#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/27/2222718.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222718_Fobs loop_ _publ_author_name 'Dong, Wen-Kui' 'Tong, Jun-Feng' 'An, Li-Li' 'Wu, Jian-Chao' 'Yao, Jian' _publ_section_title ; Bis{(E)-4-bromo-2-[(2-chloro-3-pyridyl)iminomethyl]phenolato-\k^2^N,O}copper(II) ; _journal_coeditor_code HG2538 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m945 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.212 _cell_angle_gamma 90.000 _cell_length_a 20.4055 _cell_length_b 11.6378 _cell_length_c 10.5787 _exptl_crystal_F_000 1340.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file hg2538Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090618c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 398.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 70304.29 69291.67 653.16 o 3 0 0 296.01 311.03 70.18 o 4 0 0 34937.70 35456.50 483.29 o 5 0 0 259.83 282.32 78.16 o 6 0 0 4609.48 4912.01 173.46 o 7 0 0 5688.47 5425.14 141.87 o 8 0 0 36260.05 35518.70 384.80 o 9 0 0 459.27 444.82 69.31 o 10 0 0 2939.05 2550.74 128.06 o 11 0 0 807.47 774.07 91.30 o 12 0 0 0.84 -15.08 70.25 o 13 0 0 1545.69 1332.58 109.01 o 14 0 0 589.66 456.16 227.69 o 15 0 0 4803.38 4476.42 334.16 o 16 0 0 947.59 1169.95 220.91 o 18 0 0 3533.77 3634.25 378.02 o 19 0 0 206.57 317.41 237.66 o 20 0 0 15.30 39.88 177.05 o 21 0 0 1.20 -23.13 178.64 o 22 0 0 208.31 149.13 254.41 o 23 0 0 622.38 378.02 279.13 o 24 0 0 176.65 173.86 268.76 o 1 1 0 10461.39 10340.24 155.05 o 2 1 0 437.14 415.30 28.66 o 3 1 0 12680.51 12413.10 163.34 o 4 1 0 5620.75 5844.12 166.54 o 5 1 0 63153.86 62022.60 1025.35 o 6 1 0 5571.70 5775.26 116.70 o 7 1 0 588.78 599.26 59.76 o 8 1 0 2822.55 2583.93 96.37 o 9 1 0 4993.42 4973.95 180.30 o 10 1 0 2991.86 2886.57 116.89 o 11 1 0 315.32 272.12 65.84 o 12 1 0 681.31 741.18 88.64 o 13 1 0 15624.64 15473.57 212.60 o 14 1 0 666.39 532.36 115.80 o 15 1 0 7781.26 7951.50 498.44 o 16 1 0 1341.97 1622.81 172.20 o 17 1 0 3296.98 2727.97 211.76 o 18 1 0 1879.62 1940.22 207.55 o 19 1 0 24.01 -2.49 136.36 o 20 1 0 422.53 307.69 178.31 o 21 1 0 58.54 218.20 154.28 o 22 1 0 111.01 137.56 181.31 o 23 1 0 1178.62 1322.04 256.40 o 24 1 0 10.57 72.45 183.03 o 0 2 0 44018.53 44881.85 769.29 o 1 2 0 381.19 373.70 26.13 o 2 2 0 747.08 783.70 36.65 o 3 2 0 846.55 858.28 42.82 o 4 2 0 620.53 561.29 43.55 o 5 2 0 55.62 81.02 37.37 o 6 2 0 1713.28 2199.12 123.40 o 7 2 0 2152.81 2052.91 86.11 o 8 2 0 16110.85 16917.24 475.49 o 9 2 0 1850.02 2015.29 112.40 o 10 2 0 21772.41 23392.19 782.08 o 11 2 0 218.15 222.19 67.15 o 12 2 0 4414.49 4415.61 149.40 o 13 2 0 2263.84 2430.67 169.33 o 14 2 0 6.08 -18.91 67.08 o 15 2 0 604.05 457.34 123.82 o 16 2 0 1419.14 1506.38 183.82 o 17 2 0 2.70 -90.38 149.37 o 18 2 0 4943.43 4936.07 285.56 o 19 2 0 76.58 44.70 124.79 o 20 2 0 1052.77 961.29 206.61 o 21 2 0 135.03 183.10 137.32 o 22 2 0 303.36 259.22 167.47 o 23 2 0 79.50 65.41 187.81 o 24 2 0 58.18 -67.02 182.61 o 1 3 0 25.27 15.15 30.28 o 2 3 0 25407.33 25877.68 391.40 o 3 3 0 6828.90 7114.66 164.38 o 4 3 0 1580.07 1458.34 60.36 o 5 3 0 9351.02 9274.44 241.67 o 6 3 0 22184.86 22041.97 587.52 o 7 3 0 13951.95 14248.56 322.03 o 8 3 0 5023.34 4930.45 137.29 o 9 3 0 15701.85 16101.80 658.83 o 10 3 0 3184.06 3223.20 123.56 o 11 3 0 2060.32 1792.38 100.73 o 12 3 0 33.15 55.05 63.37 o 13 3 0 615.01 690.67 91.43 o 14 3 0 469.03 503.85 91.22 o 15 3 0 920.35 1043.87 160.52 o 16 3 0 744.48 643.48 153.62 o 17 3 0 1017.22 1239.82 183.44 o 18 3 0 409.19 277.50 147.62 o 19 3 0 565.21 443.48 146.24 o 20 3 0 249.66 229.88 181.75 o 21 3 0 107.54 158.04 160.74 o 22 3 0 25.60 -16.93 145.37 o 23 3 0 1.69 11.81 150.77 o 0 4 0 57458.20 59886.50 843.29 o 1 4 0 308.20 290.44 28.44 o 2 4 0 4308.45 4162.78 99.11 o 3 4 0 9109.73 9126.20 141.81 o 4 4 0 36245.53 35794.23 846.29 o 5 4 0 387.77 422.24 51.62 o 6 4 0 8250.77 8347.16 147.62 o 7 4 0 1357.10 1375.38 77.27 o 8 4 0 599.59 672.93 62.09 o 9 4 0 140.25 181.00 82.75 o 10 4 0 5814.26 5930.55 277.51 o 11 4 0 4058.16 4370.20 186.62 o 12 4 0 5689.31 5976.60 180.57 o 13 4 0 57.95 128.81 76.35 o 14 4 0 3363.65 3559.36 155.90 o 15 4 0 1901.28 1768.67 191.56 o 16 4 0 4.32 -51.98 120.95 o 17 4 0 314.19 280.28 144.58 o 18 4 0 73.49 99.80 139.39 o 19 4 0 307.71 140.98 147.38 o 20 4 0 872.95 1054.56 196.49 o 21 4 0 364.56 453.91 160.20 o 22 4 0 327.73 566.75 189.76 o 23 4 0 80.22 -10.12 142.61 o 1 5 0 7690.10 7973.78 155.84 o 2 5 0 1155.96 1246.07 81.61 o 3 5 0 657.85 574.71 61.09 o 4 5 0 2726.35 2652.23 95.57 o 5 5 0 2890.20 2889.61 96.99 o 6 5 0 8059.63 8309.58 168.15 o 7 5 0 3761.56 3528.85 115.58 o 8 5 0 251.27 264.24 63.02 o 9 5 0 17421.72 16879.36 351.68 o 10 5 0 5063.76 5231.75 143.52 o 11 5 0 4497.07 4806.47 354.68 o 12 5 0 73.98 42.73 75.15 o 13 5 0 60.86 -9.52 70.81 o 14 5 0 1416.84 1507.27 124.07 o 15 5 0 79.86 -20.11 148.90 o 16 5 0 371.16 361.37 149.60 o 17 5 0 275.60 570.99 169.56 o 18 5 0 331.54 432.90 147.60 o 19 5 0 638.29 661.83 166.77 o 20 5 0 62.57 95.74 162.69 o 21 5 0 258.10 150.77 147.47 o 22 5 0 254.25 198.84 165.88 o 0 6 0 22142.84 23242.96 278.84 o 1 6 0 5.01 -19.95 39.14 o 2 6 0 623.33 566.59 37.83 o 3 6 0 23.71 10.87 52.58 o 4 6 0 9389.21 9169.55 210.19 o 5 6 0 1270.45 1126.30 77.57 o 6 6 0 11032.26 11349.17 238.74 o 7 6 0 3148.20 2974.93 120.66 o 8 6 0 25.04 -37.88 68.67 o 9 6 0 606.85 516.65 83.49 o 10 6 0 61.86 -25.54 72.24 o 11 6 0 394.44 332.16 78.90 o 12 6 0 372.06 454.41 110.67 o 13 6 0 1865.14 1816.46 139.33 o 14 6 0 2420.82 2777.24 180.38 o 15 6 0 78.92 162.80 158.84 o 16 6 0 680.67 435.53 154.63 o 17 6 0 279.51 258.04 158.80 o 18 6 0 10.76 -61.00 146.05 o 19 6 0 388.68 319.58 194.61 o 20 6 0 104.14 144.87 166.71 o 21 6 0 14.80 58.67 170.52 o 1 7 0 5369.49 5569.89 154.93 o 2 7 0 13965.23 15051.50 690.35 o 3 7 0 356.98 298.96 64.54 o 4 7 0 249.85 218.49 70.46 o 5 7 0 132.79 101.55 74.65 o 6 7 0 7794.89 7550.50 184.81 o 7 7 0 477.97 444.07 81.73 o 8 7 0 5180.45 4962.63 207.28 o 9 7 0 963.80 926.27 96.22 o 10 7 0 118.50 75.15 78.86 o 11 7 0 655.23 661.42 98.69 o 12 7 0 1424.38 1402.08 113.76 o 13 7 0 1.98 10.63 95.78 o 14 7 0 16.78 -0.35 90.90 o 15 7 0 134.98 184.57 144.10 o 16 7 0 739.91 848.62 202.49 o 17 7 0 7.22 -11.77 143.35 o 18 7 0 3.46 40.78 161.08 o 19 7 0 247.90 424.54 183.38 o 20 7 0 180.43 341.78 177.77 o 0 8 0 3370.17 3320.06 192.17 o 1 8 0 2315.38 2350.40 119.35 o 2 8 0 29.00 86.04 71.09 o 3 8 0 10207.24 10178.11 220.85 o 4 8 0 145.12 95.15 67.80 o 5 8 0 10.83 -1.45 74.00 o 6 8 0 5491.32 5656.56 177.93 o 7 8 0 6774.20 6847.62 300.84 o 8 8 0 1826.38 1674.95 114.89 o 9 8 0 2805.70 2859.96 136.82 o 10 8 0 1961.33 1817.31 129.14 o 11 8 0 419.35 558.73 100.28 o 12 8 0 1164.73 1083.04 106.23 o 13 8 0 568.22 544.01 115.84 o 14 8 0 212.22 339.74 116.90 o 15 8 0 249.38 328.07 190.45 o 16 8 0 838.36 845.44 214.44 o 17 8 0 281.00 517.44 210.14 o 18 8 0 30.36 112.08 197.94 o 19 8 0 11.90 -82.37 150.46 o 1 9 0 334.10 341.35 92.14 o 2 9 0 8694.51 8676.42 216.30 o 3 9 0 132.24 110.73 79.47 o 4 9 0 116.97 16.62 77.48 o 5 9 0 11.73 -69.61 82.36 o 6 9 0 9550.63 10160.74 242.81 o 7 9 0 509.45 514.96 95.32 o 8 9 0 1649.22 1734.57 121.49 o 9 9 0 141.15 182.62 91.87 o 10 9 0 4790.15 4775.32 183.74 o 11 9 0 952.28 906.55 118.22 o 12 9 0 1586.38 1746.35 158.74 o 13 9 0 319.05 505.63 176.12 o 14 9 0 64.38 111.24 114.01 o 15 9 0 274.69 298.11 214.53 o 16 9 0 882.97 1131.33 233.74 o 17 9 0 105.07 118.47 189.81 o 18 9 0 0.24 55.24 156.16 o 0 10 0 113.86 7.47 107.94 o 1 10 0 1228.11 1317.22 140.82 o 2 10 0 106.77 70.80 107.56 o 3 10 0 4520.45 4652.67 183.60 o 4 10 0 291.75 254.06 95.38 o 5 10 0 103.98 66.46 104.11 o 6 10 0 4.52 -116.41 99.72 o 7 10 0 27.81 71.52 83.35 o 8 10 0 311.53 278.70 101.67 o 9 10 0 264.07 318.60 99.87 o 10 10 0 115.68 88.97 110.20 o 11 10 0 688.15 670.04 113.39 o 12 10 0 59.57 107.14 115.61 o 13 10 0 15.55 69.41 113.66 o 14 10 0 3.44 81.98 159.53 o 15 10 0 78.36 128.90 174.04 o 16 10 0 65.72 12.59 203.32 o 1 11 0 9.29 -38.97 110.51 o 2 11 0 22.57 97.54 101.41 o 3 11 0 139.27 116.37 103.30 o 4 11 0 332.29 303.14 109.31 o 5 11 0 388.53 340.68 120.69 o 6 11 0 222.29 277.03 121.93 o 7 11 0 127.25 103.51 100.54 o 8 11 0 46.43 133.08 93.43 o 9 11 0 3.12 30.07 96.96 o 10 11 0 78.28 -11.74 117.63 o 11 11 0 30.18 -2.30 99.52 o 12 11 0 2.80 -133.08 103.33 o 13 11 0 111.26 129.78 114.26 o 14 11 0 25.55 97.87 175.91 o 0 12 0 1864.81 1961.38 219.40 o 1 12 0 736.28 612.73 122.94 o 2 12 0 106.99 101.38 105.45 o 3 12 0 1652.52 1855.31 165.35 o 4 12 0 583.20 628.86 145.19 o 5 12 0 227.66 305.45 122.51 o 6 12 0 156.91 164.84 118.14 o 7 12 0 687.63 470.86 144.52 o 8 12 0 1572.96 1430.26 165.30 o 9 12 0 31.93 115.15 132.06 o 10 12 0 277.02 287.50 133.80 o 11 12 0 121.79 19.88 126.50 o 12 12 0 262.59 266.27 138.20 o 1 13 0 75.80 126.64 154.44 o 2 13 0 1274.26 1366.90 194.82 o 3 13 0 524.91 602.20 183.71 o 4 13 0 35.82 37.42 135.78 o 5 13 0 607.67 503.86 199.51 o 6 13 0 916.26 1251.41 223.65 o 7 13 0 6.11 -50.59 130.35 o 8 13 0 406.66 609.20 181.36 o -24 1 1 69.18 107.61 166.11 o -23 1 1 17.28 -41.01 154.89 o -22 1 1 7.83 58.01 157.51 o -21 1 1 122.26 70.36 154.60 o -20 1 1 38.84 120.80 148.47 o -19 1 1 1476.23 1295.68 196.05 o -18 1 1 86.94 93.39 138.90 o -17 1 1 59.09 30.81 129.89 o -16 1 1 9.67 121.22 199.38 o -15 1 1 4337.63 4365.23 246.15 o -14 1 1 1348.22 1368.55 159.41 o -13 1 1 829.85 896.61 264.37 o -12 1 1 2020.31 1953.26 82.01 o -11 1 1 1840.74 1786.96 83.90 o -10 1 1 1569.96 1593.49 122.20 o -9 1 1 6958.53 7308.37 278.76 o -8 1 1 71.26 45.06 38.24 o -7 1 1 470.90 485.48 42.92 o -6 1 1 4786.58 4911.58 87.13 o -5 1 1 3540.88 3628.02 93.64 o -4 1 1 15341.79 15144.38 272.54 o -3 1 1 5272.27 5610.67 78.23 o -2 1 1 235.56 208.01 18.00 o -1 1 1 8005.66 8231.78 212.57 o 0 1 1 521.81 490.26 38.71 o 1 1 1 237.54 228.84 46.55 o 2 1 1 3.95 8.14 29.64 o 3 1 1 918.48 899.74 51.89 o 4 1 1 6591.03 6551.17 154.24 o 5 1 1 6048.24 6114.46 134.01 o 6 1 1 472.20 461.06 58.47 o 7 1 1 1710.67 1599.57 81.18 o 8 1 1 5637.02 5335.47 141.87 o 9 1 1 388.33 331.36 65.60 o 10 1 1 1247.39 1401.89 90.99 o 11 1 1 1455.52 1125.96 96.70 o 12 1 1 3267.12 3078.59 135.52 o 13 1 1 335.28 416.53 69.06 o 14 1 1 734.61 710.04 81.26 o 15 1 1 3900.33 3928.41 145.96 o 16 1 1 723.80 833.18 153.75 o 17 1 1 2301.10 2114.02 192.84 o 18 1 1 105.22 64.88 117.52 o 19 1 1 92.16 76.52 140.28 o 20 1 1 49.66 74.62 138.78 o 21 1 1 7.64 69.10 168.00 o 22 1 1 126.06 178.07 157.38 o 23 1 1 19.90 22.24 175.39 o 24 1 1 43.86 71.27 141.26 o -23 2 1 7.32 -32.75 154.38 o -22 2 1 536.95 436.22 160.99 o -21 2 1 4.24 126.86 178.74 o -20 2 1 295.68 353.95 146.10 o -19 2 1 16.22 96.77 141.49 o -18 2 1 2261.25 2534.62 231.00 o -17 2 1 311.48 295.01 141.27 o -16 2 1 131.18 69.95 152.97 o -15 2 1 1088.34 1001.59 149.55 o -14 2 1 5792.87 6150.62 276.31 o -13 2 1 939.65 893.33 155.20 o -12 2 1 2482.57 2681.65 184.13 o -11 2 1 241.84 186.54 61.26 o -10 2 1 6921.34 6745.46 144.02 o -9 2 1 1231.28 1274.62 74.30 o -8 2 1 14991.22 16396.78 370.30 o -7 2 1 1124.13 1015.72 50.97 o -6 2 1 47226.55 46569.95 565.19 o -5 2 1 456.02 541.80 39.03 o -4 2 1 70.69 54.00 26.33 o -3 2 1 1962.80 1940.75 73.57 o -2 2 1 88.58 128.19 19.66 o -1 2 1 1106.54 1146.68 37.29 o 0 2 1 1238.01 1186.38 41.36 o 1 2 1 11452.49 11552.83 120.44 o 2 2 1 200.18 215.02 32.92 o 3 2 1 11682.50 11809.66 272.22 o 4 2 1 14502.25 14121.61 182.22 o 5 2 1 20255.51 20190.94 370.79 o 6 2 1 658.72 535.09 56.36 o 7 2 1 3554.09 3250.27 133.75 o 8 2 1 10553.24 10636.59 193.88 o 9 2 1 33276.53 33786.24 863.81 o 10 2 1 2774.68 2849.10 174.53 o 11 2 1 806.97 638.20 76.07 o 12 2 1 84.67 65.58 66.10 o 13 2 1 1702.68 1579.83 117.75 o 14 2 1 1.81 82.96 86.66 o 15 2 1 119.02 40.44 86.01 o 16 2 1 593.02 462.50 145.79 o 17 2 1 4895.08 4853.84 276.02 o 18 2 1 350.49 269.78 210.94 o 19 2 1 573.85 589.98 160.84 o 20 2 1 12.54 181.55 149.13 o 21 2 1 499.48 324.03 185.47 o 22 2 1 3.51 23.61 151.76 o 23 2 1 2.93 -26.71 131.68 o -23 3 1 12.96 -45.54 140.25 o -22 3 1 0.27 44.05 183.65 o -21 3 1 37.23 -21.62 130.70 o -20 3 1 69.23 19.39 175.34 o -19 3 1 1709.27 1612.56 211.93 o -18 3 1 2.09 -2.15 141.22 o -17 3 1 168.68 176.60 141.90 o -16 3 1 72.18 32.19 108.61 o -15 3 1 2186.45 2152.61 197.36 o -14 3 1 626.71 715.76 131.11 o -13 3 1 781.13 505.03 111.61 o -12 3 1 1411.95 1344.85 95.60 o -11 3 1 3660.50 3374.19 125.17 o -10 3 1 749.68 820.41 76.21 o -9 3 1 26096.80 26310.79 454.61 o -8 3 1 2615.92 2436.06 83.82 o -7 3 1 83.36 63.60 40.12 o -6 3 1 15877.95 15396.91 169.46 o -5 3 1 15638.66 15813.29 147.95 o -4 3 1 18614.90 18784.34 158.17 o -3 3 1 2132.12 2151.32 57.76 o -2 3 1 15763.88 16455.48 367.31 o -1 3 1 83574.66 82952.16 882.61 o 0 3 1 2680.96 2620.51 70.17 o 1 3 1 1250.32 1150.82 54.80 o 2 3 1 2973.38 2840.54 75.90 o 3 3 1 1525.45 1473.21 60.87 o 4 3 1 22296.23 22567.72 286.40 o 5 3 1 971.77 924.32 65.25 o 6 3 1 206.02 169.74 56.96 o 7 3 1 7319.97 7322.39 310.24 o 8 3 1 1681.69 1526.27 89.29 o 9 3 1 761.50 739.93 77.29 o 10 3 1 235.18 302.92 72.35 o 11 3 1 544.24 523.35 77.62 o 12 3 1 10438.18 10396.33 436.86 o 13 3 1 1053.08 1017.99 120.03 o 14 3 1 3969.72 3822.57 166.05 o 15 3 1 111.54 73.02 98.09 o 16 3 1 69.11 154.53 126.57 o 17 3 1 74.00 77.57 117.18 o 18 3 1 10.16 123.72 137.92 o 19 3 1 161.29 153.56 133.22 o 20 3 1 319.48 471.84 166.93 o 21 3 1 1.89 21.22 131.83 o 22 3 1 577.81 711.06 174.90 o 23 3 1 0.40 7.67 185.76 o -23 4 1 102.44 152.57 267.96 o -22 4 1 100.99 189.91 178.27 o -21 4 1 113.42 195.48 147.50 o -20 4 1 131.21 223.24 164.79 o -19 4 1 75.04 248.73 331.37 o -18 4 1 271.79 447.33 186.49 o -17 4 1 219.27 204.98 169.34 o -16 4 1 170.61 65.60 142.55 o -15 4 1 131.82 107.04 154.31 o -14 4 1 3450.09 3638.22 237.13 o -13 4 1 1880.38 1779.44 113.14 o -12 4 1 1020.90 978.35 93.07 o -11 4 1 4341.09 4157.52 147.93 o -10 4 1 912.93 946.02 72.55 o -9 4 1 1113.88 1142.03 72.17 o -8 4 1 350.74 414.36 56.83 o -7 4 1 26.76 39.55 46.15 o -6 4 1 9419.69 9785.78 235.98 o -5 4 1 845.41 813.43 52.17 o -4 4 1 11734.91 11771.81 193.05 o -3 4 1 19166.10 19136.29 242.93 o -2 4 1 24.95 56.26 33.76 o -1 4 1 5347.30 5274.66 110.94 o 0 4 1 3829.01 3929.02 113.37 o 1 4 1 24.92 30.03 46.33 o 2 4 1 127.89 125.73 45.48 o 3 4 1 1577.98 1662.04 71.86 o 4 4 1 12933.86 13345.14 385.85 o 5 4 1 2586.94 2451.17 90.68 o 6 4 1 4960.63 4703.02 122.08 o 7 4 1 13173.67 12765.77 282.72 o 8 4 1 110.96 154.99 63.23 o 9 4 1 7380.08 7260.75 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