#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/27/2222754.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222754_Fobs loop_ _publ_author_name 'Strasser, Christoph E.' 'Cronje, Stephanie' 'Raubenheimer, Helgard G.' _publ_section_title ; Bis[\m-1,2-bis(diphenylphosphino)ethane-\k^2^P:P']digold(I)(Au---Au) bis(trifluoromethanesulfonate) acetonitrile disolvate ; _journal_coeditor_code IM2111 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m914 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.011 _cell_angle_gamma 90.000 _cell_length_a 11.7888 _cell_length_b 36.9980 _cell_length_c 14.3767 _exptl_crystal_F_000 3072.00 _reflns_d_resolution_high 0.7519 _[local]_cod_data_source_file im2111Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'I in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 650.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 422639.97 499195.69 13258.41 o 2 0 0 92143.25 98648.92 2501.87 o 3 0 0 111232.32 124280.52 3168.96 o 4 0 0 141260.45 157958.97 4025.38 o 5 0 0 134421.45 139855.31 3620.75 o 6 0 0 145372.00 154743.59 3345.05 o 7 0 0 350.68 136.68 211.99 o 8 0 0 11479.60 11108.27 1234.53 o 9 0 0 50653.42 51987.86 1824.86 o 10 0 0 2080.34 1601.99 811.24 o 11 0 0 1138.90 479.37 711.37 o 12 0 0 1245.34 497.81 659.13 o 13 0 0 657.74 571.55 743.12 o 1 1 0 6982.28 7705.94 202.64 o 2 1 0 12742.03 13455.04 293.92 o 3 1 0 56348.31 60680.61 1030.35 o 4 1 0 25858.29 26646.94 572.06 o 5 1 0 42979.38 45411.80 850.46 o 6 1 0 9846.62 9862.23 310.90 o 7 1 0 1281.77 1609.75 157.42 o 8 1 0 31512.62 32574.46 898.13 o 9 1 0 57381.45 59033.18 1424.49 o 10 1 0 68875.03 59846.51 2603.23 o 11 1 0 14762.41 13981.88 1083.92 o 12 1 0 623.22 866.63 523.29 o 13 1 0 6473.39 6315.24 882.66 o 1 2 0 1387.94 1000.07 72.11 o 2 2 0 106.97 -46.90 46.90 o 3 2 0 269.85 308.24 73.35 o 4 2 0 46433.73 52037.92 925.25 o 5 2 0 14704.85 16141.61 390.50 o 6 2 0 686.66 847.05 125.07 o 7 2 0 895.13 1105.66 144.00 o 8 2 0 5066.65 4877.35 410.39 o 9 2 0 2046.55 2143.76 456.64 o 10 2 0 1474.54 1799.24 404.18 o 11 2 0 62.36 148.15 456.28 o 12 2 0 1876.45 2312.68 636.12 o 13 2 0 1390.39 1148.26 611.40 o 1 3 0 1991.99 2196.88 154.94 o 2 3 0 488.13 432.22 56.90 o 3 3 0 77935.95 89505.89 1478.61 o 4 3 0 79835.45 86172.43 1454.94 o 5 3 0 12089.05 12268.23 330.86 o 6 3 0 818.50 1052.47 129.35 o 7 3 0 554.81 799.09 174.35 o 8 3 0 19740.06 17380.98 696.11 o 9 3 0 31607.45 30655.49 1126.38 o 10 3 0 44513.73 40857.46 1817.96 o 11 3 0 10707.78 9900.40 960.16 o 12 3 0 984.37 1395.17 549.52 o 13 3 0 9838.08 8582.05 980.39 o 0 4 0 339591.84 418893.84 14584.36 o 1 4 0 125134.88 148979.78 2360.31 o 2 4 0 174842.64 201866.70 3198.86 o 3 4 0 82067.38 90362.41 1474.25 o 4 4 0 169697.36 192698.86 3106.08 o 5 4 0 93804.38 94507.07 1614.08 o 6 4 0 25698.53 25252.71 557.15 o 7 4 0 3572.74 3968.73 279.87 o 8 4 0 5697.40 5605.69 429.50 o 9 4 0 22202.21 21787.87 1458.08 o 10 4 0 10069.52 9525.96 1123.38 o 11 4 0 3219.44 3299.47 808.93 o 12 4 0 1530.62 2059.27 828.65 o 13 4 0 61.82 91.88 495.67 o 1 5 0 993.24 1112.89 145.70 o 2 5 0 13394.09 14277.97 297.57 o 3 5 0 3492.56 3923.11 270.78 o 4 5 0 7406.71 7489.91 200.40 o 5 5 0 32408.56 32129.97 934.67 o 6 5 0 58721.77 62302.69 1152.66 o 7 5 0 3455.82 3234.15 259.74 o 8 5 0 16066.04 16674.88 1070.75 o 9 5 0 22826.84 21857.00 1078.40 o 10 5 0 54625.88 53122.87 1950.84 o 11 5 0 31889.84 29077.67 1586.88 o 12 5 0 440.63 94.95 703.94 o 13 5 0 10735.12 10660.43 1078.40 o 0 6 0 11707.49 13216.93 619.70 o 1 6 0 1754.01 2075.52 137.86 o 2 6 0 41952.31 46120.20 911.41 o 3 6 0 1290.49 1071.23 115.25 o 4 6 0 17544.77 17972.91 444.61 o 5 6 0 3009.43 2893.70 147.03 o 6 6 0 4324.34 4594.30 180.60 o 7 6 0 238.48 159.55 153.46 o 8 6 0 6830.61 6460.33 442.27 o 9 6 0 50.45 60.16 310.12 o 10 6 0 4688.97 5117.19 756.69 o 11 6 0 354.40 415.07 345.77 o 12 6 0 1411.42 1250.29 536.62 o 13 6 0 56.41 196.54 501.94 o 1 7 0 14487.84 16152.72 384.14 o 2 7 0 6409.68 6212.69 178.53 o 3 7 0 3755.73 3703.43 151.89 o 4 7 0 16328.55 16012.36 369.84 o 5 7 0 6822.08 7462.35 276.24 o 6 7 0 2165.96 1938.06 152.27 o 7 7 0 78.27 -39.31 145.74 o 8 7 0 392.25 691.20 236.68 o 9 7 0 11230.53 11652.41 816.20 o 10 7 0 6883.89 8168.12 757.46 o 11 7 0 2464.84 3369.27 578.91 o 12 7 0 137.31 -369.64 454.46 o 13 7 0 5051.41 4845.84 792.56 o 0 8 0 7431.70 9643.18 557.21 o 1 8 0 19752.39 18580.77 434.90 o 2 8 0 1239.56 1429.36 178.15 o 3 8 0 15922.20 16202.42 356.57 o 4 8 0 90410.26 96528.92 1630.88 o 5 8 0 121853.50 126702.19 2367.89 o 6 8 0 23893.19 23707.58 578.56 o 7 8 0 3310.03 3303.12 266.13 o 8 8 0 9431.13 8527.74 508.62 o 9 8 0 13285.91 14371.55 884.98 o 10 8 0 10151.94 10195.02 838.30 o 11 8 0 1254.15 1485.87 483.20 o 12 8 0 793.77 851.28 521.34 o 13 8 0 13.67 547.17 531.67 o 1 9 0 702.22 856.31 116.00 o 2 9 0 57569.16 64046.43 1250.95 o 3 9 0 3320.37 3222.53 193.51 o 4 9 0 25720.83 26745.15 548.09 o 5 9 0 87694.92 90564.82 1565.61 o 6 9 0 87090.20 87404.01 1718.12 o 7 9 0 21098.55 20618.91 909.71 o 8 9 0 9384.80 8817.55 526.59 o 9 9 0 49635.70 46919.12 1749.99 o 10 9 0 47960.50 48333.55 1849.89 o 11 9 0 17276.35 16976.83 1445.02 o 12 9 0 86.18 -123.30 476.26 o 13 9 0 12037.45 12548.08 1167.22 o 0 10 0 44792.04 49513.18 1991.22 o 1 10 0 3091.37 3499.55 185.70 o 2 10 0 151.31 260.44 100.03 o 3 10 0 11246.56 11021.63 370.72 o 4 10 0 22676.36 22799.93 485.45 o 5 10 0 30053.72 28274.66 593.93 o 6 10 0 339.24 87.71 95.53 o 7 10 0 6967.52 6818.66 447.83 o 8 10 0 26151.17 25356.47 889.69 o 9 10 0 16023.41 14502.38 920.65 o 10 10 0 170.26 220.81 356.65 o 11 10 0 810.19 211.89 746.71 o 12 10 0 129.31 38.35 847.86 o 13 10 0 672.94 471.20 548.40 o 1 11 0 27147.26 31211.24 788.59 o 2 11 0 16128.45 16388.07 439.15 o 3 11 0 16687.50 17132.11 598.10 o 4 11 0 800.35 801.87 113.30 o 5 11 0 6889.07 6673.85 327.01 o 6 11 0 1901.14 1894.74 272.12 o 7 11 0 2212.40 2557.24 399.83 o 8 11 0 139.21 379.38 237.60 o 9 11 0 5874.22 6478.71 791.01 o 10 11 0 1598.40 1285.45 453.27 o 11 11 0 6203.99 6562.08 1055.02 o 12 11 0 2440.16 1521.09 530.17 o 13 11 0 438.53 -1.49 479.70 o 0 12 0 78279.64 91633.54 3490.27 o 1 12 0 112743.35 130531.80 2786.96 o 2 12 0 8108.14 9020.68 313.42 o 3 12 0 10226.83 9906.08 339.88 o 4 12 0 82308.45 82517.70 1433.66 o 5 12 0 122029.52 128398.45 2166.16 o 6 12 0 33943.28 32823.23 1725.04 o 7 12 0 5799.70 6133.82 940.81 o 8 12 0 2400.29 2921.51 403.37 o 9 12 0 454.91 710.31 386.37 o 10 12 0 11038.38 11510.41 1006.62 o 11 12 0 3157.75 1941.84 579.24 o 12 12 0 2920.22 2429.93 589.21 o 13 12 0 376.17 776.41 769.75 o 1 13 0 5280.89 6459.65 404.38 o 2 13 0 4392.21 4413.94 239.81 o 3 13 0 4723.87 5241.30 275.14 o 4 13 0 34299.39 36268.53 842.15 o 5 13 0 54640.49 55604.88 1035.09 o 6 13 0 50544.78 49537.63 1784.60 o 7 13 0 718.73 537.71 236.90 o 8 13 0 12963.90 13668.22 867.14 o 9 13 0 49042.53 45357.18 1852.43 o 10 13 0 42003.91 40829.01 1700.01 o 11 13 0 8698.08 10601.97 1053.48 o 12 13 0 1863.07 2468.45 603.72 o 13 13 0 17811.57 21109.09 2091.09 o 0 14 0 44729.53 47325.29 1999.42 o 1 14 0 22125.40 23265.89 668.14 o 2 14 0 13167.79 13682.64 531.84 o 3 14 0 38539.20 40401.60 930.82 o 4 14 0 54973.32 57625.66 1228.13 o 5 14 0 45600.48 47442.98 1066.29 o 6 14 0 3618.69 3427.93 361.12 o 7 14 0 4196.60 4301.12 408.10 o 8 14 0 41822.71 41145.18 1596.37 o 9 14 0 20611.42 21930.20 1541.81 o 10 14 0 9405.37 9382.68 861.39 o 11 14 0 133.74 553.84 423.46 o 12 14 0 392.56 505.00 596.39 o 13 14 0 2997.48 2307.21 992.54 o 1 15 0 4115.28 4557.00 282.25 o 2 15 0 16261.50 17169.42 497.69 o 3 15 0 6418.92 6794.54 315.22 o 4 15 0 2424.36 2369.52 218.70 o 5 15 0 999.88 1055.23 223.97 o 6 15 0 294.68 192.42 233.06 o 7 15 0 4942.66 5166.28 524.08 o 8 15 0 3163.69 3321.29 412.84 o 9 15 0 4876.52 5062.82 478.85 o 10 15 0 1849.46 1893.92 713.16 o 11 15 0 109.16 -401.27 401.27 o 12 15 0 187.78 606.36 442.33 o 13 15 0 33.73 862.04 499.82 o 0 16 0 204021.81 240023.53 8721.32 o 1 16 0 129565.26 151708.78 3267.12 o 2 16 0 12418.08 12533.62 439.17 o 3 16 0 28307.94 29312.20 738.34 o 4 16 0 37406.61 36761.73 887.15 o 5 16 0 99109.02 101595.85 2037.25 o 6 16 0 66691.38 66353.91 1730.48 o 7 16 0 15902.73 14764.15 1229.11 o 8 16 0 44.34 225.13 240.27 o 9 16 0 1701.81 2012.64 597.16 o 10 16 0 4211.87 5099.61 991.77 o 11 16 0 884.74 1284.59 509.28 o 12 16 0 2726.72 3410.22 767.45 o 13 16 0 213.26 -1.92 480.49 o 1 17 0 1716.62 2594.53 420.47 o 2 17 0 1561.88 1837.15 199.99 o 3 17 0 7747.16 8238.88 359.52 o 4 17 0 31297.69 32030.39 807.83 o 5 17 0 36972.77 36746.47 907.91 o 6 17 0 17115.75 15666.19 674.15 o 7 17 0 1022.52 903.36 276.08 o 8 17 0 14846.60 16073.16 1673.94 o 9 17 0 69019.91 66272.41 1856.73 o 10 17 0 56350.92 55037.18 2109.52 o 11 17 0 22610.24 22426.18 1289.50 o 12 17 0 22.20 -70.99 419.28 o 13 17 0 12136.41 12856.38 1527.22 o 0 18 0 59358.47 64255.79 2710.78 o 1 18 0 122542.99 133911.48 2937.74 o 2 18 0 11179.99 12958.78 638.93 o 3 18 0 1793.84 1669.14 210.18 o 4 18 0 54251.73 58038.17 1563.00 o 5 18 0 41663.81 38620.28 1249.89 o 6 18 0 5695.21 5908.15 505.20 o 7 18 0 2256.42 1653.36 319.63 o 8 18 0 7244.94 6354.25 529.28 o 9 18 0 6481.35 6751.53 579.21 o 10 18 0 3830.54 4355.75 677.57 o 11 18 0 2095.38 2822.61 606.15 o 12 18 0 3078.02 3968.34 686.28 o 13 18 0 526.27 381.04 667.33 o 2 19 0 16194.42 15704.65 574.62 o 3 19 0 16793.28 18154.66 637.28 o 4 19 0 7716.09 7289.98 471.99 o 5 19 0 171.99 307.77 161.72 o 6 19 0 9524.22 9106.05 874.36 o 7 19 0 11044.91 10796.01 628.46 o 8 19 0 6498.08 6572.74 669.21 o 9 19 0 952.09 784.61 317.80 o 10 19 0 890.27 343.87 440.66 o 11 19 0 2017.64 1803.64 555.06 o 12 19 0 2385.55 2931.93 743.38 o 13 19 0 172.62 -109.09 577.19 o 0 20 0 125139.53 138633.11 5337.58 o 1 20 0 44116.14 46047.96 1021.61 o 2 20 0 21430.28 22404.36 726.44 o 3 20 0 15746.24 15554.49 522.17 o 4 20 0 15764.32 15860.38 540.56 o 5 20 0 49433.11 47469.20 1131.69 o 6 20 0 26426.34 24778.17 1458.12 o 7 20 0 1964.94 1947.36 345.15 o 8 20 0 4095.41 3537.51 567.87 o 9 20 0 9785.91 9724.70 679.91 o 10 20 0 8223.22 9436.36 2882.10 o 11 20 0 6410.39 6451.35 1524.91 o 12 20 0 1654.77 1453.37 574.16 o 13 20 0 1070.82 2552.02 815.34 o 1 21 0 2481.53 3724.47 289.77 o 2 21 0 2416.17 2984.23 227.55 o 3 21 0 3735.94 3272.24 280.22 o 4 21 0 18913.03 18059.09 1104.54 o 5 21 0 40573.48 38799.08 987.55 o 6 21 0 11166.96 11544.38 639.12 o 7 21 0 263.85 721.35 274.16 o 8 21 0 21924.73 22062.35 927.83 o 9 21 0 46523.69 48997.08 1556.72 o 10 21 0 54026.69 50445.58 2276.23 o 11 21 0 28399.55 26702.29 1439.78 o 12 21 0 447.98 451.65 578.47 o 0 22 0 99476.26 115712.05 4605.72 o 1 22 0 98900.77 107716.99 2121.03 o 2 22 0 5291.46 5214.47 290.81 o 3 22 0 5806.46 5538.81 277.46 o 4 22 0 28687.31 26944.57 973.99 o 5 22 0 28157.41 28204.94 806.53 o 6 22 0 6633.14 6303.96 508.78 o 7 22 0 285.48 325.69 272.21 o 8 22 0 8292.43 7079.21 594.51 o 9 22 0 5062.38 4252.10 520.61 o 10 22 0 87.56 -201.27 441.21 o 11 22 0 2557.53 3185.14 645.56 o 12 22 0 4436.09 5091.77 757.72 o 2 23 0 14796.26 15850.46 509.60 o 3 23 0 22063.60 19370.66 705.54 o 4 23 0 2888.46 2658.70 272.17 o 5 23 0 7056.99 6660.73 400.51 o 6 23 0 13467.24 13049.70 698.81 o 7 23 0 5614.82 5831.21 525.29 o 8 23 0 109.85 -50.13 273.18 o 9 23 0 1271.67 804.32 541.71 o 10 23 0 1225.80 1302.65 533.42 o 11 23 0 1362.88 1002.18 517.74 o 12 23 0 23.32 495.03 460.68 o 0 24 0 56481.67 54586.49 2514.63 o 1 24 0 4322.06 4396.33 297.03 o 2 24 0 13740.22 14870.60 494.81 o 3 24 0 2780.46 3269.59 336.17 o 4 24 0 2854.01 2545.52 282.06 o 5 24 0 2153.70 2251.94 275.52 o 6 24 0 12969.32 11703.98 674.54 o 7 24 0 567.73 488.18 391.38 o 8 24 0 70.49 215.02 282.12 o 9 24 0 11477.26 11395.69 768.00 o 10 24 0 7800.79 8183.25 1134.91 o 11 24 0 13820.03 13606.39 1127.88 o 12 24 0 6973.60 7803.04 1252.71 o 1 25 0 1352.59 1815.53 219.26 o 2 25 0 205.41 270.24 152.18 o 3 25 0 8398.77 8390.94 502.21 o 4 25 0 8399.43 8975.88 464.73 o 5 25 0 47615.91 48591.96 1545.05 o 6 25 0 5035.76 4784.63 487.59 o 7 25 0 1784.47 2106.29 380.17 o 8 25 0 4756.14 4393.61 587.98 o 9 25 0 27938.29 27375.76 1112.11 o 10 25 0 27952.95 27924.85 1469.61 o 11 25 0 17089.49 17789.55 1287.83 o 12 25 0 0.97 682.69 625.33 o 1 26 0 29854.02 30411.86 805.88 o 2 26 0 692.93 598.73 174.30 o 3 26 0 30118.52 31032.67 1000.22 o 4 26 0 76518.44 78069.46 1846.62 o 5 26 0 75186.91 74499.95 2007.63 o 6 26 0 13085.99 14845.27 1306.30 o 7 26 0 6373.33 5527.65 538.29 o 8 26 0 7254.76 8092.57 656.07 o 9 26 0 13141.70 14083.31 1691.88 o 10 26 0 925.21 2010.96 582.90 o 11 26 0 820.84 1837.87 555.51 o 1 27 0 8485.90 10101.10 649.64 o 2 27 0 7247.64 7199.23 384.43 o 3 27 0 4970.52 5316.98 434.68 o 4 27 0 343.92 679.72 244.01 o 5 27 0 6586.17 7525.28 577.40 o 6 27 0 7717.35 7995.00 612.74 o 7 27 0 5071.51 4990.38 519.67 o 8 27 0 39.63 133.81 284.12 o 9 27 0 4603.54 4372.49 646.98 o 10 27 0 1218.14 1489.41 542.97 o 11 27 0 278.35 318.72 461.46 o 1 28 0 9022.29 9396.68 523.96 o 2 28 0 6064.57 7198.42 487.21 o 3 28 0 281.02 516.80 266.40 o 4 28 0 2275.00 2255.62 332.03 o 5 28 0 7776.14 7851.41 605.09 o 6 28 0 13062.82 12093.46 1051.70 o 7 28 0 10458.46 8515.92 662.43 o 8 28 0 2448.11 2896.62 461.40 o 9 28 0 170.91 620.37 351.89 o 10 28 0 785.49 677.15 395.48 o 11 28 0 4189.72 4366.21 976.40 o 1 29 0 4623.37 4532.49 337.38 o 2 29 0 4349.13 4856.94 652.88 o 3 29 0 5886.78 6423.14 490.21 o 4 29 0 23915.95 23181.92 1485.34 o 5 29 0 39190.49 37280.77 1273.51 o 6 29 0 13575.70 12441.44 1320.70 o 7 29 0 1422.73 1424.40 356.49 o 8 29 0 13046.56 11942.77 801.88 o 9 29 0 32720.80 29965.84 1223.82 o 10 29 0 18423.51 18317.21 1927.76 o 1 30 0 43587.73 45392.22 1119.76 o 2 30 0 5653.76 6829.48 562.17 o 3 30 0 26558.78 25886.72 931.43 o 4 30 0 87943.50 85894.98 2204.25 o 5 30 0 68667.72 69290.39 2386.51 o 6 30 0 22854.95 21429.64 1146.91 o 7 30 0 1927.85 2032.43 399.57 o 8 30 0 13433.64 13915.05 875.51 o 9 30 0 10933.13 10508.24 803.40 o 10 30 0 5093.44 5018.09 743.58 o 1 31 0 8470.52 9375.00 468.62 o 2 31 0 34564.56 30588.45 1038.12 o 3 31 0 10283.23 10613.42 619.29 o 4 31 0 1199.80 1508.31 350.56 o 5 31 0 6539.66 6639.55 722.42 o 6 31 0 16350.55 17172.89 906.96 o 7 31 0 7098.65 7277.92 653.73 o 8 31 0 191.64 436.06 340.05 o 9 31 0 2312.48 1640.19 419.47 o 10 31 0 4904.96 5704.73 644.08 o 0 32 0 3900.88 3620.35 730.83 o 1 32 0 11818.93 12436.71 902.03 o 2 32 0 4114.61 4666.02 451.20 o 3 32 0 6250.30 6791.04 530.31 o 4 32 0 2544.60 2622.36 386.66 o 5 32 0 24473.51 23621.65 1904.41 o 6 32 0 15180.87 15871.31 889.56 o 7 32 0 25133.98 23887.86 1063.07 o 8 32 0 9607.06 10133.12 1088.55 o 9 32 0 8957.77 9747.60 793.53 o 10 32 0 152.09 1127.50 402.15 o 1 33 0 4170.19 5160.36 496.38 o 2 33 0 25886.58 25080.42 943.03 o 3 33 0 18878.02 18187.56 811.25 o 4 33 0 11834.10 10708.38 667.50 o 5 33 0 8384.44 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