#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/25/2222509.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222509_Fobs loop_ _publ_author_name 'H\"okelek, Tuncer' 'Y\?ilmaz, Filiz' 'Tercan, Bar\?i\,s' '\"Ozbek, F. Elif' 'Necefo\(glu, Hacali' _publ_section_title ; Diaquabis(2-bromobenzoato-\kO)bis(nicotinamide-\kN^1^)nickel(II) ; _journal_coeditor_code XU2538 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m768 _journal_page_last m769 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.609 _cell_angle_gamma 90.000 _cell_length_a 7.8851 _cell_length_b 18.2865 _cell_length_c 9.7574 _exptl_crystal_F_000 740.00 _reflns_d_resolution_high 0.7463 _[local]_cod_data_source_file xu2538Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' el25 in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 205.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9916.56 13674.67 157.06 o 4 0 0 5471.10 7398.05 95.50 o 6 0 0 399.09 495.95 19.07 o 8 0 0 3824.24 4331.39 198.63 o 10 0 0 934.87 906.11 65.13 o 1 1 0 9023.52 10764.51 118.79 o 2 1 0 7106.50 8881.03 92.34 o 3 1 0 1312.23 1515.51 15.91 o 4 1 0 7059.42 9236.84 83.04 o 5 1 0 1840.33 2217.01 24.38 o 6 1 0 537.42 601.85 20.35 o 7 1 0 2110.07 2441.25 39.71 o 8 1 0 2255.18 2565.85 56.96 o 9 1 0 655.30 656.54 30.19 o 10 1 0 111.73 157.53 59.92 o 0 2 0 175.16 198.60 6.40 o 1 2 0 465.77 520.88 20.90 o 2 2 0 98.77 151.39 5.94 o 3 2 0 5328.53 6728.66 64.06 o 4 2 0 11885.52 14633.03 137.30 o 5 2 0 111.38 126.54 5.16 o 6 2 0 9975.93 11548.59 203.81 o 7 2 0 694.55 859.66 26.01 o 8 2 0 348.49 398.33 23.84 o 9 2 0 192.58 221.69 23.84 o 10 2 0 764.41 847.26 44.21 o 1 3 0 6312.77 6468.29 80.11 o 2 3 0 16389.35 17938.66 189.58 o 3 3 0 1058.49 1152.29 15.04 o 4 3 0 2962.34 3567.95 35.87 o 5 3 0 13.72 14.43 4.06 o 6 3 0 1937.74 2081.56 27.66 o 7 3 0 569.79 591.67 20.60 o 8 3 0 1635.17 1804.21 45.67 o 9 3 0 1630.90 1787.00 48.98 o 10 3 0 12.45 9.99 37.77 o 0 4 0 10216.74 9990.14 194.48 o 1 4 0 17478.28 18294.10 260.88 o 2 4 0 2788.24 2950.50 42.53 o 3 4 0 5131.60 5568.49 66.26 o 4 4 0 1954.63 2230.74 25.18 o 5 4 0 12.66 12.31 4.26 o 6 4 0 56.92 57.87 8.91 o 7 4 0 63.55 61.45 9.75 o 8 4 0 550.62 517.07 26.00 o 9 4 0 145.15 177.00 22.84 o 1 5 0 17215.00 18261.82 250.23 o 2 5 0 28.66 33.02 3.48 o 3 5 0 2465.40 2427.84 30.90 o 4 5 0 486.67 498.87 10.15 o 5 5 0 13279.98 14455.47 245.97 o 6 5 0 83.43 120.89 9.90 o 7 5 0 2270.91 2464.20 40.15 o 8 5 0 331.75 372.68 23.77 o 9 5 0 258.93 278.30 32.43 o 0 6 0 950.10 961.46 23.10 o 1 6 0 296.15 322.89 8.76 o 2 6 0 3059.89 3239.48 43.01 o 3 6 0 11366.02 12104.18 157.46 o 4 6 0 7062.67 7400.99 95.07 o 5 6 0 34.55 53.75 5.56 o 6 6 0 1239.58 1154.11 23.74 o 7 6 0 2222.34 2217.91 37.22 o 8 6 0 102.89 97.11 13.72 o 9 6 0 1959.93 1922.35 99.43 o 1 7 0 13806.44 13600.69 187.83 o 2 7 0 1196.76 1248.49 19.32 o 3 7 0 346.11 372.21 9.33 o 4 7 0 1.54 36.01 6.70 o 5 7 0 2172.91 2114.84 33.71 o 6 7 0 783.72 726.03 18.82 o 7 7 0 115.70 122.70 11.65 o 8 7 0 26.21 36.80 12.87 o 9 7 0 2329.55 2317.99 55.27 o 0 8 0 105.17 86.72 9.77 o 1 8 0 6680.52 6785.31 96.16 o 2 8 0 4885.43 5091.21 66.42 o 3 8 0 9269.74 9391.08 119.17 o 4 8 0 1091.38 1090.76 19.27 o 5 8 0 21.06 24.36 8.00 o 6 8 0 80.49 90.84 10.97 o 7 8 0 3466.77 3291.43 58.04 o 8 8 0 451.61 426.88 23.81 o 9 8 0 255.78 242.69 25.69 o 1 9 0 56.45 46.33 7.76 o 2 9 0 19.69 23.85 5.08 o 3 9 0 1227.29 1124.06 19.35 o 4 9 0 1796.94 1841.00 28.59 o 5 9 0 3401.39 3274.60 48.40 o 6 9 0 534.73 495.74 19.35 o 7 9 0 2057.39 1991.18 41.39 o 8 9 0 233.70 251.71 18.02 o 9 9 0 5.33 7.41 17.63 o 0 10 0 6749.68 6358.71 129.22 o 1 10 0 28.09 22.12 5.18 o 2 10 0 6221.44 6395.63 83.26 o 3 10 0 2534.33 2458.12 35.83 o 4 10 0 16.86 8.01 8.10 o 5 10 0 90.98 91.35 11.43 o 6 10 0 318.39 300.63 16.37 o 7 10 0 667.02 697.72 25.63 o 8 10 0 290.19 291.10 29.26 o 9 10 0 533.07 582.05 31.52 o 1 11 0 1205.68 1111.44 18.40 o 2 11 0 3640.02 3574.02 45.56 o 3 11 0 105.72 107.42 7.61 o 4 11 0 1511.69 1417.64 34.82 o 5 11 0 7.66 -8.87 10.67 o 6 11 0 559.26 534.59 21.12 o 7 11 0 236.29 236.99 17.89 o 8 11 0 746.48 725.95 27.26 o 9 11 0 1060.05 1050.18 34.53 o 0 12 0 2193.64 2093.05 41.73 o 1 12 0 152.54 198.35 8.16 o 2 12 0 53.93 46.86 6.84 o 3 12 0 385.84 373.15 14.01 o 4 12 0 1423.81 1340.37 34.66 o 5 12 0 115.53 110.50 16.11 o 6 12 0 4858.79 4681.63 78.01 o 7 12 0 29.78 31.97 15.14 o 8 12 0 58.51 49.04 16.27 o 1 13 0 81.66 67.55 8.06 o 2 13 0 8198.45 8070.43 118.90 o 3 13 0 978.79 926.32 23.60 o 4 13 0 1055.49 1002.83 29.91 o 5 13 0 462.71 461.17 30.27 o 6 13 0 1776.85 1668.01 38.35 o 7 13 0 24.34 27.54 15.37 o 8 13 0 1393.04 1345.84 37.92 o 0 14 0 5449.71 5214.70 92.32 o 1 14 0 174.11 205.83 10.12 o 2 14 0 1994.05 1909.36 36.58 o 3 14 0 115.56 78.04 14.35 o 4 14 0 438.49 408.44 20.63 o 5 14 0 1145.17 1121.91 30.07 o 6 14 0 669.43 671.32 25.62 o 7 14 0 78.00 81.30 17.20 o 8 14 0 186.05 203.87 21.02 o 1 15 0 156.72 125.02 12.24 o 2 15 0 2141.69 2006.26 38.90 o 3 15 0 356.15 360.46 22.03 o 4 15 0 97.87 88.57 15.78 o 5 15 0 1301.73 1302.38 33.24 o 6 15 0 809.80 803.98 30.55 o 7 15 0 270.13 258.24 24.75 o 0 16 0 255.55 261.80 35.60 o 1 16 0 505.07 512.22 20.59 o 2 16 0 584.53 584.46 21.14 o 3 16 0 566.55 574.49 40.54 o 4 16 0 2094.07 2139.54 50.44 o 5 16 0 456.67 475.82 21.71 o 6 16 0 1708.09 1721.81 41.19 o 7 16 0 224.78 189.39 20.72 o 1 17 0 3483.03 3585.14 61.42 o 2 17 0 1121.78 1098.63 34.03 o 3 17 0 45.08 40.33 15.57 o 4 17 0 272.75 263.85 21.36 o 5 17 0 158.78 149.47 17.36 o 6 17 0 133.06 169.47 20.95 o 7 17 0 1.06 -1.91 20.40 o 0 18 0 1070.24 1138.83 68.16 o 1 18 0 467.47 525.44 33.77 o 2 18 0 188.23 178.16 18.41 o 3 18 0 2936.70 2919.04 63.79 o 4 18 0 273.23 299.05 19.51 o 5 18 0 5.34 7.81 15.72 o 6 18 0 77.74 64.43 18.72 o 1 19 0 840.87 885.83 44.36 o 2 19 0 51.62 73.37 36.90 o 3 19 0 2308.08 2311.06 55.17 o 4 19 0 52.57 66.59 16.18 o 5 19 0 3437.35 3527.49 74.14 o 6 19 0 337.23 349.58 27.58 o 0 20 0 905.32 1108.87 75.98 o 1 20 0 554.46 672.71 40.98 o 2 20 0 1010.30 933.90 68.16 o 3 20 0 1134.66 1168.79 74.68 o 4 20 0 339.36 358.43 29.39 o 5 20 0 46.80 7.92 18.08 o 1 21 0 2875.76 3149.91 128.08 o 2 21 0 255.17 260.50 49.06 o 3 21 0 33.34 -20.84 38.21 o 4 21 0 51.73 23.90 29.31 o 5 21 0 398.60 450.01 29.25 o 0 22 0 132.82 97.25 46.46 o 1 22 0 109.68 225.77 50.80 o 2 22 0 26.79 -20.41 43.85 o 3 22 0 924.20 1061.11 76.41 o 1 23 0 17.78 75.55 50.36 o 2 23 0 883.98 890.92 73.81 o 3 23 0 798.86 773.69 72.94 o 1 24 0 20.51 -17.80 50.36 o -9 0 1 1580.28 1765.90 59.70 o -7 0 1 2815.89 3319.26 59.22 o -5 0 1 3138.46 4140.64 63.61 o -3 0 1 11498.55 14915.63 370.56 o -1 0 1 1319.17 1392.82 40.81 o 1 0 1 2948.88 3752.18 90.34 o 3 0 1 136.07 143.13 17.99 o 5 0 1 2596.32 2960.52 59.79 o 7 0 1 15423.52 17143.23 490.18 o 9 0 1 1326.62 1296.87 71.20 o -10 1 1 1365.32 1601.75 48.15 o -9 1 1 387.44 478.95 23.14 o -8 1 1 1573.52 1874.44 39.77 o -7 1 1 1509.23 1727.63 25.45 o -6 1 1 7.72 8.30 4.58 o -5 1 1 7987.39 9751.47 92.04 o -4 1 1 3829.00 5039.89 55.10 o -3 1 1 468.76 498.06 11.34 o -2 1 1 807.42 1008.33 18.88 o -1 1 1 11223.92 12362.05 142.15 o 0 1 1 2231.67 2409.78 28.48 o 1 1 1 1538.63 1763.77 33.19 o 2 1 1 1218.97 1260.01 13.35 o 3 1 1 10514.93 12663.83 153.35 o 4 1 1 1630.21 1828.97 23.50 o 5 1 1 4206.25 4732.28 58.83 o 6 1 1 12.04 12.72 7.73 o 7 1 1 520.16 622.88 46.83 o 8 1 1 559.53 585.74 32.38 o 9 1 1 1340.24 1378.93 51.88 o -10 2 1 178.35 238.80 25.24 o -9 2 1 3524.08 3879.23 82.67 o -8 2 1 1.11 9.02 11.56 o -7 2 1 2503.44 2907.65 40.66 o -6 2 1 1223.40 1308.31 18.24 o -5 2 1 5.17 19.39 4.03 o -4 2 1 396.81 396.56 8.93 o -3 2 1 4837.27 5383.08 81.68 o -2 2 1 1634.91 1724.26 31.42 o -1 2 1 9950.13 10661.88 134.72 o 0 2 1 518.06 457.86 8.15 o 1 2 1 17353.01 17649.79 282.69 o 2 2 1 539.05 504.04 7.81 o 3 2 1 12259.51 13881.24 167.17 o 4 2 1 218.22 202.17 6.37 o 5 2 1 11.16 15.43 5.03 o 6 2 1 169.94 186.01 12.57 o 7 2 1 37.40 52.49 15.84 o 8 2 1 250.91 280.75 26.66 o 9 2 1 3.80 22.42 24.47 o -10 3 1 28.01 58.01 29.22 o -9 3 1 123.65 157.09 25.05 o -8 3 1 7.80 4.34 12.60 o -7 3 1 474.42 494.94 12.50 o -6 3 1 1671.84 1793.65 21.41 o -5 3 1 470.54 469.18 8.84 o -4 3 1 15523.83 17735.34 188.74 o -3 3 1 4115.75 4827.02 62.75 o -2 3 1 4991.02 5341.63 53.86 o -1 3 1 3093.30 3091.06 42.96 o 0 3 1 39.11 44.41 2.01 o 1 3 1 11265.96 12146.53 206.12 o 2 3 1 240.90 222.43 6.93 o 3 3 1 1623.07 1843.30 30.42 o 4 3 1 810.18 916.85 23.26 o 5 3 1 2582.21 2737.52 63.55 o 6 3 1 1438.37 1586.21 31.16 o 7 3 1 1027.93 1143.72 28.68 o 8 3 1 3034.75 3108.56 66.66 o 9 3 1 1502.37 1517.12 55.26 o -10 4 1 878.94 893.44 49.06 o -9 4 1 162.12 163.64 32.35 o -8 4 1 259.70 287.24 14.38 o -7 4 1 322.93 307.73 12.91 o -6 4 1 8861.04 9614.31 126.57 o -5 4 1 4220.08 4533.30 51.81 o -4 4 1 8.76 14.45 3.77 o -3 4 1 6350.08 6510.42 75.05 o -2 4 1 460.66 472.77 11.36 o -1 4 1 928.20 922.10 13.07 o 0 4 1 632.21 787.04 10.42 o 1 4 1 3765.17 4223.33 45.20 o 2 4 1 757.77 798.28 13.96 o 3 4 1 3031.26 3552.54 44.60 o 4 4 1 2774.39 2715.77 39.96 o 5 4 1 2954.61 3060.91 44.72 o 6 4 1 4694.65 4865.55 92.80 o 7 4 1 1901.90 2050.85 40.62 o 8 4 1 850.63 895.63 33.80 o 9 4 1 582.12 570.08 42.77 o -10 5 1 1105.40 1194.75 118.75 o -9 5 1 6.89 -7.90 25.03 o -8 5 1 7077.46 7123.58 97.28 o -7 5 1 3.79 6.06 8.76 o -6 5 1 4950.34 5410.23 57.82 o -5 5 1 3305.28 3504.05 44.60 o -4 5 1 35.84 50.81 4.88 o -3 5 1 364.24 344.28 10.29 o -2 5 1 3647.82 3693.57 47.74 o -1 5 1 159.57 181.26 5.68 o 0 5 1 18986.73 19196.58 219.89 o 1 5 1 254.91 294.69 7.06 o 2 5 1 18230.17 19164.64 283.16 o 3 5 1 1529.54 1493.36 21.73 o 4 5 1 1731.71 1774.15 26.02 o 5 5 1 8.71 14.85 7.39 o 6 5 1 1501.88 1594.81 36.07 o 7 5 1 4.56 10.26 10.14 o 8 5 1 388.26 400.31 24.25 o 9 5 1 274.49 299.01 34.37 o -10 6 1 700.96 710.74 59.05 o -9 6 1 71.29 81.86 16.26 o -8 6 1 4.61 10.29 11.97 o -7 6 1 53.72 64.75 9.93 o -6 6 1 2818.44 2772.50 42.19 o -5 6 1 1606.78 1616.33 25.47 o -4 6 1 1178.05 1143.47 17.64 o -3 6 1 2689.47 2666.54 46.15 o -2 6 1 9696.04 9752.66 135.88 o -1 6 1 570.67 595.67 10.64 o 0 6 1 27440.74 28514.43 355.81 o 1 6 1 3918.97 3959.85 47.98 o 2 6 1 4.47 7.05 2.83 o 3 6 1 4812.48 5035.70 66.93 o 4 6 1 10828.82 11136.55 148.32 o 5 6 1 1496.62 1499.23 26.96 o 6 6 1 1179.18 1105.49 23.46 o 7 6 1 594.21 590.06 24.53 o 8 6 1 290.09 280.54 22.75 o 9 6 1 494.25 510.46 39.43 o -9 7 1 320.92 352.42 19.29 o -8 7 1 1107.19 1041.85 28.58 o -7 7 1 287.37 281.89 15.19 o -6 7 1 880.03 795.76 19.03 o -5 7 1 586.52 611.45 14.51 o -4 7 1 7793.15 7550.72 109.94 o -3 7 1 51.54 67.13 5.75 o -2 7 1 18762.79 18981.30 301.62 o -1 7 1 609.60 632.04 11.58 o 0 7 1 85.52 90.34 6.16 o 1 7 1 49.22 66.02 4.92 o 2 7 1 6618.20 7008.20 97.12 o 3 7 1 222.43 231.64 12.13 o 4 7 1 82.25 90.87 8.20 o 5 7 1 55.23 43.52 8.72 o 6 7 1 9522.33 9553.95 125.94 o 7 7 1 459.23 464.97 22.66 o 8 7 1 2406.89 2264.20 46.44 o 9 7 1 16.11 3.83 28.43 o -9 8 1 562.65 551.06 33.65 o -8 8 1 100.07 104.68 14.46 o -7 8 1 726.12 698.76 29.51 o -6 8 1 6045.24 6038.44 93.00 o -5 8 1 107.18 119.46 7.78 o -4 8 1 1795.74 1832.27 27.87 o -3 8 1 115.77 111.30 6.66 o -2 8 1 556.13 494.23 15.87 o -1 8 1 1315.51 1380.74 21.10 o 0 8 1 9669.91 9963.82 125.49 o 1 8 1 2985.87 2780.69 38.46 o 2 8 1 699.46 703.11 12.86 o 3 8 1 5778.91 5741.30 77.00 o 4 8 1 4584.75 4583.66 63.30 o 5 8 1 1787.54 1765.48 30.88 o 6 8 1 1729.62 1668.18 30.81 o 7 8 1 413.56 417.23 21.62 o 8 8 1 1241.73 1159.62 32.44 o 9 8 1 93.26 90.36 30.59 o -9 9 1 65.36 53.27 15.54 o -8 9 1 2513.78 2525.31 49.55 o -7 9 1 1255.78 1112.67 29.25 o -6 9 1 1991.77 1910.90 52.22 o -5 9 1 669.36 648.09 22.84 o -4 9 1 1725.15 1658.12 26.22 o -3 9 1 62.98 66.60 6.82 o -2 9 1 250.37 269.85 10.49 o -1 9 1 3152.49 3061.98 41.96 o 0 9 1 4122.57 4081.59 54.46 o 1 9 1 1138.46 1286.91 21.10 o 2 9 1 7088.08 6620.24 85.86 o 3 9 1 1377.84 1305.12 19.93 o 4 9 1 618.98 587.35 16.03 o 5 9 1 191.50 194.41 11.79 o 6 9 1 598.16 560.16 23.80 o 7 9 1 33.41 10.14 14.02 o 8 9 1 144.24 146.80 16.47 o 9 9 1 87.99 64.08 20.04 o -9 10 1 45.69 58.72 16.27 o -8 10 1 81.10 83.27 16.77 o -7 10 1 2.11 -12.08 12.08 o -6 10 1 899.43 895.91 29.13 o -5 10 1 255.29 241.24 15.24 o -4 10 1 54.39 67.08 8.37 o -3 10 1 7212.36 7211.62 103.47 o -2 10 1 1860.43 1883.03 28.18 o -1 10 1 2775.78 2803.55 39.33 o 0 10 1 3992.63 4120.17 55.43 o 1 10 1 1243.84 1333.11 22.22 o 2 10 1 130.07 120.60 7.54 o 3 10 1 1370.08 1368.60 21.26 o 4 10 1 813.69 769.26 18.68 o 5 10 1 3622.63 3533.51 52.77 o 6 10 1 11.36 10.86 12.63 o 7 10 1 2967.87 2853.05 58.16 o 8 10 1 402.47 336.87 20.99 o -9 11 1 1.89 2.70 16.18 o -8 11 1 9.48 -1.79 13.56 o -7 11 1 1495.26 1423.54 34.39 o -6 11 1 1273.45 1205.24 34.57 o -5 11 1 1186.00 1150.05 31.68 o -4 11 1 2366.81 2246.30 46.94 o -3 11 1 254.08 238.22 13.40 o -2 11 1 3584.14 3519.89 48.53 o -1 11 1 3953.01 3717.93 50.95 o 0 11 1 35.40 43.50 10.56 o 1 11 1 3472.49 3487.96 48.61 o 2 11 1 116.36 170.59 8.79 o 3 11 1 2761.47 2676.06 36.05 o 4 11 1 166.22 158.22 10.84 o 5 11 1 4715.67 4483.41 73.21 o 6 11 1 2060.90 1923.30 41.06 o 7 11 1 96.55 125.19 16.76 o 8 11 1 147.27 159.14 18.26 o -9 12 1 3630.17 3546.74 135.46 o -8 12 1 1.81 -14.98 14.98 o -7 12 1 3180.30 3208.65 58.92 o -6 12 1 130.45 151.71 17.44 o -5 12 1 211.95 206.34 16.20 o -4 12 1 5.03 12.65 8.65 o -3 12 1 2933.92 2759.24 53.26 o -2 12 1 108.98 75.88 10.98 o -1 12 1 201.77 202.61 8.57 o 0 12 1 367.51 392.23 12.02 o 1 12 1 12523.32 12514.93 159.05 o 2 12 1 787.07 837.06 18.61 o 3 12 1 6394.94 6371.85 104.73 o 4 12 1 72.38 45.12 11.33 o 5 12 1 4.76 2.80 12.05 o 6 12 1 80.59 92.17 15.33 o 7 12 1 1449.98 1443.18 37.23 o 8 12 1 15.16 -16.41 16.41 o -8 13 1 670.83 637.03 26.97 o -7 13 1 1110.35 1093.18 31.87 o -6 13 1 762.66 704.14 27.96 o -5 13 1 4932.41 4711.92 91.83 o -4 13 1 164.65 190.75 15.46 o -3 13 1 132.88 121.62 11.02 o -2 13 1 1587.93 1538.00 35.43 o -1 13 1 4649.33 4676.70 63.93 o 0 13 1 512.73 545.14 14.80 o 1 13 1 2039.38 2074.86 34.03 o 2 13 1 753.50 771.78 31.72 o 3 13 1 1903.65 1801.47 35.74 o 4 13 1 407.31 420.06 20.37 o 5 13 1 3305.06 3269.45 58.44 o 6 13 1 170.27 161.32 16.90 o 7 13 1 166.40 191.58 22.15 o 8 13 1 134.12 167.78 19.75 o -8 14 1 51.35 49.74 17.55 o -7 14 1 64.10 45.85 16.07 o -6 14 1 6.38 4.38 15.04 o -5 14 1 656.17 622.32 26.36 o -4 14 1 194.55 173.18 15.86 o -3 14 1 11797.34 11414.15 165.33 o -2 14 1 8.13 -8.07 10.91 o -1 14 1 2910.94 2974.23 57.65 o 0 14 1 3.77 -1.82 7.31 o 1 14 1 976.79 960.31 20.75 o 2 14 1 75.95 99.89 11.42 o 3 14 1 824.58 820.51 23.62 o 4 14 1 347.41 364.27 21.49 o 5 14 1 3007.09 2957.15 61.73 o 6 14 1 145.65 133.75 17.07 o 7 14 1 2994.63 2960.00 58.75 o 8 14 1 18.39 36.41 19.04 o -8 15 1 470.74 476.58 25.77 o -7 15 1 1931.75 2006.33 45.60 o -6 15 1 96.58 98.06 17.17 o -5 15 1 1392.94 1335.05 38.56 o -4 15 1 141.95 138.62 15.93 o -3 15 1 1931.17 1940.39 38.24 o -2 15 1 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