.11 18.17 o 4 0 1 178.75 202.72 3.09 o 5 0 1 536.94 549.60 7.69 o 6 0 1 2.39 2.97 0.52 o 7 0 1 5.50 8.76 0.64 o 8 0 1 32.65 29.33 1.06 o 9 0 1 119.43 110.26 2.38 o 10 0 1 1.51 2.51 1.09 o 11 0 1 0.51 1.11 1.10 o -12 1 1 23.14 27.05 1.61 o -11 1 1 120.19 125.90 2.46 o -10 1 1 14.97 16.96 1.12 o -9 1 1 27.82 25.03 0.90 o -8 1 1 127.98 121.68 1.86 o -7 1 1 20.12 21.60 0.80 o -6 1 1 30.44 29.10 0.88 o -5 1 1 9.38 14.00 0.61 o -4 1 1 1625.77 1788.95 17.04 o -3 1 1 1253.94 1328.16 13.88 o -2 1 1 2726.90 2737.24 157.28 o -1 1 1 5040.14 5012.70 114.42 o 0 1 1 1281.25 1294.78 13.18 o 1 1 1 652.33 686.57 6.06 o 2 1 1 1.64 2.77 0.20 o 3 1 1 124.35 126.45 1.31 o 4 1 1 28.82 33.73 0.62 o 5 1 1 94.31 92.96 1.36 o 6 1 1 472.02 457.01 4.66 o 7 1 1 85.47 85.79 1.49 o 8 1 1 29.92 27.45 0.84 o 9 1 1 46.21 48.71 1.25 o 10 1 1 65.18 61.12 1.47 o 11 1 1 4.78 3.97 0.83 o -12 2 1 17.07 18.07 1.39 o -11 2 1 39.43 41.02 1.77 o -10 2 1 25.50 21.70 1.08 o -9 2 1 59.73 65.53 2.39 o -8 2 1 201.75 184.89 3.29 o -7 2 1 189.81 192.42 2.46 o -6 2 1 176.01 170.32 2.41 o -5 2 1 548.45 581.87 5.78 o -4 2 1 19.31 29.91 0.80 o -3 2 1 925.35 994.14 11.43 o -2 2 1 1837.39 1888.29 18.03 o -1 2 1 29.63 33.02 0.51 o 0 2 1 1402.31 1409.99 14.36 o 1 2 1 2889.18 2936.41 27.51 o 2 2 1 1421.04 1437.69 11.75 o 3 2 1 229.86 211.07 1.92 o 4 2 1 338.89 343.96 3.02 o 5 2 1 493.47 522.52 4.78 o 6 2 1 214.63 215.89 2.45 o 7 2 1 344.84 353.40 4.73 o 8 2 1 2.03 1.72 0.52 o 9 2 1 228.33 221.54 3.52 o 10 2 1 7.80 8.09 0.88 o 11 2 1 43.23 42.26 1.82 o -11 3 1 21.97 18.52 1.39 o -10 3 1 33.91 35.96 1.90 o -9 3 1 81.45 74.42 2.58 o -8 3 1 164.45 169.57 2.72 o -7 3 1 206.85 200.17 3.94 o -6 3 1 129.35 135.90 2.26 o -5 3 1 57.44 65.72 1.26 o -4 3 1 86.55 94.73 1.50 o -3 3 1 541.40 597.62 6.55 o -2 3 1 399.90 415.33 4.12 o -1 3 1 55.06 52.57 0.79 o 0 3 1 716.29 758.13 7.90 o 1 3 1 521.04 533.65 5.75 o 2 3 1 129.99 139.30 1.65 o 3 3 1 1165.40 1260.42 12.05 o 4 3 1 661.28 730.03 7.20 o 5 3 1 526.55 532.85 5.45 o 6 3 1 225.12 216.30 2.60 o 7 3 1 103.45 101.09 1.73 o 8 3 1 56.54 57.86 1.51 o 9 3 1 5.86 6.58 0.82 o 10 3 1 1.23 2.84 1.13 o 11 3 1 2.84 0.76 1.19 o -11 4 1 50.11 52.03 2.54 o -10 4 1 52.14 54.38 1.96 o -9 4 1 29.18 24.32 1.22 o -8 4 1 256.93 259.43 3.47 o -7 4 1 18.32 17.64 0.92 o -6 4 1 147.01 146.49 2.46 o -5 4 1 344.85 377.85 5.02 o -4 4 1 53.23 52.51 1.24 o -3 4 1 469.71 442.97 5.65 o -2 4 1 10.03 8.92 0.40 o -1 4 1 484.31 510.68 4.67 o 0 4 1 630.42 666.51 6.01 o 1 4 1 400.72 399.13 4.22 o 2 4 1 791.35 822.90 22.48 o 3 4 1 1021.04 1044.89 10.46 o 4 4 1 66.97 67.08 1.23 o 5 4 1 607.34 601.10 6.15 o 6 4 1 162.58 167.95 2.21 o 7 4 1 93.91 89.98 1.64 o 8 4 1 67.49 66.91 1.74 o 9 4 1 31.96 29.93 1.81 o 10 4 1 5.19 4.89 1.32 o -10 5 1 76.94 88.00 3.46 o -9 5 1 35.12 34.89 1.85 o -8 5 1 35.31 37.65 1.21 o -7 5 1 221.05 230.97 3.60 o -6 5 1 151.47 147.67 2.56 o -5 5 1 261.97 255.49 3.73 o -4 5 1 38.63 35.69 1.14 o -3 5 1 198.55 190.86 3.27 o -2 5 1 265.83 272.92 4.71 o -1 5 1 183.66 178.98 1.94 o 0 5 1 117.59 117.70 1.55 o 1 5 1 358.45 370.60 5.44 o 2 5 1 174.87 184.53 2.13 o 3 5 1 84.82 91.98 1.56 o 4 5 1 172.59 181.48 2.29 o 5 5 1 219.64 223.74 2.74 o 6 5 1 57.50 54.72 1.40 o 7 5 1 10.18 8.81 0.86 o 8 5 1 10.49 10.40 1.12 o 9 5 1 31.77 27.41 2.46 o 10 5 1 68.42 73.25 2.95 o -9 6 1 1.03 1.28 0.95 o -8 6 1 45.24 45.75 3.24 o -7 6 1 8.56 10.18 1.13 o -6 6 1 144.29 137.05 2.92 o -5 6 1 159.43 148.43 3.47 o -4 6 1 18.79 21.40 0.99 o -3 6 1 805.28 788.95 9.50 o -2 6 1 797.41 785.10 9.58 o -1 6 1 266.04 261.28 2.99 o 0 6 1 295.41 288.79 3.53 o 1 6 1 286.22 265.70 2.76 o 2 6 1 19.51 18.95 0.65 o 3 6 1 82.19 85.37 1.60 o 4 6 1 16.10 14.20 0.70 o 5 6 1 3.04 1.97 0.70 o 6 6 1 16.78 15.45 0.98 o 7 6 1 42.42 35.96 1.63 o 8 6 1 34.99 32.58 1.63 o 9 6 1 4.48 3.61 1.36 o -8 7 1 9.97 12.16 2.14 o -7 7 1 6.87 7.02 1.11 o -6 7 1 36.05 34.06 1.19 o -5 7 1 13.28 15.31 0.88 o -4 7 1 206.56 195.76 2.85 o -3 7 1 15.27 15.71 0.75 o -2 7 1 21.33 20.43 0.72 o -1 7 1 179.69 194.29 2.50 o 0 7 1 161.96 161.18 2.10 o 1 7 1 5.14 6.55 0.59 o 2 7 1 71.43 73.46 1.51 o 3 7 1 26.00 27.06 0.89 o 4 7 1 34.68 33.17 1.09 o 5 7 1 88.15 86.16 2.33 o 6 7 1 2.89 1.64 0.93 o 7 7 1 38.86 40.22 1.78 o 8 7 1 1.51 2.67 1.00 o -7 8 1 21.05 24.42 1.55 o -6 8 1 11.72 15.05 1.39 o -5 8 1 6.37 7.36 0.83 o -4 8 1 15.60 16.35 0.94 o -3 8 1 15.72 16.97 1.03 o -2 8 1 22.88 29.80 1.08 o -1 8 1 2.66 2.83 0.68 o 0 8 1 3.52 2.42 0.74 o 1 8 1 72.22 77.47 1.85 o 2 8 1 1.61 3.42 0.75 o 3 8 1 63.08 63.56 1.98 o 4 8 1 122.51 120.20 2.84 o 5 8 1 38.98 42.10 1.76 o 6 8 1 88.31 86.12 3.24 o -5 9 1 48.00 48.21 2.74 o -4 9 1 39.63 41.49 1.84 o -3 9 1 21.40 23.02 2.27 o -2 9 1 16.83 19.06 1.41 o -1 9 1 2.45 2.00 0.73 o 0 9 1 42.57 41.32 1.29 o 1 9 1 6.33 6.10 0.91 o 2 9 1 53.42 52.18 1.95 o 3 9 1 107.72 115.96 2.85 o 4 9 1 371.34 389.08 6.59 o -12 0 2 3.35 0.26 1.69 o -11 0 2 46.92 39.36 2.98 o -10 0 2 6.84 5.98 0.83 o -9 0 2 187.33 173.71 6.14 o -8 0 2 0.42 0.41 0.76 o -7 0 2 24.30 19.83 1.21 o -6 0 2 24.64 35.61 1.38 o -5 0 2 3117.34 3426.87 84.86 o -4 0 2 3292.60 3554.45 46.91 o -3 0 2 2615.98 2680.83 37.12 o -2 0 2 469.31 496.90 5.87 o -1 0 2 1493.23 1461.88 19.81 o 0 0 2 272.83 280.15 3.32 o 1 0 2 1081.04 1099.60 17.66 o 2 0 2 869.75 883.61 23.94 o 3 0 2 4.93 3.51 0.54 o 4 0 2 246.60 256.39 4.00 o 5 0 2 9.52 8.11 0.78 o 6 0 2 2.29 2.44 0.48 o 7 0 2 48.90 47.51 1.56 o 8 0 2 14.42 13.50 0.81 o 9 0 2 176.30 180.59 4.49 o 10 0 2 2.16 2.43 1.06 o 11 0 2 240.24 250.05 8.27 o -12 1 2 41.23 47.18 2.34 o -11 1 2 12.71 14.88 1.00 o -10 1 2 30.91 34.31 1.12 o -9 1 2 6.32 5.35 0.58 o -8 1 2 19.74 24.25 1.30 o -7 1 2 350.32 394.01 4.54 o -6 1 2 607.95 665.27 8.04 o -5 1 2 2410.09 2728.01 31.29 o -4 1 2 612.87 662.94 7.11 o -3 1 2 165.56 196.70 2.56 o -2 1 2 1855.98 1851.16 21.46 o -1 1 2 77.52 71.34 0.75 o 0 1 2 474.17 475.19 5.48 o 1 1 2 1356.55 1400.92 10.93 o 2 1 2 1909.86 1970.54 16.93 o 3 1 2 133.14 131.82 1.47 o 4 1 2 253.81 260.49 2.71 o 5 1 2 25.84 21.11 0.61 o 6 1 2 44.36 46.58 0.84 o 7 1 2 257.58 267.26 2.78 o 8 1 2 227.88 215.15 2.41 o 9 1 2 102.66 111.02 1.76 o 10 1 2 31.11 29.60 1.21 o 11 1 2 15.33 15.61 1.29 o -12 2 2 39.43 40.18 1.55 o -11 2 2 76.46 75.46 1.90 o -10 2 2 26.01 26.10 1.18 o -9 2 2 34.29 35.02 1.57 o -8 2 2 24.17 22.38 1.05 o -7 2 2 0.22 1.27 0.47 o -6 2 2 240.52 273.88 3.32 o -5 2 2 43.70 47.84 1.56 o -4 2 2 66.63 61.92 1.23 o -3 2 2 586.76 594.72 6.40 o -2 2 2 536.18 566.91 6.25 o -1 2 2 677.51 677.70 5.95 o 0 2 2 658.39 666.30 10.41 o 1 2 2 681.65 702.07 6.72 o 2 2 2 120.70 145.34 1.64 o 3 2 2 801.33 884.92 7.30 o 4 2 2 52.64 49.32 0.73 o 5 2 2 45.20 46.74 0.79 o 6 2 2 64.22 65.23 1.08 o 7 2 2 265.90 261.24 3.70 o 8 2 2 25.61 25.93 0.94 o 9 2 2 1.28 0.91 0.66 o 10 2 2 5.46 5.56 0.76 o 11 2 2 80.06 84.60 2.47 o -11 3 2 27.26 31.09 1.32 o -10 3 2 7.49 8.32 0.99 o -9 3 2 11.26 10.35 0.96 o -8 3 2 44.72 44.67 1.50 o -7 3 2 34.52 33.44 1.00 o -6 3 2 85.12 93.63 1.79 o -5 3 2 116.35 132.65 2.15 o -4 3 2 50.88 59.20 1.25 o -3 3 2 164.51 170.51 2.14 o -2 3 2 212.94 236.27 2.21 o -1 3 2 17.74 16.21 0.42 o 0 3 2 364.85 355.68 4.92 o 1 3 2 1404.09 1542.11 15.80 o 2 3 2 2486.17 2810.36 24.42 o 3 3 2 415.42 433.16 4.05 o 4 3 2 215.07 224.78 2.30 o 5 3 2 425.09 403.78 4.26 o 6 3 2 274.56 263.69 3.32 o 7 3 2 26.07 26.35 1.01 o 8 3 2 40.03 35.32 1.54 o 9 3 2 64.35 63.68 1.73 o 10 3 2 12.29 11.51 1.39 o 11 3 2 38.90 35.84 4.19 o -11 4 2 8.67 9.87 1.43 o -10 4 2 64.08 69.92 3.22 o -9 4 2 20.18 22.42 1.30 o -8 4 2 14.45 13.41 0.90 o -7 4 2 55.18 53.08 1.45 o -6 4 2 354.93 335.52 4.63 o -5 4 2 31.85 34.48 1.12 o -4 4 2 42.38 44.54 1.17 o -3 4 2 69.88 68.81 1.13 o -2 4 2 411.79 438.75 3.82 o -1 4 2 309.20 306.34 3.17 o 0 4 2 311.95 333.84 4.04 o 1 4 2 345.31 362.35 4.58 o 2 4 2 196.82 190.72 2.20 o 3 4 2 150.21 157.41 1.93 o 4 4 2 780.56 801.67 7.95 o 5 4 2 30.91 30.37 0.85 o 6 4 2 496.11 490.09 6.85 o 7 4 2 29.55 27.10 1.15 o 8 4 2 81.77 74.82 2.16 o 9 4 2 8.48 8.79 1.11 o 10 4 2 80.34 89.25 3.16 o -10 5 2 3.63 2.46 0.96 o -9 5 2 46.72 47.36 1.43 o -8 5 2 43.95 46.62 1.52 o -7 5 2 75.73 70.26 1.76 o -6 5 2 40.78 36.81 1.55 o -5 5 2 6.05 5.34 0.71 o -4 5 2 27.79 28.03 1.05 o -3 5 2 64.82 59.19 1.20 o -2 5 2 39.23 34.42 0.80 o -1 5 2 350.18 372.76 7.02 o 0 5 2 59.39 65.36 1.14 o 1 5 2 171.57 175.68 2.33 o 2 5 2 23.26 23.66 0.71 o 3 5 2 115.84 124.53 1.70 o 4 5 2 56.06 51.31 1.08 o 5 5 2 159.72 160.60 2.15 o 6 5 2 203.22 203.14 3.30 o 7 5 2 9.42 10.36 0.89 o 8 5 2 15.06 16.22 1.08 o 9 5 2 49.29 54.31 2.07 o 10 5 2 19.98 22.66 3.55 o -9 6 2 0.68 -1.38 0.92 o -8 6 2 25.45 30.49 1.14 o -7 6 2 29.98 25.20 1.17 o -6 6 2 8.36 9.02 0.89 o -5 6 2 183.91 181.56 3.00 o -4 6 2 489.67 465.58 5.48 o -3 6 2 379.39 353.77 4.33 o -2 6 2 215.43 205.00 3.16 o -1 6 2 270.54 254.05 2.52 o 0 6 2 79.92 78.06 1.50 o 1 6 2 36.32 35.36 0.91 o 2 6 2 178.08 156.57 4.03 o 3 6 2 356.31 343.87 3.83 o 4 6 2 58.45 50.58 1.44 o 5 6 2 208.39 189.91 3.16 o 6 6 2 9.00 9.28 1.03 o 7 6 2 86.32 85.36 2.26 o 8 6 2 0.35 -0.50 0.79 o 9 6 2 33.78 32.50 1.73 o -8 7 2 16.02 17.90 1.41 o -7 7 2 14.39 12.73 0.92 o -6 7 2 12.89 14.82 1.02 o -5 7 2 31.73 31.38 1.26 o -4 7 2 47.21 45.05 1.47 o -3 7 2 343.71 339.92 4.31 o -2 7 2 132.85 120.07 3.19 o -1 7 2 145.71 155.48 2.39 o 0 7 2 2.66 3.07 0.51 o 1 7 2 9.12 10.06 0.74 o 2 7 2 39.30 39.06 1.04 o 3 7 2 74.74 78.66 1.61 o 4 7 2 18.62 17.04 1.01 o 5 7 2 134.99 129.05 3.10 o 6 7 2 4.23 3.06 0.95 o 7 7 2 5.72 6.88 1.53 o 8 7 2 64.05 66.36 2.33 o -7 8 2 8.70 7.66 1.75 o -6 8 2 10.59 13.09 0.95 o -5 8 2 41.77 43.21 1.37 o -4 8 2 5.08 4.71 0.83 o -3 8 2 11.62 9.62 0.81 o -2 8 2 20.23 18.86 1.15 o -1 8 2 36.24 32.28 1.16 o 0 8 2 71.73 77.26 1.84 o 1 8 2 3.96 4.14 0.66 o 2 8 2 57.49 64.75 1.53 o 3 8 2 0.28 1.42 0.73 o 4 8 2 15.38 16.59 1.06 o 5 8 2 65.38 70.40 2.33 o 6 8 2 32.95 34.27 1.72 o -5 9 2 6.53 7.81 1.20 o -4 9 2 15.94 15.87 1.68 o -3 9 2 11.54 11.56 1.29 o -2 9 2 1.25 0.59 0.99 o -1 9 2 2.30 1.11 0.97 o 0 9 2 24.67 27.13 1.08 o 1 9 2 129.27 146.04 3.23 o 2 9 2 106.53 109.97 5.43 o 3 9 2 60.13 61.24 3.15 o 4 9 2 28.92 33.97 1.68 o -12 0 3 30.34 32.66 2.85 o -11 0 3 26.42 27.95 2.56 o -10 0 3 75.35 70.00 4.34 o -9 0 3 0.12 0.38 0.87 o -8 0 3 57.29 51.04 1.99 o -7 0 3 495.26 608.34 10.58 o -6 0 3 999.74 1087.50 18.08 o -5 0 3 73.21 85.15 1.60 o -4 0 3 71.63 86.66 2.59 o -3 0 3 169.95 175.92 2.29 o -2 0 3 144.67 151.05 1.95 o -1 0 3 4497.70 4591.76 75.84 o 0 0 3 1415.75 1464.20 16.92 o 1 0 3 126.56 126.18 2.37 o 2 0 3 120.89 120.48 2.36 o 3 0 3 38.66 41.94 2.85 o 4 0 3 2.07 2.33 0.56 o 5 0 3 384.19 397.68 5.81 o 6 0 3 43.60 43.41 1.28 o 7 0 3 716.03 734.69 10.40 o 8 0 3 217.03 215.56 3.76 o 9 0 3 121.19 124.13 2.66 o 10 0 3 70.41 73.76 3.91 o 11 0 3 10.72 10.96 1.96 o -12 1 3 8.19 11.15 1.53 o -11 1 3 54.50 56.08 1.63 o -10 1 3 65.58 67.10 1.96 o -9 1 3 57.82 58.25 1.46 o -8 1 3 191.69 197.71 3.45 o -7 1 3 160.33 172.01 2.30 o -6 1 3 202.94 236.91 2.86 o -5 1 3 48.94 55.27 2.03 o -4 1 3 163.38 173.10 2.12 o -3 1 3 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