#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222717.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222717_Fobs loop_ _publ_author_name 'Kashif, M. Kalim' 'Khawar Rauf, M.' 'Bolte, Michael' 'Hameed, Shahid' _publ_section_title ; 3-(4-Chlorophenylsulfonyl)-8-methyl-1,3-diazaspiro[4.5]decane-2,4-dione ; _journal_coeditor_code HG2537 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1893 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.460 _cell_angle_gamma 90.000 _cell_length_a 6.1722 _cell_length_b 17.4561 _cell_length_c 15.1355 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.8104 _[local]_cod_data_source_file hg2537Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rauf43 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 198.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14706.38 13633.37 466.19 o 2 0 0 1717.24 1461.05 13.61 o 3 0 0 756.50 795.80 4.98 o 4 0 0 191.64 145.01 3.13 o 5 0 0 92.77 79.43 1.87 o 6 0 0 618.55 567.53 3.86 o 7 0 0 861.26 845.45 6.96 o 1 1 0 115.45 98.25 1.98 o 2 1 0 2644.09 2573.19 32.38 o 3 1 0 4097.92 4255.64 35.35 o 4 1 0 497.61 494.28 2.78 o 5 1 0 177.23 160.61 1.63 o 6 1 0 263.27 288.97 3.33 o 7 1 0 30.35 28.54 1.31 o 1 2 0 3823.36 3636.03 28.67 o 2 2 0 1543.28 1484.44 11.89 o 3 2 0 96.30 110.84 1.61 o 4 2 0 285.71 276.24 1.88 o 5 2 0 0.02 0.11 1.09 o 6 2 0 80.05 85.25 1.52 o 7 2 0 198.24 189.94 2.66 o 1 3 0 11644.94 11752.66 150.24 o 2 3 0 1042.05 1128.31 7.06 o 3 3 0 158.07 154.24 1.73 o 4 3 0 127.90 124.31 1.70 o 5 3 0 347.71 326.70 4.63 o 6 3 0 4.21 5.21 1.16 o 7 3 0 4.00 2.76 1.17 o 0 4 0 22042.80 21958.35 374.18 o 1 4 0 2303.08 2307.26 41.12 o 2 4 0 294.03 347.82 2.63 o 3 4 0 754.93 788.87 11.07 o 4 4 0 117.32 103.41 2.26 o 5 4 0 74.04 64.42 1.24 o 6 4 0 279.90 273.75 2.41 o 7 4 0 205.85 194.91 3.04 o 1 5 0 11036.62 10778.32 84.83 o 2 5 0 20.79 18.79 1.04 o 3 5 0 66.20 92.00 1.48 o 4 5 0 19.80 21.32 1.10 o 5 5 0 293.54 287.06 3.82 o 6 5 0 255.12 277.53 4.77 o 7 5 0 16.76 15.08 1.35 o 0 6 0 608.18 620.06 4.06 o 1 6 0 1395.45 1447.26 27.00 o 2 6 0 406.70 440.88 6.38 o 3 6 0 66.66 84.04 1.54 o 4 6 0 5.67 7.32 0.95 o 5 6 0 1441.32 1401.54 15.84 o 6 6 0 241.63 243.68 2.30 o 7 6 0 14.10 19.79 1.19 o 1 7 0 1945.72 1945.14 19.20 o 2 7 0 1066.56 1118.72 17.55 o 3 7 0 1.02 5.42 0.91 o 4 7 0 36.87 34.08 1.22 o 5 7 0 568.20 556.96 10.00 o 6 7 0 122.69 116.28 1.62 o 7 7 0 20.03 22.34 1.36 o 0 8 0 4452.00 4261.03 83.11 o 1 8 0 771.70 884.14 14.35 o 2 8 0 1530.68 1453.38 26.19 o 3 8 0 1.64 3.96 0.95 o 4 8 0 577.27 583.96 9.29 o 5 8 0 544.53 547.13 12.02 o 6 8 0 24.32 21.44 1.27 o 7 8 0 62.87 59.75 1.53 o 1 9 0 2663.87 2599.30 32.64 o 2 9 0 150.26 134.12 2.88 o 3 9 0 8.10 9.28 0.88 o 4 9 0 12.87 11.41 1.05 o 5 9 0 762.56 739.08 14.83 o 6 9 0 400.84 417.80 12.03 o 0 10 0 134.24 170.87 2.06 o 1 10 0 19.24 26.05 0.97 o 2 10 0 115.30 93.79 2.27 o 3 10 0 0.00 0.94 0.94 o 4 10 0 1368.32 1325.93 21.17 o 5 10 0 145.79 139.16 2.69 o 6 10 0 64.38 57.27 1.99 o 1 11 0 1391.79 1285.30 13.91 o 2 11 0 222.90 235.68 4.55 o 3 11 0 257.22 282.57 3.96 o 4 11 0 1.11 2.01 1.06 o 5 11 0 163.65 157.13 2.87 o 6 11 0 1.28 1.03 1.13 o 0 12 0 750.44 711.56 14.17 o 1 12 0 69.19 64.20 1.62 o 2 12 0 16.53 14.47 0.95 o 3 12 0 144.52 127.00 2.49 o 4 12 0 249.09 252.63 5.38 o 5 12 0 9.74 13.98 1.03 o 6 12 0 114.90 120.05 4.03 o 1 13 0 2429.29 2441.19 35.68 o 2 13 0 415.81 388.41 8.91 o 3 13 0 0.71 1.83 0.95 o 4 13 0 230.19 250.52 2.93 o 5 13 0 110.80 110.61 4.06 o 6 13 0 249.49 248.15 10.60 o 0 14 0 1677.15 1692.12 28.99 o 1 14 0 631.53 605.22 7.43 o 2 14 0 7.16 5.87 0.88 o 3 14 0 1.51 2.44 1.04 o 4 14 0 151.31 138.56 3.49 o 5 14 0 27.06 35.29 1.25 o 1 15 0 98.70 83.36 1.41 o 2 15 0 25.99 23.79 1.32 o 3 15 0 221.07 216.65 5.17 o 4 15 0 1.54 -1.12 1.26 o 5 15 0 8.81 12.27 1.18 o 0 16 0 2896.53 2924.83 41.48 o 1 16 0 693.68 715.25 8.13 o 2 16 0 1.53 2.83 0.91 o 3 16 0 6.64 8.46 1.11 o 4 16 0 135.86 141.39 3.98 o 5 16 0 0.49 0.90 1.33 o 1 17 0 219.33 217.13 3.28 o 2 17 0 131.18 133.35 4.07 o 3 17 0 0.07 2.58 1.00 o 4 17 0 49.51 56.88 1.47 o 0 18 0 454.46 450.95 5.29 o 1 18 0 167.50 170.90 2.01 o 2 18 0 20.67 25.50 1.15 o 3 18 0 11.80 15.18 1.10 o 4 18 0 36.69 38.10 1.45 o 1 19 0 5.86 6.94 0.92 o 2 19 0 23.49 25.95 1.43 o 3 19 0 108.55 110.49 3.91 o 0 20 0 212.94 222.60 4.99 o 1 20 0 99.23 103.63 2.54 o 2 20 0 25.36 26.19 1.22 o 1 21 0 95.12 103.35 2.56 o -7 1 1 29.75 29.32 1.33 o -6 1 1 138.59 135.12 1.50 o -5 1 1 208.22 201.15 1.89 o -4 1 1 126.48 177.22 2.71 o -3 1 1 163.24 174.69 1.75 o -2 1 1 11581.31 11565.07 119.08 o -1 1 1 17.88 19.82 1.10 o 1 1 1 1274.13 1141.97 13.89 o 2 1 1 0.14 1.38 0.93 o 3 1 1 4767.49 4921.34 22.71 o 4 1 1 711.73 810.58 3.83 o 5 1 1 550.76 543.04 6.73 o 6 1 1 97.35 96.19 1.78 o 7 1 1 51.72 58.32 1.40 o -7 2 1 121.34 101.48 1.62 o -6 2 1 37.74 45.70 1.30 o -5 2 1 67.62 90.10 1.40 o -4 2 1 13.27 12.35 0.96 o -3 2 1 3214.10 3103.84 16.65 o -2 2 1 2126.73 2108.01 31.13 o -1 2 1 39512.18 41558.65 807.08 o 1 2 1 14.06 8.76 1.31 o 2 2 1 160.87 158.45 1.98 o 3 2 1 426.55 524.58 3.45 o 4 2 1 2180.49 2138.71 17.12 o 5 2 1 18.63 19.99 1.22 o 6 2 1 1039.61 1000.12 12.13 o 7 2 1 183.85 182.91 4.73 o -7 3 1 15.98 20.59 1.24 o -6 3 1 19.71 26.77 1.20 o -5 3 1 8.94 13.24 1.10 o -4 3 1 918.17 985.00 6.71 o -3 3 1 578.61 637.13 12.17 o -2 3 1 1058.47 948.12 9.83 o -1 3 1 470.02 472.13 3.93 o 0 3 1 6514.39 5841.36 188.17 o 1 3 1 1677.84 1547.84 24.24 o 2 3 1 46.57 37.71 1.23 o 3 3 1 429.18 407.64 5.22 o 4 3 1 124.30 127.60 2.57 o 5 3 1 748.64 782.18 10.93 o 6 3 1 102.72 95.82 1.57 o 7 3 1 0.76 1.82 1.22 o -7 4 1 9.14 12.96 1.32 o -6 4 1 45.35 39.17 1.26 o -5 4 1 1.41 1.87 0.96 o -4 4 1 20.69 30.59 1.12 o -3 4 1 2056.03 2238.75 22.30 o -2 4 1 110.83 114.38 1.76 o -1 4 1 8969.60 9130.90 125.39 o 0 4 1 326.63 317.15 3.07 o 1 4 1 599.47 533.96 9.67 o 2 4 1 2.19 3.77 1.01 o 3 4 1 0.65 0.96 0.84 o 4 4 1 336.26 351.80 3.81 o 5 4 1 373.73 394.20 2.54 o 6 4 1 170.32 173.69 4.75 o 7 4 1 7.92 7.86 1.16 o -7 5 1 37.95 31.17 1.30 o -6 5 1 123.98 116.53 1.56 o -5 5 1 142.21 138.16 2.35 o -4 5 1 98.16 90.98 1.32 o -3 5 1 0.40 0.49 1.05 o -2 5 1 266.94 238.70 4.56 o -1 5 1 51.18 55.95 1.18 o 0 5 1 818.88 779.38 11.07 o 1 5 1 43.26 27.40 0.94 o 2 5 1 3350.80 3573.41 47.66 o 3 5 1 164.23 211.11 2.93 o 4 5 1 88.08 80.30 1.37 o 5 5 1 216.62 201.00 3.29 o 6 5 1 71.32 66.76 1.45 o 7 5 1 0.01 0.27 1.11 o -7 6 1 59.78 56.87 1.99 o -6 6 1 5.16 5.74 1.28 o -5 6 1 135.91 159.31 2.98 o -4 6 1 1.95 5.97 1.06 o -3 6 1 951.31 856.80 14.99 o -2 6 1 406.36 390.38 7.38 o -1 6 1 484.85 410.30 6.28 o 0 6 1 565.52 514.50 3.24 o 1 6 1 167.75 167.04 1.63 o 2 6 1 64.30 63.26 1.31 o 3 6 1 1.99 1.43 0.95 o 4 6 1 1638.97 1701.61 24.55 o 5 6 1 113.20 112.09 2.78 o 6 6 1 612.39 587.20 14.97 o 7 6 1 103.92 104.31 1.89 o -7 7 1 220.07 232.23 4.60 o -6 7 1 248.83 265.95 5.55 o -5 7 1 420.27 405.79 8.03 o -4 7 1 564.68 565.67 7.47 o -3 7 1 49.54 42.29 1.30 o -2 7 1 10987.98 11779.31 140.31 o -1 7 1 655.46 662.11 6.98 o 0 7 1 494.94 388.54 4.35 o 1 7 1 250.61 228.05 3.20 o 2 7 1 73.81 61.76 1.29 o 3 7 1 844.97 863.07 14.02 o 4 7 1 554.64 504.24 8.35 o 5 7 1 1784.42 1823.91 28.47 o 6 7 1 398.33 410.25 6.72 o 7 7 1 10.92 11.96 1.24 o -7 8 1 33.39 35.56 1.29 o -6 8 1 33.99 42.76 1.25 o -5 8 1 353.09 334.30 4.45 o -4 8 1 292.10 271.97 4.57 o -3 8 1 724.11 764.07 11.41 o -2 8 1 449.04 485.00 5.12 o -1 8 1 355.46 346.14 4.35 o 0 8 1 349.17 374.16 6.37 o 1 8 1 197.80 223.37 2.96 o 2 8 1 1419.28 1449.07 18.39 o 3 8 1 324.68 337.01 5.28 o 4 8 1 1.14 3.09 0.87 o 5 8 1 146.16 149.23 2.13 o 6 8 1 0.63 1.77 1.05 o 7 8 1 63.90 51.38 2.72 o -6 9 1 109.53 88.16 2.78 o -5 9 1 47.36 43.30 2.03 o -4 9 1 450.78 432.24 7.84 o -3 9 1 59.66 64.67 1.23 o -2 9 1 1042.57 1153.87 11.38 o -1 9 1 3059.00 3347.80 49.05 o 0 9 1 23.50 23.72 0.94 o 1 9 1 279.35 265.23 2.59 o 2 9 1 496.90 471.95 6.45 o 3 9 1 1173.48 1177.59 22.74 o 4 9 1 14.48 15.86 1.04 o 5 9 1 1531.67 1431.78 49.76 o 6 9 1 81.72 74.38 2.58 o -6 10 1 186.28 168.15 5.72 o -5 10 1 0.03 2.31 0.91 o -4 10 1 0.55 1.28 0.92 o -3 10 1 513.53 549.38 7.10 o -2 10 1 117.56 129.59 2.55 o -1 10 1 191.34 135.79 2.43 o 0 10 1 1531.25 1581.80 22.00 o 1 10 1 250.62 269.87 4.42 o 2 10 1 657.30 693.68 12.24 o 3 10 1 17.88 24.10 1.13 o 4 10 1 277.21 278.47 4.12 o 5 10 1 304.67 310.26 8.25 o 6 10 1 2.27 1.57 1.15 o -6 11 1 183.55 185.84 4.32 o -5 11 1 11.63 9.88 1.09 o -4 11 1 0.50 1.30 0.91 o -3 11 1 62.26 55.54 1.26 o -2 11 1 2349.29 2424.45 35.20 o -1 11 1 11.84 24.03 0.87 o 0 11 1 1020.91 1002.15 9.92 o 1 11 1 18.11 22.57 0.92 o 2 11 1 7.92 5.57 0.92 o 3 11 1 87.40 96.33 2.01 o 4 11 1 593.27 591.99 8.89 o 5 11 1 546.73 543.16 18.92 o 6 11 1 115.72 119.04 4.09 o -6 12 1 26.69 28.21 1.47 o -5 12 1 124.22 105.74 1.98 o -4 12 1 162.97 171.59 3.02 o -3 12 1 199.17 207.09 3.05 o -2 12 1 29.98 27.68 0.99 o -1 12 1 1570.72 1524.44 20.73 o 0 12 1 2.34 4.88 0.70 o 1 12 1 377.22 348.00 4.92 o 2 12 1 94.19 94.69 1.65 o 3 12 1 62.89 51.68 1.13 o 4 12 1 252.65 214.67 4.91 o 5 12 1 36.16 35.40 1.33 o 6 12 1 72.57 67.93 2.18 o -6 13 1 29.59 25.82 1.60 o -5 13 1 0.16 1.02 1.05 o -4 13 1 13.74 15.09 1.07 o -3 13 1 39.45 42.04 1.16 o -2 13 1 1.02 3.25 0.96 o -1 13 1 453.23 489.48 7.89 o 0 13 1 24.38 27.50 0.93 o 1 13 1 1194.98 1243.57 20.45 o 2 13 1 141.74 156.81 2.83 o 3 13 1 8.35 7.12 0.90 o 4 13 1 3.12 3.76 1.35 o 5 13 1 128.90 126.41 4.49 o -5 14 1 55.84 56.35 1.30 o -4 14 1 0.47 2.36 1.17 o -3 14 1 5.69 10.30 1.24 o -2 14 1 492.65 477.86 9.06 o -1 14 1 2202.98 2144.59 25.67 o 0 14 1 1324.17 1283.57 19.36 o 1 14 1 361.79 336.17 3.28 o 2 14 1 402.13 405.54 8.72 o 3 14 1 205.41 215.66 4.86 o 4 14 1 421.76 421.59 12.07 o 5 14 1 29.36 32.74 1.20 o -5 15 1 40.14 41.28 1.84 o -4 15 1 2.24 3.05 1.00 o -3 15 1 223.90 206.59 1.70 o -2 15 1 2344.28 2311.58 41.38 o -1 15 1 203.68 206.14 1.92 o 0 15 1 699.06 646.89 12.61 o 1 15 1 19.06 23.56 0.94 o 2 15 1 4.85 6.66 0.91 o 3 15 1 270.39 285.01 6.07 o 4 15 1 0.20 0.26 1.20 o 5 15 1 45.55 39.78 1.37 o -5 16 1 22.17 24.27 1.25 o -4 16 1 19.72 22.37 1.19 o -3 16 1 229.88 216.20 1.83 o -2 16 1 0.05 1.35 0.85 o -1 16 1 277.90 267.00 4.70 o 0 16 1 10.84 8.67 0.95 o 1 16 1 24.23 25.14 0.98 o 2 16 1 228.58 236.83 4.55 o 3 16 1 93.98 103.15 2.35 o 4 16 1 9.64 10.91 1.21 o 5 16 1 131.71 128.46 4.88 o -4 17 1 82.90 80.45 2.89 o -3 17 1 145.79 131.18 2.82 o -2 17 1 0.97 1.53 0.96 o -1 17 1 2.10 2.12 0.85 o 0 17 1 0.11 1.33 0.91 o 1 17 1 1.40 3.09 0.87 o 2 17 1 53.28 57.83 2.70 o 3 17 1 54.64 57.94 1.64 o 4 17 1 0.20 0.72 1.22 o -4 18 1 22.48 25.34 1.27 o -3 18 1 197.98 180.78 4.45 o -2 18 1 150.23 141.31 3.24 o -1 18 1 122.82 119.89 1.30 o 0 18 1 371.33 368.91 4.22 o 1 18 1 376.07 370.52 4.01 o 2 18 1 10.27 8.31 1.01 o 3 18 1 197.84 218.08 4.69 o 4 18 1 122.36 118.38 2.28 o -3 19 1 0.00 0.87 1.11 o -2 19 1 327.01 346.00 6.50 o -1 19 1 123.78 127.09 1.53 o 0 19 1 38.30 38.52 1.08 o 1 19 1 0.39 0.85 0.92 o 2 19 1 12.73 11.11 1.07 o 3 19 1 82.48 84.28 1.84 o -2 20 1 7.95 7.41 1.27 o -1 20 1 430.42 407.18 10.01 o 0 20 1 13.01 12.41 0.96 o 1 20 1 97.71 98.28 1.97 o 2 20 1 5.62 6.73 1.07 o -1 21 1 39.80 38.40 1.23 o 0 21 1 15.98 14.82 1.03 o 1 21 1 55.67 57.38 1.29 o -7 0 2 0.60 2.62 1.61 o -6 0 2 309.93 274.55 6.28 o -5 0 2 177.22 171.48 3.61 o -4 0 2 4261.31 4270.49 23.48 o -3 0 2 3250.85 3670.37 115.40 o -2 0 2 4864.01 4732.78 21.36 o -1 0 2 4705.87 4203.09 138.49 o 1 0 2 6837.53 6980.89 197.62 o 2 0 2 361.06 396.86 8.24 o 3 0 2 2626.74 2522.30 26.39 o 4 0 2 1803.69 1836.10 37.12 o 5 0 2 0.66 1.16 1.53 o 6 0 2 92.09 73.57 1.92 o 7 0 2 16.98 19.58 2.13 o -7 1 2 16.60 28.84 1.73 o -6 1 2 43.72 55.35 1.21 o -5 1 2 98.38 96.38 1.31 o -4 1 2 204.31 220.44 2.62 o -3 1 2 1302.88 1260.77 6.34 o -2 1 2 1878.14 1661.97 22.51 o -1 1 2 7660.77 7385.44 158.42 o 0 1 2 183.38 166.38 10.55 o 1 1 2 48.60 42.62 1.57 o 2 1 2 2989.22 2793.61 32.65 o 3 1 2 1862.91 1853.85 22.22 o 4 1 2 365.37 374.41 3.25 o 5 1 2 938.45 935.99 10.57 o 6 1 2 167.11 163.28 2.28 o 7 1 2 79.72 81.49 1.96 o -7 2 2 14.58 14.34 1.17 o -6 2 2 22.36 22.42 1.09 o -5 2 2 70.48 72.11 1.31 o -4 2 2 980.25 1047.10 4.39 o -3 2 2 43.16 70.01 1.33 o -2 2 2 2031.28 1999.00 14.84 o -1 2 2 5742.29 6040.21 67.06 o 0 2 2 59.45 62.46 1.64 o 1 2 2 2345.04 2314.32 26.90 o 2 2 2 1065.75 1087.36 8.92 o 3 2 2 135.99 133.34 1.74 o 4 2 2 32.48 37.61 1.15 o 5 2 2 0.00 1.11 1.11 o 6 2 2 0.04 0.40 1.06 o 7 2 2 1.56 2.78 1.26 o -7 3 2 1.97 5.39 1.22 o -6 3 2 4.87 2.85 1.08 o -5 3 2 1288.80 1247.30 12.25 o -4 3 2 25.40 35.65 1.13 o -3 3 2 2590.98 2664.45 19.65 o -2 3 2 4129.37 3870.88 59.67 o -1 3 2 4095.36 4046.04 76.49 o 0 3 2 1784.72 1651.76 14.54 o 1 3 2 850.10 786.05 10.80 o 2 3 2 256.39 298.70 2.69 o 3 3 2 8.04 7.34 0.99 o 4 3 2 284.65 272.32 2.17 o 5 3 2 279.58 283.53 3.40 o 6 3 2 149.32 147.14 2.79 o 7 3 2 76.14 85.45 1.84 o -7 4 2 0.10 0.44 1.03 o -6 4 2 39.59 32.38 1.21 o -5 4 2 65.88 60.68 1.27 o -4 4 2 2003.12 2070.36 17.75 o -3 4 2 363.38 415.95 5.32 o -2 4 2 319.91 284.92 2.68 o -1 4 2 2782.10 2556.68 14.90 o 0 4 2 20.39 28.60 1.07 o 1 4 2 245.46 189.46 2.03 o 2 4 2 127.25 118.77 2.05 o 3 4 2 1036.85 940.92 9.89 o 4 4 2 1434.78 1403.85 15.35 o 5 4 2 140.04 138.13 1.67 o 6 4 2 534.56 504.91 10.34 o 7 4 2 72.52 74.07 1.66 o -7 5 2 99.91 116.54 2.32 o -6 5 2 2.13 1.28 0.93 o -5 5 2 367.47 374.09 3.20 o -4 5 2 0.80 2.25 1.21 o -3 5 2 1610.48 1613.38 20.06 o -2 5 2 1141.85 1110.29 14.92 o -1 5 2 66.09 82.31 1.43 o 0 5 2 807.84 711.87 9.75 o 1 5 2 883.85 823.30 4.09 o 2 5 2 1216.31 1111.75 15.37 o 3 5 2 0.52 1.46 1.05 o 4 5 2 1579.27 1590.80 25.13 o 5 5 2 401.32 401.25 4.36 o 6 5 2 30.58 31.93 1.24 o 7 5 2 9.44 8.52 1.21 o -7 6 2 158.29 161.50 2.96 o -6 6 2 15.03 20.27 1.14 o -5 6 2 19.14 32.24 1.66 o -4 6 2 2123.84 2176.96 37.73 o -3 6 2 22.80 22.88 1.00 o -2 6 2 1198.90 1242.29 11.93 o -1 6 2 184.56 162.33 2.50 o 0 6 2 69.67 82.75 1.37 o 1 6 2 2710.43 2704.17 30.73 o 2 6 2 476.54 493.30 10.56 o 3 6 2 619.72 649.96 9.45 o 4 6 2 95.97 93.08 1.93 o 5 6 2 20.93 22.44 1.30 o 6 6 2 1.49 1.93 1.08 o 7 6 2 0.20 0.16 1.35 o -7 7 2 34.84 33.20 1.74 o -6 7 2 28.10 27.71 1.16 o -5 7 2 717.06 667.68 10.65 o -4 7 2 476.54 525.99 9.11 o -3 7 2 1361.11 1461.47 24.82 o -2 7 2 1100.70 1143.61 12.33 o -1 7 2 44.14 41.65 1.13 o 0 7 2 533.72 573.86 9.32 o 1 7 2 98.92 76.19 1.22 o 2 7 2 54.02 41.79 1.52 o 3 7 2 15.18 18.10 1.15 o 4 7 2 898.48 887.62 23.44 o 5 7 2 625.54 638.34 9.18 o 6 7 2 137.95 138.01 2.61 o 7 7 2 0.26 -0.19 1.29 o -7 8 2 86.88 81.10 2.98 o -6 8 2 410.13 367.45 6.72 o -5 8 2 0.05 -0.37 1.01 o -4 8 2 2700.77 2727.82 49.53 o -3 8 2 1783.55 1697.76 26.64 o -2 8 2 12.61 21.19 1.01 o -1 8 2 2218.53 2260.86 23.10 o 0 8 2 555.53 516.44 4.87 o 1 8 2 731.82 726.81 6.88 o 2 8 2 0.57 2.81 0.90 o 3 8 2 462.14 465.81 8.22 o 4 8 2 224.73 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