#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222747.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222747_Fobs loop_ _publ_author_name 'Ma, Zhi-Hong' 'Dong, Gui-Ying' 'Liu, Xiao-Huan' 'Lin, Jin' _publ_section_title ; trans-Di-\m-carbonyl-bis{carbonyl[\h^5^-2,3,4,5-tetramethyl-1-(2-thienyl)cyclopentadienyl]ruthenium(I)}(Ru---Ru) ; _journal_coeditor_code HY2205 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m894 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.826 _cell_angle_beta 76.083 _cell_angle_gamma 82.876 _cell_length_a 8.2690 _cell_length_b 8.8990 _cell_length_c 10.0560 _exptl_crystal_F_000 362.00 _reflns_d_resolution_high 0.8393 _[local]_cod_data_source_file hy2205Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 127.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9968.74 13667.60 380.70 o 2 0 0 4016.94 4163.45 109.96 o 3 0 0 4297.91 4402.55 78.69 o 4 0 0 1574.92 1671.53 30.48 o 5 0 0 1744.52 1684.54 30.92 o 6 0 0 1232.84 1238.68 35.09 o 7 0 0 1844.91 1775.96 49.57 o 8 0 0 565.67 506.00 16.68 o 9 0 0 79.82 77.16 5.04 o -9 1 0 610.53 601.16 19.93 o -8 1 0 210.34 217.65 9.09 o -7 1 0 1314.91 1373.54 39.27 o -6 1 0 3114.59 3364.44 60.95 o -5 1 0 1368.09 1407.00 26.18 o -4 1 0 2995.04 2976.62 79.63 o -3 1 0 7142.10 7267.90 192.56 o -2 1 0 6849.82 6898.50 182.16 o -1 1 0 10509.19 11317.18 299.70 o 0 1 0 6325.71 5907.61 158.68 o 1 1 0 16267.70 14169.50 375.47 o 2 1 0 4.00 7.27 0.82 o 3 1 0 2234.66 2240.37 44.05 o 4 1 0 802.72 673.51 14.17 o 5 1 0 264.63 261.72 8.81 o 6 1 0 879.87 831.60 24.28 o 7 1 0 89.30 89.75 4.76 o 8 1 0 118.86 101.90 5.41 o 9 1 0 10.68 11.68 2.16 o -9 2 0 270.46 300.40 12.10 o -8 2 0 473.51 494.46 16.83 o -7 2 0 196.05 211.70 6.59 o -6 2 0 1694.03 1783.25 33.32 o -5 2 0 1660.87 1690.75 46.62 o -4 2 0 1633.77 1736.09 47.34 o -3 2 0 2758.65 2718.92 72.59 o -2 2 0 10.66 15.55 1.17 o -1 2 0 179.37 214.39 6.49 o 0 2 0 2473.52 2637.62 69.95 o 1 2 0 35.38 42.22 1.83 o 2 2 0 2016.06 2087.48 41.02 o 3 2 0 2.18 5.64 0.62 o 4 2 0 25.75 50.67 1.96 o 5 2 0 274.69 313.74 7.52 o 6 2 0 90.07 84.87 4.25 o 7 2 0 0.26 0.44 1.07 o 8 2 0 176.01 164.66 7.36 o 9 2 0 90.95 90.58 5.39 o -8 3 0 45.36 45.35 3.78 o -7 3 0 152.98 161.87 4.85 o -6 3 0 3.03 3.23 1.24 o -5 3 0 471.68 473.41 14.92 o -4 3 0 3.50 4.71 1.07 o -3 3 0 28.05 46.14 2.53 o -2 3 0 26.87 31.27 1.85 o -1 3 0 837.08 794.45 16.87 o 0 3 0 308.98 293.41 8.73 o 1 3 0 0.26 -0.52 0.35 o 2 3 0 1998.19 2105.43 41.44 o 3 3 0 982.98 1166.47 23.55 o 4 3 0 1939.92 1961.13 39.09 o 5 3 0 319.66 293.03 7.18 o 6 3 0 545.36 588.84 13.24 o 7 3 0 409.63 412.69 13.78 o 8 3 0 139.56 134.31 6.45 o 9 3 0 346.62 358.50 13.30 o -8 4 0 0.19 -0.33 1.26 o -7 4 0 98.90 110.52 3.98 o -6 4 0 7.55 7.41 1.68 o -5 4 0 459.34 455.29 14.66 o -4 4 0 19.10 25.52 2.16 o -3 4 0 518.94 540.25 16.17 o -2 4 0 281.63 239.55 7.95 o -1 4 0 26.18 27.95 1.28 o 0 4 0 1862.52 1728.99 46.57 o 1 4 0 1387.60 1411.23 28.12 o 2 4 0 1590.88 1524.25 30.42 o 3 4 0 1221.29 1181.25 23.99 o 4 4 0 1487.88 1636.80 33.00 o 5 4 0 1568.74 1565.90 31.88 o 6 4 0 326.11 335.45 8.38 o 7 4 0 707.19 720.44 16.22 o 8 4 0 413.37 390.70 13.80 o 9 4 0 274.68 263.83 10.72 o -7 5 0 212.37 203.90 6.00 o -6 5 0 508.60 541.36 17.78 o -5 5 0 116.93 121.24 5.67 o -4 5 0 894.98 874.73 25.63 o -3 5 0 136.45 130.73 5.50 o -2 5 0 2220.28 2110.91 57.39 o -1 5 0 1619.13 1439.09 26.70 o 0 5 0 685.17 669.23 19.20 o 1 5 0 2789.65 2601.70 51.22 o 2 5 0 434.68 418.56 9.28 o 3 5 0 1580.02 1604.24 32.33 o 4 5 0 2700.30 2907.33 57.65 o 5 5 0 1558.66 1614.43 33.04 o 6 5 0 791.62 834.06 18.29 o 7 5 0 204.40 200.56 6.06 o 8 5 0 328.67 333.70 9.04 o -7 6 0 216.22 218.11 6.55 o -6 6 0 696.13 709.53 22.51 o -5 6 0 869.32 883.67 26.59 o -4 6 0 84.83 91.08 4.79 o -3 6 0 1419.21 1351.28 38.20 o -2 6 0 1314.82 1260.51 35.59 o -1 6 0 1895.94 1888.78 34.88 o 0 6 0 1228.83 1255.93 34.90 o 1 6 0 1564.11 1613.16 35.65 o 2 6 0 2819.17 2786.69 55.12 o 3 6 0 469.85 463.03 10.49 o 4 6 0 1242.05 1252.02 25.93 o 5 6 0 724.57 754.21 16.62 o 6 6 0 179.94 177.13 7.30 o 7 6 0 242.66 268.01 7.60 o 8 6 0 51.11 52.99 3.10 o -6 7 0 232.04 236.11 9.98 o -5 7 0 675.72 682.38 21.68 o -4 7 0 406.91 409.95 14.10 o -3 7 0 42.89 52.23 3.59 o -2 7 0 1237.41 1214.30 34.83 o -1 7 0 1077.87 1092.10 21.18 o 0 7 0 1127.15 1112.41 31.51 o 1 7 0 1047.91 958.11 20.03 o 2 7 0 306.52 296.81 7.25 o 3 7 0 114.36 118.84 5.44 o 4 7 0 2.07 3.00 0.84 o 5 7 0 100.23 107.55 3.89 o 6 7 0 72.72 81.08 3.49 o 7 7 0 27.62 24.00 2.20 o -5 8 0 63.39 60.05 4.37 o -4 8 0 157.97 159.18 7.44 o -3 8 0 45.45 44.31 3.47 o -2 8 0 27.42 24.07 2.66 o -1 8 0 124.38 114.01 6.79 o 0 8 0 26.58 20.34 1.44 o 1 8 0 30.59 28.23 2.50 o 2 8 0 36.45 59.19 3.60 o 3 8 0 169.66 150.51 6.54 o 4 8 0 2.12 3.45 1.36 o 5 8 0 44.06 42.42 3.58 o 6 8 0 69.76 72.27 4.93 o -4 9 0 39.48 42.70 3.93 o -3 9 0 39.70 42.49 3.80 o -2 9 0 110.97 121.97 6.37 o -1 9 0 138.43 149.23 4.89 o 0 9 0 288.55 289.07 9.44 o 1 9 0 189.44 190.15 7.74 o 2 9 0 54.65 55.73 3.66 o 3 9 0 235.28 222.52 8.88 o 4 9 0 353.80 363.49 13.03 o 5 9 0 320.74 295.20 11.41 o -2 10 0 198.05 181.83 8.61 o -1 10 0 338.89 353.48 13.53 o 0 10 0 173.43 182.44 8.22 o 1 10 0 246.98 236.29 9.37 o 2 10 0 425.23 430.61 14.75 o 3 10 0 315.05 286.14 10.92 o -3 -10 1 331.40 321.69 12.15 o -2 -10 1 306.26 278.84 10.83 o -1 -10 1 236.06 221.80 9.15 o 0 -10 1 284.73 291.95 18.49 o 1 -10 1 374.93 383.01 10.37 o -5 -9 1 393.42 361.31 13.49 o -4 -9 1 523.38 524.70 17.64 o -3 -9 1 290.49 299.19 11.24 o -2 -9 1 415.84 440.96 14.87 o -1 -9 1 526.76 501.21 16.38 o 0 -9 1 661.82 669.04 19.76 o 1 -9 1 380.07 380.43 15.58 o 2 -9 1 513.92 504.18 17.32 o 3 -9 1 484.18 431.37 15.46 o 4 -9 1 96.98 106.38 6.34 o -6 -8 1 440.89 460.95 16.43 o -5 -8 1 229.15 218.88 9.27 o -4 -8 1 462.42 483.37 16.16 o -3 -8 1 700.54 699.08 21.59 o -2 -8 1 277.86 278.75 10.21 o -1 -8 1 685.44 676.80 20.64 o 0 -8 1 366.79 342.62 11.76 o 1 -8 1 644.91 618.76 17.76 o 2 -8 1 247.90 247.20 9.84 o 3 -8 1 108.75 107.13 5.82 o 4 -8 1 58.38 59.25 4.41 o 5 -8 1 0.08 -1.02 1.15 o -7 -7 1 121.63 125.93 6.79 o -6 -7 1 117.78 120.41 6.39 o -5 -7 1 272.24 289.40 11.04 o -4 -7 1 383.96 358.83 12.58 o -3 -7 1 834.49 793.65 23.74 o -2 -7 1 449.98 423.64 13.72 o -1 -7 1 1.40 1.92 0.98 o 0 -7 1 147.96 148.49 6.16 o 1 -7 1 77.33 76.51 3.10 o 2 -7 1 112.21 101.56 5.21 o 3 -7 1 1.31 -0.33 0.94 o 4 -7 1 124.40 122.62 6.16 o 5 -7 1 23.78 19.91 2.54 o 6 -7 1 105.84 111.99 6.21 o -8 -6 1 0.89 5.75 2.11 o -7 -6 1 0.24 1.06 1.26 o -6 -6 1 35.17 26.98 2.01 o -5 -6 1 16.74 14.19 1.44 o -4 -6 1 191.41 189.05 7.68 o -3 -6 1 55.77 53.85 3.36 o -2 -6 1 17.81 20.71 2.00 o -1 -6 1 225.40 214.12 11.21 o 0 -6 1 1231.46 1289.19 35.99 o 1 -6 1 126.99 146.47 4.16 o 2 -6 1 1101.01 1086.75 31.24 o 3 -6 1 48.99 55.98 3.58 o 4 -6 1 157.65 157.54 6.88 o 5 -6 1 440.31 463.36 15.54 o 6 -6 1 305.76 293.02 11.31 o 7 -6 1 455.59 509.71 17.76 o -8 -5 1 1.52 0.93 1.44 o -7 -5 1 114.00 131.83 6.61 o -6 -5 1 123.19 112.41 4.01 o -5 -5 1 571.59 568.35 12.91 o -4 -5 1 1021.85 1000.75 21.00 o -3 -5 1 333.00 353.85 8.22 o -2 -5 1 744.57 719.46 20.97 o -1 -5 1 1276.96 1326.41 26.68 o 0 -5 1 2042.12 2059.39 55.74 o 1 -5 1 3698.85 3591.38 74.23 o 2 -5 1 439.72 472.11 14.66 o 3 -5 1 2228.21 2195.79 60.01 o 4 -5 1 382.64 449.04 14.50 o 5 -5 1 504.51 513.53 16.55 o 6 -5 1 1048.71 1071.34 31.71 o 7 -5 1 463.90 454.84 15.97 o 8 -5 1 299.73 322.41 8.54 o -8 -4 1 301.43 281.48 10.96 o -7 -4 1 424.49 413.17 14.18 o -6 -4 1 1245.67 1230.69 25.82 o -5 -4 1 1770.61 1771.44 35.92 o -4 -4 1 2915.04 2988.60 59.03 o -3 -4 1 1158.22 1147.20 23.43 o -2 -4 1 804.17 804.20 16.61 o -1 -4 1 2915.85 2663.42 52.27 o 0 -4 1 4196.45 4344.10 115.18 o 1 -4 1 2645.65 2462.85 76.67 o 2 -4 1 3059.58 3148.11 84.28 o 3 -4 1 1584.59 1624.39 44.69 o 4 -4 1 2525.25 2389.84 65.00 o 5 -4 1 139.18 131.99 5.78 o 6 -4 1 573.97 557.09 17.88 o 7 -4 1 628.16 635.54 20.38 o 8 -4 1 82.51 78.76 3.44 o -9 -3 1 262.13 271.89 11.03 o -8 -3 1 510.64 503.41 16.88 o -7 -3 1 1023.25 1038.15 30.53 o -6 -3 1 517.84 530.00 16.67 o -5 -3 1 1310.75 1302.22 26.79 o -4 -3 1 832.64 847.10 17.71 o -3 -3 1 4025.18 4126.07 62.71 o -2 -3 1 1329.27 1297.38 20.12 o -1 -3 1 599.22 630.31 14.60 o 0 -3 1 5831.20 5819.24 153.45 o 1 -3 1 3897.82 3924.86 81.43 o 2 -3 1 884.35 750.59 21.21 o 3 -3 1 1547.30 1467.76 40.28 o 4 -3 1 519.92 532.40 16.07 o 5 -3 1 290.19 269.38 9.45 o 6 -3 1 1.20 0.96 1.09 o 7 -3 1 437.54 442.23 15.10 o 8 -3 1 80.74 74.78 4.95 o -9 -2 1 515.83 502.78 17.14 o -8 -2 1 249.39 232.43 9.32 o -7 -2 1 192.60 204.96 8.19 o -6 -2 1 457.53 482.02 15.23 o -5 -2 1 359.31 343.53 11.11 o -4 -2 1 1352.89 1296.95 20.25 o -3 -2 1 0.56 1.56 0.45 o -2 -2 1 3415.96 3678.66 71.60 o -1 -2 1 0.54 -0.43 0.29 o 0 -2 1 22.84 23.03 1.38 o 1 -2 1 4609.54 4500.91 80.40 o 2 -2 1 17.97 10.31 1.14 o 3 -2 1 13.95 27.23 1.87 o 4 -2 1 76.24 72.95 3.48 o 5 -2 1 160.54 147.08 5.95 o 6 -2 1 48.09 39.57 2.91 o 7 -2 1 41.34 45.95 3.45 o 8 -2 1 0.48 -0.28 1.22 o 9 -2 1 77.51 90.41 5.70 o -9 -1 1 50.35 47.26 4.11 o -8 -1 1 340.11 319.28 11.74 o -7 -1 1 19.97 21.74 2.38 o -6 -1 1 5.53 5.28 1.30 o -5 -1 1 275.61 280.90 9.40 o -4 -1 1 53.80 52.44 2.72 o -3 -1 1 33.72 20.41 1.53 o -2 -1 1 1980.43 1988.97 53.05 o 1 -1 1 737.92 857.18 23.39 o 2 -1 1 258.08 266.72 7.93 o 3 -1 1 2808.04 2695.77 71.82 o 4 -1 1 337.30 331.37 10.32 o 5 -1 1 1693.30 1803.96 49.41 o 6 -1 1 1117.20 1140.48 32.61 o 7 -1 1 43.22 51.68 3.50 o 8 -1 1 492.96 483.60 16.31 o 9 -1 1 199.22 199.62 9.01 o -9 0 1 0.11 -1.84 1.23 o -8 0 1 3.75 7.32 1.73 o -7 0 1 5.84 6.90 1.68 o -6 0 1 424.25 368.08 12.13 o -5 0 1 99.52 118.46 3.13 o -4 0 1 64.84 54.26 2.80 o -3 0 1 682.22 726.98 13.62 o -2 0 1 743.17 863.10 15.81 o -1 0 1 6105.09 6614.01 176.00 o 2 0 1 4850.15 4899.05 157.86 o 3 0 1 1013.65 1095.14 30.58 o 4 0 1 5501.03 5861.54 154.88 o 5 0 1 1588.59 1547.73 42.58 o 6 0 1 1820.82 1875.91 51.67 o 7 0 1 1209.54 1226.21 35.23 o 8 0 1 240.17 244.16 9.59 o 9 0 1 468.00 454.20 15.79 o -9 1 1 84.32 89.52 5.63 o -8 1 1 155.15 151.16 7.04 o -7 1 1 648.80 651.38 20.32 o -6 1 1 1007.39 1027.75 19.80 o -5 1 1 812.96 790.24 15.34 o -4 1 1 51.74 43.07 3.32 o -3 1 1 2112.70 1999.61 36.27 o -2 1 1 5534.42 5955.33 147.48 o -1 1 1 2577.95 2640.28 49.13 o 0 1 1 13686.93 15972.67 451.85 o 1 1 1 7908.00 8623.94 244.29 o 2 1 1 2085.65 2023.48 39.62 o 3 1 1 1529.06 1382.88 27.55 o 4 1 1 1737.44 1878.59 39.01 o 5 1 1 4386.98 4528.99 68.73 o 6 1 1 392.15 361.84 11.77 o 7 1 1 811.99 827.68 24.56 o 8 1 1 1013.22 937.42 27.97 o 9 1 1 121.73 107.67 5.86 o -8 2 1 236.40 262.08 10.53 o -7 2 1 759.08 775.81 23.76 o -6 2 1 1952.60 2019.05 39.00 o -5 2 1 2010.22 2080.43 38.40 o -4 2 1 2926.00 2732.65 49.61 o -3 2 1 1524.07 1396.74 25.77 o -2 2 1 7379.89 7438.90 197.29 o -1 2 1 3899.99 4075.31 108.39 o 0 2 1 749.22 710.65 19.19 o 1 2 1 6755.59 6057.86 207.12 o 2 2 1 6457.61 6660.05 130.12 o 3 2 1 1090.50 1080.38 21.73 o 4 2 1 567.23 516.52 11.14 o 5 2 1 887.57 910.53 19.04 o 6 2 1 812.66 777.09 16.77 o 7 2 1 9.95 10.16 1.74 o 8 2 1 156.72 147.78 6.75 o 9 2 1 37.42 23.93 2.82 o -8 3 1 624.14 705.90 22.74 o -7 3 1 354.82 370.82 8.75 o -6 3 1 1813.38 1880.84 35.37 o -5 3 1 2459.48 2511.09 46.12 o -4 3 1 1109.94 1135.70 21.57 o -3 3 1 1735.37 1597.76 43.44 o -2 3 1 11.02 7.38 0.88 o -1 3 1 2227.74 2200.82 58.69 o 0 3 1 514.85 565.22 15.64 o 1 3 1 2197.42 2513.98 66.78 o 2 3 1 4608.22 4406.67 141.08 o 3 3 1 25.25 24.52 1.19 o 4 3 1 74.18 74.88 2.55 o 5 3 1 49.38 43.75 5.91 o 6 3 1 164.78 169.59 4.91 o 7 3 1 81.87 76.20 3.17 o 8 3 1 92.03 81.32 4.69 o 9 3 1 13.04 8.55 1.95 o -8 4 1 180.44 177.89 8.43 o -7 4 1 418.57 438.84 10.28 o -6 4 1 24.76 30.62 2.75 o -5 4 1 326.49 367.54 8.41 o -4 4 1 179.57 183.17 6.91 o -3 4 1 187.19 192.16 6.82 o -2 4 1 382.75 351.09 10.82 o -1 4 1 41.11 49.85 2.46 o 0 4 1 152.37 156.42 5.20 o 1 4 1 590.72 745.59 20.75 o 2 4 1 33.03 41.68 2.36 o 3 4 1 41.90 59.48 2.13 o 4 4 1 1212.60 1224.22 25.02 o 5 4 1 129.32 131.89 4.00 o 6 4 1 688.81 648.07 27.61 o 7 4 1 754.27 695.68 15.67 o 8 4 1 68.10 58.90 3.01 o 9 4 1 164.06 176.04 8.06 o -7 5 1 7.51 10.04 1.49 o -6 5 1 1.93 0.70 0.79 o -5 5 1 540.76 538.18 11.71 o -4 5 1 95.84 85.15 4.34 o -3 5 1 79.50 84.44 4.07 o -2 5 1 1082.86 1086.96 30.51 o -1 5 1 71.25 96.70 2.80 o 0 5 1 2706.35 2665.04 71.18 o 1 5 1 896.63 924.40 25.73 o 2 5 1 1614.10 1711.90 34.18 o 3 5 1 1921.36 1862.88 37.22 o 4 5 1 1281.94 1287.45 26.41 o 5 5 1 1217.61 1302.42 27.00 o 6 5 1 400.05 416.39 10.09 o 7 5 1 604.65 599.15 13.95 o 8 5 1 462.24 474.38 11.76 o 9 5 1 284.52 273.09 10.99 o -7 6 1 146.13 149.77 5.23 o -6 6 1 254.25 270.14 7.36 o -5 6 1 325.15 335.64 11.94 o -4 6 1 957.13 965.67 28.31 o -3 6 1 942.86 910.94 26.56 o -2 6 1 1159.64 1100.29 31.23 o -1 6 1 1606.04 1571.31 29.17 o 0 6 1 561.63 528.12 15.63 o 1 6 1 2859.57 2815.42 75.45 o 2 6 1 1135.48 1145.00 23.50 o 3 6 1 2304.49 2307.20 46.03 o 4 6 1 2015.97 2100.50 42.20 o 5 6 1 650.05 702.86 15.56 o 6 6 1 829.25 850.47 18.71 o 7 6 1 523.83 501.36 12.19 o 8 6 1 418.97 395.43 10.41 o -6 7 1 342.00 359.28 9.27 o -5 7 1 702.15 694.81 15.06 o -4 7 1 644.29 663.13 20.71 o -3 7 1 823.85 808.84 24.30 o -2 7 1 1140.27 1136.28 32.60 o -1 7 1 1038.48 1094.79 21.10 o 0 7 1 814.68 791.92 15.73 o 1 7 1 643.72 661.61 19.48 o 2 7 1 1914.20 1928.83 38.81 o 3 7 1 759.70 724.55 15.70 o 4 7 1 737.63 703.16 15.49 o 5 7 1 612.73 606.99 13.88 o 6 7 1 561.76 553.26 13.10 o 7 7 1 337.05 307.31 8.49 o -5 8 1 440.41 451.82 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144.48 131.01 6.20 o -1 1 10 167.22 171.39 7.20 o 0 1 10 293.01 291.75 10.28 o 1 1 10 223.04 232.87 8.70 o 2 1 10 770.30 856.29 23.92 o 3 1 10 1253.54 1315.45 34.85 o 4 1 10 1960.19 1932.10 49.61 o 5 1 10 787.12 787.89 21.88 o 6 1 10 441.45 441.49 13.42 o -3 2 10 572.73 519.90 16.32 o -2 2 10 846.82 849.92 24.27 o -1 2 10 301.09 313.44 10.91 o 0 2 10 917.28 975.98 27.02 o 1 2 10 1065.69 1067.53 29.11 o 2 2 10 493.50 527.37 15.96 o 3 2 10 1549.62 1711.67 44.41 o 4 2 10 1379.97 1419.07 37.22 o 5 2 10 1084.63 1091.78 22.40 o 6 2 10 238.63 243.09 10.39 o 7 2 10 131.27 134.88 7.37 o -2 3 10 835.07 774.88 22.41 o -1 3 10 931.47 915.38 25.72 o 0 3 10 546.08 535.46 16.33 o 1 3 10 750.62 750.71 21.46 o 2 3 10 529.81 529.67 12.19 o 3 3 10 325.92 348.29 8.72 o 4 3 10 581.98 608.54 13.54 o 5 3 10 203.10 196.02 5.81 o 6 3 10 390.02 398.19 15.30 o 7 3 10 77.55 82.32 5.71 o -2 4 10 281.66 253.89 9.58 o -1 4 10 328.15 313.24 10.94 o 0 4 10 492.75 457.50 14.41 o 1 4 10 148.12 146.06 6.44 o 2 4 10 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